CN110283653A - The alcohol extracting method and gained sea cucumber intestine egg oil of sea cucumber intestine egg oil - Google Patents

The alcohol extracting method and gained sea cucumber intestine egg oil of sea cucumber intestine egg oil Download PDF

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Publication number
CN110283653A
CN110283653A CN201910403009.XA CN201910403009A CN110283653A CN 110283653 A CN110283653 A CN 110283653A CN 201910403009 A CN201910403009 A CN 201910403009A CN 110283653 A CN110283653 A CN 110283653A
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Prior art keywords
sea cucumber
cucumber intestine
egg oil
extracting method
oil
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CN201910403009.XA
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Chinese (zh)
Inventor
柯亚夫
仇登宇
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Chizhou Moon Bay Biotechnology Co Ltd
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Chizhou Moon Bay Biotechnology Co Ltd
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Priority to CN201910403009.XA priority Critical patent/CN110283653A/en
Publication of CN110283653A publication Critical patent/CN110283653A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/007Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/925Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/001Refining fats or fatty oils by a combination of two or more of the means hereafter

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Microbiology (AREA)
  • Food Science & Technology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Zoology (AREA)
  • Nutrition Science (AREA)
  • Dermatology (AREA)
  • Fats And Perfumes (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The present invention proposes the alcohol extracting method and gained sea cucumber intestine egg oil of a kind of sea cucumber intestine egg oil, belongs to field of biotechnology, and the extracting method not only simple and safe operation but also without complicated high equipment can greatly speed up the development and utilization of sea cucumber intestine ovum.The technical solution includes by material vacuum freeze-drying, crushing, extraction, vacuum desolvation, purifying, vacuum drying and deodorization.During the depth redevelopment that the present invention can be applied to sea cucumber intestine egg oil utilizes.

