CN110051617A - A kind of sunscreen and preparation method thereof of high SPF - Google Patents
A kind of sunscreen and preparation method thereof of high SPF Download PDFInfo
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- CN110051617A CN110051617A CN201910397067.6A CN201910397067A CN110051617A CN 110051617 A CN110051617 A CN 110051617A CN 201910397067 A CN201910397067 A CN 201910397067A CN 110051617 A CN110051617 A CN 110051617A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention discloses a kind of sunscreens and preparation method thereof of high SPF, including following raw material: water, ethylhexyl methoxy cinnamate, bis-ethylhexoxyphenol methoxyphenyl triazine, carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate, Octocrilene, propylene glycol, the own ester of diethylamino oxybenzene formylbenzoate, glycerol, methylene bis-benzotriazolyl tetramethyl butyl phenol, Plantacare 818, propylene glycol, xanthan gum, Sucrose Polystearic Acid Esters, cetanol stearate, butanediol, Uvinul T 150, Phenoxyethanol, pungent glycol, Sodium Polyacrylate, tocopherol acetate, bisabolol, stearoyl-glutamic acid sodium, dimethyl silicone polymer, Sodium Hyaluronate, tetra- sodium of EDTA, Glucomannan, tea fungus dispersion, microcrystalline cellulose.The present invention is reinforcement system by using Glucomannan, tea fungus dispersion, microcrystalline cellulose, improves the sun protection and persistence of the sunscreen of high SPF.
Description
Technical field
The invention belongs to sun-proof fields, and in particular to a kind of sunscreen and preparation method thereof of high SPF.
Background technique
The wavelength of ultraviolet light in sunlight is 200-400nm, since ultraviolet wavelength is very short, energy is very high, it
Destructive power it is very big, for a long time irradiation can make human body skin damage, cause inflammation or sunburn, it is serious to generate cutaneum carcinoma.?
For outside work personnel, since body skin is largely perspired salt discharge, the permanent conservation degree of suncream can be made sharply to decline.For
This, demand of the society to various sun-screening agents and sun-proof skin care agent increases rapidly.Sun-proof articles in the prior art after testing, is prevented
Shine index less than 20, ultraviolet light percent of pass is greater than 1%, therefore far from be unsatisfactory for it is most of need long when work in the sunlight
The sun-proof requirement of personnel.
Chinese patent application document " a kind of sunscreen emulsion (publication number: CN103040694A) " discloses sunscreen emulsion,
It is characterized in that it includes following composition: the hard formicester acid first of menthyl anthranilate, cycloform, hydroxyl
Ester, four contracting Monooleins, poly propylene oxide octadecyl rouge, aluminum stearate, vaseline, paraffin, mineral oil, thioesters
Magnesium, methylparaben, propylben, cactus liquid, essence, ethyl cellulose N-10, deionized water.The present invention solves existing
There is the problem that the sun-proof performance of sunscreen products is low in technology.The invention has the following advantages: SPF is greater than 25, ultraviolet light is logical
Rate is crossed less than 0.5%.
