CN110179913A - A kind of root of Dahurain angelica powder and preparation method thereof for treating acute mastitis swelling and pain - Google Patents
A kind of root of Dahurain angelica powder and preparation method thereof for treating acute mastitis swelling and pain Download PDFInfo
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Abstract
The invention discloses a kind of root of Dahurain angelica powders and preparation method thereof for treating acute mastitis swelling and pain, belong to chinese medicine material technical field.Resin, natural gum, volatile oil, water are stirred by the present invention, obtain olibanum solution；Fritillaria thunbergii is added in olibanum solution；Radix Notoginseng, cleaning, drying are taken, fine ground powder takes net Radix Notoginseng to smash；The property of will volatilize oil is mixed with water, after standing swelling, heating stirring dissolution；By olibanum, the broken angle mixing of Radix Notoginseng is then added when angelica body mixing and ball milling in the root of Dahurain angelica, and injection molding is hot-forming, demoulds, dry, obtains drying material；Drying material is placed in sterile workshop encapsulation, is vacuumized, seals the root of Dahurain angelica powder to get treatment acute mastitis swelling and pain to get the root of Dahurain angelica powder for treating acute mastitis swelling and pain.The root of Dahurain angelica powder for the treatment of acute mastitis swelling and pain provided by the invention has excellent therapeutic effect.
Description
Technical field
The invention discloses a kind of root of Dahurain angelica powders and preparation method thereof for treating acute mastitis swelling and pain, belong to chinese medicine material technology neck
Domain.
Background technique
Acute mastitis is with breast congestion and swelling pain, and milk discharge is unsmooth, so that acute festering type disease of the knot purulence at carbuncle.It is mainly in
The puerpera of postpartum breastfeeding, especially primipara are more common.It is commonly called as mastitis.According to the difference of occurrent time, and there are several titles:
Nursing period person is betided, postpartum mastitis is claimed；Betide period of pregnancy person, name acute mastitis during pregnancy；Occur in non-lactation period and non-period of pregnancy
Person, name non-lactation period acute mastitis.The acute purulent mammitis of modern medicine belongs to acute mastitis scope.Existing traditional external physical therapy
Acute mastitis swelling and pain are treated since pain coefficient is very high, so that the therapeutic effect decline of acute mastitis swelling and pain, and caused many other
Problem, therefore develop that a kind of therapeutic effect is good and root of Dahurain angelica powder easy to use needs in a hurry.
Summary of the invention
It is existing to solve the purpose of the present invention is to provide a kind of root of Dahurain angelica powder and preparation method thereof for treating acute mastitis swelling and pain
The problems in technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain, the raw material including following parts by weight: the 3-5 parts of broken angles of Radix Notoginseng, 6-8 parts
Olibanum, 80~100 parts of roots of Dahurain angelica, 2~3 parts are worked as angelica body, 1~2 portion of fritillaria thunbergii.
The Radix Notoginseng is to grind root in class cone or cylindrical, long 1~6cm, the medicinal material of diameter about 1~4cm, the Radix Notoginseng
Broken angle is the Radix Notoginseng powder after clean dry and fine ground powder.
The olibanum is that volatile oil 3~8% is modified to be made by resin 60~70%, natural gum 27~35%.
The root of Dahurain angelica is up to 2.5 meters, and stem thickness is big, and being bordering on cylindrical base portion, slightly about 5~9 centimetres of perennial herbs are planted
Object, the root of Dahurain angelica are to take its root, are ground for superfine end, be incorporated into a bottle be sufficiently stirred with it is even, adhere to using injection water changes
Property be made.
The Radix Angelicae Sinensis has supporting root 3~5 or more as lower part, long 15~25cm.For surface yellowish-brown to sepia, tool is vertical
The medicinal material of wrinkle and horizontally long hole skin, it is described.
The Radix Angelicae Sinensis has supporting root 3~5 or more as lower part, long 15~25cm.For surface yellowish-brown to sepia, tool is vertical
The medicinal material of wrinkle and horizontally long hole skin, it is described.
The root of Dahurain angelica powder of the treatment acute mastitis swelling and pain includes the raw material of following parts by weight: 20 parts of mixed glue solutions, 10 parts change
Property diatomite, 100 parts of modified sawdusts, 3 parts of low-melting alloys, 2 parts of odium stearate.
A kind of preparation method of root of Dahurain angelica powder that treating acute mastitis swelling and pain, it is specific the preparation method is as follows:
(1) match frankincense solution；
(2) fritillaria thunbergii is handled；
(3) the broken angle of Radix Notoginseng is prepared；
(4) angelica body is worked as in processing；
(5) mixing, molding；
(6) it encapsulates；
(7) it detects.
