CN107027926A - A kind of Sugarless type blue or green money willow drink and production process - Google Patents

A kind of Sugarless type blue or green money willow drink and production process Download PDF

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Publication number
CN107027926A
CN107027926A CN201710214367.7A CN201710214367A CN107027926A CN 107027926 A CN107027926 A CN 107027926A CN 201710214367 A CN201710214367 A CN 201710214367A CN 107027926 A CN107027926 A CN 107027926A
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China
Prior art keywords
blue
green money
extraction
willow
money willow
Prior art date
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Pending
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CN201710214367.7A
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Chinese (zh)
Inventor
李彦坡
郑晓杰
胡珊珊
胡必澄
章志成
李燕
何跃
钟兵
钟一兵
钟海锋
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Wenzhou Polytechnic
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Wenzhou Polytechnic
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Priority to CN201710214367.7A priority Critical patent/CN107027926A/en
Publication of CN107027926A publication Critical patent/CN107027926A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/34Tea substitutes, e.g. matè; Extracts or infusions thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/60Sweeteners
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention discloses a kind of Sugarless type blue or green money willow drink and production process, comprise the following steps:(1)Qingqian Willow leaf is crushed:It is crushed to 40 ~ 120 mesh;(2)One time ultrasonic wave temperature control is extracted;(4)Secondary ultra high pressure extraction;(5)Extract solution and secondary raffinate are mixed, blue or green money blue or green money willow is obtained and extracts mixed liquor;(6)Seasoning, addition xylitol and beta cyclodextrin in mixed liquor are extracted to blue or green money blue or green money willow;(7)Filtering, by deployed beverage by ultrafiltration membrance filter system, further removes the fine impurities in beverage;(8)Sterilizing:Beverage is sterilized;(9)It is filling:Sterile filling.It is an advantage of the invention that good mouthfeel, and Active components recovery rate is high, bioactivity is good.