Chinese patent application document " cosmetic composition that CN100348166C contains microcrystalline cellulose " on the one hand, group
Closing object includes sun-screening agent or sun-proof pharmaceutical mixture；Emulsifier or emulsifier mixture；It selectively include emollient or emollient
Mixture；Rheology control agent；And water.The rheology control agent is microcrystalline cellulose.It is of the invention when being sprayed on skin and hair
Cosmetic composition generates equally distributed mist, drips without generating, does not also generate aggregation and drop.But present invention discover that
It can be improved the uniformity of distribution in sunscreen in individually addition microcrystalline cellulose, but permanent stop can not be improved well
The ability of skin surface, and sun-proof efficiency is higher in short-term for the composition of CN103040694A, after 1h sun-proof efficiency substantially under
Drop；Chinese patent (CN108014060A) discloses a kind of sun-proof synergistic composition and its application, the composition by weight hundred
Divide the race extraction than including the tocopherol acetate of 50-80%, the Ascorbyl Tetraisopalmitate of 10-15%, 20-30%
The bisabolol of object and 0.1-0.3%；Cosmetics further include A phase, wherein A phase be EDETATE SODIUM, sodium chloride, butanediol, glycerol,
In parahydroxyacet-ophenone, silica and Sodium Hyaluronate any one or at least two combination.Sunscreen composition selects four kinds
Active functional component, is used to prepare sunscreen cosmetic, and the sun-proof result of collaboration enhancing sun-screening agent reduces the type and use of sun-screening agent
Amount improves safety, validity and the use skin sense of sunscreen cosmetic, but its sun-proof persistence is poor, and sun-proof result is not
Very well；Chinese patent discloses a kind of osmosis type beautifying face and moistering lotion cosmetics and preparation method, including microcrystalline cellulose dispersion liquid 80-
90,30~35 parts by weight of Alphalin aliphatic ester, 15~20 parts by weight of lecithin, 18~25 parts by weight of saualane, beet alkali carries
Take 20~37 parts by weight of object, 29~52 parts by weight of aeroge, 15~20 parts by weight of glycerin monostearate, 12~20 weight of glycerol
Part, 3~5 parts by weight of sapn, 12~15 parts by weight of methylparaben, 2~3 parts by weight of dimethyl silicone polymer, gallic acid 4~
8 parts by weight.Cosmetics obtained have anti-aging, anti-oxidant, ultra-violet radiation resisting (i.e. sun-proof), beauty face-whitening-nourishing and other effects, but
Its sun-proof persistence is poor, and sun-proof result is general, and primary efficacy is anti-oxidant, anti-aging；Chinese patent (CN109316367A)
Disclose a kind of ultra light sun block lotion containing nano-cellulose: with the total weight of lotion, the content of nano-cellulose is 10~
50%, nano-cellulose partial size is 20~100nm；Further include emulsifier, propylene glycol, olive oil, stearic acid, vaseline, glycerol,
Sericin, hyaluronic acid, saualane, essence, butylated hydroxytoluene and deionized water；: it further include nano zine oxide, dimension life
One or more of plain derivative and fat-soluble fungicide；The vitamin derivative be vitamin A fatty acid ester,
One or more of vitamin C phosphoric ester and Vitwas E.Also contain a large amount of hydroxyl in nano-cellulose surface
Base can form hydrogen bond with the polar component in lotion, combine and consolidate in ultra light sun block lotion, avoid in conventional physical ultra light sun block lotion
The problem that falls off of particle, although nano-cellulose can prevent from shining the problem that falls off of particle in lotion, it can improve sun-proof
Persistence, but its sun-proof lasting effects is unobvious, and sun-proof result is not significant；Although nano-cellulose is added in it, its
Sun-proof persistence is poor, and sun-proof result is not significant.For deficiency existing for sunscreen product existing in the prior art, applicant's warp
Cross long-term exploration and research, a kind of creative sunscreen for having found high SPF.
Summary of the invention
The object of the present invention is to provide a kind of sunscreens and preparation method thereof of high SPF, when guaranteeing long to skin
Between stop simultaneously, it is insufficient to solve the problems, such as sun-proof persistence, while component is naturally pollution-free, it is high to human body compatibility.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A kind of sunscreen of high SPF, which is characterized in that including following raw material: water, methoxy cinnamic acid ethyl hexyl