Description

The alcohol extracting method and gained sea cucumber intestine egg oil of sea cucumber intestine egg oil
Technical field
The invention belongs to field of biotechnology more particularly to the alcohol extracting methods and gained sea cucumber intestine of a kind of sea cucumber intestine egg oil Egg oil.
Background technique
Sea cucumber belongs to Holothuroidea (Holothuroidea), is the ocean echinoderm to 8000 meters by the sea that lives, away from the present Existing more than 600,000,000 years history, sea cucumber are food with seabed algae and planktonic organism.Sea cucumber is not only precious food and rare Medicinal material.The nutritional ingredients such as phosphatide rich in, unsaturated fatty acid, have the elderly and women good in oil of sea cucumber Meal supplement effect.However, traditional oil of sea cucumber is often due to containing histamine and bringing serious seafood allergy, so that largely Crowd can not take.
Traditional oil of sea cucumber is after the extraction, it is difficult to which secondary operation uses.At the same time, sea cucumber intestine ovum is in process Generally it is dropped or as fertilizers for potted flowers, brings serious waste.With going deep into for research, Holothurian machining byproduct is originally belonged to Intestines ovum (internal organ and sexual gland, be also sea cucumber) it has been investigated that also various nutriments of sea cucumber rich in, such as contain More rich Sea Cucumber Glycosides, a variety of sea cucumber polypeptides and a variety of amino acid and unsaturated fat sour component rich in, have It improves immunity of organisms, inhibit tumour, anticoagulation, the physiological function for protecting nerve fiber.
Currently, the lipid component of various animals and plants materials, which extracts, usually all uses carbon dioxide supercritical extraction technique, but The prior art is not registered the extraction process of sea cucumber intestine egg oil, it is main the possible reason is: on the one hand, carbon dioxide supercritical extraction Equipment is expensive, too high with carbon dioxide supercritical extraction sea cucumber intestine egg oil cost, and investment is too big, for sea cucumber byproduct (sea cucumber Intestines ovum) processing it is economically not cost-effective;On the other hand, it may be possible to because CO 2 supercritical process requirement under super-pressure into Row operation, production safety have hidden danger, and production environment, personnel requirement are high.So develop one kind i.e. simple and safe operation, be not required to again Wanting the extracting method of the sea cucumber intestine egg oil of complicated high equipment just becomes very necessary, can greatly speed up the exploitation of sea cucumber intestine ovum And utilization.
Summary of the invention
The present invention proposes that a kind of alcohol extracting method of sea cucumber intestine egg oil and its gained sea cucumber intestine egg oil, the extracting method were both grasped Make it is safe and simple, again without complicated high equipment, the development and utilization of sea cucumber intestine ovum can be greatly speeded up.
In order to achieve the above object, the present invention provides a kind of alcohol extracting methods of sea cucumber intestine egg oil, comprising the following steps:
It chooses the sea cucumber intestine ovum raw material that pre-sifted is chosen to be freeze-dried, obtains freeze-drying sea cucumber intestine ovum raw material;
After the crushing of sea cucumber intestine ovum raw material will be lyophilized, primary heating stirring extraction is successively carried out using dehydrated alcohol and is added with secondary Thermal agitation is extracted, and centrifugal treating after the extracting solution obtained twice is merged obtains centrifugate;
Centrifugate is removed into ethyl alcohol under cryogenic vacuum, until centrifugate without ethanol flavor, obtains sea cucumber intestine ovum crude oil;
Phosphoric acid is added into sea cucumber intestine ovum crude oil and carries out degumming, sodium hydroxide solution is then added and is carried out under hot conditions Alkali-refining deacidification after centrifugal treating, obtains alkali refining oil;
Alkali refining oil is dried and is deodorized under vacuum condition, sea cucumber intestine egg oil is obtained.
Preferably, the freeze-drying smashed partial size of sea cucumber intestine ovum raw material >=60 mesh, the weight for the dehydrated alcohol being added are It is lyophilized 1-5 times of sea cucumber intestine ovum raw material.
Preferably, the Extracting temperature that primary heating stirring is extracted and reheating stirring is extracted is 40 DEG C -70 DEG C, stirring Speed 60-1000RPM, time 30min-240min.
Preferably, the condition of centrifugal treating is centrifugal rotational speed 4000- after the extracting solution obtained twice is merged 9000RPM, centrifugation time 3-20min.
Preferably, the temperature of centrifugate removing ethyl alcohol is 60-65 DEG C, vacuum condition 0.01MPA.
Preferably, the phosphoric acid concentration being added is 85%, the Baume degrees of the sodium hydroxide solution of addition is 5-10 ° of B é, high Warm condition is 80-90 DEG C, and the alkali refining time is 1-15s.
The alcohol extracting method for the sea cucumber intestine egg oil as described in any of the above-described technical solution that the present invention also provides a kind of obtains Sea cucumber intestine egg oil.
Preferably, acid value mgKOH/g < 10, the iodine number g/100g of the sea cucumber intestine egg oil are 70-150, peroxide value G/100g < 2.
