CN110283653A - The alcohol extracting method and gained sea cucumber intestine egg oil of sea cucumber intestine egg oil - Google Patents
The alcohol extracting method and gained sea cucumber intestine egg oil of sea cucumber intestine egg oil Download PDFInfo
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- CN110283653A CN110283653A CN201910403009.XA CN201910403009A CN110283653A CN 110283653 A CN110283653 A CN 110283653A CN 201910403009 A CN201910403009 A CN 201910403009A CN 110283653 A CN110283653 A CN 110283653A
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- sea cucumber
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- 241000251511 Holothuroidea Species 0.000 title claims abstract description 77
- 210000000936 intestine Anatomy 0.000 title claims abstract description 64
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 27
- 102000002322 Egg Proteins Human genes 0.000 claims abstract description 27
- 108010000912 Egg Proteins Proteins 0.000 claims abstract description 27
- 210000004681 ovum Anatomy 0.000 claims abstract description 27
- 238000000605 extraction Methods 0.000 claims abstract description 13
- 239000003921 oil Substances 0.000 claims description 40
- 235000019441 ethanol Nutrition 0.000 claims description 22
- 239000002994 raw material Substances 0.000 claims description 21
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 15
- 238000009874 alkali refining Methods 0.000 claims description 13
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 9
- 229960004756 ethanol Drugs 0.000 claims description 8
- 238000004108 freeze drying Methods 0.000 claims description 8
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 7
- 238000003303 reheating Methods 0.000 claims description 7
- 239000010779 crude oil Substances 0.000 claims description 6
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 5
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 238000005119 centrifugation Methods 0.000 claims description 3
- 239000000796 flavoring agent Substances 0.000 claims description 3
- 235000019634 flavors Nutrition 0.000 claims description 3
- 229910052740 iodine Inorganic materials 0.000 claims description 3
- 239000011630 iodine Substances 0.000 claims description 3
- 150000002978 peroxides Chemical class 0.000 claims description 3
- 235000013361 beverage Nutrition 0.000 claims description 2
- 239000002537 cosmetic Substances 0.000 claims description 2
- 239000004519 grease Substances 0.000 claims description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 238000011161 development Methods 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 4
- 238000004332 deodorization Methods 0.000 abstract 1
- 238000004807 desolvation Methods 0.000 abstract 1
- 238000001291 vacuum drying Methods 0.000 abstract 1
- 238000009777 vacuum freeze-drying Methods 0.000 abstract 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 238000012545 processing Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 239000001569 carbon dioxide Substances 0.000 description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 238000000194 supercritical-fluid extraction Methods 0.000 description 3
- NTYJJOPFIAHURM-UHFFFAOYSA-N Histamine Chemical compound NCCC1=CN=CN1 NTYJJOPFIAHURM-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 241000195493 Cryptophyta Species 0.000 description 1
- 241000258955 Echinodermata Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010016946 Food allergy Diseases 0.000 description 1
- 240000007058 Halophila ovalis Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000010100 anticoagulation Effects 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 229960001340 histamine Drugs 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 210000004126 nerve fiber Anatomy 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229920001184 polypeptide Polymers 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 235000021081 unsaturated fats Nutrition 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Microbiology (AREA)
- Food Science & Technology (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Zoology (AREA)
- Nutrition Science (AREA)
- Dermatology (AREA)
- Fats And Perfumes (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention proposes the alcohol extracting method and gained sea cucumber intestine egg oil of a kind of sea cucumber intestine egg oil, belongs to field of biotechnology, and the extracting method not only simple and safe operation but also without complicated high equipment can greatly speed up the development and utilization of sea cucumber intestine ovum.The technical solution includes by material vacuum freeze-drying, crushing, extraction, vacuum desolvation, purifying, vacuum drying and deodorization.During the depth redevelopment that the present invention can be applied to sea cucumber intestine egg oil utilizes.
Description
Technical field
The invention belongs to field of biotechnology more particularly to the alcohol extracting methods and gained sea cucumber intestine of a kind of sea cucumber intestine egg oil
Egg oil.
Background technique
Sea cucumber belongs to Holothuroidea (Holothuroidea), is the ocean echinoderm to 8000 meters by the sea that lives, away from the present
Existing more than 600,000,000 years history, sea cucumber are food with seabed algae and planktonic organism.Sea cucumber is not only precious food and rare
Medicinal material.The nutritional ingredients such as phosphatide rich in, unsaturated fatty acid, have the elderly and women good in oil of sea cucumber
Meal supplement effect.However, traditional oil of sea cucumber is often due to containing histamine and bringing serious seafood allergy, so that largely
Crowd can not take.