Ester, bis-ethylhexoxyphenol methoxyphenyl triazine, carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate, Octocrilene, the third two
Alcohol, the own ester of diethylamino oxybenzene formylbenzoate, glycerol, methylene bis-benzotriazolyl tetramethyl butyl phenol, decyl glucose
Glycosides, propylene glycol, xanthan gum, Sucrose Polystearic Acid Esters, cetanol stearate, butanediol, Uvinul T 150, benzene oxygen second
Alcohol, pungent glycol, Sodium Polyacrylate, tocopherol acetate, bisabolol, stearoyl-glutamic acid sodium, dimethyl silicone polymer are transparent
Matter acid sodium, tetra- sodium of EDTA, Glucomannan, tea fungus dispersion, microcrystalline cellulose；
The Glucomannan, tea fungus dispersion, the ratio of microcrystalline cellulose are (0.02-0.04): (0.06-0.08)
∶(0.01-0.03)。
Further, the ratio of the Glucomannan, tea fungus dispersion, microcrystalline cellulose is 0.03: 0.07:
0.02。
Further, the sunscreen of the high SPF is as unit of parts by weight, including following raw material: 10-14 parts of water,
0.04-0.06 parts of ethylhexyl methoxy cinnamate, 0.01-0.03 parts of bis-ethylhexoxyphenol methoxyphenyl triazine, carbonic acid two
0.01-0.03 parts of monooctyl ester, lauric alcohol-caprylate/0.01-0.03 parts of decylate, 0.01-0.03 parts of Octocrilene, propylene glycol
0.3-0.4 parts, own ester 0.01-0.03 parts of diethylamino oxybenzene formylbenzoate, 2-4 parts of glycerol, di-2-ethylhexylphosphine oxide-benzotriazole base
0.01-0.03 parts of tetramethyl butyl phenol, 0.02-0.04 parts of Plantacare 818,0.2-0.4 parts of propylene glycol, xanthan gum 0.1-0.2
Part, 0.1-0.2 parts of Sucrose Polystearic Acid Esters, 0.1-0.2 parts of cetanol stearate, 0.1-0.2 parts of butanediol, ethylhexyl three
0.02-0.04 parts of piperazine ketone, 0.02-0.04 parts of Phenoxyethanol, pungent glycol 0.02-0.04 parts, 0.02-0.04 parts of Sodium Polyacrylate,
0.02-0.04 parts of tocopherol acetate, 0.01-0.03 parts of bisabolol, 0.01-0.03 parts of stearoyl-glutamic acid sodium, poly- diformazan
0.01-0.03 parts of radical siloxane, 0.01-0.03 parts of Sodium Hyaluronate, 0.01-0.03 parts of tetra- sodium of EDTA, Glucomannan 0.02-
0.04 part, 0.06-0.08 parts of tea fungus dispersion, 0.01-0.03 parts of microcrystalline cellulose.
Further, the sunscreen of the high SPF is as unit of parts by weight, including following raw material: 12 parts of water, first
0.05 part of oxygroup 2-Ethylhexyl cinnamate, 0.02 part of bis-ethylhexoxyphenol methoxyphenyl triazine, 0.02 part of carbonic acid dioctyl ester,
Lauric alcohol -0.02 part of caprylate/decylate, 0.02 part of Octocrilene, 0.35 part of propylene glycol, diethylamino oxybenzene formylbenzoate
0.02 part of own ester, 3 parts of glycerol, 0.02 part of methylene bis-benzotriazolyl tetramethyl butyl phenol, 0.03 part of Plantacare 818, third
0.3 part of glycol, 0.15 part of xanthan gum, 0.15 part of Sucrose Polystearic Acid Esters, 0.15 part of cetanol stearate, butanediol 0.15
Part, 0.03 part of Uvinul T 150,0.03 part of Phenoxyethanol, 0.03 part of pungent glycol, 0.03 part of Sodium Polyacrylate, tocopherol second
0.03 part of acid esters, 0.02 part of bisabolol, 0.02 part of stearoyl-glutamic acid sodium, 0.02 part of dimethyl silicone polymer, hyaluronic acid
0.02 part of sodium, 0.02 part, 0.03 part of Glucomannan, 0.07 part of tea fungus dispersion, 0.02 part of microcrystalline cellulose of tetra- sodium of EDTA.
Further, the average particle size of the microcrystalline cellulose is 50um or less.
Further, the tea fungus dispersion the preparation method comprises the following steps: by tea fungus in water with 800 revs/min
The revolving speed of clock quickly stirs 24 hours.
A kind of preparation method of the sunscreen according to above-mentioned high SPF, which comprises the following steps:
(1) tea fungus is quickly stirred 24 hours in water with 800 revs/min of revolving speed；(2) by methoxy cinnamic acid ethyl hexyl
Ester, bis-ethylhexoxyphenol methoxyphenyl triazine, carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate, Octocrilene, the third two
Alcohol, the own ester of diethylamino oxybenzene formylbenzoate, glycerol, methylene bis-benzotriazolyl tetramethyl butyl phenol, decyl glucose
Glycosides, propylene glycol, xanthan gum, Sucrose Polystearic Acid Esters, cetanol stearate, butanediol, Uvinul T 150, benzene oxygen second
Alcohol, pungent glycol, Sodium Polyacrylate, tocopherol acetate, bisabolol, stearoyl-glutamic acid sodium, dimethyl silicone polymer are transparent
Matter acid sodium, tetra- sodium of EDTA, Glucomannan, microcrystalline cellulose are added in the aqueous solution of step 1, and after mixing, stirring 24 is small
Shi Hou, it is filling after above-mentioned mixed liquor is stablized 7 days at 0-5 DEG C.
