CN110236170A - A kind of preparation method of edible salt - Google Patents

A kind of preparation method of edible salt Download PDF

Info

Publication number
CN110236170A
CN110236170A CN201910491877.8A CN201910491877A CN110236170A CN 110236170 A CN110236170 A CN 110236170A CN 201910491877 A CN201910491877 A CN 201910491877A CN 110236170 A CN110236170 A CN 110236170A
Authority
CN
China
Prior art keywords
brine
edible salt
preparation
salt
maifanitum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910491877.8A
Other languages
Chinese (zh)
Inventor
张红宇
陈学德
王丹枫
潘秀云
周继东
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Benefits Of Salt Tang (yingcheng) Health Salt Salt Co Ltd
Original Assignee
Benefits Of Salt Tang (yingcheng) Health Salt Salt Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Benefits Of Salt Tang (yingcheng) Health Salt Salt Co Ltd filed Critical Benefits Of Salt Tang (yingcheng) Health Salt Salt Co Ltd
Priority to CN201910491877.8A priority Critical patent/CN110236170A/en
Publication of CN110236170A publication Critical patent/CN110236170A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/40Table salts; Dietetic salt substitutes

Landscapes

  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention discloses a kind of preparation methods of edible salt, comprising: prepares brine in step 1, brine storage device;Step 2,1 gained brine of extraction step successively pass through first order reaction bucket, second order reaction bucket and smart halogen bucket and carry out chemical cleaning method, obtain refined brine;The resulting refined brine of step 2 is passed through medical stone batch extractor progress adsorption cleaning by step 3, obtains deep purifying salt water;Maifanitum is equipped in the medical stone batch extractor;The resulting deep purifying salt water of step 3 is squeezed into crystallizing evaporator and is crystallized by step 4;After step 5, crystallization by drying plus after iodine and packing i.e. finished product;Maifanitum is applied in the purification process of salt production, the content that there is good clean-up effect to improve microelement in edible salt simultaneously edible salt.