Description

A kind of Sugarless type blue or green money willow drink and production process
Technical field
The present invention relates to a kind of health beverages, a kind of Sugarless type blue or green money willow drink and production process is specifically referred to.
Background technology
According to《Chinese medicine resource will will》Record, Qingqian Willow leaf tool heat-clearing is quenched one's thirst the effect of removing toxic substances, available for treating stubborn dermatitis. 《National Chinese herbal medicine name mirror》Record:Blue or green money willow bark, leaf, root have desinsection antipruritic, the effect of anti-inflammatory analgetic wind-dispelling.Modern science is real Existing Qingqian Willow leaf is issued after examination and approval containing a variety of important effective components such as polysaccharide, triterpene, saponin(e, flavones, while also detection amino acid, dimension life A variety of precious trace elements such as element, germanium, selenium, chromium, vanadium, zinc, iron, calcium, the interaction of multiple element so that blue or green money willow has Multi-biological activity, suitable for modern " three high " class chronic disease crowd uses.In addition, blue or green money willow is to strengthening body immunity, resisting Also there is unique effect in terms of the clinical symptoms such as oxidation, anti-aging, weak, neurasthenia, climacteric metancholia, liver protection.20 generation Record since the eighties, some primary care product by primary raw material of Qingqian Willow leaf are listed successively.
Existing many companies develop the products such as cyclocarya paliurus tea, and drinking method is identical with green tea, are dissolved in boiling water or stir Mix in food, but technological process is complicated, the extracted amount of blue or green money willow is relatively low, and mouthfeel is poor, still there is a kind of unpleasant blue or green smelly Gas and bitter taste.
Therefore, by retrieval, China Patent Publication No. CN104585417A discloses a kind of blue or green money willow beverage and its preparation Add momordica grosvenori sugar 2-3%, food additives 0.15-3% in technique, its technique, flavoring essence 0.05-0.15% improves it Mouthfeel, but technique still has blue or green money willow that active component recovery rate is low, the problem of active component is easy to be lost in.Therefore, having must This is improved.
The content of the invention
The invention aims to overcome the shortcoming and defect that prior art is present, and a kind of good mouthfeel is provided, and A kind of Sugarless type blue or green money willow drink and production process that Active components recovery rate is high, bioactivity is good.
To achieve the above object, the technical scheme is that comprising the following steps:
(1)Qingqian Willow leaf is crushed:It is crushed to 40 ~ 120 mesh;
(2)One time ultrasonic wave temperature control is extracted, using ultrasonic-leaching device, and ultrasonic power is 50 ~ 300kw, and extract solution is water, Feed liquid(Qingqian Willow leaf crushed material and extract solution)Mass ratio is 1:8—1:50, extraction temperature is 30 ~ 70 DEG C, and extraction time is 30 ±5min;Extract solution is drawn using centrifugal separator separation and separation slag is once extracted;This step uses ultrasonic wave once Extract, obtain higher polysaccharide;
(4)Secondary ultra high pressure extraction:By step(2)Separated once extraction separation slag adds water, and inserts ultra high pressure extraction equipment In secondary ultra high pressure extraction, its technological parameter is that ultra high pressure extraction hydrostatic pressure is 100 ~ 400MPa, extraction time is 30 ± 5min, feed liquid(Once extract separation slag and water)Mass ratio is 1:8-1:15, Extracting temperature is 10 ~ 50 DEG C;It is then centrifuged for separation Obtain secondary raffinate;Super-pressure second extraction bits, obtain higher flavones and residual polysaccharide, and low temperature extracts active polysaccharide and protected Stay more preferably, while ultra high pressure extraction can improve extracting flavonoids rate, crack the problem of water extraction flavones content is relatively low, make to contain in beverage More active blue or green money willow health-care components;
(5)Extract solution and secondary raffinate are mixed, blue or green money willow is obtained and extracts mixed liquor;
(6)Seasoning, extracts addition xylitol and beta-schardinger dextrin in mixed liquor, the wherein addition of xylitol is blue or green money to blue or green money willow Willow extracts the 1 ~ 10% of mixed liquor gross mass, and the addition of beta-schardinger dextrin extracts the 0.1 ~ 2% of mixed liquor gross mass for blue or green money willow;
(7)Filtering, by deployed beverage by ultrafiltration membrance filter system, further removes the fine impurities in beverage;
(8)Sterilizing:Beverage is sterilized;
(9)It is filling:Sterile filling.
It is described step further to set(8)Sterilizing to be sterilized by ultra high temperature short time sterilization system, sterilizing Technique is sterilizing 15 seconds at 120 DEG C ~ 135 DEG C.
Ultra high pressure extraction is a kind of by the hydrostatic pressure to the quick 100 ~ 600MPa of application of feed liquid, and pressurize one is regularly Between, solvent permeates rapidly in the presence of hyperpressure, the active ingredient in raw material can comparatively fast dissolution, and reach in a short time Balance, after rapid pressure release, under super-pressure permeable pressure head, active ingredient is rapidly diffused into solution.