The invention has the following advantages:
Glucomannan in the present invention, tea fungus dispersion, microcrystalline cellulose is in the sunscreen for preparing high SPF
Synergistic effect is played, collaboration improves the persistence and sun-proof performance of the sunscreen of high SPF.Speculate its possible mechanism
It is to belong to soluble hemicellulose for Glucomannan, there are the spies such as water-soluble, water holding thickening, stable, suspension, gelling, bonding, film forming
It is fixed, there is good compatibility to skin, moisture can be locked on the skin and the film forming that extends, increase duration；Tea fungus
Dispersion its with membranoid substance property, and with Knowledge On Bacterial Biofilm natural compatibility, after being administered to skin surface, superelevation ratio
Surface area can be bonded human skin, under the action of Glucomannan, be adhered to human skin surface, under excessive water flushing
It does not fall out, guarantees that the effective component of sunscreen composition is adsorbed in mycoderm, promote persistence；Microcrystalline cellulose is whole in addition to improving
A system adherency keeps composition more uniform outer in skin surface dispersion, can also make the tiling of tea fungus dispersion more
Whole, the contact area of increase mycoderm and skin, while its crystallization feature are added, can effectively prevent sunlight direct in mycoderm
Irradiate skin.
Glucomannan, tea fungus dispersion, the common addition of microcrystalline cellulose can be fast after being applied in skin surface
Speed reconstruct, forms multi-level multilayered structure, however it is not limited to include: the tea fungus of multilayer, the Glucomannan bonding film of multilayer
Layer, the microcrystalline cellulose of multilayer, the multilayered structure of the mutual superimposed formation of three also can more be effectively prevented sunlight, and can have
There is the effect of multilayer flashing.
All components in the present invention are naturally pollution-free, high to human body compatibility, non-stimulated, are a kind of shields of natural environmental-protective
Skin product.
Specific embodiment
To facilitate a better understanding of the present invention, it is illustrated by the following examples, these examples belong to protection of the invention
Range, but do not limit the scope of the invention.
Embodiment 1
A kind of sunscreen of high SPF is as unit of parts by weight, including following raw material: 12 parts of water, methoxy cinnamic acid
0.05 part of ethylhexyl, 0.02 part of bis-ethylhexoxyphenol methoxyphenyl triazine, 0.02 part of carbonic acid dioctyl ester, lauric alcohol-octanoic acid
0.02 part of ester/decylate, 0.02 part of Octocrilene, 0.35 part of propylene glycol, 0.02 part of the own ester of diethylamino oxybenzene formylbenzoate,
It is 3 parts of glycerol, 0.02 part of methylene bis-benzotriazolyl tetramethyl butyl phenol, 0.03 part of Plantacare 818,0.3 part of propylene glycol, yellow
0.15 part of virgin rubber, 0.15 part of Sucrose Polystearic Acid Esters, 0.15 part of cetanol stearate, 0.15 part of butanediol, ethylhexyl three
0.03 part of piperazine ketone, 0.03 part of Phenoxyethanol, 0.03 part of pungent glycol is 0.03 part of Sodium Polyacrylate, 0.03 part of tocopherol acetate, red
0.02 part of bisabol, 0.02 part of stearoyl-glutamic acid sodium, 0.02 part of dimethyl silicone polymer, 0.02 part of Sodium Hyaluronate, EDTA
Four 0.02 part of sodium, 0.03 part of Glucomannan, 0.07 part of tea fungus dispersion, 0.02 part of microcrystalline cellulose.
A kind of preparation method of the sunscreen according to above-mentioned high SPF, comprising the following steps: (1) by tea fungus
In water with 800 revs/min of revolving speed, quickly stir 24 hours；(2) by ethylhexyl methoxy cinnamate, double-ethyl hexyl oxygen
Phenol anisyl triazine, carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate, Octocrilene, propylene glycol, diethylamino oxybenzene first
Acyl group hexyl-benzoate, glycerol, methylene bis-benzotriazolyl tetramethyl butyl phenol, Plantacare 818, propylene glycol, xanthan gum,
Sucrose Polystearic Acid Esters, cetanol stearate, butanediol, Uvinul T 150, Phenoxyethanol, pungent glycol, polyacrylic acid
Sodium, tocopherol acetate, bisabolol, stearoyl-glutamic acid sodium, dimethyl silicone polymer, Sodium Hyaluronate, tetra- sodium of EDTA, Portugal
Sweet glycan, microcrystalline cellulose are added in the aqueous solution of step 1, and after mixing, after stirring 24 hours, above-mentioned mixed liquor is existed
It is filling after stablizing 7 days at 0-5 DEG C.