The preparation step of the root of Dahurain angelica powder of the treatment acute mastitis swelling and pain are as follows:
(1) gummy by resin, volatile oil, water is stirred, and obtains olibanum solution；
(2) fritillaria thunbergii is added in olibanum solution, the neutral Precerving liquid in part and water mixed precipitation are subsequently added into pure water
Solution is stirred, and is filtered, and is washed, and is freezed, and is crushed, sieving, dry to get bulb of thunberg fritillary rubber master batch turbid；
(3) Radix Notoginseng, cleaning, drying are taken, fine ground powder takes net Radix Notoginseng to smash, and size block is separated, with edible frying to surface palm fibre
Yellow is taken out, and oil is leached, and finely ground powder is added organic siliconresin and is placed in batch mixer, then be drawn off, cleans, and steams thoroughly, takes out,
Slice in time, dry the broken angle of Radix Notoginseng；
(4) property of will volatilize oil is mixed with water, and after standing swelling, heating stirring dissolution is subsequently added into and works as angelica body, pure water,
Sucrose mixed precipitation, adds ethereal oil, is subsequently added into sodium bicarbonate and adjusts pH to 7.8~8.1, be stirred, filter, does
It is dry, it is subsequently added into ice crystal, mixing and ball milling is sieved, and cooling low-temperature treatment obtains Radix Angelicae Sinensis material material；
(5) by olibanum, when angelica body mixing and ball milling the broken angle mixing of Radix Notoginseng is then added, injection molding is hot-forming, takes off in the root of Dahurain angelica
Mould, it is dry, obtain drying material；
(6) drying material is placed in sterile workshop encapsulation, vacuumized, seal the root of Dahurain angelica powder to get treatment acute mastitis swelling and pain；
(7) properties of product detect.
The specific preparation process of the root of Dahurain angelica powder of the treatment acute mastitis swelling and pain are as follows:
(1) gummy by resin, volatile oil, water is placed in large size beaker, under the conditions of revolving speed is 300~500r/min, is stirred
40~60min of mixing is mixed, olibanum solution is obtained；
(2) fritillaria thunbergii, olibanum solution, part neutrality Precerving liquid and water mixing are placed in large size stillpot, are in temperature
Under the conditions of 32~35 DEG C, precipitate 3~5 days, then into large size stillpot be added mass fraction be 10~20% it is pure water-soluble
Liquid, under the conditions of revolving speed is 400~600r/min, after being stirred 40~60min, filtering obtains filter residue, then uses deionized water
By residue washing 3~5 times, then the filter residue after washing is placed in liquid nitrogen and is freezed, obtained frozen block, frozen block is then placed in powder
After being crushed in broken machine, the sieve of 360 mesh is crossed, crushed material is obtained, then crushed material is placed in vacuum freezing drying oven and is dried to get Zhejiang
Fritillaria glue turbid；
(3) Radix Notoginseng 100g, cleaning, drying are taken, fine ground powder is added organic siliconresin and is placed in the funnel of batch mixer, counterweight
Block can be with steady operation, the switch being then first turned on station on operation panel, then toward filling the water in water tank, passes through later
Water closes, and opens water valve, is discharged from outlet, and knob is arranged, under the conditions of revolving speed is 1000~1200r/min, it is stirred 40~
60min, later by opening, outlet valve is pale brown to surface with 500 degrees Celsius of edible frying from discharge hole for discharge, then by it
Color is cleaned, and steam with the temperature of loss degree Celsius in boiler, is taken out, and is sliced in time, dry that Radix Notoginseng is broken
Angle；
(4) peach gum powder and water are placed in No. 2 beakers, and stir 10~20min with glass bar, after standing 3~5h of swelling,
No. 2 beakers are placed in digital display to test the speed in constant temperature blender with magnetic force, are 90~95 DEG C in temperature, revolving speed is 600~800r/min item
Under part, heating stirring dissolves 40~60min, obtains peach colloidal solution, and then by peach colloidal solution, diatomite, biogas slurry, sucrose is placed in No. 2 fermentations
In kettle, under the conditions of temperature is 28~32 DEG C, mixed fermentation 5~8 days, rethinking and mass fraction is added in fermentation cauldron was 10~20%
Aluminum nitrate solution, be subsequently added into mass fraction be 20~30% ammonium hydroxide adjust pH to 7.8~8.1, in revolving speed be 600~
Under the conditions of 800r/min, after being stirred 40~60min, filtering obtains filter cake, then filter cake is placed in baking oven, is in temperature
It is dry to constant weight under the conditions of 105~110 DEG C, dry cake is obtained, then dry cake and ice crystal are placed in No. 1 ball mill
Mixing and ball milling, cross 120 mesh sieve, obtain ball milling material, then ball milling material be placed in sintering furnace, and with 60~90mL/min rate to
It is filled with nitrogen in furnace, is then warming up to 1450~1550 DEG C with 8~10 DEG C of heating rates, and be passed through 280~320kA direct current,
After 1~2h of energization high-temperature process, it is down to room temperature with furnace, obtains modification infusorial earth；
(5) by olibanum, the root of Dahurain angelica obtains ball milling powder, will mix when angelica body and fritillaria thunbergii are placed in mixing and ball milling in small size ball mill
It closes ball milling powder to be placed in blender, the broken angle of Radix Notoginseng is added followed by atomizing lance, followed by the atomization that mixing liquid feeding is added
The broken angle of Radix Notoginseng is added into blender for spray gun, under the conditions of revolving speed is 1000~1200r/min, is stirred 40~60r/min,
Homogenate must be mixed, then will be in mixing homogenate injection mold, then mold is placed in hot press, in temperature be 180~195 DEG C of items
Under part, after hot-forming, demoulding obtains core material, then core material is placed in baking oven, under the conditions of temperature is 105~110 DEG C, does
It is dry to constant weight, obtain drying material；
(6) drying material is placed in sterile workshop encapsulation, after being evacuated to 0.03~0.05Pa, sealing is to get treatment cream
The root of Dahurain angelica powder of carbuncle and painful swelling；
(7) properties of product detect.
