CN110151641A - A kind of solid-state shampoo to economize on resources and preparation method thereof and application method - Google Patents
A kind of solid-state shampoo to economize on resources and preparation method thereof and application method Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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Abstract
The invention discloses a kind of solid-state shampoos to economize on resources, ingredient includes: flat 5 ~ 20 parts of leaf Vanilla annamica berry extract, 5 ~ 20 parts of Lupinus albus seed extract, 5 ~ 20 parts of ginger-root extract, 5 ~ 10 parts of sodium carboxymethyl starch, 1 ~ 5 part of laureth sulfuric ester ammonium, 5 ~ 20 parts of Cocoamidopropyl betaine, 5 ~ 20 parts of glycerol, coconut oleoyl amine DEA5 ~ 20 part, 1 ~ 5 part of polyquaternium, 1 ~ 5 part of laruyl alcohol sodium sulfovinate, 2 ~ 15 parts of glycol distearate, 1 ~ 5 part of cetostearyl alcohol, 1 ~ 5 part of rose oil, 0.5 ~ 2 part of sodium chloride, 1 ~ 5 part of guar hydroxypropyltrimonium chloride, 2 ~ 5 parts of pH adjusting agent, 0.05 ~ 1 part of preservative, 2 ~ 5 parts of desiccant.Solid-state is made in liquid shampoo by Freeze Drying Technique, disintegrating agent is added and particle is made in desiccant.It by the amount of 1/10ml, is mixed into water, waits 2 ~ 3 minutes, that is, can be used.
Description
Technical field
The present invention relates to daily chemical product technical field, in particular to a kind of solid-state shampoo to economize on resources and its preparation sides
Method and application method.
Background technique
Shampoo is that a kind of smell is good, anti-dandruff function, treatment oil function, hair dyeing function, prevents hair loss, submissive nutrition, prevents
Only fork, the unification of certain hair quality finished proprietary item, natural function, multiple-effect, wash shield separate, wash shield, containing tartaric acid, go to itch, other protect
Hair-care articles is daily necessities indispensable in life.China is current have one's hair wash in the world water production and the highest country of sales volume,
Shampoo brand on domestic market is more than 3000, and shampoo market scale is estimated to exceed 20,000,000,000 yuan, and family's shampoo year is flat
Purchase number is 5 times, and Chinese shampoo production reaches 400,000 tons.
Existing shampoo liquid processed, the shampoo of liquid condition become the main product of market shampoo substantially, but
That must be contained using the bottle body of relative closure using liquid shampoo, this bottle body need to waste a large amount of resource into
The packaging of row product, it is also extremely inconvenient to carry.Existing solid-state shampoo has hair soap, directly will during hair washing
In hair soap erasing to hair, then it is rinsed, but since cleaning effect is poor compared to the shampoo of liquid, moves back substantially
Hair care market is gone out to wash.80% ingredient is made of water in shampoo, why not solid-state is made in shampoo, then allowed
Concentrate is taken home to add water and be used by people, yet there are no the shampoo solid relevant report is made.
Summary of the invention
The purpose of the present invention is to provide a kind of solid-state shampoos to economize on resources.
It is another object of the present invention to provide the preparation methods of above-mentioned solid-state shampoo.
It is also an object of the present invention to provide the application methods of above-mentioned solid-state shampoo.
The present invention is achieved through the following technical solutions: a kind of solid-state shampoo to economize on resources, by weight, including with
Lower ingredient:
Flat 5 ~ 20 parts of leaf Vanilla annamica berry extract, 5 ~ 20 parts of Lupinus albus seed extract, 5 ~ 20 parts of ginger-root extract, carboxymethyl form sediment
5 ~ 10 parts of powder sodium, 1 ~ 5 part of laureth sulfuric ester ammonium, 5 ~ 20 parts of Cocoamidopropyl betaine, 5 ~ 20 parts of glycerol, cocounut oil acyl
Amine DEA5 ~ 20 part, 1 ~ 5 part of polyquaternium, 1 ~ 5 part of laruyl alcohol sodium sulfovinate, 2 ~ 15 parts of glycol distearate, cetearyl alcohol
1 ~ 5 part of alcohol, 1 ~ 5 part of rose oil, 0.5 ~ 2 part of sodium chloride, 1 ~ 5 part of guar hydroxypropyltrimonium chloride, pH adjusting agent 2 ~ 5
Part, 0.05 ~ 1 part of preservative, 2 ~ 5 parts of desiccant.
