CN110179845A - A kind of Yellow Fructus Gardeniae electuary and preparation method thereof - Google Patents
A kind of Yellow Fructus Gardeniae electuary and preparation method thereof Download PDFInfo
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- CN110179845A CN110179845A CN201910560180.1A CN201910560180A CN110179845A CN 110179845 A CN110179845 A CN 110179845A CN 201910560180 A CN201910560180 A CN 201910560180A CN 110179845 A CN110179845 A CN 110179845A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/233—Bupleurum
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/287—Chrysanthemum, e.g. daisy
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/74—Rubiaceae (Madder family)
- A61K36/744—Gardenia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
- A61K9/1605—Excipients; Inactive ingredients
- A61K9/1629—Organic macromolecular compounds
- A61K9/1652—Polysaccharides, e.g. alginate, cellulose derivatives; Cyclodextrin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P39/00—General protective or antinoxious agents
- A61P39/02—Antidotes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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Abstract
The invention discloses a kind of Yellow Fructus Gardeniae electuaries, are made from the following raw materials in parts by weight: Yellow Fructus Gardeniae 10-12, inonotus obliquus 8-10, honeysuckle 5-7, radix bupleuri 6-8, chrysanthemum 5-7, almond powder 5-7, microcrystalline cellulose 3-5, maltodextrin 60-80, sucrose 30-40, lactose 30-40, beta-cyclodextrin 1-2, bacteria cellulose 4-5.The Chinese herbal medicines such as Yellow Fructus Gardeniae, inonotus obliquus are added in formula of the invention, have the function of it is clearing heat and detoxicating, improve the immunity of the human body;And Chinese herbal medicine is concentrated at normal temperature with the extraction of high-pressure pulse electric method, then using freeze concentration method, is avoided high temperature and is extracted, is concentrated so that the heat-sensitive ingredients in Chinese herbal medicine are destroyed;In addition, the bacteria cellulose added in the present invention as dispersing agent, can be improved the dispersibility of water-insoluble materials in the solution in electuary.
Description
Technical field
The present invention relates to technical field of traditional Chinese medicines more particularly to a kind of Yellow Fructus Gardeniae electuary and preparation method thereof.
Background technique
" excessive internal heat " is that civil common saying also known as " hot gas " can be explained from theory of traditional Chinese medical science, belong to Heat Syndrome of TCM scope.Chinese medicine
Think that yin-Yang is unbalance, endogenous fire is vigorous, i.e., can get angry.Therefore so-called " fire " is to describe certain hot symptoms in body,
And excessive internal heat i.e. the unbalance rear interior heat symptom-complex occurred of yin-Yang are waited, specific symptom such as inflamed eyes, perleche, yellow urine, tooth
Bitterly, sore-throat etc.." excessive internal heat " is easier to occur in dry climate and unbroken damp and hot weather.
With the development of society, people's lives, operating pressure are increasing, along with irregular diet and work and rest are practised
Used, the people of excessive internal heat is also more and more.But the product for having clearing heat and detoxicating lower fiery effect on the market is seldom.
Summary of the invention
In order to solve the problems, such as to be previously mentioned in above-mentioned background technique, the present invention provides a kind of Yellow Fructus Gardeniae electuary and its preparations
Method, Yellow Fructus Gardeniae electuary obtained have clearing heat and detoxicating effect.
A kind of Yellow Fructus Gardeniae electuary, is made from the following raw materials in parts by weight: Yellow Fructus Gardeniae 10-12, inonotus obliquus 8-10, honeysuckle 5-
7, radix bupleuri 6-8, chrysanthemum 5-7, almond powder 5-7, microcrystalline cellulose 3-5, maltodextrin 60-80, sucrose 30-40, lactose 30-40,
Beta-cyclodextrin 1-2, bacteria cellulose 4-5.
The invention also discloses a kind of preparation methods of Yellow Fructus Gardeniae electuary, comprising the following steps:
(1) by Yellow Fructus Gardeniae, inonotus obliquus, honeysuckle, radix bupleuri, chrysanthemum co-grinding, water is added to carry out off field in high-voltage pulse electric
It extracts, filtering and removing slag obtain extracting solution;
(2) medicinal extract, gained medicinal extract and almond powder, microcrystalline cellulose, maltodextrin, sugarcane is made in extracting solution freeze concentration
Sugar, lactose, beta-cyclodextrin, bacteria cellulose mixing, be added ethyl alcohol adjust humidity of materials to material can hand pinch agglomerating, obtain soft
Material;
(3) softwood is granulated, is dry, sieving, pack to get.