Compared with prior art, the beneficial effects of the present invention are:
(1) by the present invention in that with centering Chinese medicine, including the broken angle of Radix Notoginseng, during the preparation process, so that the effect of Radix Notoginseng
Further promoted, furthermore, some Chinese medicines used, not any side effect, and be deposited in calcium carbonate microspheres
Some Chinese traditional medicine molecules are heated in the hot pressing in later period, in system occurs explosive decomposition, and releases some of oneself
Element so that in therapeutic process can better exposing cell so that treatment acute mastitis swelling and pain therapeutic effect obtain into
One step is promoted；
(2) present invention is obtained by addition olibanum, the root of Dahurain angelica when angelica body and fritillaria thunbergii are placed in mixing and ball milling in small size ball mill
Ball milling powder can preferably absorb, and then mixing and ball milling powder is placed in blender, and Radix Notoginseng is added using atomizing lance later
Broken angle the broken angle of Radix Notoginseng is added into blender followed by the atomizing lance that mixing liquid feeding is added, then by the way that sodium bicarbonate is added
PH is adjusted, so that the pH value in system is more suitable for human body, so that the therapeutic effect of acute mastitis swelling and pain is further promoted.
Detailed description of the invention
Fig. 1 is batch mixer device overall structure diagram；
Fig. 2 is entire manufacturing process structural schematic diagram.
Drawing reference numeral: 1, clump weight；2, station；3, water tank；4, Shui Guan；5, water valve；6, it exports；7, funnel；8, it is discharged
Valve；9, discharge port；10, operation panel；11, knob；12, it switchs.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Example 1
A kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain, the raw material including following parts by weight: 3 parts of broken angles of Radix Notoginseng, 6 parts of creams
Perfume (or spice), 80 parts of roots of Dahurain angelica, 2 parts are worked as angelica body, 1 portion of fritillaria thunbergii.
The Radix Notoginseng is to grind root in class cone or cylindrical, long 1~6cm, the medicinal material of diameter about 1~4cm.
The olibanum is that volatile oil 3~8% is modified to be made by resin 60~70%, natural gum 27~35%.
The root of Dahurain angelica is up to 2.5 meters, and stem thickness is big, and being bordering on cylindrical base portion, slightly about 5~9 centimetres of perennial herbs are planted
Object.
The Radix Angelicae Sinensis has supporting root 3~5 or more as lower part, long 15~25cm.
The root of Dahurain angelica powder of the treatment acute mastitis swelling and pain includes the raw material of following parts by weight: 20 parts of broken angles of Radix Notoginseng, 10 parts of creams
Perfume (or spice), 100 parts of roots of Dahurain angelica, 3 parts are worked as angelica body, 2 portions of fritillaria thunbergiis.
