CN110330229A - A kind of ground coat enamel being rapidly fired to suitable for glazed tile, glazed tile and preparation method thereof - Google Patents
A kind of ground coat enamel being rapidly fired to suitable for glazed tile, glazed tile and preparation method thereof Download PDFInfo
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- CN110330229A CN110330229A CN201910445824.2A CN201910445824A CN110330229A CN 110330229 A CN110330229 A CN 110330229A CN 201910445824 A CN201910445824 A CN 201910445824A CN 110330229 A CN110330229 A CN 110330229A
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- ground coat
- coat enamel
- glazed tile
- glaze
- overglaze
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Finishing Walls (AREA)
Abstract
The present invention provides a kind of ground coat enamels being rapidly fired to suitable for glazed tile, including ground coat enamel material, the ground coat enamel material includes following component by mass percentage: potassium feldspar 27~35%, albite 8~14% burns talcum 1~4%, medium temperature frit 2.5~4.8%, high expansion frit 0.5~2.2%, quartz 20~35%, kaolin 10~14%, calcined alumina 7~15%.In addition, the present invention also provides the glazed tiles comprising the ground coat enamel.The dosage of quartz and calcined alumina is used while promoted in the formula design of the invention ground coat enamel, first promote the hair color effect and firing temperature of formula, then again using the method for dosing medium temperature frit, realize the target of formula cooling, to which the firing range of glazed tile can not only be widened, meet the requirement burnt fastly, and there is preferable hair color effect.
Description
Technical field
The invention belongs to ceramic technology fields, and in particular to a kind of ground coat enamel being rapidly fired to suitable for glazed tile, glazed tile
And preparation method thereof.
Background technique
Full glaze product of throwing is one of the main product in architectural pottery, pattern, rich in color, due to glaze colour image
Between overglaze in layer of transparent, pattern will not occur because of the growth of time in use and color subtracts light phenomenon,
Therefore deep to be pursued by consumer.
Currently, glazed tile exists in process of production, body and glaze associativity is bad, firing range is narrow, requires strictly firing
Problem.For this problem, existing method of adjustment is generally by the method for reducing calcined oxide aluminium content, improving quartz content
To solve；But this solution makes the firing range of glazed tile narrow, unstable product quality；And if improving and forging
The content burnt alumina content, reduce quartz, the firing range of formula can become larger, but product color development is not fine.
Therefore, it is necessary to design one kind to widen firing range, meet the requirement burnt fastly, and there is preferable hair color effect
Glazed tile.
Summary of the invention
The purpose of the present invention is overcoming existing glazed tile to exist in process of production, body and glaze associativity is bad, firing range
It is narrow, stringent problem is required to firing.
For this purpose, the present invention provides a kind of ground coat enamel being rapidly fired to suitable for glazed tile, including ground coat enamel material, the ground coat enamel material
Including following component by mass percentage: potassium feldspar 27~35%, albite 8~14% burn talcum 1~4%, medium temperature frit
2.5~4.8%, high expansion frit 0.5~2.2%, quartz 20~35%, kaolin 10~14%, calcined alumina 7~15%.
Further, the ground coat enamel material includes following component by mass percentage: potassium feldspar 32%, albite 14%,
Burn talcum 2.5%, medium temperature frit 3.9%, high expansion frit 1.1%, quartz 25%, kaolin 12%, calcined alumina 9.5%.
Further, SiO by mass percentage in the medium temperature frit2Content is 60~75%, Al2O3Content be 2~
10%。
Further, above-mentioned ground coat enamel further includes auxiliary material, each component and its accounts for ground coat enamel material mass percentage in the auxiliary material
It is as follows: zirconium silicate 5~15%, sodium carboxymethylcellulose 0.1~0.25%, sodium tripolyphosphate 0.25~0.5%.
In addition, the present invention also provides a kind of glazed tile, including idiosome, overglaze and above-mentioned ground coat enamel.