Further, the weight of added water is that Yellow Fructus Gardeniae, inonotus obliquus, honeysuckle, radix bupleuri, chrysanthemum are total in the step (1)
8-12 times of weight.
Further, the electric field strength of the high-pressure pulse electric in the step (1) is 18kVcm-1, pulse frequency be
300Hz, burst length 20-30min, Extracting temperature are 25-30 DEG C.
Further, the freeze concentration in the step (2) is that extracting solution is sent into freeze concentration machine, in condenser temperature
Freeze concentration is carried out under conditions of being -30 to -20 DEG C, stops freezing when volume is reduced to the 10-15% of extracting liquid volume.
Further, the drying temperature in the step (3) is 40-45 DEG C, and drying time is 4-5 hours.
The beneficial effects of the present invention are:
The Chinese herbal medicines such as Yellow Fructus Gardeniae, inonotus obliquus are added in formula of the invention, have it is clearing heat and detoxicating, improve the immunity of the human body
Effect;And Chinese herbal medicine is concentrated at normal temperature with the extraction of high-pressure pulse electric method, then using freeze concentration method, avoids height
Temperature is extracted, is concentrated so that the heat-sensitive ingredients in Chinese herbal medicine are destroyed;In addition, the bacteria cellulose conduct added in the present invention
Dispersing agent can be improved the dispersibility of water-insoluble materials in the solution in electuary.
Specific embodiment
Technical solution of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of Yellow Fructus Gardeniae electuary, is made from the following raw materials in parts by weight: Yellow Fructus Gardeniae 10, inonotus obliquus 8, honeysuckle 5, radix bupleuri 6,
Chrysanthemum 5, almond powder 5, microcrystalline cellulose 3, maltodextrin 60, sucrose 30, lactose 30, beta-cyclodextrin 1, bacteria cellulose 4.
A kind of preparation method of Yellow Fructus Gardeniae electuary, comprising the following steps:
(1) by Yellow Fructus Gardeniae, inonotus obliquus, honeysuckle, radix bupleuri, chrysanthemum co-grinding, add 8 times of water high-voltage pulse electric off field
It extracts, wherein the electric field strength of high-pressure pulse electric is 18kVcm-1, pulse frequency 300Hz, burst length be
20min, Extracting temperature are 30 DEG C, using slag is filtered out, obtain extracting solution;
(2) extracting solution is sent into freeze concentration machine, carries out freeze concentration under conditions of condenser temperature is -30 DEG C, to
Volume stops freezing when being reduced to the 10% of extracting liquid volume, obtains medicinal extract, gained medicinal extract and almond powder, microcrystalline cellulose, wheat
Bud dextrin, sucrose, lactose, beta-cyclodextrin, bacteria cellulose mixing, be added ethyl alcohol adjust humidity of materials to material can hand pinch into
Group, obtains softwood;
(3) softwood is granulated, then dry 4 hours at 40 DEG C, using sieve, pack to get.
Embodiment 2
A kind of Yellow Fructus Gardeniae electuary, is made from the following raw materials in parts by weight: Yellow Fructus Gardeniae 12, inonotus obliquus 10, honeysuckle 7, radix bupleuri
8, chrysanthemum 7, almond powder 7, microcrystalline cellulose 5, maltodextrin 80, sucrose 40, lactose 40, beta-cyclodextrin 2, bacteria cellulose 5.
A kind of preparation method of Yellow Fructus Gardeniae electuary, comprising the following steps:
(1) by Yellow Fructus Gardeniae, inonotus obliquus, honeysuckle, radix bupleuri, chrysanthemum co-grinding, add 12 times of water in high-pressure pulse electric
Under extract, wherein the electric field strength of high-pressure pulse electric be 18kVcm-1, pulse frequency 300Hz, burst length be
30min, Extracting temperature are 25 DEG C, using slag is filtered out, obtain extracting solution;
(2) extracting solution is sent into freeze concentration machine, carries out freeze concentration under conditions of condenser temperature is -30 DEG C, to
Volume stops freezing when being reduced to the 15% of extracting liquid volume, obtains medicinal extract, gained medicinal extract and almond powder, microcrystalline cellulose, wheat
Bud dextrin, sucrose, lactose, beta-cyclodextrin, bacteria cellulose mixing, be added ethyl alcohol adjust humidity of materials to material can hand pinch into
Group, obtains softwood;
(3) softwood is granulated, then dry 4 hours at 45 DEG C, using sieve, pack to get.