Embodiment 2
A kind of sunscreen of high SPF is as unit of parts by weight, including following raw material: 10 parts of water, methoxy cinnamic acid
0.06 part of ethylhexyl, 0.01 part of bis-ethylhexoxyphenol methoxyphenyl triazine, 0.03 part of carbonic acid dioctyl ester, lauric alcohol-octanoic acid
0.01 part of ester/decylate, 0.03 part of Octocrilene, 0.3 part of propylene glycol, 0.03 part of the own ester of diethylamino oxybenzene formylbenzoate,
It is 2 parts of glycerol, 0.03 part of methylene bis-benzotriazolyl tetramethyl butyl phenol, 0.02 part of Plantacare 818,0.4 part of propylene glycol, yellow
0.1 part of virgin rubber, 0.2 part of Sucrose Polystearic Acid Esters, 0.1 part of cetanol stearate, 0.2 part of butanediol, Uvinul T 150
0.02 part, 0.04 part of Phenoxyethanol, 0.02 part of pungent glycol, 0.04 part of Sodium Polyacrylate, 0.02 part of tocopherol acetate, opopanax
0.03 part of alcohol, 0.01 part of stearoyl-glutamic acid sodium, 0.03 part of dimethyl silicone polymer, 0.01 part of Sodium Hyaluronate, tetra- sodium of EDTA
0.03 part, 0.02 part of Glucomannan, 0.08 part of tea fungus dispersion, 0.01 part of microcrystalline cellulose.
A kind of preparation method of the sunscreen according to above-mentioned high SPF, comprising the following steps: (1) by tea fungus
In water with 800 revs/min of revolving speed, quickly stir 24 hours；(2) by ethylhexyl methoxy cinnamate, double-ethyl hexyl oxygen
Phenol anisyl triazine, carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate, Octocrilene, propylene glycol, diethylamino oxybenzene first
Acyl group hexyl-benzoate, glycerol, methylene bis-benzotriazolyl tetramethyl butyl phenol, Plantacare 818, propylene glycol, xanthan gum,
Sucrose Polystearic Acid Esters, cetanol stearate, butanediol, Uvinul T 150, Phenoxyethanol, pungent glycol, polyacrylic acid
Sodium, tocopherol acetate, bisabolol, stearoyl-glutamic acid sodium, dimethyl silicone polymer, Sodium Hyaluronate, tetra- sodium of EDTA, Portugal
Sweet glycan, microcrystalline cellulose are added in the aqueous solution of step 1, and after mixing, after stirring 24 hours, above-mentioned mixed liquor is existed
It is filling after stablizing 7 days at 0-5 DEG C.
Embodiment 3
A kind of sunscreen of high SPF is as unit of parts by weight, including following raw material: 14 parts of water, methoxy cinnamic acid
0.04 part of ethylhexyl, 0.03 part of bis-ethylhexoxyphenol methoxyphenyl triazine, 0.01 part of carbonic acid dioctyl ester, lauric alcohol-octanoic acid
0.03 part of ester/decylate, 0.01 part of Octocrilene, 0.4 part of propylene glycol, 0.01 part of the own ester of diethylamino oxybenzene formylbenzoate,
It is 4 parts of glycerol, 0.01 part of methylene bis-benzotriazolyl tetramethyl butyl phenol, 0.04 part of Plantacare 818,0.2 part of propylene glycol, yellow
0.2 part of virgin rubber, 0.1 part of Sucrose Polystearic Acid Esters, 0.2 part of cetanol stearate, 0.1 part of butanediol, Uvinul T 150
0.04 part, 0.02 part of Phenoxyethanol, 0.04 part of pungent glycol, 0.02 part of Sodium Polyacrylate, 0.04 part of tocopherol acetate, opopanax
0.01 part of alcohol, 0.03 part of stearoyl-glutamic acid sodium, 0.01 part of dimethyl silicone polymer, 0.03 part of Sodium Hyaluronate, tetra- sodium of EDTA
0.01 part, 0.04 part of Glucomannan, 0.06 part of tea fungus dispersion, 0.03 part of microcrystalline cellulose.