Description

A kind of preparation method of edible salt
Technical field
The present invention relates to edible sodium chloride technical field more particularly to a kind of preparation methods of edible salt.
Background technique
Salt is flavouring important in human lives, occupies very important status in people's lives.Salt is tool There is the flavoring agent of important physiological function, be adjustable the osmotic balance of human body, maintains the normal excitability of nerves and muscles.When eating Food in when lacking salt, intracorporal sodium ions content will be reduced, and potassium ion enters blood from cell, it may occur that blood becomes The illnesss such as dense, oliguria, cholesteroderma.
Maifanitum is one kind of medical stone, originates in the medical stone in Naiman Banner in Inner Mongolia table mountain " Chinese wheat meal Stone ", is a kind of special nonmetal mineral resource, and likeness in form plaque-like is yellow or white, quite like wheat.Early in Christian era 300 years, Shanxi Medical stone is referred to as " slightly managing Huangshi ", the Thousand Golden Prescriptions of the Tang Dynasty SUN Si miao, the Northern Song Dynasty in medical skill handbook of Prescription for Emergency written by Dai Gehong The Holy Benevolent Prescriptions of Wang Huaiyin adopt.It Christian era 1061, proposes " slightly to manage Huangshi, class in " Bencao Tujing " written by Northern Song Dynasty Su Song Wheat meal ".Southern Song Dynasty physician Li Xun note in " this collection of school tests back subcutaneous ulcer side " has " medical stone, or such as fist, or such as small cup, a shape such as wheat Meal ".The big physician's Li Shizhen (1518-1593 A.D.) of the Ming Dynasty, China is recorded in Compendium of Material Medica: " shape such as holds a poly- wheat meal, there is grain such as beans such as rice, Its color is yellowish-white." medical stone is so gain the name.Medical stone powder enters Chinese medicine, and the water impregnated can be drunk, also for take a shower, have body-building and The drug effect promoted longevity.In recent years Maifanitum passes to the good name of Japanese " healthy remedies " (health-stone) again.In reality In the application of border, Maifanitum has the effects that strong adsorption force, dissolution are beneficial to the minerals of human body, adjustment water quality.
Summary of the invention
It is an object of the invention to overcome the defect of the prior art, a kind of preparation method of edible salt is provided, it will be Chinese Medical stone is applied in the purification process of salt production, there is good clean-up effect to improve in edible salt simultaneously edible salt The content of microelement.
The present invention is implemented as follows:
It is an object of that present invention to provide a kind of preparation methods of edible salt, and described method includes following steps:
Brine is prepared in step 1, brine storage device;
Step 2,1 gained brine of extraction step successively pass through first order reaction bucket, second order reaction bucket and smart halogen bucket and carry out chemistry Purification, obtains refined brine;
The resulting refined brine of step 2 is passed through medical stone batch extractor progress adsorption cleaning by step 3, obtains deep purifying Salt water;Maifanitum is equipped in the medical stone batch extractor;
The resulting deep purifying salt water of step 3 is squeezed into crystallizing evaporator and is crystallized by step 4;
After step 5, crystallization by drying plus after iodine and packing i.e. finished product.
Compared with prior art, the invention has the advantages that and effect:
A kind of preparation method of edible salt provided by the invention there is good clean-up effect to improve simultaneously edible salt The content of microelement (iron, zinc) in edible salt.
Specific embodiment
Embodiment 1
A kind of preparation method of edible salt, which is characterized in that described method includes following steps:
Step 1 carries out adopting halogen using aqueous solution or fresh water the injection saltcake type mine of chloride containing calcium, produces high calcium halogen Water;
Step 2,1 gained brine of extraction step successively pass through first order reaction bucket, second order reaction bucket and smart halogen bucket and carry out chemistry Purification, obtains refined brine;The first order reaction bucket addition has milk of lime and soda ash;The second order reaction bucket addition has lime Cream and flocculant, the flocculant include Sodium Polyacrylate and sodium citrate;Mole of calcium in the sodium citrate and brine Amount is than being 2.2:1;The mass volume ratio of the Sodium Polyacrylate and brine is 13mg/L;
The resulting refined brine of step 2 is passed through medical stone batch extractor progress adsorption cleaning by step 3, obtains deep purifying Salt water;Maifanitum is equipped in the medical stone batch extractor;The Maifanitum is purchased from Inner Mongol Naiman Banner Maifanitum Development corporation, Ltd.;The medical stone leaches filling treatment effeciency control and handles 10 tons of purified salts per hour in Maifanitum per ton Water;After magnificent medical stone is handled refined brine 72 hours, carry out being used to be recycled after clear water leaches cleaning.
The resulting deep purifying salt water of step 3 is squeezed into collet crystallizing evaporator and is crystallized by step 4;
After step 5, crystallization by drying plus after iodine and packing i.e. finished product.
Embodiment 2
A kind of preparation method of edible salt, which is characterized in that described method includes following steps:
Step 1 carries out adopting halogen using aqueous solution or fresh water the injection saltcake type mine of chloride containing calcium, produces high calcium halogen Water;
Step 2,1 gained brine of extraction step successively pass through first order reaction bucket, second order reaction bucket and smart halogen bucket and carry out chemistry Purification, obtains refined brine;The first order reaction bucket addition has milk of lime and soda ash;The second order reaction bucket addition has lime Cream and flocculant, the flocculant include Sodium Polyacrylate and sodium citrate;Mole of calcium in the sodium citrate and brine Amount is than being 2:1;The mass volume ratio of the Sodium Polyacrylate and brine is 12mg/L;
The resulting refined brine of step 2 is passed through medical stone batch extractor progress adsorption cleaning by step 3, obtains deep purifying Salt water;Maifanitum is equipped in the medical stone batch extractor;The Maifanitum is purchased from Inner Mongol Naiman Banner Maifanitum Development corporation, Ltd.;The medical stone leaches filling treatment effeciency control and handles 8 tons of purified salts per hour in Maifanitum per ton Water;After magnificent medical stone is handled refined brine 72 hours, carry out being used to be recycled after clear water leaches cleaning.
The resulting deep purifying salt water of step 3 is squeezed into collet crystallizing evaporator and is crystallized by step 4;
After step 5, crystallization by drying plus after iodine and packing i.e. finished product.
Embodiment 3
A kind of preparation method of edible salt, which is characterized in that described method includes following steps:
Step 1 carries out adopting halogen using aqueous solution or fresh water the injection saltcake type mine of chloride containing calcium, produces high calcium halogen Water;
Step 2,1 gained brine of extraction step successively pass through first order reaction bucket, second order reaction bucket and smart halogen bucket and carry out chemistry Purification, obtains refined brine;The first order reaction bucket addition has milk of lime and soda ash;The second order reaction bucket addition has lime Cream and flocculant, the flocculant include Sodium Polyacrylate and sodium citrate;Mole of calcium in the sodium citrate and brine Amount is than being 2.5:1;The mass volume ratio of the Sodium Polyacrylate and brine is 15mg/L;
The resulting refined brine of step 2 is passed through medical stone batch extractor progress adsorption cleaning by step 3, obtains deep purifying Salt water;Maifanitum is equipped in the medical stone batch extractor;The Maifanitum is purchased from Inner Mongol Naiman Banner Maifanitum Development corporation, Ltd.;The medical stone leaches filling treatment effeciency control and handles 12 tons of purified salts per hour in Maifanitum per ton Water;After magnificent medical stone is handled refined brine 72 hours, carry out being used to be recycled after clear water leaches cleaning.
The resulting deep purifying salt water of step 3 is squeezed into collet crystallizing evaporator and is crystallized by step 4;
After step 5, crystallization by drying plus after iodine and packing i.e. finished product.
Comparative example 1
The comparative example except without step 3 be passed through medical stone batch extractor carry out adsorption cleaning step in addition to, remaining with implement Example 1.
Comparative example 2
Sodium citrate is not added in the step 3 of the comparative example, remaining is the same as embodiment 1.
Experimental example
1, the edible salt product detection Comparative result of embodiment 1-3 and comparative example 1-2, as shown in table 1:
Table 1
As shown in Table 1, the preparation method of a kind of edible salt provided by the invention has good clean-up effect to edible salt (improving deliming rate), while improving the content of microelement in edible salt (iron, zinc).
2, in addition, the present inventor leaches through a large amount of Making Innovation Experiments discovery medical stone fills treatment effeciency control in China per ton When medical stone handles 8~12 tons of refined brines per hour, there is good clean-up effect to mention to the maximum extent simultaneously edible salt The content of microelement (iron, zinc) in high edible salt.
3, in sodium citrate and brine the mole ratio of calcium exploration
Experimental group 1-10 is arranged by table 2, and other conditions with embodiment 1, test the deliming rate of each group.
Table 2
As shown in Table 2, the mole ratio of sodium citrate and calcium in brine is preferably 2:1~2.5:1;And flocculant selects simultaneously Deliming rate can be greatly increased with Sodium Polyacrylate and sodium citrate.
Described is only presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and Within principle, any modification, equivalent replacement, improvement and so on should all include within protection scope of the present invention.