Traditional oil of sea cucumber is after the extraction, it is difficult to which secondary operation uses.At the same time, sea cucumber intestine ovum is in process
Generally it is dropped or as fertilizers for potted flowers, brings serious waste.With going deep into for research, Holothurian machining byproduct is originally belonged to
Intestines ovum (internal organ and sexual gland, be also sea cucumber) it has been investigated that also various nutriments of sea cucumber rich in, such as contain
More rich Sea Cucumber Glycosides, a variety of sea cucumber polypeptides and a variety of amino acid and unsaturated fat sour component rich in, have
It improves immunity of organisms, inhibit tumour, anticoagulation, the physiological function for protecting nerve fiber.
Currently, the lipid component of various animals and plants materials, which extracts, usually all uses carbon dioxide supercritical extraction technique, but
The prior art is not registered the extraction process of sea cucumber intestine egg oil, it is main the possible reason is: on the one hand, carbon dioxide supercritical extraction
Equipment is expensive, too high with carbon dioxide supercritical extraction sea cucumber intestine egg oil cost, and investment is too big, for sea cucumber byproduct (sea cucumber
Intestines ovum) processing it is economically not cost-effective；On the other hand, it may be possible to because CO 2 supercritical process requirement under super-pressure into
Row operation, production safety have hidden danger, and production environment, personnel requirement are high.So develop one kind i.e. simple and safe operation, be not required to again
Wanting the extracting method of the sea cucumber intestine egg oil of complicated high equipment just becomes very necessary, can greatly speed up the exploitation of sea cucumber intestine ovum
And utilization.
Summary of the invention
The present invention proposes that a kind of alcohol extracting method of sea cucumber intestine egg oil and its gained sea cucumber intestine egg oil, the extracting method were both grasped
Make it is safe and simple, again without complicated high equipment, the development and utilization of sea cucumber intestine ovum can be greatly speeded up.
In order to achieve the above object, the present invention provides a kind of alcohol extracting methods of sea cucumber intestine egg oil, comprising the following steps:
It chooses the sea cucumber intestine ovum raw material that pre-sifted is chosen to be freeze-dried, obtains freeze-drying sea cucumber intestine ovum raw material；
After the crushing of sea cucumber intestine ovum raw material will be lyophilized, primary heating stirring extraction is successively carried out using dehydrated alcohol and is added with secondary
Thermal agitation is extracted, and centrifugal treating after the extracting solution obtained twice is merged obtains centrifugate；
Centrifugate is removed into ethyl alcohol under cryogenic vacuum, until centrifugate without ethanol flavor, obtains sea cucumber intestine ovum crude oil；
Phosphoric acid is added into sea cucumber intestine ovum crude oil and carries out degumming, sodium hydroxide solution is then added and is carried out under hot conditions
Alkali-refining deacidification after centrifugal treating, obtains alkali refining oil；
Alkali refining oil is dried and is deodorized under vacuum condition, sea cucumber intestine egg oil is obtained.
Preferably, the freeze-drying smashed partial size of sea cucumber intestine ovum raw material >=60 mesh, the weight for the dehydrated alcohol being added are
It is lyophilized 1-5 times of sea cucumber intestine ovum raw material.
Preferably, the Extracting temperature that primary heating stirring is extracted and reheating stirring is extracted is 40 DEG C -70 DEG C, stirring
Speed 60-1000RPM, time 30min-240min.
Preferably, the condition of centrifugal treating is centrifugal rotational speed 4000- after the extracting solution obtained twice is merged
9000RPM, centrifugation time 3-20min.
Preferably, the temperature of centrifugate removing ethyl alcohol is 60-65 DEG C, vacuum condition 0.01MPA.
Preferably, the phosphoric acid concentration being added is 85%, the Baume degrees of the sodium hydroxide solution of addition is 5-10 ° of B é, high
Warm condition is 80-90 DEG C, and the alkali refining time is 1-15s.
The alcohol extracting method for the sea cucumber intestine egg oil as described in any of the above-described technical solution that the present invention also provides a kind of obtains
Sea cucumber intestine egg oil.
