CN1704043A - Konjac glucomanna paint - Google Patents

Konjac glucomanna paint Download PDF

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Publication number
CN1704043A
CN1704043A CN 200410045202 CN200410045202A CN1704043A CN 1704043 A CN1704043 A CN 1704043A CN 200410045202 CN200410045202 CN 200410045202 CN 200410045202 A CN200410045202 A CN 200410045202A CN 1704043 A CN1704043 A CN 1704043A
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CN
China
Prior art keywords
glucomannoglycan
water
paint
carboxymethyl cellulose
sodium carboxymethyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 200410045202
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Chinese (zh)
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CN1291708C (en
Inventor
庞杰
徐秋兰
谢建华
余清
陈青青
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Fujian Agriculture and Forestry University
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Fujian Agriculture and Forestry University
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Publication date
Application filed by Fujian Agriculture and Forestry University filed Critical Fujian Agriculture and Forestry University
Priority to CN 200410045202 priority Critical patent/CN1291708C/en
Publication of CN1704043A publication Critical patent/CN1704043A/en
Application granted granted Critical
Publication of CN1291708C publication Critical patent/CN1291708C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Medicinal Preparation (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to a glucomannan pigmentum which is a non-toxic and antibiotic mask. It is formed by glucomannan, sodium carboxymethyl cellulose, vitamin C, glycerin, potassium sobate and water. The glucomannan pigmentum has high chemical attraction with human body's skin and can be absorbed fully by human body so as to improve the water-holding capacity of skin and effectively delay the senility of cell.

