CN110040964A - Clear frit and the method for preparing high white pottery ceramic products thoroughly with it - Google Patents
Clear frit and the method for preparing high white pottery ceramic products thoroughly with it Download PDFInfo
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- CN110040964A CN110040964A CN201910392106.3A CN201910392106A CN110040964A CN 110040964 A CN110040964 A CN 110040964A CN 201910392106 A CN201910392106 A CN 201910392106A CN 110040964 A CN110040964 A CN 110040964A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
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Abstract
The invention discloses a kind of clear frit and the methods for preparing high white pottery ceramic products thoroughly with it, belong to ceramic technology field.Clear frit of the invention includes following component: kaolin, aluminium oxide, dolomite, pyrophillite 10, magnesite, cerium oxide, yttrium oxide, terbium oxide, zirconium oxide, solid, clay, modified zeolite powder, strontium carbonate, sodium phosphite and dispersing agent.With the method for the high white pottery ceramic products thoroughly of clear frit preparation, includes the following steps: to be crushed except iron, prepare modified zeolite powder, mixing, prepare glaze, glazing and firing.High white pottery ceramic products whiteness thoroughly obtained is high, has high gloss and Gao Baidu, and thermal shock resistance is strong, and surface strength is high, and in anti-crack detection, secondly circulation is not cracked, and lead, chromium the amount of dissolution are met the requirements of the standard.
Description
Technical field
The invention belongs to ceramic technology fields, and in particular to a kind of clear frit and the side with the high white pottery ceramic products thoroughly of its preparation
Method.
Background technique
Since ancient times, Chinese ceramic is exported at home and abroad, and ceramic product type is innumerable.Chinese white pottery, also known as
" building white ", " Chinese white ", under illumination, tire glaze is bright, and pink or milky of maying be seen indistinctly is commonly called as " lard white ware ", " ivory
It is white ".The glaze whiteness of the saturating white pottery ceramic products of common height can no longer meet demand of the people to whiteness, and traditional white pottery porcelain
It is heat-resisting, present demand is also unable to satisfy in intensity.
In use for some time, not only glossiness can reduce traditional white pottery porcelain, and outer surface is easily stained with other colors,
Phenomena such as influencing aesthetics, or even glaze cracking can occur, different degrees of health hazard is caused to user.
Summary of the invention
It is beautiful that it is an object of the invention to overcome the deficiencies of the prior art and provide a kind of glaze patterns, glaze surface intensity
Height, almost furnace transmutation glaze ceramic under flawless glaze.
The present invention adopts the following technical scheme:
Clear frit, including the following component according to mass fraction meter: 8~10 parts of kaolin, 7~11 parts of aluminium oxide, white clouds
3~6 parts of stone, 10~13 parts of pyrophillite, 11~15 parts of magnesite, 11~15 parts of cerium oxide, 13~14 parts of yttrium oxide, terbium oxide 8
~9 parts, 16~18 parts of zirconium oxide, 4~8 parts of solid, 6~8 parts of clay, 11~13 parts of modified zeolite powder, strontium carbonate 13~15
Part, 1~5 part of sodium phosphite, 4~6 parts of dispersing agent.
Further, the solid is terpene resin, and the clay is bentonite, and the dispersing agent is lignin.
With the method for the high white pottery ceramic products thoroughly of clear frit preparation, include the following steps:
Step 1: broken remove iron:
According to the mass fraction, by the kaolin, aluminium oxide, dolomite, pyrophillite, magnesite, cerium oxide, oxidation
Yttrium, terbium oxide, zirconium oxide, clay and strontium carbonate are crushed respectively, and carry out handling except iron respectively, are then mixed said components equal
It is even, obtain pre-feed；
Step 2: preparing modified zeolite powder:
Zeolite powder is modified processing, obtains modified zeolite powder；
Step 3: mixing:
According to the mass fraction, successively by the solid, sodium phosphite, dispersing agent, pre-feed obtained by step 1 and
Modified zeolite powder obtained by step 2 is uniformly mixed, and obtains mixture；
Step 4: preparing glaze:
The concentration of three gained mixture of regulating step obtains marzacotto to 43~46 Baume degrees；
Step 5: glazing:
By marzacotto glazing obtained by step 4 to ceramic body outer surface, glazed ceramics green body is obtained；
Step 6: firing:
Glazed ceramics green body obtained by step 5 is fired, obtains high white pottery ceramic products after cooling.