The specific preparation process of the root of Dahurain angelica powder of the treatment acute mastitis swelling and pain are as follows:
(1) according to parts by weight, successively by 2 parts of resins, 1 part of natural gum, 5 parts of volatile oil, water is placed in large size beaker, in turning
Under the conditions of speed is 300~500r/min, it is stirred 40~60min, obtains olibanum solution；
(2) according to parts by weight, 3 portions of fritillaria thunbergiis, 5 parts of olibanum solution, 2 parts of neutral Precerving liquids in part and 1 part of water are successively taken
Mixing is placed in large size stillpot, under the conditions of temperature is 32~35 DEG C, is precipitated 3~5 days, is then added into large size stillpot
The pure aqueous solution that mass fraction is 10~20% is stirred 40~60min under the conditions of revolving speed is 400~600r/min
Afterwards, it filters, obtains filter residue, then with deionized water by residue washing 3~5 times, be then placed in the filter residue after washing cold in liquid nitrogen
Freeze, obtain frozen block, then frozen block is placed in pulverizer after crushing, crosses the sieve of 360 mesh, crushed material is obtained, then by crushed material
It is placed in vacuum freezing drying oven and dries to get bulb of thunberg fritillary rubber master batch turbid；
(3) according to parts by weight, Radix Notoginseng 100g is successively taken, cleaning, drying, fine ground powder, addition organic siliconresin is placed in mixed
In the funnel 7 of material machine, clump weight 1 can be with steady operation, the switch 12 being then first turned on station 2 on operation panel 10,
Then toward the inner water filling of water tank 3, later by water close 4, open water valve 5, from outlet 6 be discharged, be arranged knob 11, in revolving speed be 1000
Under the conditions of~1200r/min, be stirred 40~60min, later by open, outlet valve 8, from discharge port 9 discharge, then by its
With 500 degrees Celsius of edible fryings to surface brown color, is cleaned, steamed in boiler with the temperature of loss degree Celsius
Thoroughly, it takes out, is sliced in time, dry the broken angle of Radix Notoginseng；
(4) according to parts by weight, successively 3 parts of ethereal oils and 2 parts of water are placed in small size beaker, and are stirred with glass bar
After standing 3~5h of swelling, small size beaker is placed in oil bath pan by 10~20min, in temperature be 90~95 DEG C, revolving speed 600
Under the conditions of~800r/min, heating stirring dissolves 40~60min, obtains 2 parts of peach colloidal solutions, then by 2 parts of peach colloidal solutions, works as angelica body, pure
Water purification, sucrose are placed in small size stillpot, under the conditions of temperature is 28~32 DEG C, mixed precipitation 5~8 days, then into stillpot
Be added mass fraction be 10~20% ethereal oil, be subsequently added into mass fraction be 20~30% sodium bicarbonate adjust pH to
7.8~8.1, under the conditions of revolving speed is 600~800r/min, after being stirred 40~60min, filtering obtains filter cake, then will filter
Cake is placed in baking oven, dry to constant weight under the conditions of temperature is 105~110 DEG C, obtains dry cake, then by dry cake and
Ice crystal is placed in mixing and ball milling in large size ball mill, crosses the sieve of 120 mesh, obtains ball milling material, then ball milling material is placed in sintering furnace,
Then 1450~1550 DEG C are warming up to 8~10 DEG C of heating rates, and are passed through 280~320kA direct current, cooling low-temperature treatment 1
After~2h, it is down to room temperature with furnace, obtains Radix Angelicae Sinensis material material；
(5) according to parts by weight, successively by 3 parts of olibanums, 2 parts of roots of Dahurain angelica, 4 parts are placed in small size when angelica body and 5 portions of fritillaria thunbergiis
Mixing and ball milling in grinding machine obtains ball milling powder, and mixing and ball milling powder is placed in blender, and it is broken that Radix Notoginseng is added followed by atomizing lance
Angle, followed by be added mixing liquid feeding atomizing lance the broken angle of Radix Notoginseng is added into blender, in revolving speed be 1000~1200r/
Under the conditions of min, it is stirred 40~60r/min, obtains mixing homogenate, then mixing is homogenized in injection mold, then mold is set
In hot press, under the conditions of temperature is 180~195 DEG C, after hot-forming, demoulding obtains core material, core material is then placed in baking oven
In, it is dry to constant weight under the conditions of temperature is 105~110 DEG C, obtain drying material；
(6) dry core material is placed in sterile workshop encapsulation, after being evacuated to 0.05Pa, sealing is to get treatment acute mastitis swelling and pain
Root of Dahurain angelica powder；
(7) properties of product detect.
Example 2
A kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain, the raw material including following parts by weight: 3 parts of broken angles of Radix Notoginseng, 6 parts of creams
Perfume (or spice), 80 parts of roots of Dahurain angelica, 2 parts are worked as angelica body, 1 portion of fritillaria thunbergii.
The Radix Notoginseng is to grind root in class cone or cylindrical, long 1~6cm, the medicinal material of diameter about 1~4cm.
The olibanum is that volatile oil 3~8% is modified to be made by resin 60~70%, natural gum 27~35%.
The root of Dahurain angelica is up to 2.5 meters, and stem thickness is big, and being bordering on cylindrical base portion, slightly about 5~9 centimetres of perennial herbs are planted
Object.
The Radix Angelicae Sinensis has supporting root 3~5 or more as lower part, long 15~25cm.
The root of Dahurain angelica powder of the treatment acute mastitis swelling and pain includes the raw material of following parts by weight: 20 parts of broken angles of Radix Notoginseng, 10 parts of creams
Perfume (or spice), 100 parts of roots of Dahurain angelica, 3 parts are worked as angelica body, 2 portions of fritillaria thunbergiis.