Description

A kind of glucomannoglycan paint
Affiliated technical field the present invention relates to a kind of paint, particularly a kind of glucomannoglycan paint.
The background technology paint is normally used for spreading upon the surface of protected object, makes that protected object is relative with air isolates, and dries the back and forms thin film on the surface of protected object, reaches to slow down purposes such as oxidation, delay putrefaction be rotten.General paint has kinds such as natural resin paint, oils and fats paint, chitosan paint, albumen paint, can be used as film former and natural antiseptic agent.
" storage and processing " delivers the article " preparation of several coating antistaling agents and use " of Zhao Xiyan, Gao Haisheng on the 1st the 6th phase of volume of calendar year 2001, introduced the method for making of oils and fats paint, natural paint etc., with the oil membrane paint is example, earlier arabic gum is immersed in the water, treat that the stirring of swelling post-heating makes its dissolving, add sorbitol anhydride fatty acid fat and Oleum Gossypii semen then, adding thermal agitation makes it become emulsion, fruit is flooded in this emulsion, taking-up is dried the back and is formed thin film, can case into storage.
" food science and technology " nineteen ninety the 44th is rolled up the article " edibility glutenin paint " of delivering Gennadios and Weller, and the glutenin film is to O 2And CO 2Be good blockage, their mechanical performance can compare favourably with the poly film, but these films are because their hydrophilic habits have high saturating property to water.
Because paint is the excellent drug carrier, people also are used for human medical treatment and health care aspect to it, and more common is useful on the liniment that applies the human body wound and is coated in facial face-beautifying and spot-removing facial film etc.
" Chinese experimental pharmacology of Chinese medical formulae magazine " delivers the article " preparation of face-beautifying and spot-removing facial film and observation of curative effect " of Gao Huiqin on 2002 the 8th the 3rd phases of volume, its preparation method: the Chinese medicine of recipe quantity is decocted with water twice (each 1h) collecting decoction be concentrated into 500mI, add an amount of 95% ethanol cold preservation 48h, cold preservation liquid elder generation siphon supernatant, use centrifuge with the centrifugal 30min of 2200r/min precipitate, further separate, merge cold preservation liquid, standby behind the water-bath volatilization ethanol.PVA sodium carboxymethyl cellulose adding distil water is soaked 24h, the fully rearmounted 85 ℃ of heating in water bath dissolving of swelling slurrying, and add Chinese medicine extraction liquid, glycerol, ethyl hydroxybenzoate, distilled water successively and be stirred well to 1000mI.Place froth breaking, get product.
" Zunyi Medical College's journal " delivers Li Datie on 2000 the 23rd the 1st phases of volume, the article of Zheng Quan etc. " Chinese medicine goes speckle medicine film treatment chloasma curative effect contrast observing ", adopt the effective ingredient in water, ethanol and the organic solvent extraction Chinese medicine, purify, filter out impurities through refining, after being concentrated into biological content desired concn, add suitable film former, packing, airtight, autoclave sterilization is standby.
Patent of invention " burn film-coating agent " (in please number: 02109103), introduced a kind of at the burn mainly be to be substrate with the chitin, add liniment such as broken Carapax et Plastrum Testudinis, charred Radix Sanguisorbae, Colla Corii Asini bead.
(application number: 99112620), introduced a kind of is the liniment that raw material is made with Radix aconiti szechenyiani, Oletum Trogopterori, Rhizoma Corydalis, Borneolum Syntheticum etc. to patent of invention " mulation for analgesia smearing agent and preparation technology thereof ".
The raw material of above-mentioned various liniment is not raw material with the glucomannoglycan.
Summary of the invention purpose of the present invention is a film forming principle of utilizing glucomannoglycan, cooperates other medicaments, makes nontoxicly, has water-retaining property, conformality, and a kind of glucomannoglycan paint of antibiotic health care.
A kind of glucomannoglycan paint of the present invention is a kind of facial film, and its product is an Emulsion; By glucomannoglycan [(C 20H 32O 16) n], sodium carboxymethyl cellulose [(C 9H 13O 7Na) n], vitamin C (C 6H 8O 6), glycerol (C 3H 8O 3), potassium sorbate (C 6H 7O 2K) and water (H 2O) form, the percentage by weight of each raw material and water is respectively glucomannoglycan 0.1%-2.0%, sodium carboxymethyl cellulose 0.025%-0.5%, vitamin C 0.25%-0.5%, glycerol 0.5%-1.0%, potassium sorbate 0.001%-0.002%.
The preparation method of a kind of glucomannoglycan paint of the present invention is made up of following steps:
(1) percentage by weight according to sodium carboxymethyl cellulose and water is 0.025-0.5%, sodium carboxymethyl cellulose is added be equipped with in the container of water, and heated and stirred is to dissolving on magnetic stirring apparatus to put container, and the temperature of heating is controlled at 70-80 ℃;
(2) percentage by weight according to glucomannoglycan and water is 0.1-2.0%, and glucomannoglycan is slowly added in the above-mentioned solution, continues to be stirred to fully the dissolving back and takes out, and it is standby to be cooled to room temperature;
(3) be glycerol 0.5-1.0% according to the percentage by weight with water, vitamin C 0.25-0.5%, potassium sorbate 0.001-0.002% join in the mixed solution of glucomannoglycan and sodium carboxymethyl cellulose;
(4) stir after, use the centrifuge of 3000r/min, outgased 20-30 minute, remove the gas that exists in the paint;
(5) through sterilization, bottled respectively according to different specifications is the product of Different Weight.
A kind of glucomannoglycan paint of the present invention is a primary raw material with the glucomannoglycan, has special physicochemical property and antibiotic, health-care effects such as the original composition of good maintenance, water conservation, conformal, plastic, film forming.But also has advantage such as draw materials conveniently, cheap.A kind of glucomannoglycan paint of the present invention is nontoxic, even eat by mistake also harmless.It is used for cosmetics outstanding advantage, can delaying skin in the migration and the diffusion of moisture content and other composition; Can also have antibacterial effect as the carrier of medicinal ingredient.Glucomannoglycan has the macromolecule network structure, by mixing with other material, can form the film with superperformance, is the good material of preparation paint.It and human skin have high-affinity, can be absorbed by the body fully, and deep layer is improved and the nutrition human skin, significantly improves the skin moisturizing ability, effectively delaying cell aging.Glycerol has the good moisture preserving effect in the active ingredient; Vitamin C mainly is to adjust film formation time, improves to be coated with the exhibition greasy property; Sodium carboxymethyl cellulose helps film forming, and no mesh occurs in the film, and film can be uncovered by full wafer.
Specific embodiment: in order fully to disclose a kind of glucomannoglycan paint of the present invention, below in conjunction with
Embodiment is illustrated.
Embodiment:
A kind of glucomannoglycan paint, be made up of glucomannoglycan, sodium carboxymethyl cellulose, vitamin C, glycerol, potassium sorbate and water, the percentage by weight of each raw material and water is respectively glucomannoglycan 2.0%, sodium carboxymethyl cellulose 0.5%, vitamin 0.5%, glycerol 1.0%, potassium sorbate 0.002%.Its preparation method is as follows:
(1) percentage by weight according to sodium carboxymethyl cellulose and water is 0.5%, sodium carboxymethyl cellulose is added be equipped with in the container of water, and heated and stirred is to dissolving on magnetic stirring apparatus to put container, and the temperature of heating is 75 ℃;
(2) percentage by weight according to glucomannoglycan and water is 2.0%, and glucomannoglycan is slowly added in the above-mentioned solution, continues to be stirred to fully the dissolving back and takes out, and it is standby to be cooled to room temperature;
(3) be glycerol 1.0%, vitamin C 0.5%, potassium sorbate 0.002% with following material according to percentage by weight, join in the mixed solution of glucomannoglycan and sodium carboxymethyl cellulose with water;
(4) stir after, use the centrifuge of 3000r/min, outgas 30 minutes, remove the gas that exists in the film liquid, the film of generation is uniform and smooth when guaranteeing to use;
(5) through sterilization, bottled respectively according to different specifications is the product of Different Weight.
Using method: water is cleaned face, takes out an amount of Emulsion, evenly is applied to face, behind the 10-15min, forms the thin film of layer of transparent; Press...withing one's finger rubs pat facial 10min after, the thin film full wafer taken off getting final product twice weekly.This mask product structure exquisiteness is often used to help improving the skin nutrition absorbability, makes skin be rich in gloss, and is tender smooth.