Further, the detailed process of modification described in step 2 is as follows: according to the mass fraction, first by zeolite powder
It puts into container, then 6~8ml/L ammonium chloride is placed in container, and stir and boil 10~15min, boiling must be modified after filtering
Mountain flour.
Further, sintering procedure described in step 6 is as follows:
First burning section: 700~850 DEG C are first warming up to, then 0.8~1.3h of constant temperature；
Second burning section: 900~1000 DEG C are warming up to from 700~850 DEG C, then 0.5~1h of constant temperature；
Third burning section: being warming up to 1100~1150 DEG C from 900~1000 DEG C, then 1.5~2h of constant temperature, last naturally cold
But, the method for high white pottery ceramic products is obtained.
Compared with the prior art, the present invention has the following beneficial effects:
The first, clear frit of the invention, research staff's discovery, by obtaining modified zeolite after being modified to zeolite powder
Powder, meanwhile, the clear frit containing modified zeolite powder, magnesite, cerium oxide and yttrium oxide, the glaze layer after firing is than traditional white glaze
Whiteness increased, and glossiness is stronger.Gloss can be improved with the consistency between glaze layer component by magnesite, and led to
After the addition of peroxidating cerium and yttrium oxide, the light transmittance of glaze layer can be improved, enhance visual effect；
The second, clear frit of the invention with kaolin for main glaze layer skeleton, using strontium carbonate and sodium phosphite as skeleton
Auxiliary material, dolomite improve glaze by having the aluminium oxide for improving intensity and zirconium oxide to be used in mixed way jointly as fluxing agent
Intensity, prevent crackle.Moreover, in order to improve the viscosity of glaze layer and ceramic body surface, falling off for glaze layer is prevented, by
Solid improves the adhesive force of glaze layer and the dispersion effect of dispersing agent, guarantees that each position of glaze layer can reach strong adhesive force,
Improve the intensity of glaze layer.
Specific embodiment
Raw material used in the present invention is commercially available product.
Embodiment 1
Clear frit, including the following component according to mass fraction meter: 8 parts of kaolin, 7 parts of aluminium oxide, 3 parts of dolomite, leaf
10 parts of cured stone, 11 parts of magnesite, 11 parts of cerium oxide, 13 parts of yttrium oxide, 8 parts of terbium oxide, 16 parts of zirconium oxide, 4 parts of solid, clay
6 parts, 11 parts of modified zeolite powder, 13 parts of strontium carbonate, 1 part of sodium phosphite, 4 parts of dispersing agent.
The solid is terpene resin, and the clay is bentonite, and the dispersing agent is lignin.
The method of the high white pottery ceramic products thoroughly of the preparation of the clear frit described in claim 1, which is characterized in that including walking as follows
It is rapid:
Step 1: broken remove iron:
According to the mass fraction, by the kaolin, aluminium oxide, dolomite, pyrophillite, magnesite, cerium oxide, oxidation
Yttrium, terbium oxide, zirconium oxide, clay and strontium carbonate are crushed respectively, and carry out handling except iron respectively, are then mixed said components equal
It is even, obtain pre-feed；
Step 2: preparing modified zeolite powder:
Zeolite powder is modified processing, obtains modified zeolite powder；
The detailed process of the modification is as follows: according to the mass fraction, first putting into zeolite powder in container, then
6ml/L ammonium chloride is placed in container, and stirs and boils 10min, modified zeolite powder is obtained after filtering.
Step 3: mixing:
According to the mass fraction, successively by the solid, sodium phosphite, dispersing agent, pre-feed obtained by step 1 and
Modified zeolite powder obtained by step 2 is uniformly mixed, and obtains mixture；
Step 4: preparing glaze:
The concentration of three gained mixture of regulating step obtains marzacotto to 43 Baume degrees；
Step 5: glazing:
By marzacotto glazing obtained by step 4 to ceramic body outer surface, glazed ceramics green body is obtained；
Step 6: firing:
Glazed ceramics green body obtained by step 5 is fired, obtains high white pottery ceramic products after cooling.
Wherein, the sintering procedure is as follows:
First burning section: 700 DEG C are first warming up to, then constant temperature 1.3h；
Second burning section: 900 DEG C are warming up to from 700 DEG C, then constant temperature 1h；
Third burning section: being warming up to 1100 DEG C from 900 DEG C, then constant temperature 2h, and last natural cooling obtains high white ceramic system
The method of product.