Formula is added to flat leaf Vanilla annamica berry extract, and flat leaf Vanilla annamica berry extract is that the water of flat leaf Vanilla annamica fruit mentions
Object can eliminate free radical, inhibit the work of matrix metalloproteinase containing high-efficiency antioxidant agent catechin (being a kind of Polyphenols)
Property have the function of it is anti-oxidant and anti-inflammatory, to inhibit scalp itch have positive effect.Raw material contains nature fragrance, also can be used as day
Right fragrance uses, so product is without adding daily chemical essence.
Lupinus albus seed extract hydrolysis anti-oxidation peptide albumen rich in replaces animal to hydrolyze with plant protein hydrolysate
Albumen makes hair more smooth.Believing vegetarian diet personage is enabled to trust selection.
Ginger-root extract is the water-soluble extractive of ginger.Ginger is warm-natured, has effects that inducing diaphoresis, diverging, so external application
It is put on the skin on scalp outside ginger juice, local skin blood vessel dilatation can be stimulated, increase local blood circulation, make local blood supply
Increase, can hair follicle stimulating open, promote hair regeneration.
The hair care effect of rose oil is very significant.Rose oil is extracted form natural plant, without chemical addition agent, is had
Effect repairs injured hair, moistens moisturizing, keeps hair glossy submissive.The oily hair for especially sending out the easy jag of the tip, uses rose oil
Nourishes effect becomes apparent from.
In order to which the present invention is better achieved, further, by weight, including following component:
Flat 10 parts of leaf Vanilla annamica berry extract, 10 parts of Lupinus albus seed extract, 10 parts of ginger-root extract, sodium carboxymethyl starch 5
Part, 2 parts of laureth sulfuric ester ammonium, 15 parts of Cocoamidopropyl betaine, 15 parts of glycerol, DEA15 parts of coconut oleoyl amine, poly- season
2 parts of ammonium salt, 2 parts of laruyl alcohol sodium sulfovinate, 8 parts of glycol distearate, 2 parts of cetostearyl alcohol, 2 parts of rose oil, chlorination
1 part of sodium, 2 parts of guar hydroxypropyltrimonium chloride, 3 parts of pH adjusting agent, 0.5 part of preservative, 3 parts of desiccant.
In order to which the present invention is better achieved, further, the preservative in the shampoo is Kathon CG or ethylparaben.
In order to which the present invention is better achieved, further, the pH adjusting agent in the shampoo is citric acid.
In order to which the present invention is better achieved, further, the desiccant in the shampoo is silica gel.