Claims (7)

1. a kind of preparation method of edible salt, which is characterized in that described method includes following steps:
Brine is prepared in step 1, brine storage device;
Step 2,1 gained brine of extraction step successively pass through first order reaction bucket, second order reaction bucket and smart halogen bucket and carry out chemical cleaning method, Obtain refined brine;
The resulting refined brine of step 2 is passed through medical stone batch extractor progress adsorption cleaning by step 3, obtains deep purifying salt water; Maifanitum is equipped in the medical stone batch extractor;
The resulting deep purifying salt water of step 3 is squeezed into crystallizing evaporator and is crystallized by step 4;
After step 5, crystallization by drying plus after iodine and packing i.e. finished product.
2. the preparation method of edible salt as described in claim 1, which is characterized in that utilize chloride containing calcium in the step 1 Aqueous solution or fresh water injection saltcake type mine carry out adopting halogen, produce high calcium brine.
3. the preparation method of edible salt as described in claim 1, which is characterized in that the first order reaction in the step 2 Bucket, which is added, milk of lime and soda ash;The second order reaction bucket addition has milk of lime and flocculant, and the flocculant includes poly- third Olefin(e) acid sodium and sodium citrate.
4. the preparation method of edible salt as described in claim 1, which is characterized in that the sodium citrate rubs with calcium in brine Your amount ratio is 2.0~2.5:1;The mass volume ratio of the Sodium Polyacrylate and brine is 12~15mg/L.
5. the preparation method of edible salt as described in claim 1, which is characterized in that in step 3 Maifanitum is purchased from Cover Naimanqi Chinese Medical Stone Development Co., Ltd.;It is every in Maifanitum per ton that the medical stone leaches filling treatment effeciency control 8~12 tons of refined brines of hour processing.
6. the preparation method of edible salt as described in claim 1, which is characterized in that the step 3 Maifanitum processing essence After salt manufacturing water 72 hours, carry out being used to be recycled after clear water leaches cleaning.
7. the preparation method of edible salt as described in claim 1, which is characterized in that crystallizing evaporator is folder in the step 4 Cover crystallizing evaporator.
CN201910491877.8A 2019-06-06 2019-06-06 A kind of preparation method of edible salt Pending CN110236170A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910491877.8A CN110236170A (en) 2019-06-06 2019-06-06 A kind of preparation method of edible salt