The present invention also provides a kind of cosmetics, sea cucumber intestine egg oil described in techniques described above scheme is main component.
The present invention also provides a kind of grease or beverage, sea cucumber intestine egg oil described in techniques described above scheme is main former Material.
Compared with prior art, the advantages and positive effects of the present invention are:
1, sea cucumber intestine egg oil alcohol extracting method provided by the invention uses dehydrated alcohol as Extraction solvent, non-toxic, easy Recycle, remain it is low, and using Freeze Drying Technique processing raw material and using cryogenic vacuum remove solvent, can not only have in this way Effect avoids the problems such as heat treatment bring raw material oxidation deterioration, and raw material freshness and nutritional ingredient can also utmostly be kept to protect It stays.
2, sea cucumber intestine egg oil alcohol extracting method and process provided by the invention rationally, simple and safe operation and do not need complexity High equipment, this is particularly important effective extraction of sea cucumber intestine egg oil, can greatly speed up the development and utilization of sea cucumber intestine ovum.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects It encloses.
Embodiment 1
It chooses with the preferable sea cucumber intestine ovum raw material of batch integrality, it is desirable that raw material is fresh, free from admixture, free from extraneous odour etc..Sabot It is freeze-dried after processing in -40 DEG C, obtains freeze-drying sea cucumber intestine ovum raw material;
Freeze-drying sea cucumber intestine ovum raw material is crushed using pulverizer, Particle size requirements >=60 mesh check cleanliness, such as after crushing There are the foreign matters such as shell class, sea grass to remove in time;
It carries out primary heating stirring in 40 DEG C, with 60RPM using dehydrated alcohol to extract, time 240min, then in 40 DEG C, with 60RPM carry out reheating stirring extract, time 240min, by the extracting solution obtained twice merge after in 4000RPM Centrifugal treating 20min, obtains centrifugate;
Centrifugate is removed into ethyl alcohol under the conditions of 60-65 DEG C, 0.01MPA cryogenic vacuum, until centrifugate without ethanol flavor, obtains To sea cucumber intestine ovum crude oil;
The phosphoric acid that concentration 85% is added into sea cucumber intestine ovum crude oil carries out degumming, and the hydrogen-oxygen that Baume degrees is 5 ° of B é is then added Change sodium solution and carries out alkali-refining deacidification 15s under 80 DEG C of hot conditions, after centrifugal treating, it is oily to obtain alkali refining;
Alkali refining oil is dried and is deodorized under 0.015MPa vacuum condition, sea cucumber intestine egg oil is obtained.
Embodiment 2
It is identical as 1 step of embodiment, the difference is that, the condition that primary heating stirring is extracted is in 50 DEG C, 200RPM 180min is handled under revolving speed, the condition that reheating stirring is extracted is to handle 180min, lightning strip under 50 DEG C, 200RPM revolving speed Part is 5000RPM centrifugal treating 15min.
Embodiment 3
It is identical as 1 step of embodiment, the difference is that, the condition that primary heating stirring is extracted is in 60 DEG C, 450RPM 140min is handled under revolving speed, the condition that reheating stirring is extracted is to handle 140min, lightning strip under 60 DEG C, 450RPM revolving speed Part is 6500RPM centrifugal treating 11min.
Embodiment 4
It is identical as 1 step of embodiment, the difference is that, the condition that primary heating stirring is extracted is in 70 DEG C, 1000RPM 30min is handled under revolving speed, the condition that reheating stirring is extracted is to handle 30min, lightning strip under 70 DEG C, 1000RPM revolving speed Part is 8500RPM centrifugal treating 5min.
Embodiment 5
It is identical as 1 step of embodiment, the difference is that, it is the sodium hydroxide solution of 8 ° of B é in 85 DEG C of height that Baume degrees, which is added, Alkali-refining deacidification 10s is carried out under the conditions of temperature.
Embodiment 6
It is identical as 1 step of embodiment, the difference is that, it is the sodium hydroxide solution of 10 ° of B é in 90 DEG C that Baume degrees, which is added, Alkali-refining deacidification 3s is carried out under hot conditions.
Performance test
The properties of product of the embodiment 1-6 sea cucumber intestine egg oil being prepared are analyzed as follows, data are shown in Table 1.
The properties of product data of 1 sea cucumber intestine egg oil of table
It analyzes in conjunction with table 1 it is found that the sea cucumber intestine egg oil that preparation method provided by through the embodiment of the present invention is prepared Its acid value, iodine number, peroxide value reach standard, further, since easily being returned using dehydrated alcohol as Extraction solvent when extracting Receive, remain it is low, and using Freeze Drying Technique processing raw material and using cryogenic vacuum remove solvent, can effectively avoid hot place The problems such as managing bring raw material oxidation deterioration can utmostly keep raw material freshness and nutritional ingredient to retain, and extraction efficiency can Up to 95% or more.Compared to traditional extraction process, this method rational technology, simple and safe operation and complicated high set is not needed Standby, this is particularly important effective extraction of sea cucumber intestine egg oil, can greatly speed up the development and utilization of sea cucumber intestine ovum.