The preparation method of the above-mentioned solid-state shampoo to economize on resources, comprising the following steps:
(1) it is extracted, then will be extracted respectively using method dialogue lupine seed that water mentions, flat leaf Vanilla annamica fruit, race
Medicinal extract, in mass ratio 1:1:1 uniformly mix, and cross 15 meshes, spare；
(2) it is added guar hydroxypropyltrimonium chloride bubble 2 hours or more using 45 DEG C of warm water, prepares melon rubber hydroxypropyl
The dispersion liquid of trimethyl ammonium chloride is spare；
(3) laruyl alcohol sodium sulfovinate is dissolved using purified water and be added in reaction pot, then cocounut oil acyl is successively added into reaction pot
Amine propyl betaine, coconut oleoyl amine DEA, polyquaternium, laureth sulfuric ester ammonium, are heated to 75 DEG C -80 DEG C, with 38r/
The speed of min, average rate stir 30 minutes；
(4) glycol distearate, cetostearyl alcohol are then added into reaction pot, in 75 DEG C of -80 DEG C of ranges, with 28r/
The speed of min stirs 30min, while emulsifying 5min with the shear velocity of 2000r/min, wait be cooled to 65 DEG C, is added step (2)
Dispersion liquid, rose oil and the glycerol of the guar hydroxypropyltrimonium chloride of preparation, at 60 DEG C -65 DEG C, with 28r/min's
Speed, average rate stir 60min；
(5) glycol distearate, cetostearyl alcohol are then added into reaction pot, in 75 DEG C of -80 DEG C of ranges, with 28r/
The speed of min stirs 30min, while emulsifying 5min with the shear velocity of 2000r/min, sodium chloride is added, with stirring for 28r/min
After mixing speed stirring 30min, stop stirring；
(6) wait be cooled to 40 DEG C, Lupinus albus seed extract, flat leaf Vanilla annamica berry extract, ginger-root extract, with 28r/min
Speed, average rate stir 30min after, stop stirring, be added pH adjusting agent, adjust pH to 6.5 ~ 7.5, be added preservative, stirring
It is uniformly mixed；
(8) vacuum freeze drying is carried out for 24 hours, after vacuum freezedrying, testing product moisture content, it is qualification that moisture content, which is≤5%,
Otherwise continue to be freeze-dried；
(10) it by the product after qualification, is placed in powder pulverizer, powder is made, sieve with 100 mesh sieve；
(11) sodium carboxymethyl starch powder and desiccant powder are mixed into powder made of step (10), spent material mixing
Machine is uniformly mixed it, obtains finished product mixed-powder；
(12) granulator is used, into processing, to be made into particle of uniform size to mixed-powder, particle size is 1 ~ 2cm, i.e.,
Finished product is obtained, production line encapsulation is sent into.
Technology pharmacy in the preparation process of the shampoo is as follows:
First, the extracting mode of plant component, flat leaf Vanilla annamica fruit, Lupinus albus seed, race must mention in such a way that water mentions
The medicinal extract taken just has and can preferably act on；
Second, the proportion of each group plant extracts ingredient, by test of many times gained, optimum proportioning 1:1:1；
After freeze powder is made in solid shampoo by third, then mixes sodium carboxymethyl starch and desiccant powder
End is because the surfactant in shampoo is cationic compound, and sodium carboxymethyl starch spreads out for anionic starch
Biology is easy to happen reaction if being all liquid condition, adverse effect is caused to shampoo, similarly in the shampoo of liquid
In desiccant can not also be added.
In order to which method of the invention is better achieved, further, comprising the following steps: in the step (1), white feather fan
It is to take air-dried Lupinus albus seed to shred to read into coarse powder that the water of beans seed, which proposes process, crosses 40 meshes, it is placed in flask, be added
Deionized water, is totally submerged Lupinus albus seed, impregnate 12 ~ for 24 hours, 1 ~ 2h is boiled in heating, and flask opening setting condenser pipe continues cold
It is solidifying；After it is completely cooling, impurity is filtered off, is directly distilled, obtained medicinal extract is the water extract of Lupinus albus seed.
In order to which method of the invention is better achieved, further, comprising the following steps: in the step (1), flat Ye Xiang
It is to take air-dried flat leaf Vanilla annamica fruit to shred to read into coarse powder that the water of fruit orchid fruit, which proposes process, crosses 40 meshes, it is placed in flask,
Deionized water is added, soaks flat leaf Vanilla annamica fruit completely and does not have a purple ball algae, impregnate 12 ~ for 24 hours, 1 ~ 2h, flask opening setting are boiled in heating
Condenser pipe, it is lasting to condense；After it is completely cooling, impurity is filtered off, is directly distilled, obtained medicinal extract is flat leaf Vanilla annamica fruit
Water extract.
In order to which method of the invention is better achieved, further, comprising the following steps: in the step (1), race
Water proposes process, takes air-dried race to shred and reads into coarse powder, crosses 40 meshes, it is placed in flask, deionized water is added, completely
Leaching race does not have a purple ball algae, impregnate 12 ~ for 24 hours, 1 ~ 2h is boiled in heating, and flask opening setting condenser pipe is lasting to condense；It is completely cold to it
But after, impurity is filtered off, is directly distilled, obtained medicinal extract is the water extract of race.