A kind of preparation method of the sunscreen according to above-mentioned high SPF, comprising the following steps: (1) by tea fungus
In water with 800 revs/min of revolving speed, quickly stir 24 hours；(2) by ethylhexyl methoxy cinnamate, double-ethyl hexyl oxygen
Phenol anisyl triazine, carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate, Octocrilene, propylene glycol, diethylamino oxybenzene first
Acyl group hexyl-benzoate, glycerol, methylene bis-benzotriazolyl tetramethyl butyl phenol, Plantacare 818, propylene glycol, xanthan gum,
Sucrose Polystearic Acid Esters, cetanol stearate, butanediol, Uvinul T 150, Phenoxyethanol, pungent glycol, polyacrylic acid
Sodium, tocopherol acetate, bisabolol, stearoyl-glutamic acid sodium, dimethyl silicone polymer, Sodium Hyaluronate, tetra- sodium of EDTA, Portugal
Sweet glycan, microcrystalline cellulose are added in the aqueous solution of step 1, and after mixing, after stirring 24 hours, above-mentioned mixed liquor is existed
It is filling after stablizing 7 days at 0-5 DEG C.
Comparative example 1
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing the raw material of the sunscreen of high SPF
In lack Glucomannan, tea fungus dispersion, microcrystalline cellulose.
Comparative example 2
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing the raw material of the sunscreen of high SPF
In lack Glucomannan.
Comparative example 3
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing the raw material of the sunscreen of high SPF
In lack tea fungus dispersion.
Comparative example 4
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing the raw material of the sunscreen of high SPF
In lack microcrystalline cellulose.
Comparative example 5
Using specific embodiment 1 in Chinese patent application document " a kind of sunscreen emulsion (publication number: CN103040694A) "
The method prepares sunscreen.
Comparative example 6
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing the raw material of the sunscreen of high SPF
Middle Glucomannan is 0.01 part, tea fungus dispersion is 0.1 part, microcrystalline cellulose is 0.04 part.
Comparative example 7
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing the raw material of the sunscreen of high SPF
Middle Glucomannan is 0.05 part, tea fungus dispersion is 0.04 part, microcrystalline cellulose is 0.05 part.
Comparative example 8
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing the raw material of the sunscreen of high SPF
Middle Glucomannan is 0.05 part, tea fungus dispersion is 0.1 part, microcrystalline cellulose is 0.005 part.
To product made from embodiment 1-3 and comparative example 1-8, test initial SPF, SPF (sun protection factor) SPF according to
COPLIA scheme (94/289 Sun Protection Factor Test method publiShed By of Test Method
The Europea cosmetic s, Toiletry and Perfume Association, Brussels, Belgium,
October 1994) it carries out.Persistence test method are as follows: smear same amount of suncream in the back of the hand, be put into clear water 3 times every time
5s, mild agitation, progress test record are 0-SPF, and every the above-mentioned experiment of repetition in 30 minutes, test record was 5- after 2 hours
SPF.As a result as shown in the table.
As seen from the above table: by embodiment 1 and the data of comparative example 1-4 as it can be seen that Glucomannan, tea fungus dispersion are micro-
Crystalline cellulose plays synergistic effect in the sunscreen for preparing high SPF, and collaboration improves the sunscreen of high SPF
Compatibility and persistence.By the data of comparative example 6-8 as it can be seen that when embodiment 1-3 prepares the sunscreen of high SPF
By adding Glucomannan, the weight ratio of tea fungus dispersion, microcrystalline cellulose is (0.02-0.04): (0.06-0.08):
(0.01-0.03), collaboration improve the compatibility and persistence of the sunscreen of high SPF.
The above content is it cannot be assumed that present invention specific implementation is only limited to these instructions, for the technical field of the invention
Those of ordinary skill for, under the premise of not departing from present inventive concept, a number of simple deductions or replacements can also be made, all answers
When being considered as belonging to present invention scope of patent protection determined by the appended claims.