Further, the overglaze includes glaze material and overglaze auxiliary material, and the glaze material includes by mass percentage
Following component: potassium feldspar 15~20%, albite 13~18%, dolomite 3~8%, wollastonite 5~8% burn talcum 1~3%, carbonic acid
Barium 3~10%, calcining zinc oxide 2~6%, water-washed kaoline 5~12%, quartz 1~5%, calcined alumina 2~4%, high temperature dumb light
Frit 26~32%；The overglaze auxiliary material includes sodium carboxymethylcellulose and sodium tripolyphosphate, the carboxymethylcellulosodium sodium content
The 0.1~0.15% of glaze material quality is accounted for, the tripolyphosphate sodium content accounts for the 0.25~0.4% of glaze material quality.
Further, calcium oxide mass percent 4~8% in the glaze material, barium monoxide mass percent 3~5%, oxidation
Magnesium mass percent 1.5~2.5%.
The present invention also provides the preparation methods of above-mentioned glazed tile, firstly, by idiosome shaping and drying, to drying after green body
Surface applies ground coat enamel, applies overglaze to the surface for applying ground coat enamel again after dry, enters roller kilns after dry, firing temperature 1000~
It is burnt into 20~35min at 1240 DEG C, obtains glazed tile.
Compared with prior art, beneficial effects of the present invention:
(1) dosage of quartz and calcined alumina is used while promoted in the formula design of this ground coat enamel provided by the invention, first
The hair color effect and firing temperature of formula are promoted, the target of formula cooling is then realized using the method for dosing medium temperature frit again,
To which the firing range of glazed tile can not only be widened, meet the requirement burnt fastly, and there is preferable hair color effect.
(2) in glazed tile provided by the invention design ground coat enamel formula simultaneously by adjusting calcium oxide in overglaze, barium monoxide,
The ratio of magnesia, not only solve glazed tile in process of production be easy needle outlet, fusion hole the defects of the problem of, and promoted
It is the saturating sense of product, clear patterns, well arranged, simultaneously because the presence of calcium oxide, magnesia composition helps to widen overglaze
Firing range and hardness of glaze surface.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel all other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment 1:
A kind of ground coat enamel being rapidly fired to suitable for glazed tile, including ground coat enamel material are present embodiments provided, the ground coat enamel material includes pressing
The following component of mass percent meter: potassium feldspar 32%, albite 14% burn talcum 2.5%, medium temperature frit 3.9%, high expansion frit
1.1%, quartz 25%, kaolin 12%, calcined alumina 9.5%.Wherein, SiO by mass percentage in medium temperature frit2Content is
60~75%, Al2O3Content is 2~10%.
Further, auxiliary material can be added in above-mentioned ground coat enamel also to improve the performance of glaze slip, the auxiliary material include zirconium silicate,
Sodium carboxymethylcellulose and sodium tripolyphosphate, wherein the additive amount of zirconium silicate is the 10% of above-mentioned ground coat enamel material quality, for improving
The whiteness of ground coat enamel, the additive amount of sodium carboxymethylcellulose are the 0.13% of above-mentioned ground coat enamel material quality, for adjust glaze slip viscosity and
Performance, the additive amount of sodium tripolyphosphate is the 0.35% of above-mentioned ground coat enamel material quality, for adjusting the slurry suspension of glaze slip.
Can be rapidly fired to glazed tile using above-mentioned ground coat enamel, detailed process is as follows: firstly, extrusion forming idiosome, to idiosome into
Row drying；Then, the water of the additional ground coat enamel material quality 35% of above-mentioned ground coat enamel is mixed and made into glaze slip, the glaze slip of the ground coat enamel is applied to
The ground coat enamel on idiosome surface is dried in idiosome surface；Apply a level glaze on dry ground coat enamel surface again, to the cover coat into
Row drying；Finally, idiosome after the drying, which is entered roller kilns, carries out high-temperature calcination, firing temperature is 1100 DEG C, and firing time is
30min, up to glazed tile after polishing treatment.Wherein, the molding of idiosome, ground coat enamel, the application of overglaze and drying belong to existing skill
Art, details are not described herein again.