Claims (10)

1. the alcohol extracting method of sea cucumber intestine egg oil, which comprises the following steps:
It chooses the sea cucumber intestine ovum raw material that pre-sifted is chosen to be freeze-dried, obtains freeze-drying sea cucumber intestine ovum raw material;
After the crushing of sea cucumber intestine ovum raw material will be lyophilized, primary heating stirring extraction is successively carried out using dehydrated alcohol and reheating is stirred Extraction is mixed, centrifugal treating after the extracting solution obtained twice is merged obtains centrifugate;
Centrifugate is removed into ethyl alcohol under cryogenic vacuum, until centrifugate without ethanol flavor, obtains sea cucumber intestine ovum crude oil;
Phosphoric acid is added into sea cucumber intestine ovum crude oil and carries out degumming, sodium hydroxide solution is then added and carries out alkali refining under hot conditions Depickling after centrifugal treating, obtains alkali refining oil;
Alkali refining oil is dried and is deodorized under vacuum condition, sea cucumber intestine egg oil is obtained.
2. alcohol extracting method according to claim 1, which is characterized in that the freeze-drying smashed partial size of sea cucumber intestine ovum raw material >= 60 mesh, the weight for the dehydrated alcohol being added are 1-5 times that sea cucumber intestine ovum raw material is lyophilized.
3. alcohol extracting method according to claim 1, which is characterized in that primary heating stirring is extracted and reheating stirring The Extracting temperature of extraction is 40 DEG C -70 DEG C, mixing speed 60-1000RPM, time 30min-240min.
4. alcohol extracting method according to claim 1, which is characterized in that after merging the extracting solution obtained twice at centrifugation The condition of reason is centrifugal rotational speed 4000-9000RPM, centrifugation time 3-20min.
5. alcohol extracting method according to claim 1, which is characterized in that the temperature that centrifugate removes ethyl alcohol is 60-65 DEG C, Vacuum condition is 0.01MPA.
6. alcohol extracting method according to claim 1, which is characterized in that the phosphoric acid concentration of addition is 85%, the hydrogen of addition The Baume degrees of sodium hydroxide solution is 5-10 ° of B é, and hot conditions are 80-90 DEG C, and the alkali refining time is 1-15s.
7. the sea cucumber intestine egg oil that the alcohol extracting method of sea cucumber intestine egg oil described in -6 obtains according to claim 1.
8. sea cucumber intestine egg oil according to claim 7, which is characterized in that the acid value mgKOH/g < of the sea cucumber intestine egg oil 10, iodine number g/100g is 70-150, peroxide value g/100g < 2.
9. cosmetics, which is characterized in that using sea cucumber intestine egg oil according to claim 7 as main component.
10. grease or beverage, which is characterized in that using sea cucumber intestine egg oil according to claim 7 as primary raw material.
CN201910403009.XA 2019-05-15 2019-05-15 The alcohol extracting method and gained sea cucumber intestine egg oil of sea cucumber intestine egg oil Pending CN110283653A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112451546A (en) * 2020-11-26 2021-03-09 烟台东宇海珍品有限公司 Apostichopus japonicus sea cucumber flower lipid extract and preparation method and application thereof
CN113430047A (en) * 2021-06-24 2021-09-24 大连平岛天然产物科技有限公司 Method for extracting grease and peptide from sea cucumber eggs

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1432368A (en) * 2002-12-31 2003-07-30 通化市中心医院 Woodfrog egg oil capsule and its production process
CN101773195A (en) * 2009-10-30 2010-07-14 浙江海一方生物工程有限公司 Preparation method of sea cucumber polypeptide
CN107699359A (en) * 2017-11-24 2018-02-16 黑龙江美丽石岛科技开发有限公司 A kind of extraction process of sea cucumber intestine egg oil and the method that sea cucumber intestine ovum oil soft capsule is prepared using sea cucumber intestine egg oil

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1432368A (en) * 2002-12-31 2003-07-30 通化市中心医院 Woodfrog egg oil capsule and its production process
CN101773195A (en) * 2009-10-30 2010-07-14 浙江海一方生物工程有限公司 Preparation method of sea cucumber polypeptide
CN107699359A (en) * 2017-11-24 2018-02-16 黑龙江美丽石岛科技开发有限公司 A kind of extraction process of sea cucumber intestine egg oil and the method that sea cucumber intestine ovum oil soft capsule is prepared using sea cucumber intestine egg oil

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112451546A (en) * 2020-11-26 2021-03-09 烟台东宇海珍品有限公司 Apostichopus japonicus sea cucumber flower lipid extract and preparation method and application thereof
CN113430047A (en) * 2021-06-24 2021-09-24 大连平岛天然产物科技有限公司 Method for extracting grease and peptide from sea cucumber eggs

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Application publication date: 20190927