Claims (7)
1. a kind of sunscreen of high SPF, which is characterized in that including following raw material: water, ethylhexyl methoxy cinnamate,
Bis-ethylhexoxyphenol methoxyphenyl triazine, carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate, Octocrilene, propylene glycol,
The own ester of diethylamino oxybenzene formylbenzoate, glycerol, methylene bis-benzotriazolyl tetramethyl butyl phenol, Plantacare 818, third
Glycol, xanthan gum, Sucrose Polystearic Acid Esters, cetanol stearate, butanediol, Uvinul T 150, Phenoxyethanol, Xin Gan
Alcohol, Sodium Polyacrylate, tocopherol acetate, bisabolol, stearoyl-glutamic acid sodium, dimethyl silicone polymer, Sodium Hyaluronate,
Tetra- sodium of EDTA, Glucomannan, tea fungus dispersion, microcrystalline cellulose；
The ratio of the Glucomannan, tea fungus dispersion, microcrystalline cellulose is (0.02-0.04): (0.06-0.08):
(0.01-0.03)。
2. the sunscreen of high SPF according to claim 1, which is characterized in that the Glucomannan, tea fungus
Dispersion, the ratio of microcrystalline cellulose are 0.03: 0.07: 0.02.
3. the sunscreen of high SPF according to claim 1, which is characterized in that the sunscreen of the high SPF
As unit of parts by weight, including following raw material: 10-14 parts of water, 0.04-0.06 parts of ethylhexyl methoxy cinnamate, double-ethyl
0.01-0.03 parts of own oxy phenol anisyl triazine, 0.01-0.03 parts of carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate
0.01-0.03 parts, 0.01-0.03 parts of Octocrilene, 0.3-0.4 parts of propylene glycol, the own ester of diethylamino oxybenzene formylbenzoate
0.01-0.03 parts, 2-4 parts of glycerol, 0.01-0.03 parts of methylene bis-benzotriazolyl tetramethyl butyl phenol, Plantacare 818
0.02-0.04 parts, 0.2-0.4 parts of propylene glycol, 0.1-0.2 parts of xanthan gum, 0.1-0.2 parts of Sucrose Polystearic Acid Esters, cetanol is hard
0.1-0.2 parts of resin acid ester, 0.1-0.2 parts of butanediol, 0.02-0.04 parts of Uvinul T 150, Phenoxyethanol 0.02-0.04
Part, pungent glycol 0.02-0.04 parts, 0.02-0.04 parts of Sodium Polyacrylate, 0.02-0.04 parts of tocopherol acetate, bisabolol
0.01-0.03 parts, 0.01-0.03 parts of stearoyl-glutamic acid sodium, 0.01-0.03 parts of dimethyl silicone polymer, Sodium Hyaluronate
0.01-0.03 parts, 0.01-0.03 parts of tetra- sodium of EDTA, 0.02-0.04 parts of Glucomannan, tea fungus dispersion 0.06-0.08
Part, 0.01-0.03 parts of microcrystalline cellulose.
4. the sunscreen of high SPF according to claim 1, which is characterized in that the sunscreen of the high SPF
As unit of parts by weight, including following raw material: 12 parts of water, 0.05 part of ethylhexyl methoxy cinnamate, double-ethyl hexyl oxy phenol
0.02 part of anisyl triazine, 0.02 part of carbonic acid dioctyl ester, lauric alcohol -0.02 part of caprylate/decylate, Octocrilene 0.02
Part, 0.35 part of propylene glycol, 0.02 part of the own ester of diethylamino oxybenzene formylbenzoate, 3 parts of glycerol, di-2-ethylhexylphosphine oxide-benzotriazole base
0.02 part of tetramethyl butyl phenol, 0.03 part of Plantacare 818,0.3 part of propylene glycol, 0.15 part of xanthan gum, Sucrose Polystearic Acid Esters
0.15 part, 0.15 part of cetanol stearate, 0.15 part of butanediol, 0.03 part of Uvinul T 150,0.03 part of Phenoxyethanol,
0.03 part of pungent glycol, 0.03 part of Sodium Polyacrylate, 0.03 part of tocopherol acetate, 0.02 part of bisabolol, stearoyl-glutamic acid
0.02 part of sodium, 0.02 part of dimethyl silicone polymer, 0.02 part of Sodium Hyaluronate, 0.02 part of tetra- sodium of EDTA, 0.03 part of Glucomannan,
0.07 part of tea fungus dispersion, 0.02 part of microcrystalline cellulose.