Optimization, the overglaze includes glaze material and overglaze auxiliary material, and glaze material includes by mass percentage such as the following group
Point: potassium feldspar 17%, albite 16%, dolomite 5%, wollastonite 6% burn talcum 2%, barium carbonate 5%, calcining zinc oxide 4%, washing
Kaolin 6%, quartz 4%, calcined alumina 3%, high temperature Matt frit 32%.The overglaze auxiliary material include sodium carboxymethylcellulose and
Sodium tripolyphosphate, the carboxymethylcellulosodium sodium content account for the 0.12% of glaze material quality, and the tripolyphosphate sodium content accounts for overglaze
Expect the 0.35% of quality.Wherein, calcium oxide mass percent is 6% in the glaze material, barium monoxide mass percent 4%, magnesia
Mass percent 2%.The water of the additional glaze material quality 35% of the overglaze is mixed and made into glaze slip, is applied on ground glaze layer.Due to existing
Overglaze be high potassium, high sodium system, this glaze sintering process high temperature viscosity is bigger than normal, beginning fusing point is low, cause gas not have
Drained within a limited period of time, overglaze begins to melt, and the glaze planar defect such as pin hole, fusion hole occurs, in the present embodiment overglaze chemistry at
The ratio of calcium oxide, barium monoxide, magnesia in point solves the defects of glazed tile is easy needle outlet, fusion hole in process of production
The problem of, and the saturating sense of product, clear patterns, well arranged is improved, simultaneously because the presence of calcium oxide, magnesia composition
Help to widen the firing range and hardness of glaze surface of overglaze.
Embodiment 2:
A kind of ground coat enamel being rapidly fired to suitable for glazed tile, including ground coat enamel material are present embodiments provided, the ground coat enamel material includes pressing
The following component of mass percent meter: potassium feldspar 27%, albite 14% burn talcum 4%, medium temperature frit 2.5%, high expansion frit
0.5%, quartz 35%, kaolin 10%, calcined alumina 7%.
Further, auxiliary material can be added in above-mentioned ground coat enamel also to improve the performance of glaze slip, the auxiliary material include zirconium silicate,
Sodium carboxymethylcellulose and sodium tripolyphosphate, wherein the additive amount of zirconium silicate is the 5% of above-mentioned ground coat enamel material quality, for improving bottom
The whiteness of glaze, the additive amount of sodium carboxymethylcellulose is the 0.25% of above-mentioned ground coat enamel material quality, for adjusting the viscosity and property of glaze slip
Can, the additive amount of sodium tripolyphosphate is the 0.5% of above-mentioned ground coat enamel material quality, for adjusting the slurry suspension of glaze slip.
Can be rapidly fired to glazed tile using above-mentioned ground coat enamel, detailed process is as follows: firstly, extrusion forming idiosome, to idiosome into
Row drying；Then, the water of the additional ground coat enamel material quality 35% of above-mentioned ground coat enamel is mixed and made into glaze slip, the glaze slip of the ground coat enamel is applied to
The ground coat enamel on idiosome surface is dried in idiosome surface；Apply a level glaze on dry ground coat enamel surface again, to the cover coat into
Row drying；Finally, idiosome after the drying, which is entered roller kilns, carries out high-temperature calcination, firing temperature is 1000 DEG C, and firing time is
35min, up to glazed tile after polishing treatment.Wherein, the molding of idiosome, ground coat enamel, the application of overglaze and drying belong to existing skill
Art, details are not described herein again.