Embodiment 2
Clear frit, including the following component according to mass fraction meter: 9 parts of kaolin, 8 parts of aluminium oxide, 4 parts of dolomite, leaf
11 parts of cured stone, 12 parts of magnesite, 12 parts of cerium oxide, 14 parts of yttrium oxide, 9 parts of terbium oxide, 17 parts of zirconium oxide, 5 parts of solid, clay
7 parts, 12 parts of modified zeolite powder, 14 parts of strontium carbonate, 2 parts of phosphorous acid, 5 parts of dispersing agent.
The solid is terpene resin, and the clay is bentonite, and the dispersing agent is lignin.
With the method for the high white pottery ceramic products thoroughly of clear frit preparation, include the following steps:
Step 1: broken remove iron:
According to the mass fraction, by the kaolin, aluminium oxide, dolomite, pyrophillite, magnesite, cerium oxide, oxidation
Yttrium, terbium oxide, zirconium oxide, clay and strontium carbonate are crushed respectively, and carry out handling except iron respectively, are then mixed said components equal
It is even, obtain pre-feed；
Step 2: preparing modified zeolite powder:
Zeolite powder is modified processing, obtains modified zeolite powder；
The detailed process of the modification is as follows: according to the mass fraction, first putting into zeolite powder in container, then
7ml/L ammonium chloride is placed in container, and stirs and boils 11min, modified zeolite powder is obtained after filtering.
Step 3: mixing:
According to the mass fraction, successively by the solid, sodium phosphite, dispersing agent, pre-feed obtained by step 1 and
Modified zeolite powder obtained by step 2 is uniformly mixed, and obtains mixture；
Step 4: preparing glaze:
The concentration of three gained mixture of regulating step obtains marzacotto to 44 Baume degrees；
Step 5: glazing:
By marzacotto glazing obtained by step 4 to ceramic body outer surface, glazed ceramics green body is obtained；
Step 6: firing:
Glazed ceramics green body obtained by step 5 is fired, obtains high white pottery ceramic products after cooling.
Wherein, the sintering procedure is as follows:
First burning section: 780 DEG C are first warming up to, then constant temperature 1.1h；
Second burning section: 950 DEG C are warming up to from 780 DEG C, then constant temperature 0.8h；
Third burning section: being warming up to 1120 DEG C from 950 DEG C, then constant temperature 1.8h, and last natural cooling obtains high white pottery porcelain
The method of product.
Embodiment 3
Clear frit, including the following component according to mass fraction meter: 10 parts of kaolin, 9 parts of aluminium oxide, 5 parts of dolomite, leaf
12 parts of cured stone, 14 parts of magnesite, 14 parts of cerium oxide, 13 parts of yttrium oxide, 8 parts of terbium oxide, 16 parts of zirconium oxide, 6 parts of solid, clay
7 parts, 11 parts of modified zeolite powder, 13 parts of strontium carbonate, 3 parts of sodium phosphite, 5 parts of dispersing agent.
The solid is terpene resin, and the clay is bentonite, and the dispersing agent is lignin.
The method of the high white pottery ceramic products thoroughly of the preparation of the clear frit described in claim 1, which is characterized in that including walking as follows
It is rapid:
Step 1: broken remove iron:
According to the mass fraction, by the kaolin, aluminium oxide, dolomite, pyrophillite, magnesite, cerium oxide, oxidation
Yttrium, terbium oxide, zirconium oxide, clay and strontium carbonate are crushed respectively, and carry out handling except iron respectively, are then mixed said components equal
It is even, obtain pre-feed；
Step 2: preparing modified zeolite powder:
Zeolite powder is modified processing, obtains modified zeolite powder；
The detailed process of the modification is as follows: according to the mass fraction, first putting into zeolite powder in container, then
8ml/L ammonium chloride is placed in container, and stirs and boils 14min, modified zeolite powder is obtained after filtering.
Step 3: mixing:
According to the mass fraction, successively by the solid, sodium phosphite, dispersing agent, pre-feed obtained by step 1 and
Modified zeolite powder obtained by step 2 is uniformly mixed, and obtains mixture；
Step 4: preparing glaze:
The concentration of three gained mixture of regulating step obtains marzacotto to 45 Baume degrees；
Step 5: glazing:
By marzacotto glazing obtained by step 4 to ceramic body outer surface, glazed ceramics green body is obtained；
Step 6: firing:
Glazed ceramics green body obtained by step 5 is fired, obtains high white pottery ceramic products after cooling.