Preferably, acid value mgKOH/g < 10, the iodine number g/100g of the sea cucumber intestine egg oil are 70-150, peroxide value
G/100g < 2.
The present invention also provides a kind of cosmetics, sea cucumber intestine egg oil described in techniques described above scheme is main component.
The present invention also provides a kind of grease or beverage, sea cucumber intestine egg oil described in techniques described above scheme is main former
Material.
Compared with prior art, the advantages and positive effects of the present invention are:
1, sea cucumber intestine egg oil alcohol extracting method provided by the invention uses dehydrated alcohol as Extraction solvent, non-toxic, easy
Recycle, remain it is low, and using Freeze Drying Technique processing raw material and using cryogenic vacuum remove solvent, can not only have in this way
Effect avoids the problems such as heat treatment bring raw material oxidation deterioration, and raw material freshness and nutritional ingredient can also utmostly be kept to protect
It stays.
2, sea cucumber intestine egg oil alcohol extracting method and process provided by the invention rationally, simple and safe operation and do not need complexity
High equipment, this is particularly important effective extraction of sea cucumber intestine egg oil, can greatly speed up the development and utilization of sea cucumber intestine ovum.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment 1
It chooses with the preferable sea cucumber intestine ovum raw material of batch integrality, it is desirable that raw material is fresh, free from admixture, free from extraneous odour etc..Sabot
It is freeze-dried after processing in -40 DEG C, obtains freeze-drying sea cucumber intestine ovum raw material；
Freeze-drying sea cucumber intestine ovum raw material is crushed using pulverizer, Particle size requirements >=60 mesh check cleanliness, such as after crushing
There are the foreign matters such as shell class, sea grass to remove in time；
It carries out primary heating stirring in 40 DEG C, with 60RPM using dehydrated alcohol to extract, time 240min, then in 40
DEG C, with 60RPM carry out reheating stirring extract, time 240min, by the extracting solution obtained twice merge after in 4000RPM
Centrifugal treating 20min, obtains centrifugate；
Centrifugate is removed into ethyl alcohol under the conditions of 60-65 DEG C, 0.01MPA cryogenic vacuum, until centrifugate without ethanol flavor, obtains
To sea cucumber intestine ovum crude oil；
The phosphoric acid that concentration 85% is added into sea cucumber intestine ovum crude oil carries out degumming, and the hydrogen-oxygen that Baume degrees is 5 ° of B é is then added
Change sodium solution and carries out alkali-refining deacidification 15s under 80 DEG C of hot conditions, after centrifugal treating, it is oily to obtain alkali refining；
Alkali refining oil is dried and is deodorized under 0.015MPa vacuum condition, sea cucumber intestine egg oil is obtained.
Embodiment 2
It is identical as 1 step of embodiment, the difference is that, the condition that primary heating stirring is extracted is in 50 DEG C, 200RPM
180min is handled under revolving speed, the condition that reheating stirring is extracted is to handle 180min, lightning strip under 50 DEG C, 200RPM revolving speed
Part is 5000RPM centrifugal treating 15min.
Embodiment 3
It is identical as 1 step of embodiment, the difference is that, the condition that primary heating stirring is extracted is in 60 DEG C, 450RPM
140min is handled under revolving speed, the condition that reheating stirring is extracted is to handle 140min, lightning strip under 60 DEG C, 450RPM revolving speed
Part is 6500RPM centrifugal treating 11min.
Embodiment 4
It is identical as 1 step of embodiment, the difference is that, the condition that primary heating stirring is extracted is in 70 DEG C, 1000RPM
30min is handled under revolving speed, the condition that reheating stirring is extracted is to handle 30min, lightning strip under 70 DEG C, 1000RPM revolving speed
Part is 8500RPM centrifugal treating 5min.
Embodiment 5
It is identical as 1 step of embodiment, the difference is that, it is the sodium hydroxide solution of 8 ° of B é in 85 DEG C of height that Baume degrees, which is added,
Alkali-refining deacidification 10s is carried out under the conditions of temperature.
Embodiment 6
It is identical as 1 step of embodiment, the difference is that, it is the sodium hydroxide solution of 10 ° of B é in 90 DEG C that Baume degrees, which is added,
Alkali-refining deacidification 3s is carried out under hot conditions.
Performance test
The properties of product of the embodiment 1-6 sea cucumber intestine egg oil being prepared are analyzed as follows, data are shown in Table 1.