The application method of the above-mentioned solid-state shampoo to economize on resources, specifically: the hair washing of wash my hair needs as needed
The dosage of water selects how many solid shampoos that the granular solid-state shampoo is mixed into water by the amount of 1/10ml
In, it waits 2 ~ 3 minutes, the suspension shampoo of liquid can be become, then directly carrying out hair cleaning using the shampoo is
It can.
Compared with prior art, the present invention have the following advantages that and the utility model has the advantages that
(1) present invention by the way that solid-state is made in shampoo, only need to be added water can in a short time become liquid shampoo,
The cleaning of hair is carried out for people, people only need to get the container that may be reused ready at home, are greatly saved and wash
The packing cost of shampoo in a disguised form reduces the use of plastic material, energy conservation and environmental protection, the solid-state shampoo；
(2) it joined super-disintegrant in shampoo formula of the invention, can make the hair washing particle water after meeting water, quickly collapse
Solution is at liquid shampoo, and for general partial size in the hair washing particle water of 2cm, the time being disintegrated completely is no more than 2min, practical, side
Persons who happens to be on hand for an errand carry；
(3) present invention produces solid shampoo by way of freeze-drying, after super-disintegrant is added, can guarantee to collapse
The effect of agent is solved, while also ensuring the effect of liquid shampoo after dissolution, preparation flow is new reasonable, is suitable for being widely popularized
Using.
Specific embodiment
The present invention is described in further detail below with reference to embodiment, embodiments of the present invention are not limited thereto,
Without departing from the idea case in the present invention described above, according to ordinary skill knowledge and customary means, various replace is made
It changes and changes, should all be included within the scope of the invention.
For the purpose of the present invention, process conditions and advantage effect is more clearly understood, in conjunction with following embodiment, to this
Invention is described in further detail, and specific implementation example described herein only to explain the present invention, is not used to limit this
Invention.
Embodiment 1:
A kind of solid-state shampoo to economize on resources of the present embodiment, by weight, including following component:
Flat 10 parts of leaf Vanilla annamica berry extract, 10 parts of Lupinus albus seed extract, 10 parts of ginger-root extract, sodium carboxymethyl starch 5
Part, 2 parts of laureth sulfuric ester ammonium, 15 parts of Cocoamidopropyl betaine, 15 parts of glycerol, DEA15 parts of coconut oleoyl amine, poly- season
2 parts of ammonium salt, 2 parts of laruyl alcohol sodium sulfovinate, 8 parts of glycol distearate, 2 parts of cetostearyl alcohol, 2 parts of rose oil, chlorination
1 part of sodium, 2 parts of guar hydroxypropyltrimonium chloride, 3 parts of pH adjusting agent, 0.5 part of preservative, 3 parts of desiccant.