Wherein, the sintering procedure is as follows:
First burning section: 830 DEG C are first warming up to, then constant temperature 1.0h；
Second burning section: 980 DEG C are warming up to from 830 DEG C, then constant temperature 0.6h；
Third burning section: being warming up to 1130 DEG C from 980 DEG C, then constant temperature 1.7h, and last natural cooling obtains high white pottery porcelain
The method of product.
Embodiment 4
Clear frit, including the following component according to mass fraction meter: 10 parts of kaolin, 11 parts of aluminium oxide, 6 parts of dolomite,
It 13 parts of pyrophillite, 15 parts of magnesite, 15 parts of cerium oxide, 14 parts of yttrium oxide, 9 parts of terbium oxide, 18 parts of zirconium oxide, 8 parts of solid, glues
8 parts, 13 parts of modified zeolite powder, 15 parts of strontium carbonate, 5 parts of sodium phosphite, 6 parts of dispersing agent of soil.
The solid is terpene resin, and the clay is bentonite, and the dispersing agent is lignin.
With the method for the high white pottery ceramic products thoroughly of clear frit preparation, include the following steps:
Step 1: broken remove iron:
According to the mass fraction, by the kaolin, aluminium oxide, dolomite, pyrophillite, magnesite, cerium oxide, oxidation
Yttrium, terbium oxide, zirconium oxide, clay and strontium carbonate are crushed respectively, and carry out handling except iron respectively, are then mixed said components equal
It is even, obtain pre-feed；
Step 2: preparing modified zeolite powder:
Zeolite powder is modified processing, obtains modified zeolite powder；
The detailed process of the modification is as follows: according to the mass fraction, first putting into zeolite powder in container, then
8ml/L ammonium chloride is placed in container, and stirs and boils 15min, modified zeolite powder is obtained after filtering.
Step 3: mixing:
According to the mass fraction, successively by the solid, sodium phosphite, dispersing agent, pre-feed obtained by step 1 and
Modified zeolite powder obtained by step 2 is uniformly mixed, and obtains mixture；
Step 4: preparing glaze:
The concentration of three gained mixture of regulating step obtains marzacotto to 46 Baume degrees；
Step 5: glazing:
By marzacotto glazing obtained by step 4 to ceramic body outer surface, glazed ceramics green body is obtained；
Step 6: firing:
Glazed ceramics green body obtained by step 5 is fired, obtains high white pottery ceramic products after cooling.
Wherein, the sintering procedure is as follows:
First burning section: 850 DEG C are first warming up to, then constant temperature 0.8h；
Second burning section: 1000 DEG C are warming up to from 850 DEG C, then constant temperature 0.5h；
Third burning section: being warming up to 1150 DEG C from 1000 DEG C, then constant temperature 1.5h, and last natural cooling obtains high white pottery
The method of ceramic products.
Reference examples 1
Difference with embodiment 4 is that clear frit does not contain magnesite and modified zeolite powder.
Examples 1 to 4, the resulting high white pottery ceramic products thoroughly of reference examples 1 are detected, in which:
Whiteness is measured using " QBT 1503-2011 domestic ceramics measuring brightness method "；
Glossiness, thermal shock resistance, lead chromium the amount of dissolution are measured using " GBT 3532-2009 domestic porcelain "；
It splits test method using the anti-glaze of GB/T 34252-2017 domestic ceramics device and furnace transmutation glaze ceramic under glaze is detected and resist
Crack detection；
Its testing result such as the following table 1:
Table 1: the testing result of Examples 1 to 4 and the resulting high white pottery ceramic products thoroughly of reference examples 1
As can be known from Table 1, white pottery ceramic products, whiteness reach 95 ° to height made from Examples 1 to 4 thoroughly, and glossiness reaches
95, it is higher than the whiteness without containing modified zeolite powder and the reference examples 1 of magnesite, and anti-crack testing result is that 7 circulations do not go out
Existing crackle, and lead release, chromium the amount of dissolution are met the requirements of the standard,
It should be understood by those skilled in the art that the present invention is not limited to the above embodiments, above-described embodiment and explanation
It is merely illustrated the principles of the invention described in book, without departing from the spirit and scope of the present invention, the present invention also has
Various changes and modifications, these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention
It is defined by the appending claims and its equivalent thereof.