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910491877.8A CN110236170A (en) 2019-06-06 2019-06-06 A kind of preparation method of edible salt

Publications (1)

Publication Number Publication Date
CN110236170A true CN110236170A (en) 2019-09-17

Family

ID=67886182

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910491877.8A Pending CN110236170A (en) 2019-06-06 2019-06-06 A kind of preparation method of edible salt

Country Status (1)

Country Link
CN (1) CN110236170A (en)

Citations (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1673124A (en) * 2005-01-29 2005-09-28 山西大学 Salt lake bittern purifying and decolorizing method
CN101171963A (en) * 2007-11-05 2008-05-07 赫广才 Selenium iodine common salt
CN101289200A (en) * 2007-04-16 2008-10-22 中国盐业总公司 Technological process for purifying bittern
CN102370152A (en) * 2011-11-01 2012-03-14 江苏省制盐工业研究所 Method for preparing snowflake edible salt by using mineral salt or mineral brine
CN102502711A (en) * 2011-10-20 2012-06-20 中盐金坛盐化有限责任公司 Preparation process and special device for salt with green food label
CN102976365A (en) * 2012-12-14 2013-03-20 江苏井神盐化股份有限公司 High-calcium edible salt produced by calcium-containing mirabilite-type mineral halide and producing method thereof
CN103288103A (en) * 2013-06-06 2013-09-11 中国轻工业长沙工程有限公司 Gypsum type brine purification technique using lime-carbon dioxide method
CN103303943A (en) * 2013-06-06 2013-09-18 中国轻工业长沙工程有限公司 Purifying process of mirabilite type brine by adopting lime-carbon dioxide process
CN103482655A (en) * 2013-06-06 2014-01-01 中国轻工业长沙工程有限公司 Lime-sodium sulfate-carbon dioxide method used for purifying calcium chloride type bittern
CN103637160A (en) * 2013-12-23 2014-03-19 中盐皓龙盐化有限责任公司 Preparation process of liquid edible salt
CN103689525A (en) * 2013-12-16 2014-04-02 江苏井神盐化股份有限公司 Method for producing liquid edible salt through brine extraction of well and rock salt and liquid edible salt
CN104743582A (en) * 2015-04-14 2015-07-01 中国海洋石油总公司 Method and device for producing refined brine by utilizing bromine extraction brine
CN204569443U (en) * 2015-04-14 2015-08-19 中国海洋石油总公司 The device that bromine bittern produces refined brine is carried in a kind of utilization
WO2016028018A1 (en) * 2014-08-19 2016-02-25 김춘동 Salt farm flooring and salt farm including same
CN106219574A (en) * 2016-05-19 2016-12-14 北京圣祥天宝商贸有限公司 The preparation method of fuse salt
CN107540072A (en) * 2017-09-18 2018-01-05 湖南省湘衡盐化有限责任公司 A kind of flocculant solution preparation method and bittern purifying method
CN107853669A (en) * 2017-07-20 2018-03-30 杨真诚 The special block salt processing method of a kind of health table salt and body-building salt room
CN109289539A (en) * 2018-09-18 2019-02-01 中国海洋石油集团有限公司 A kind of brine refining nanofiltration membrane cleaning agent and preparation method thereof