Specific preparation method the following steps are included:
(1) it is extracted, then will be extracted respectively using method dialogue lupine seed that water mentions, flat leaf Vanilla annamica fruit, race
Medicinal extract, in mass ratio 1:1:1 uniformly mix, and cross 15 meshes, spare；
(2) it is added guar hydroxypropyltrimonium chloride bubble 2 hours or more using 45 DEG C of warm water, prepares melon rubber hydroxypropyl
The dispersion liquid of trimethyl ammonium chloride is spare；
(3) laruyl alcohol sodium sulfovinate is dissolved using purified water and be added in reaction pot, then cocounut oil acyl is successively added into reaction pot
Amine propyl betaine, coconut oleoyl amine DEA, polyquaternium, laureth sulfuric ester ammonium, are heated to 75 DEG C -80 DEG C, with 38r/
The speed of min, average rate stir 30 minutes；
(4) glycol distearate, cetostearyl alcohol are then added into reaction pot, in 75 DEG C of -80 DEG C of ranges, with 28r/
The speed of min stirs 30min, while emulsifying 5min with the shear velocity of 2000r/min, wait be cooled to 65 DEG C, is added step (2)
Dispersion liquid, rose oil and the glycerol of the guar hydroxypropyltrimonium chloride of preparation, at 60 DEG C -65 DEG C, with 28r/min's
Speed, average rate stir 60min；
(5) glycol distearate, cetostearyl alcohol are then added into reaction pot, in 75 DEG C of -80 DEG C of ranges, with 28r/
The speed of min stirs 30min, while emulsifying 5min with the shear velocity of 2000r/min, sodium chloride is added, with stirring for 28r/min
After mixing speed stirring 30min, stop stirring；
(6) wait be cooled to 40 DEG C, Lupinus albus seed extract, flat leaf Vanilla annamica berry extract, ginger-root extract, with 28r/min
Speed, average rate stir 30min after, stop stirring, be added pH adjusting agent, adjust pH to 6.5 ~ 7.5, be added preservative, stirring
It is uniformly mixed；
(8) vacuum freeze drying is carried out for 24 hours, after vacuum freezedrying, testing product moisture content, it is qualification that moisture content, which is≤5%,
Otherwise continue to be freeze-dried；
(10) it by the product after qualification, is placed in powder pulverizer, powder is made, sieve with 100 mesh sieve；
(11) sodium carboxymethyl starch powder and desiccant powder are mixed into powder made of step (10), spent material mixing
Machine is uniformly mixed it, obtains finished product mixed-powder；
(12) granulator is used, into processing, to be made into particle of uniform size to mixed-powder, particle size is 1 ~ 2cm, i.e.,
Finished product is obtained, production line encapsulation is sent into.
Specifically used method are as follows: the dosage of the shampoo of wash my hair needs as needed, how many of selection is solid to wash
Shampoo, by the amount of 1/10ml, which is mixed into water, is waited 2 ~ 3 minutes, and liquid can be become
Then suspension shampoo directly carries out hair cleaning using the shampoo.
Embodiment 2:
The present embodiment on the basis of the above embodiments, further define preservative, desiccant, pH adjusting agent material, point
It is not that preservative is Kathon CG or ethylparaben；PH adjusting agent is citric acid；Desiccant in shampoo is silica gel.
Wherein, for silica gel as desiccant, soaking effect is strong, and stability is good, will not generate heat, to the reason of solid-state shampoo
Changing property will not impact, as preferred.The present embodiment other parts are same as the previously described embodiments, do not repeating here.
Embodiment 3:
The present embodiment further defines the extraction process of plant component extraction object on the basis of the above embodiments, as follows,
It is to take air-dried Lupinus albus seed to shred to read into coarse powder that the water of Lupinus albus seed, which proposes process, crosses 40 meshes, it is placed in burning
In bottle, deionized water is added, is totally submerged Lupinus albus seed, impregnate 12 ~ for 24 hours, 1 ~ 2h, flask opening setting condensation are boiled in heating
Pipe, it is lasting to condense；After it is completely cooling, impurity is filtered off, is directly distilled, obtained medicinal extract is that the water of Lupinus albus seed mentions
Object.
It is to take air-dried flat leaf Vanilla annamica fruit to shred to read into coarse powder that the water of flat leaf Vanilla annamica fruit, which proposes process, crosses 40 meshes, will
Be placed in flask, deionized water is added, soaks flat leaf Vanilla annamica fruit completely and does not have a purple ball algae, impregnates 12 ~ for 24 hours, 1 ~ 2h is boiled in heating,
Flask opening setting condenser pipe, it is lasting to condense；After it is completely cooling, impurity is filtered off, is directly distilled, obtained medicinal extract is as flat
The water extract of leaf Vanilla annamica fruit.
It is to take air-dried race to shred to read into coarse powder that the water of race, which proposes process, crosses 40 meshes, it is placed in flask, is added
Enter deionized water, soaks race completely and do not have a purple ball algae, impregnate 12 ~ for 24 hours, 1 ~ 2h is boiled in heating, and flask opening setting condenser pipe continues
Condensation；After it is completely cooling, impurity is filtered off, is directly distilled, obtained medicinal extract is the water extract of race.