The specific preparation process of the root of Dahurain angelica powder of the treatment acute mastitis swelling and pain are as follows:
(1) according to parts by weight, successively by 3 parts of resins, 2 parts of natural gum, 6 parts of volatile oil, water is placed in large size beaker, in turning
Under the conditions of speed is 400~700r/min, it is stirred 60min, obtains olibanum solution；
(2) according to parts by weight, 1 portion of fritillaria thunbergii, 3 parts of olibanum solution, 4 parts of neutral Precerving liquids in part and 1 part of water are successively taken
Mixing is placed in large size stillpot, under the conditions of temperature is 36 DEG C, sinks 6 days, mass fraction then is added into large size stillpot
For 10~20% pure aqueous solution, under the conditions of revolving speed is 700r/min, after being stirred 40~60min, filtering must be filtered
Filter residue after washing is then then placed in liquid nitrogen and is freezed, obtain frozen block with deionized water by slag by residue washing 3~5 times,
Then frozen block is placed in pulverizer after crushing, crosses the sieve of 360 mesh, obtains crushed material, crushed material is then placed in vacuum refrigeration
It dries in drying box to get bulb of thunberg fritillary rubber master batch turbid；
(3) according to parts by weight, Radix Notoginseng 100g, cleaning, drying are taken, fine ground powder is added organic siliconresin and is placed in batch mixer
Funnel 7 in, clump weight 1 can be with steady operation, the switch 12 being then first turned on station 2 on operation panel 10, then
Toward the inner water filling of water tank 3, close 4 by water later, open water valve 5, be discharged from outlet 6, knob 11 is set, in revolving speed for 1000~
Under the conditions of 1200r/min, it is stirred 40~60min, later by opening, outlet valve 8 discharges from discharge port 9, then used
500 degrees Celsius of edible frying is cleaned, is steamed in boiler with the temperature of loss degree Celsius to surface brown color
Thoroughly, it takes out, is sliced in time, dry the broken angle of Radix Notoginseng；
(4) according to parts by weight, successively 4 parts of ethereal oils and 1 part of water are placed in small size beaker, and are stirred with glass bar
After standing swelling 6h, small size beaker is placed in oil bath pan by 30min, in temperature be 90~95 DEG C, revolving speed 1000r/min
Under the conditions of, heating stirring dissolves 80min, obtains 5 parts of peach colloidal solutions, then by 7 parts of peach colloidal solutions, works as angelica body, pure water, sucrose is placed in small
In number stillpot, under the conditions of temperature is 28~32 DEG C, mixed precipitation 5~8 days, then mass fraction is added into stillpot and is
40% ethereal oil is subsequently added into the sodium bicarbonate that mass fraction is 20~30% and adjusts pH to 7.8~8.1, is in revolving speed
Under the conditions of 1000r/min, after being stirred 60min, filtering, obtain filter cake, then filter cake be placed in baking oven, in temperature be 210
It is dry to constant weight under the conditions of DEG C, dry cake is obtained, then dry cake and ice crystal are placed in large size ball mill and mix ball
Mill is crossed the sieve of 360 mesh, obtains ball milling material, then ball milling material is placed in sintering furnace, be then warming up to 8~10 DEG C of heating rates
1450~1550 DEG C, and it is passed through 280~320kA direct current, after cooling 1~2h of low-temperature treatment, it is down to room temperature with furnace, obtains Radix Angelicae Sinensis material
Material；
(5) according to parts by weight, successively by 5 parts of olibanums, 1 part of root of Dahurain angelica, 7 parts are placed in small size when angelica body and 5 portions of fritillaria thunbergiis
Mixing and ball milling in grinding machine obtains ball milling powder, and mixing and ball milling powder is placed in blender, and it is broken that Radix Notoginseng is added followed by atomizing lance
Angle, followed by be added mixing liquid feeding atomizing lance the broken angle of Radix Notoginseng is added into blender, in revolving speed be 800r/min condition
Under, it is stirred 40~60r/min, obtains mixing homogenate, then mixing is homogenized in injection mold, then mold is placed in hot press
In, under the conditions of temperature is 180~195 DEG C, after hot-forming, demoulding obtains core material, then core material is placed in baking oven, Yu Wen
It is dry to constant weight under the conditions of degree is 200 DEG C, obtain drying material；
(6) dry core material is placed in sterile workshop encapsulation, after being evacuated to 0.1Pa, sealed to get treatment acute mastitis swelling and pain
Root of Dahurain angelica powder；
(7) properties of product detect.
Comparative example
A kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain, the raw material including following parts by weight: 3 parts of broken angles of Radix Notoginseng, 6 parts of creams
Perfume (or spice), 80 parts of roots of Dahurain angelica, 2 parts are worked as angelica body, 1 portion of fritillaria thunbergii.
The Radix Notoginseng is to grind root in class cone or cylindrical, long 1~6cm, the medicinal material of diameter about 1~4cm.
The olibanum is that volatile oil 3~8% is modified to be made by resin 60~70%, natural gum 27~35%.
The root of Dahurain angelica is up to 2.5 meters, and stem thickness is big, and being bordering on cylindrical base portion, slightly about 5~9 centimetres of perennial herbs are planted
Object.
The Radix Angelicae Sinensis has supporting root 3~5 or more as lower part, long 15~25cm.