The blue or green money willow polysaccharide and part Flavonoid substances for once extracting and being remained in separation slag are extracted, to improve raw material utilization Health-care components content in rate, increase beverage.
It is an advantage of the invention that:
(1)Blue or green money willow has blood sugar reducing function, by extraction, tea beverage is made, conveniently drinks;
(2)Ultrasonic wave temperature control is extracted, and is prevented the rise of extraction process temperature from causing active component to reduce, is kept its bioactivity, and So that prepared Sugarless type blue or green money willow beverage has more preferable health-care effect;
(3)Super-pressure second extraction, reduces energy consumption, increases Flavonoid substances content, more preferably, its technological principle is to apply to health-care effect Plus 100 ~ 400MPa hydrostatic pressure, and pressurize certain time, solvent permeates rapidly in the presence of hyperpressure, in raw material Active ingredient can comparatively fast dissolution, and reach balance in a short time, after rapid pressure release, under super-pressure permeable pressure head, effectively Composition is rapidly diffused into solution, and compared with the conventional art such as traditional decoction, backflow, surname extraction, super-pressure can contract significantly Short extraction time, energy consumption is reduced, and extraction conditions are normal temperature, it is to avoid blue or green money willow polysaccharide causes active ingredient knot because high temperature is extracted The problem of structure change, loss and activity reduction.Super-pressure second extraction blue or green money willow slag is used simultaneously, can fully be extracted in slag and be remained Blue or green money willow polysaccharide, also can extract the Flavonoid substances that conventional water extraction method is difficult to extract, reduce energy consumption, improve the health care of product Component content and yield.
(4)Functional oligose xylitol, no sweetener etc. are added, bitterness sense, green and healthy, Sugarless type beverage is reduced (both no cane sugar type beverages), is adapted to diabetes patients;
The present invention is described further with reference to embodiment.
Embodiment
The present invention is specifically described below by embodiment, is served only for that the present invention is further described, no It is understood that for limiting the scope of the present invention, the technician in the field can be according to the content of foregoing invention to the present invention Make some nonessential modifications and adaptations.
Embodiment 1
The preparation technology of Sugarless type blue or green money willow beverage, comprises the following steps:
(1)Qingqian Willow leaf is crushed:Selection dry or low temperature drying after Qingqian Willow leaf as raw material, in pulverizer crush, powder It is broken to 40 ~ 120 mesh;It is preferred to use 40 mesh.
(2)One time ultrasonic wave temperature control is extracted, using ultrasonic-leaching device, and ultrasonic power is 50 ~ 300kw, extract solution For water, feed liquid mass ratio is 1:8—1:50, extraction temperature is 30 ~ 70 DEG C, and extraction time is 30 ± 5min;Using centrifugation Machine separation draws an extract solution and once extracts separation slag;Ultrasonic-leaching device is ripe extraction element, can directly from In the market purchase is applied to this technique, preferably, and ultrasonic power is 220kw, and extract solution is water, and feed liquid mass ratio is 1: 20, extraction temperature is 50 DEG C, and extraction time is 30min.
(4)Secondary ultra high pressure extraction:By step(2)Separated once extraction separation slag adds water, and inserts ultra high pressure extraction Secondary ultra high pressure extraction in equipment, its technological parameter is that ultra high pressure extraction hydrostatic pressure is 100 ~ 400MPa, and extraction time is 30 ± 5min, feed liquid mass ratio is 1:8-1:15, Extracting temperature is 10 ~ 50 DEG C;It is then centrifuged for isolated secondary raffinate;Make For preferably, the present embodiment ultra high pressure extraction equipment is surpassed using the BY-600-L types of the mechanical Science and Technology Ltd.'s production in Wenzhou shore one High pressure extraction machine, the present embodiment ultra high pressure extraction hydrostatic pressure is 300MPa, and extraction time is 30min, and feed liquid mass ratio is 1:8, Extracting temperature is 27 DEG C
(5)Extract solution and secondary raffinate are mixed, blue or green money willow is obtained and extracts mixed liquor;
(6)Seasoning, extracts addition xylitol and beta-schardinger dextrin in mixed liquor, the wherein addition of xylitol is blue or green money to blue or green money willow Willow extracts the 1 ~ 10% of mixed liquor gross mass, and the addition of beta-schardinger dextrin extracts the 0.1 ~ 2% of mixed liquor gross mass for blue or green money willow;Make For preferably, the addition of the present embodiment xylitol is 4%, the addition of described beta-schardinger dextrin is 0. 2%
(7)Filtering, by deployed beverage by ultrafiltration membrance filter system, further removes the fine impurities in beverage;Ultrafiltration Membrane filtration system is ripe filtration system, directly can commercially be applied to this technique.
(8)Sterilizing:Beverage is sterilized;Preferably, the sterilizing is to be carried out by ultra high temperature short time sterilization system Sterilizing, sterilization process is sterilizing 15 seconds at 120 DEG C ~ 135 DEG C;
(9)It is filling:Sterile filling.