Claims (3)

1, a kind of glucomannoglycan paint, it is characterized in that being made up of glucomannoglycan, sodium carboxymethyl cellulose, vitamin C, glycerol, potassium sorbate and water, the percentage by weight of each raw material and water is respectively glucomannoglycan 0.1-2.0%, sodium carboxymethyl cellulose 0.025-0.5%, vitamin C 0.25-0.5%, glycerol 0.5-1.0%, potassium sorbate 0.001-0.002%.
2, a kind of glucomannoglycan paint according to claim 1 is characterized in that the percentage by weight of each raw material and water is respectively glucomannoglycan 2.0%, sodium carboxymethyl cellulose 0.5%, vitamin 0.5%, glycerol 1.0%, potassium sorbate 0.002%.
3, a kind of preparation method of glucomannoglycan paint is characterized in that
(1) percentage by weight according to sodium carboxymethyl cellulose and water is 0.025-0.5%, sodium carboxymethyl cellulose is added be equipped with in the container of water, and heated and stirred is to dissolving on magnetic stirring apparatus to put container, and the temperature of heating is controlled at 70-80 ℃;
(2) percentage by weight according to glucomannoglycan and water is 0.1-2.0%, and glucomannoglycan is slowly added in the above-mentioned solution, continues to be stirred to fully the dissolving back and takes out, and it is standby to be cooled to room temperature;
(3) be glycerol 0.5-1.0% according to the percentage by weight with water, vitamin C 0.25-0.5%, potassium sorbate 0.001-0.002% join in the mixed solution of glucomannoglycan and sodium carboxymethyl cellulose;
(4) stir after, use the centrifuge of 3000r/min, outgased 20-30 minute, remove the gas that exists in the paint.
CN 200410045202 2004-05-27 2004-05-27 Konjac glucomanna paint Expired - Fee Related CN1291708C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 200410045202 CN1291708C (en) 2004-05-27 2004-05-27 Konjac glucomanna paint

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200410045202 CN1291708C (en) 2004-05-27 2004-05-27 Konjac glucomanna paint

Publications (2)

Publication Number Publication Date
CN1704043A true CN1704043A (en) 2005-12-07
CN1291708C CN1291708C (en) 2006-12-27

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103405350A (en) * 2013-07-16 2013-11-27 福建农林大学 Granular glucomannan moisturizing mask and preparation method thereof
CN103405374A (en) * 2013-07-16 2013-11-27 福建农林大学 Freckle-removing and skin-whitening type gulcomannan particle facial mask and preparation method thereof
CN110051617A (en) * 2019-05-14 2019-07-26 连云港诗碧曼生物科技有限公司 A kind of sunscreen and preparation method thereof of high SPF

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103405350A (en) * 2013-07-16 2013-11-27 福建农林大学 Granular glucomannan moisturizing mask and preparation method thereof
CN103405374A (en) * 2013-07-16 2013-11-27 福建农林大学 Freckle-removing and skin-whitening type gulcomannan particle facial mask and preparation method thereof
CN103405374B (en) * 2013-07-16 2015-07-08 福建农林大学 Freckle-removing and skin-whitening type gulcomannan particle facial mask and preparation method thereof
CN110051617A (en) * 2019-05-14 2019-07-26 连云港诗碧曼生物科技有限公司 A kind of sunscreen and preparation method thereof of high SPF
CN110051617B (en) * 2019-05-14 2020-07-24 连云港诗碧曼生物科技有限公司 Sunscreen emulsion with high sun protection index and preparation method thereof

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Publication number Publication date
CN1291708C (en) 2006-12-27

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C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
EE01 Entry into force of recordation of patent licensing contract

Assignee: Fujian XinriXi'an Group Co., Ltd.

Assignor: Fujian Agricultural and Forestry University

Contract fulfillment period: 2009.7.28 to 2014.7.27 contract change

Contract record no.: 2009350000173

Denomination of invention: Konjac glucomanna paint

Granted publication date: 20061227

License type: Exclusive license

Record date: 2009.8.18

LIC Patent licence contract for exploitation submitted for record

Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2009.7.28 TO 2014.7.27; CHANGE OF CONTRACT

Name of requester: FUJIAN XINRIXIAN GROUP CO.,LTD.

Effective date: 20090818

C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20061227

Termination date: 20140527