The root of Dahurain angelica powder of the treatment acute mastitis swelling and pain includes the raw material of following parts by weight: 20 parts of broken angles of Radix Notoginseng, 10 parts of creams
Perfume (or spice), 100 parts of roots of Dahurain angelica, 3 parts are worked as angelica body, 2 portions of fritillaria thunbergiis.
The specific preparation process of the root of Dahurain angelica powder of the treatment acute mastitis swelling and pain are as follows:
(1) according to parts by weight, successively by 5 parts of resins, 1 part of natural gum, 4 parts of volatile oil, water is placed in large size beaker, in turning
Under the conditions of speed is 800r/min, it is stirred 30min, obtains olibanum solution；
(2) according to parts by weight, 1 portion of fritillaria thunbergii, 3 parts of olibanum solution, 4 parts of neutral Precerving liquids in part and 1 part of water are successively taken
Mixing is placed in large size stillpot, under the conditions of temperature is 36 DEG C, sinks 6 days, mass fraction then is added into large size stillpot
For 10~20% pure aqueous solution, under the conditions of revolving speed is 700r/min, after being stirred 40~60min, filtering must be filtered
Filter residue after washing is then then placed in liquid nitrogen and is freezed, obtain frozen block with deionized water by slag by residue washing 3~5 times,
Then frozen block is placed in pulverizer after crushing, crosses the sieve of 360 mesh, obtains crushed material, crushed material is then placed in vacuum refrigeration
It dries in drying box to get bulb of thunberg fritillary rubber master batch turbid；
(3) according to parts by weight, Radix Notoginseng 100g, cleaning, drying are taken, fine ground powder is added organic siliconresin and is placed in batch mixer
Funnel 7 in, clump weight 1 can be with steady operation, the switch 12 being then first turned on station 2 on operation panel 10, then
Toward the inner water filling of water tank 3, close 4 by water later, open water valve 5, be discharged from outlet 6, knob 11 is set, in revolving speed for 1000~
Under the conditions of 1200r/min, it is stirred 40~60min, later by opening, outlet valve 8 discharges from discharge port 9, then used
500 degrees Celsius of edible frying is cleaned, is steamed in boiler with the temperature of loss degree Celsius to surface brown color
Thoroughly, it takes out, is sliced in time, dry the broken angle of Radix Notoginseng；
(4) according to parts by weight, successively 8 parts of ethereal oils and 1 part of water are placed in small size beaker, and are stirred with glass bar
After standing swelling 3h, small size beaker is placed in oil bath pan by 30min, in temperature be 90~95 DEG C, revolving speed 1000r/min
Under the conditions of, heating stirring dissolves 80min, obtains 5 parts of peach colloidal solutions, then by 7 parts of peach colloidal solutions, works as angelica body, pure water, sucrose is placed in small
In number stillpot, under the conditions of temperature is 28~32 DEG C, mixed precipitation 9 days, then it is 40% that mass fraction, which is added, into stillpot
Ethereal oil, be subsequently added into mass fraction be 20~30% sodium bicarbonate adjust pH to 7.8~8.1, in revolving speed be 1000r/
Under the conditions of min, after being stirred 60min, filtering, obtain filter cake, then filter cake be placed in baking oven, in temperature be 210 DEG C of conditions
Under, it is dry to constant weight, dry cake is obtained, dry cake and ice crystal are then placed in mixing and ball milling in large size ball mill, crosses 360
Purpose sieve, obtains ball milling material, then ball milling material is placed in sintering furnace, then 1450 are warming up to 8~10 DEG C of heating rates~
1550 DEG C, and it is passed through 280~320kA direct current, after cooling 1~2h of low-temperature treatment, it is down to room temperature with furnace, obtains Radix Angelicae Sinensis material material；
(5) according to parts by weight, successively by 10 parts of olibanums, 8 parts of roots of Dahurain angelica, 6 parts are placed in small size when angelica body and 5 portions of fritillaria thunbergiis
Mixing and ball milling in grinding machine obtains ball milling powder, and mixing and ball milling powder is placed in blender, and it is broken that Radix Notoginseng is added followed by atomizing lance
Angle, followed by be added mixing liquid feeding atomizing lance the broken angle of Radix Notoginseng is added into blender, in revolving speed be 800r/min condition
Under, it is stirred 40~60r/min, obtains mixing homogenate, then mixing is homogenized in injection mold, then mold is placed in hot press
In, under the conditions of temperature is 180~195 DEG C, after hot-forming, demoulding obtains core material, then core material is placed in baking oven, Yu Wen
It is dry to constant weight under the conditions of degree is 200 DEG C, obtain drying material；
(6) dry core material is placed in sterile workshop encapsulation, after being evacuated to 0.1Pa, sealed to get treatment acute mastitis swelling and pain
Root of Dahurain angelica powder；
(7) properties of product detect.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (9)
1. a kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain, it is characterised in that: the raw material including following parts by weight: 3-5 portions of Radix Notoginseng
Broken angle, 6-8 parts of olibanums, 80~100 parts of roots of Dahurain angelica, 2~3 parts are worked as angelica body, 1~2 portion of fritillaria thunbergii.