Claims (2)

1. a kind of Sugarless type blue or green money willow drink and production process, it is characterised in that comprise the following steps:
(1)Qingqian Willow leaf is crushed:It is crushed to 40 ~ 120 mesh;
(2)One time ultrasonic wave temperature control is extracted, using ultrasonic-leaching device, and ultrasonic power is 50 ~ 300kw, and extract solution is water, Feed liquid mass ratio is 1:8—1:50, extraction temperature is 30 ~ 70 DEG C, and extraction time is 30 ± 5min;Separated using centrifugal separator Draw an extract solution and once extract separation slag;
(4)Secondary ultra high pressure extraction:By step(2)Separated once extraction separation slag adds water, and inserts ultra high pressure extraction equipment In secondary ultra high pressure extraction, its technological parameter is that ultra high pressure extraction hydrostatic pressure is 100 ~ 400MPa, extraction time is 30 ± 5min, feed liquid mass ratio is 1:8-1:15, Extracting temperature is 10 ~ 50 DEG C;It is then centrifuged for isolated secondary raffinate;
(5)Extract solution and secondary raffinate are mixed, blue or green money willow is obtained and extracts mixed liquor;
(6)Seasoning, extracts addition xylitol and beta-schardinger dextrin in mixed liquor, the wherein addition of xylitol is blue or green money to blue or green money willow Willow extracts the 1 ~ 10% of mixed liquor gross mass, and the addition of beta-schardinger dextrin extracts the 0.1 ~ 2% of mixed liquor gross mass for blue or green money willow;
(7)Filtering, by deployed beverage by ultrafiltration membrance filter system, further removes the fine impurities in beverage;
(8)Sterilizing:Beverage is sterilized;
(9)It is filling:Sterile filling.
2. a kind of Sugarless type blue or green money willow drink and production process according to claim 1, it is characterised in that:Described step (8)Sterilizing to be sterilized by ultra high temperature short time sterilization system, sterilization process is sterilizing 15 seconds at 120 DEG C ~ 135 DEG C.
CN201710214367.7A 2017-04-01 2017-04-01 A kind of Sugarless type blue or green money willow drink and production process Pending CN107027926A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107691940A (en) * 2017-09-12 2018-02-16 茂名阿奎叔食品有限公司 A kind of Qingqian Willow leaf heat-clearing beverage
CN107712524A (en) * 2017-11-10 2018-02-23 何培文 A kind of Ganoderma lucidum drink preparation technology
CN107736523A (en) * 2017-11-10 2018-02-27 何培文 A kind of black meal fruit beverage preparation technology
CN110074223A (en) * 2019-04-30 2019-08-02 福建安溪铁观音集团股份有限公司 The deep process of a kind of tealeaves leftover bits and pieces and applied to the ultrasonic extractor in the technique

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102525945A (en) * 2012-01-11 2012-07-04 南京林业大学 Preparation method for cyclocarya paliurus(Batal)Ijinskaja hypoglycemic granules
CN103749778A (en) * 2013-12-31 2014-04-30 湖南中医药大学 Cyclocarya paliurus tea beverage and preparation method thereof
CN105054202A (en) * 2015-08-28 2015-11-18 江西万茂科技有限公司 Cyclocarya paliurus herbal plant drink and production technology thereof

Patent Citations (3)

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Publication number Priority date Publication date Assignee Title
CN102525945A (en) * 2012-01-11 2012-07-04 南京林业大学 Preparation method for cyclocarya paliurus(Batal)Ijinskaja hypoglycemic granules
CN103749778A (en) * 2013-12-31 2014-04-30 湖南中医药大学 Cyclocarya paliurus tea beverage and preparation method thereof
CN105054202A (en) * 2015-08-28 2015-11-18 江西万茂科技有限公司 Cyclocarya paliurus herbal plant drink and production technology thereof

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107691940A (en) * 2017-09-12 2018-02-16 茂名阿奎叔食品有限公司 A kind of Qingqian Willow leaf heat-clearing beverage
CN107712524A (en) * 2017-11-10 2018-02-23 何培文 A kind of Ganoderma lucidum drink preparation technology
CN107736523A (en) * 2017-11-10 2018-02-27 何培文 A kind of black meal fruit beverage preparation technology
CN110074223A (en) * 2019-04-30 2019-08-02 福建安溪铁观音集团股份有限公司 The deep process of a kind of tealeaves leftover bits and pieces and applied to the ultrasonic extractor in the technique

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Inventor after: Li Yanpo

Inventor after: Zhou Youyou

Inventor after: Liu Yanping

Inventor after: Zheng Xiaojie

Inventor after: Hu Shanshan

Inventor after: Hu Bicheng

Inventor after: Zhang Zhicheng

Inventor after: Li Yan

Inventor after: He Yue

Inventor after: Zhong Yibing

Inventor after: Zhong Haifeng

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Application publication date: 20170811