Patent Citations (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1673124A (en) * 2005-01-29 2005-09-28 山西大学 Salt lake bittern purifying and decolorizing method
CN101289200A (en) * 2007-04-16 2008-10-22 中国盐业总公司 Technological process for purifying bittern
CN101171963A (en) * 2007-11-05 2008-05-07 赫广才 Selenium iodine common salt
CN102502711A (en) * 2011-10-20 2012-06-20 中盐金坛盐化有限责任公司 Preparation process and special device for salt with green food label
CN102370152A (en) * 2011-11-01 2012-03-14 江苏省制盐工业研究所 Method for preparing snowflake edible salt by using mineral salt or mineral brine
CN102976365A (en) * 2012-12-14 2013-03-20 江苏井神盐化股份有限公司 High-calcium edible salt produced by calcium-containing mirabilite-type mineral halide and producing method thereof
CN103482655A (en) * 2013-06-06 2014-01-01 中国轻工业长沙工程有限公司 Lime-sodium sulfate-carbon dioxide method used for purifying calcium chloride type bittern
CN103303943A (en) * 2013-06-06 2013-09-18 中国轻工业长沙工程有限公司 Purifying process of mirabilite type brine by adopting lime-carbon dioxide process
CN103288103A (en) * 2013-06-06 2013-09-11 中国轻工业长沙工程有限公司 Gypsum type brine purification technique using lime-carbon dioxide method
CN103689525A (en) * 2013-12-16 2014-04-02 江苏井神盐化股份有限公司 Method for producing liquid edible salt through brine extraction of well and rock salt and liquid edible salt
CN103637160A (en) * 2013-12-23 2014-03-19 中盐皓龙盐化有限责任公司 Preparation process of liquid edible salt
WO2016028018A1 (en) * 2014-08-19 2016-02-25 김춘동 Salt farm flooring and salt farm including same
CN104743582A (en) * 2015-04-14 2015-07-01 中国海洋石油总公司 Method and device for producing refined brine by utilizing bromine extraction brine
CN204569443U (en) * 2015-04-14 2015-08-19 中国海洋石油总公司 The device that bromine bittern produces refined brine is carried in a kind of utilization
CN106219574A (en) * 2016-05-19 2016-12-14 北京圣祥天宝商贸有限公司 The preparation method of fuse salt
CN107853669A (en) * 2017-07-20 2018-03-30 杨真诚 The special block salt processing method of a kind of health table salt and body-building salt room
CN107540072A (en) * 2017-09-18 2018-01-05 湖南省湘衡盐化有限责任公司 A kind of flocculant solution preparation method and bittern purifying method
CN109289539A (en) * 2018-09-18 2019-02-01 中国海洋石油集团有限公司 A kind of brine refining nanofiltration membrane cleaning agent and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
中国大百科全书总编辑委员会: "《中国大百科全书》", 31 December 2002, 中国大百科全书出版社 *
张建春等: "《化纤仿毛技术原理与生产实践》", 31 December 2003, 中国石化出版社 *
赵营峰等: ""精制卤水中含盐泥问题初探"", 《盐业与化工》 *

Similar Documents

Publication Publication Date Title
CN103230020A (en) Preparation method of protein short peptide chelated calcium
JP2702322B2 (en) Active amino acid calcium, beverage containing the same, and method for producing the same
JP4509568B2 (en) Method for recovering low sodium salt from bitter juice
CN107373218A (en) A kind of mineral matter drinks
JP2003063969A (en) Functional goods using concentrated mineral solution obtained from deep sea water by separation
JP2002034592A (en) Method for producing protein-zinc readily absorbable in body
CN110236170A (en) A kind of preparation method of edible salt
CN110172491A (en) A kind of multi-element biologic protein peptides and preparation method thereof
AU601150B2 (en) Mineral salt composition
EP3313448A1 (en) A highly concentrated seawater mineral extract and uses thereof
CN103169092A (en) L-asparaginic acid chelated calcium drinking water
CN104041908B (en) Preparation method of peony pollen effervescent tablet
US20040009235A1 (en) Nanometer grade hydroxyapatite composition for replenishing calcium
CN102527324A (en) Porous adsorbing material with health care function and preparation method of porous adsorbing material
CN101978903B (en) Sea cucumber stewed food buccal tablets and method for preparing same
WO2021167024A1 (en) Liquid mineral concentrate composition
WO2011079652A1 (en) Yeast product with low nucleic acid content, method preparing the same and diet product containing said yeast product with low nucleic acid content
JP3460825B2 (en) Component adjustment device in liquid food
CN106915815B (en) The preparation method and applications of material for reverse osmosis rear pure water mineralising
CN1293831C (en) Effervescent solid beverage of amino acid chelated calcium and its prepn
JP2004208668A (en) Tea prepared by using binchoutan(charcoal)
KR100858030B1 (en) The liquid sea tangle salt manufacture method
CN109430885A (en) It is a kind of using oligopeptide as nutritional agents of carrier and preparation method thereof
JP3868916B2 (en) Method for separating and extracting hardness component and nutritional supplement food containing hardness component
CN104473279A (en) Hericium erinaceus beverage

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20190917

RJ01 Rejection of invention patent application after publication