The other parts of the present embodiment are same as the previously described embodiments, repeat no more.
Although an embodiment of the present invention has been shown and described, it will be understood by those skilled in the art that: not
A variety of change, modification, replacement and modification can be carried out to these embodiments by being detached under the principle of the present invention and objective, of the invention
Range is defined by the claims and their equivalents.
Claims (10)
1. a kind of solid-state shampoo to economize on resources, which is characterized in that by weight, including following component:
Flat 5 ~ 20 parts of leaf Vanilla annamica berry extract, 5 ~ 20 parts of Lupinus albus seed extract, 5 ~ 20 parts of ginger-root extract, carboxymethyl form sediment
5 ~ 10 parts of powder sodium, 1 ~ 5 part of laureth sulfuric ester ammonium, 5 ~ 20 parts of Cocoamidopropyl betaine, 5 ~ 20 parts of glycerol, cocounut oil acyl
Amine DEA5 ~ 20 part, 1 ~ 5 part of polyquaternium, 1 ~ 5 part of laruyl alcohol sodium sulfovinate, 2 ~ 15 parts of glycol distearate, cetearyl alcohol
1 ~ 5 part of alcohol, 1 ~ 5 part of rose oil, 0.5 ~ 2 part of sodium chloride, 1 ~ 5 part of guar hydroxypropyltrimonium chloride, pH adjusting agent 2 ~ 5
Part, 0.05 ~ 1 part of preservative, 2 ~ 5 parts of desiccant.
2. a kind of solid-state shampoo to economize on resources according to claim 1, which is characterized in that by weight, including
Following component:
Flat 10 parts of leaf Vanilla annamica berry extract, 10 parts of Lupinus albus seed extract, 10 parts of ginger-root extract, sodium carboxymethyl starch 5
Part, 2 parts of laureth sulfuric ester ammonium, 15 parts of Cocoamidopropyl betaine, 15 parts of glycerol, DEA15 parts of coconut oleoyl amine, poly- season
2 parts of ammonium salt, 2 parts of laruyl alcohol sodium sulfovinate, 8 parts of glycol distearate, 2 parts of cetostearyl alcohol, 2 parts of rose oil, chlorination
1 part of sodium, 2 parts of guar hydroxypropyltrimonium chloride, 3 parts of pH adjusting agent, 0.5 part of preservative, 3 parts of desiccant.
3. a kind of solid-state shampoo to economize on resources according to claim 1 or 2, which is characterized in that in the shampoo
Preservative be Kathon CG or ethylparaben.
4. a kind of solid-state shampoo to economize on resources according to claim 1 or 2, which is characterized in that in the shampoo
PH adjusting agent be citric acid.
5. a kind of solid-state shampoo to economize on resources according to claim 1 or 2, which is characterized in that in the shampoo
Desiccant be silica gel.
6. a kind of preparation method of described in any item solid-state shampoos to economize on resources, feature exist according to claim 1 ~ 5
In, comprising the following steps:
(1) it is extracted, then will be extracted respectively using method dialogue lupine seed that water mentions, flat leaf Vanilla annamica fruit, race
Medicinal extract, in mass ratio 1:1:1 uniformly mix, and cross 15 meshes, spare；
(2) it is added guar hydroxypropyltrimonium chloride bubble 2 hours or more using 45 DEG C of warm water, prepares melon rubber hydroxypropyl
The dispersion liquid of trimethyl ammonium chloride is spare；
(3) laruyl alcohol sodium sulfovinate is dissolved using purified water and be added in reaction pot, then cocounut oil acyl is successively added into reaction pot
Amine propyl betaine, coconut oleoyl amine DEA, polyquaternium, laureth sulfuric ester ammonium, are heated to 75 DEG C -80 DEG C, with 38r/
The speed of min, average rate stir 30 minutes；
(4) glycol distearate, cetostearyl alcohol are then added into reaction pot, in 75 DEG C of -80 DEG C of ranges, with 28r/
The speed of min stirs 30min, while emulsifying 5min with the shear velocity of 2000r/min, wait be cooled to 65 DEG C, is added step (2)
Dispersion liquid, rose oil and the glycerol of the guar hydroxypropyltrimonium chloride of preparation, at 60 DEG C -65 DEG C, with 28r/min's
Speed, average rate stir 60min；