2. a kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain according to claim 1, it is characterised in that: the Radix Notoginseng is to grind root
It is clean dry and fine ground powder in class cone or cylindrical, long 1~6cm, the medicinal material of diameter about 1~4cm, the broken angle of Radix Notoginseng
Radix Notoginseng powder afterwards.
3. a kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain according to claim 2, it is characterised in that: the olibanum is by setting
Rouge 60~70%, natural gum 27~35%, volatile oil 3~8% is modified to be made.
4. a kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain according to claim 3, it is characterised in that: the root of Dahurain angelica is up to
2.5 meters, stem thickness is big, is bordering on cylindrical base portion slightly about 5~9 centimetres of herbaceos perennials, and the root of Dahurain angelica is to take its root, grinds
For superfine end, be incorporated into a bottle be sufficiently stirred with it is even, adhere to using injection water is modified to be made.
5. a kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain according to claim 4, it is characterised in that: the Radix Angelicae Sinensis is as under
Portion has supporting root 3~5 or more, long 15~25cm.Surface yellowish-brown has the medicinal material of vertical wrinkle and horizontally long hole skin to sepia,
It is described.
6. a kind of root of Dahurain angelica powder for treating acute mastitis swelling and pain according to claim 5, it is characterised in that: the treatment acute mastitis is swollen
The root of Dahurain angelica powder of pain includes the raw material of following parts by weight: 20 parts of broken angles of Radix Notoginseng, 10 parts of olibanums, 100 parts of roots of Dahurain angelica, 3 parts are worked as angelica body,
2 portions of fritillaria thunbergiis.
7. a kind of preparation method for the root of Dahurain angelica powder for treating acute mastitis swelling and pain, it is characterised in that it is specific the preparation method is as follows:
(1) match frankincense solution；
(2) fritillaria thunbergii is handled；
(3) the broken angle of Radix Notoginseng is prepared；
(4) angelica body is worked as in processing；
(5) mixing, molding；
(6) it encapsulates；
(7) it detects.
8. a kind of preparation method of root of Dahurain angelica powder for treating acute mastitis swelling and pain according to claim 7, it is characterised in that: described
The preparation step for treating the root of Dahurain angelica powder of acute mastitis swelling and pain are as follows:
(1) gummy by resin, volatile oil, water is stirred, and obtains olibanum solution；
(2) fritillaria thunbergii is added in olibanum solution, the neutral Precerving liquid in part and water mixed precipitation are subsequently added into pure water-soluble
Liquid is stirred, and is filtered, and is washed, and is freezed, and is crushed, sieving, dry to get bulb of thunberg fritillary rubber master batch turbid；
(3) Radix Notoginseng, cleaning, drying are taken, fine ground powder takes net Radix Notoginseng to smash, and separates size block, pale brown to surface with edible frying
Color takes out, and leaches oil, and finely ground powder is added organic siliconresin and is placed in batch mixer, then be drawn off, cleans, and steams thoroughly, takes out, and
When be sliced, dry the broken angle of Radix Notoginseng；
(4) property of will volatilize oil is mixed with water, and after standing swelling, heating stirring dissolution is subsequently added into and works as angelica body, pure water, sucrose
Mixed precipitation adds ethereal oil, is subsequently added into sodium bicarbonate and adjusts pH to 7.8~8.1, be stirred, filters, dry, connects
Addition ice crystal, mixing and ball milling, sieving, cooling low-temperature treatment obtain Radix Angelicae Sinensis material material；
(5) by olibanum, when angelica body mixing and ball milling the broken angle mixing of Radix Notoginseng is then added, injection molding is hot-forming, demoulds, and does in the root of Dahurain angelica
It is dry, obtain drying material；
(6) drying material is placed in sterile workshop encapsulation, vacuumized, seal the root of Dahurain angelica powder to get treatment acute mastitis swelling and pain；
(7) properties of product detect.