Claims (5)
1. clear frit, which is characterized in that including the following component according to mass fraction meter: 8 ~ 10 parts of kaolin, aluminium oxide 7 ~ 11
Part, 3 ~ 6 parts of dolomite, 10 ~ 13 parts of pyrophillite, 11 ~ 15 parts of magnesite, 11 ~ 15 parts of cerium oxide, 13 ~ 14 parts of yttrium oxide, terbium oxide
It is 8 ~ 9 parts, 16 ~ 18 parts of zirconium oxide, 4 ~ 8 parts of solid, 6 ~ 8 parts of clay, 11 ~ 13 parts of modified zeolite powder, 13 ~ 15 parts of strontium carbonate, sub-
1 ~ 5 part of sodium phosphate, 4 ~ 6 parts of dispersing agent.
2. clear frit described in claim, which is characterized in that the solid is terpene resin, and the clay is bentonite,
The dispersing agent is lignin.
3. the method for the high white pottery ceramic products thoroughly of the preparation of the clear frit described in claim 1, which comprises the steps of:
Step 1: broken remove iron:
According to the mass fraction, by the kaolin, aluminium oxide, dolomite, pyrophillite, magnesite, cerium oxide, yttrium oxide,
Terbium oxide, zirconium oxide, clay and strontium carbonate are crushed respectively, and carry out handling except iron respectively, are then mixed the above components evenly,
Obtain pre-feed；
Step 2: preparing modified zeolite powder:
Zeolite powder is modified processing, obtains modified zeolite powder；
Step 3: mixing:
According to the mass fraction, successively by pre-feed obtained by the solid, sodium phosphite, dispersing agent, step 1 and step
Two gained modified zeolite powders are uniformly mixed, and obtain mixture；
Step 4: preparing glaze:
The concentration of three gained mixture of regulating step obtains marzacotto to 43 ~ 46 Baume degrees；
Step 5: glazing:
By marzacotto glazing obtained by step 4 to ceramic body outer surface, glazed ceramics green body is obtained；
Step 6: firing:
Glazed ceramics green body obtained by step 5 is fired, obtains high white pottery ceramic products after cooling.
4. the method for the high white pottery ceramic products thoroughly of clear frit preparation according to claim 3, which is characterized in that change described in step 2
Property processing detailed process it is as follows: according to the mass fraction, first by zeolite powder put into container in, then by 6 ~ 8ml/L chlorination
Ammonium is placed in container, and is stirred and boiled 10 ~ 15min, and modified zeolite powder is obtained after filtering.
5. the method for the high white pottery ceramic products thoroughly of clear frit preparation according to claim 3, which is characterized in that burnt described in step 6
Process processed is as follows:
First burning section: 700 ~ 850 DEG C are first warming up to, then 0.8 ~ 1.3h of constant temperature；
Second burning section: 900 ~ 1000 DEG C are warming up to from 700 ~ 850 DEG C, then 0.5 ~ 1h of constant temperature；
Third burning section: being warming up to 1100 ~ 1150 DEG C from 900 ~ 1000 DEG C, then 1.5 ~ 2h of constant temperature, and last natural cooling obtains high
The method of saturating white pottery ceramic products.
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| CN113087393A (en) * | 2021-03-30 | 2021-07-09 | 福建省德化县宏泉工艺品有限公司 | Copper red kiln transformation glazed porcelain |
| CN114956565A (en) * | 2022-07-08 | 2022-08-30 | 福建省德化万达陶瓷有限公司 | Transparent glaze and preparation method of domestic ceramic product |
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| CN113087393A (en) * | 2021-03-30 | 2021-07-09 | 福建省德化县宏泉工艺品有限公司 | Copper red kiln transformation glazed porcelain |
| CN113087393B (en) * | 2021-03-30 | 2023-05-19 | 福建省德化县宏泉工艺品有限公司 | Copper red kiln change glaze porcelain ware |
| CN114956565A (en) * | 2022-07-08 | 2022-08-30 | 福建省德化万达陶瓷有限公司 | Transparent glaze and preparation method of domestic ceramic product |
| CN114956565B (en) * | 2022-07-08 | 2023-10-20 | 福建省德化万达陶瓷有限公司 | Transparent glaze and preparation method of daily ceramic product |
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