(5) glycol distearate, cetostearyl alcohol are then added into reaction pot, in 75 DEG C of -80 DEG C of ranges, with 28r/
The speed of min stirs 30min, while emulsifying 5min with the shear velocity of 2000r/min, sodium chloride is added, with stirring for 28r/min
After mixing speed stirring 30min, stop stirring；
(6) wait be cooled to 40 DEG C, Lupinus albus seed extract, flat leaf Vanilla annamica berry extract, ginger-root extract, with 28r/min
Speed, average rate stir 30min after, stop stirring, be added pH adjusting agent, adjust pH to 6.5 ~ 7.5, be added preservative, stirring
It is uniformly mixed；
(8) vacuum freeze drying is carried out for 24 hours, after vacuum freezedrying, testing product moisture content, it is qualification that moisture content, which is≤5%,
Otherwise continue to be freeze-dried；
(10) it by the product after qualification, is placed in powder pulverizer, powder is made, sieve with 100 mesh sieve；
(11) sodium carboxymethyl starch powder and desiccant powder are mixed into powder made of step (10), spent material mixing
Machine is uniformly mixed it, obtains finished product mixed-powder；
(12) granulator is used, into processing, to be made into particle of uniform size to mixed-powder, particle size is 1 ~ 2cm, i.e.,
Finished product is obtained, production line encapsulation is sent into.
7. according to a kind of described in any item preparation methods of the solid-state shampoo to economize on resources of claim 6, which is characterized in that
The following steps are included: in the step (1), the water of Lupinus albus seed propose process and be take air-dried Lupinus albus seed shred read at
Coarse powder crosses 40 meshes, it is placed in flask, and deionized water is added, is totally submerged Lupinus albus seed, impregnate 12 ~ for 24 hours, heating
1 ~ 2h is boiled, flask opening setting condenser pipe is lasting to condense；After it is completely cooling, impurity is filtered off, directly distills, obtains
Medicinal extract is the water extract of Lupinus albus seed.
8. a kind of preparation method of described in any item solid-state shampoos to economize on resources, feature exist according to claim 1 ~ 5
In, comprising the following steps: in the step (1), it is that air-dried flat leaf Vanilla annamica fruit is taken to cut that the water of flat leaf Vanilla annamica fruit, which proposes process,
It is broken to read into coarse powder, 40 meshes are crossed, it is placed in flask, deionized water is added, soaks flat leaf Vanilla annamica fruit completely and does not have purple ball algae, are soaked
Bubble 12 ~ for 24 hours, 1 ~ 2h is boiled in heating, and flask opening setting condenser pipe is lasting to condense；After it is completely cooling, impurity is filtered off, directly
Distillation is connect, obtained medicinal extract is the water extract of flat leaf Vanilla annamica fruit.
9. a kind of preparation method of described in any item solid-state shampoos to economize on resources, feature exist according to claim 1 ~ 5
In, comprising the following steps: in the step (1), it is to take air-dried race to shred to read into coarse powder that the water of race, which proposes process, crosses 40
It is placed in flask by mesh, and deionized water is added, and soaks race completely and does not have a purple ball algae, impregnate 12 ~ for 24 hours, 1 ~ 2h is boiled in heating,
Flask opening setting condenser pipe, it is lasting to condense；After it is completely cooling, impurity is filtered off, is directly distilled, obtained medicinal extract is ginger
The water extract of root.
10. the application method of described in any item a kind of solid-state shampoos to economize on resources according to claim 1 ~ 5, specifically:
The dosage of the shampoo of wash my hair needs as needed, selects how many solid shampoos, by the amount of 1/10ml, by this
Granular solid-state shampoo is mixed into water, is waited 2 ~ 3 minutes, can be become the suspension shampoo of liquid, then directly be made
Hair is carried out with the shampoo to clean.
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