Embodiment 3
A kind of Yellow Fructus Gardeniae electuary, is made from the following raw materials in parts by weight: Yellow Fructus Gardeniae 11, inonotus obliquus 9, honeysuckle 6, radix bupleuri 7,
Chrysanthemum 6, almond powder 6, microcrystalline cellulose 4, maltodextrin 70, sucrose 35, lactose 35, beta-cyclodextrin 1.5, bacteria cellulose 4.5.
A kind of preparation method of Yellow Fructus Gardeniae electuary, comprising the following steps:
(1) by Yellow Fructus Gardeniae, inonotus obliquus, honeysuckle, radix bupleuri, chrysanthemum co-grinding, add 8-12 times of water in high-voltage pulse electric
It extracts off field, wherein the electric field strength of high-pressure pulse electric is 18kVcm-1, pulse frequency 300Hz, burst length be
25min, Extracting temperature are 28 DEG C, using slag is filtered out, obtain extracting solution;
(2) extracting solution is sent into freeze concentration machine, carries out freeze concentration under conditions of condenser temperature is -25 DEG C, to
Volume stops freezing when being reduced to the 13% of extracting liquid volume, obtains medicinal extract, gained medicinal extract and almond powder, microcrystalline cellulose, wheat
Bud dextrin, sucrose, lactose, beta-cyclodextrin, bacteria cellulose mixing, be added ethyl alcohol adjust humidity of materials to material can hand pinch into
Group, obtains softwood;
(3) softwood is granulated, then dry 4 hours at 42 DEG C, using sieve, pack to get.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although referring to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features.It is all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (6)
1. a kind of Yellow Fructus Gardeniae electuary, which is characterized in that be made from the following raw materials in parts by weight: Yellow Fructus Gardeniae 10-12, inonotus obliquus 8-
10, honeysuckle 5-7, radix bupleuri 6-8, chrysanthemum 5-7, almond powder 5-7, microcrystalline cellulose 3-5, maltodextrin 60-80, sucrose 30-40,
Lactose 30-40, beta-cyclodextrin 1-2, bacteria cellulose 4-5.
2. a kind of preparation method of Yellow Fructus Gardeniae electuary, which comprises the following steps:
(1) by Yellow Fructus Gardeniae, inonotus obliquus, honeysuckle, radix bupleuri, chrysanthemum co-grinding, water is added to extract off field in high-voltage pulse electric,
Filtering and removing slag obtain extracting solution;
(2) medicinal extract, gained medicinal extract and almond powder, microcrystalline cellulose, maltodextrin, sucrose, cream is made in extracting solution freeze concentration
Sugar, beta-cyclodextrin, bacteria cellulose mixing, be added ethyl alcohol adjust humidity of materials to material can hand pinch agglomerating, obtain softwood;
(3) softwood is granulated, is dry, sieving, pack to get.
3. the preparation method of Yellow Fructus Gardeniae electuary according to claim 2, which is characterized in that added water in the step (1)
Weight be Yellow Fructus Gardeniae, inonotus obliquus, honeysuckle, radix bupleuri, 8-12 times of chrysanthemum total weight.
4. the preparation method of Yellow Fructus Gardeniae electuary according to claim 2, which is characterized in that the high pressure in the step (1)
The electric field strength of impulse electric field is 18kVcm-1, pulse frequency 300Hz, burst length 20-30min, Extracting temperature is
25-30℃。
5. the preparation method of Yellow Fructus Gardeniae electuary according to claim 2, which is characterized in that the freezing in the step (2)
Concentration is that extracting solution is sent into freeze concentration machine, carries out freeze concentration under conditions of condenser temperature is -30 to -20 DEG C, to
Volume stops freezing when being reduced to the 10-15% of extracting liquid volume.
6. the preparation method of Yellow Fructus Gardeniae electuary according to claim 2, which is characterized in that the drying in the step (3)
Temperature is 40-45 DEG C, and drying time is 4-5 hours.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114748526A (en) * | 2022-04-02 | 2022-07-15 | 长春中医药大学 | Method for extracting effective components from dicotyledonous plants |
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2019
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CN101971902A (en) * | 2010-10-20 | 2011-02-16 | 陈锦权 | Method for producing concentrated tea juice/powder by applying freezing and concentrating technology |
CN106387567A (en) * | 2016-08-29 | 2017-02-15 | 王士学 | Traditional Chinese medicine beverage and making method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114748526A (en) * | 2022-04-02 | 2022-07-15 | 长春中医药大学 | Method for extracting effective components from dicotyledonous plants |
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