5. the sunscreen of high SPF according to claim 1, which is characterized in that the average grain of the microcrystalline cellulose
Degree is 50um or less.
6. the sunscreen of high SPF according to claim 1, which is characterized in that the tea fungus dispersion
The preparation method comprises the following steps: tea fungus is quickly stirred 24 hours in water with 800 revs/min of revolving speed.
7. a kind of preparation method of the sunscreen of high SPF according to claim 1-6, which is characterized in that
The following steps are included: (1) is by tea fungus in water with 800 revs/min of revolving speed, quick stirring 24 hours；(2) by methoxyl group
2-Ethylhexyl cinnamate, bis-ethylhexoxyphenol methoxyphenyl triazine, carbonic acid dioctyl ester, lauric alcohol-caprylate/decylate are difficult to understand
Ke Lilin, propylene glycol, the own ester of diethylamino oxybenzene formylbenzoate, glycerol, di-2-ethylhexylphosphine oxide-benzotriazole base tetramethyl butyl
Phenol, Plantacare 818, propylene glycol, xanthan gum, Sucrose Polystearic Acid Esters, cetanol stearate, butanediol, ethylhexyl triazine
Ketone, Phenoxyethanol, pungent glycol, Sodium Polyacrylate, tocopherol acetate, bisabolol, stearoyl-glutamic acid sodium, poly dimethyl silicon
Oxygen alkane, Sodium Hyaluronate, tetra- sodium of EDTA, Glucomannan, microcrystalline cellulose are added in the aqueous solution of step 1, after mixing,
It is filling after above-mentioned mixed liquor is stablized 7 days at 0-5 DEG C after stirring 24 hours.
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| CN111265459A (en) * | 2020-03-12 | 2020-06-12 | 广东袋鼠妈妈生物科技有限公司 | Sun cream for children and preparation method thereof |
| CN111631973A (en) * | 2020-04-27 | 2020-09-08 | 广州艾蓓生物科技有限公司 | High-stability sunscreen stick and preparation method thereof |
| CN112156035A (en) * | 2020-10-20 | 2021-01-01 | 上海中翊日化有限公司 | Sun-proof stick and preparation method thereof |
| CN112156027A (en) * | 2020-10-27 | 2021-01-01 | 广州德芙化妆品有限公司 | Sunscreen cream with high sun protection value and preparation method thereof |
| CN112516022A (en) * | 2020-12-03 | 2021-03-19 | 深圳市琉璃光生物科技有限公司 | Sun-screening lotion and preparation method thereof |
| WO2021069158A1 (en) * | 2019-10-09 | 2021-04-15 | Beiersdorf Ag | Sunscreen containing a natural, film-forming polymer |
| CN113398034A (en) * | 2021-07-13 | 2021-09-17 | 云南贝泰妮生物科技集团股份有限公司 | Pickering children sunscreen lotion and preparation method thereof |
| CN114588072A (en) * | 2022-03-31 | 2022-06-07 | 浙江宜格企业管理集团有限公司 | Sunscreen composition and preparation method thereof |
| CN116139038A (en) * | 2022-12-29 | 2023-05-23 | 广州梵之容化妆品有限公司 | Natural flexible film-forming sun-screening synergistic composition and preparation method and application thereof |
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| WO2021069158A1 (en) * | 2019-10-09 | 2021-04-15 | Beiersdorf Ag | Sunscreen containing a natural, film-forming polymer |
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| CN113398034A (en) * | 2021-07-13 | 2021-09-17 | 云南贝泰妮生物科技集团股份有限公司 | Pickering children sunscreen lotion and preparation method thereof |
| CN113398034B (en) * | 2021-07-13 | 2023-03-21 | 云南贝泰妮生物科技集团股份有限公司 | Pickering children sunscreen lotion and preparation method thereof |
| CN114588072A (en) * | 2022-03-31 | 2022-06-07 | 浙江宜格企业管理集团有限公司 | Sunscreen composition and preparation method thereof |
| CN116139038A (en) * | 2022-12-29 | 2023-05-23 | 广州梵之容化妆品有限公司 | Natural flexible film-forming sun-screening synergistic composition and preparation method and application thereof |
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| CN110051617B (en) | 2020-07-24 |
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