The properties of product data of 1 sea cucumber intestine egg oil of table
It analyzes in conjunction with table 1 it is found that the sea cucumber intestine egg oil that preparation method provided by through the embodiment of the present invention is prepared
Its acid value, iodine number, peroxide value reach standard, further, since easily being returned using dehydrated alcohol as Extraction solvent when extracting
Receive, remain it is low, and using Freeze Drying Technique processing raw material and using cryogenic vacuum remove solvent, can effectively avoid hot place
The problems such as managing bring raw material oxidation deterioration can utmostly keep raw material freshness and nutritional ingredient to retain, and extraction efficiency can
Up to 95% or more.Compared to traditional extraction process, this method rational technology, simple and safe operation and complicated high set is not needed
Standby, this is particularly important effective extraction of sea cucumber intestine egg oil, can greatly speed up the development and utilization of sea cucumber intestine ovum.
Claims (10)
1. the alcohol extracting method of sea cucumber intestine egg oil, which comprises the following steps:
It chooses the sea cucumber intestine ovum raw material that pre-sifted is chosen to be freeze-dried, obtains freeze-drying sea cucumber intestine ovum raw material；
After the crushing of sea cucumber intestine ovum raw material will be lyophilized, primary heating stirring extraction is successively carried out using dehydrated alcohol and reheating is stirred
Extraction is mixed, centrifugal treating after the extracting solution obtained twice is merged obtains centrifugate；
Centrifugate is removed into ethyl alcohol under cryogenic vacuum, until centrifugate without ethanol flavor, obtains sea cucumber intestine ovum crude oil；
Phosphoric acid is added into sea cucumber intestine ovum crude oil and carries out degumming, sodium hydroxide solution is then added and carries out alkali refining under hot conditions
Depickling after centrifugal treating, obtains alkali refining oil；
Alkali refining oil is dried and is deodorized under vacuum condition, sea cucumber intestine egg oil is obtained.
2. alcohol extracting method according to claim 1, which is characterized in that the freeze-drying smashed partial size of sea cucumber intestine ovum raw material >=
60 mesh, the weight for the dehydrated alcohol being added are 1-5 times that sea cucumber intestine ovum raw material is lyophilized.
3. alcohol extracting method according to claim 1, which is characterized in that primary heating stirring is extracted and reheating stirring
The Extracting temperature of extraction is 40 DEG C -70 DEG C, mixing speed 60-1000RPM, time 30min-240min.
4. alcohol extracting method according to claim 1, which is characterized in that after merging the extracting solution obtained twice at centrifugation
The condition of reason is centrifugal rotational speed 4000-9000RPM, centrifugation time 3-20min.
5. alcohol extracting method according to claim 1, which is characterized in that the temperature that centrifugate removes ethyl alcohol is 60-65 DEG C,
Vacuum condition is 0.01MPA.
6. alcohol extracting method according to claim 1, which is characterized in that the phosphoric acid concentration of addition is 85%, the hydrogen of addition
The Baume degrees of sodium hydroxide solution is 5-10 ° of B é, and hot conditions are 80-90 DEG C, and the alkali refining time is 1-15s.
7. the sea cucumber intestine egg oil that the alcohol extracting method of sea cucumber intestine egg oil described in -6 obtains according to claim 1.
8. sea cucumber intestine egg oil according to claim 7, which is characterized in that the acid value mgKOH/g < of the sea cucumber intestine egg oil
10, iodine number g/100g is 70-150, peroxide value g/100g < 2.
9. cosmetics, which is characterized in that using sea cucumber intestine egg oil according to claim 7 as main component.
10. grease or beverage, which is characterized in that using sea cucumber intestine egg oil according to claim 7 as primary raw material.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112451546A (en) * | 2020-11-26 | 2021-03-09 | 烟台东宇海珍品有限公司 | Apostichopus japonicus sea cucumber flower lipid extract and preparation method and application thereof |
| CN113430047A (en) * | 2021-06-24 | 2021-09-24 | 大连平岛天然产物科技有限公司 | Method for extracting grease and peptide from sea cucumber eggs |
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| CN101773195A (en) * | 2009-10-30 | 2010-07-14 | 浙江海一方生物工程有限公司 | Preparation method of sea cucumber polypeptide |
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|---|---|---|---|---|
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