9. a kind of preparation method of root of Dahurain angelica powder for treating acute mastitis swelling and pain according to claim 8, it is characterised in that: described
The specific preparation process for treating the root of Dahurain angelica powder of acute mastitis swelling and pain are as follows:
(1) by resin, natural gum, volatile oil, water is placed in large size beaker, under the conditions of revolving speed is 300~500r/min, is stirred mixed
40~60min is closed, olibanum solution is obtained；
(2) by fritillaria thunbergii, olibanum solution, the neutral Precerving liquid in part and water mixing are placed in large size stillpot, in temperature be 32~
Under the conditions of 35 DEG C, precipitates 3~5 days, the pure aqueous solution that mass fraction is 10~20% is then added into large size stillpot, in
Under the conditions of revolving speed is 400~600r/min, after being stirred 40~60min, filtering obtains filter residue, will then be filtered with deionized water
Wash heat is washed 3~5 times, and then the filter residue after washing is placed in liquid nitrogen and is freezed, and obtains frozen block, frozen block is then placed in pulverizer
After middle crushing, the sieve of 360 mesh is crossed, crushed material is obtained, then crushed material is placed in vacuum freezing drying oven and is dried to get fritillaria thunbergii
Glue turbid；
(3) Radix Notoginseng 100g, cleaning, drying are taken, fine ground powder is added organic siliconresin and is placed in the funnel (7) of batch mixer, clump weight
(1) can be with steady operation, the switch (12) being then first turned on station (2) on operation panel (10), then toward water tank (3)
In fill the water, later by water close (4), open water valve (5), from outlet (6) be discharged, be arranged knob (11), in revolving speed be 1000~
Under the conditions of 1200r/min, it is stirred 40~60min, later by opening, outlet valve (8) discharges from discharge port (9), then will
It, to surface brown color, is cleaned, is carried out in boiler with the temperature of loss degree Celsius with 500 degrees Celsius of edible frying
It steams thoroughly, takes out, be sliced in time, dry the broken angle of Radix Notoginseng；
(4) peach gum powder and water are placed in No. 2 beakers, and stir 10~20min with glass bar, after standing 3~5h of swelling, by 2
Number beaker is placed in digital display and tests the speed in constant temperature blender with magnetic force, is 90~95 DEG C in temperature, revolving speed is 600~800r/min condition
Under, heating stirring dissolves 40~60min, obtains peach colloidal solution, and then by peach colloidal solution, diatomite, biogas slurry, sucrose is placed in No. 2 fermentation cauldrons
In, under the conditions of temperature is 28~32 DEG C, mixed fermentation 5~8 days, rethinking and mass fraction is added in fermentation cauldron was 10~20%
Aluminum nitrate solution, be subsequently added into mass fraction be 20~30% ammonium hydroxide adjust pH to 7.8~8.1, in revolving speed be 600~
Under the conditions of 800r/min, after being stirred 40~60min, filtering obtains filter cake, then filter cake is placed in baking oven, is in temperature
It is dry to constant weight under the conditions of 105~110 DEG C, dry cake is obtained, then dry cake and ice crystal are placed in No. 1 ball mill
Mixing and ball milling, cross 120 mesh sieve, obtain ball milling material, then ball milling material be placed in sintering furnace, and with 60~90mL/min rate to
It is filled with nitrogen in furnace, is then warming up to 1450~1550 DEG C with 8~10 DEG C of heating rates, and be passed through 280~320kA direct current,
After 1~2h of energization high-temperature process, it is down to room temperature with furnace, obtains modification infusorial earth；
(5) by olibanum, the root of Dahurain angelica obtains ball milling powder, will mix ball when angelica body and fritillaria thunbergii are placed in mixing and ball milling in small size ball mill
Milling is placed in blender, the broken angle of Radix Notoginseng is added followed by atomizing lance, followed by the atomizing lance that mixing liquid feeding is added
The broken angle of Radix Notoginseng is added into blender, under the conditions of revolving speed is 1000~1200r/min, is stirred 40~60r/min, obtains mixed
Close homogenate, then will be in mixing homogenate injection mold, then mold is placed in hot press, in temperature be 180~195 DEG C of conditions
Under, after hot-forming, demoulding obtains core material, then core material is placed in baking oven, dry under the conditions of temperature is 105~110 DEG C
To constant weight, drying material is obtained；
(6) drying material is placed in sterile workshop encapsulation, after being evacuated to 0.03~0.05Pa, sealing is swollen to get treatment acute mastitis
The root of Dahurain angelica powder of pain；
(7) properties of product detect.
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Citations (3)
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| CN1899351A (en) * | 2006-07-06 | 2007-01-24 | 张喜堂 | Medicine for treating hyperplasia of mammary glands and its preparing method |
| CN105311350A (en) * | 2014-06-30 | 2016-02-10 | 陈希 | Radix angelicae powder for treating swelling and pain of mastitis |
| CN109940161A (en) * | 2019-03-11 | 2019-06-28 | 肖剑 | A kind of iron base composite material and preparation method thereof of micro/nano level Carbon fibe enhancing |
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2019
- 2019-07-05 CN CN201910602195.XA patent/CN110179913A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1899351A (en) * | 2006-07-06 | 2007-01-24 | 张喜堂 | Medicine for treating hyperplasia of mammary glands and its preparing method |
| CN105311350A (en) * | 2014-06-30 | 2016-02-10 | 陈希 | Radix angelicae powder for treating swelling and pain of mastitis |
| CN109940161A (en) * | 2019-03-11 | 2019-06-28 | 肖剑 | A kind of iron base composite material and preparation method thereof of micro/nano level Carbon fibe enhancing |
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