Wherein, the overglaze includes glaze material and overglaze auxiliary material, and glaze material includes following component by mass percentage:
Potassium feldspar 15%, albite 18%, dolomite 3%, wollastonite 8% burn talcum 1%, barium carbonate 10%, calcining zinc oxide 2%, washing height
Ridge soil 12%, quartz 1%, calcined alumina 4%, high temperature Matt frit 26%.The overglaze auxiliary material include sodium carboxymethylcellulose and
Sodium tripolyphosphate, the carboxymethylcellulosodium sodium content account for the 0.1% of glaze material quality, and the tripolyphosphate sodium content accounts for overglaze
Expect the 0.25% of quality.The water of the additional glaze material quality 35% of the overglaze is mixed and made into glaze slip, is applied on ground glaze layer.
Embodiment 3:
A kind of ground coat enamel being rapidly fired to suitable for glazed tile, including ground coat enamel material are present embodiments provided, the ground coat enamel material includes pressing
The following component of mass percent meter: potassium feldspar 35%, albite 8% burn talcum 1%, medium temperature frit 4.8%, high expansion frit
2.2%, quartz 20%, kaolin 14%, calcined alumina 15%.
Further, auxiliary material can be added in above-mentioned ground coat enamel also to improve the performance of glaze slip, the auxiliary material include zirconium silicate,
Sodium carboxymethylcellulose and sodium tripolyphosphate, wherein the additive amount of zirconium silicate is the 15% of above-mentioned ground coat enamel material quality, for improving
The whiteness of ground coat enamel, the additive amount of sodium carboxymethylcellulose are the 0.1% of above-mentioned ground coat enamel material quality, for adjust glaze slip viscosity and
Performance, the additive amount of sodium tripolyphosphate is the 0.25% of above-mentioned ground coat enamel material quality, for adjusting the slurry suspension of glaze slip.
Can be rapidly fired to glazed tile using above-mentioned ground coat enamel, detailed process is as follows: firstly, extrusion forming idiosome, to idiosome into
Row drying；Then, the water of the additional ground coat enamel material quality 35% of above-mentioned ground coat enamel is mixed and made into glaze slip, the glaze slip of the ground coat enamel is applied to
The ground coat enamel on idiosome surface is dried in idiosome surface；Apply a level glaze on dry ground coat enamel surface again, to the cover coat into
Row drying；Finally, idiosome after the drying, which is entered roller kilns, carries out high-temperature calcination, firing temperature is 1240 DEG C, and firing time is
20min, up to glazed tile after polishing treatment.Wherein, the molding of idiosome, ground coat enamel, the application of overglaze and drying belong to existing skill
Art, details are not described herein again.
Wherein, the overglaze includes glaze material and overglaze auxiliary material, and glaze material includes following component by mass percentage:
Potassium feldspar 20%, albite 13%, dolomite 8%, wollastonite 5% burn talcum 3%, barium carbonate 3%, and calcining zinc oxide 6% washes kaolinite
Soil 5%, quartz 5%, calcined alumina 2%, high temperature Matt frit 30%.The overglaze auxiliary material includes sodium carboxymethylcellulose and trimerization
Sodium phosphate, the carboxymethylcellulosodium sodium content account for the 0.15% of glaze material quality, and the tripolyphosphate sodium content accounts for glaze material matter
The 0.4% of amount.The water of the additional glaze material quality 35% of the overglaze is mixed and made into glaze slip, is applied on ground glaze layer.
The foregoing examples are only illustrative of the present invention, does not constitute the limitation to protection scope of the present invention, all
It is within being all belonged to the scope of protection of the present invention with the same or similar design of the present invention.
Claims (8)
1. a kind of ground coat enamel being rapidly fired to suitable for glazed tile, which is characterized in that including ground coat enamel material, the ground coat enamel material includes pressing matter
The following component of amount percentages: potassium feldspar 27~35%, albite 8~14%, burning talcum 1~4%, medium temperature frit 2.5~
4.8%, high expansion frit 0.5~2.2%, quartz 20~35%, kaolin 10~14%, calcined alumina 7~15%.
2. the ground coat enamel being rapidly fired to as described in claim 1 suitable for glazed tile, which is characterized in that the ground coat enamel material includes pressing
The following component of mass percent meter: potassium feldspar 32%, albite 14% burn talcum 2.5%, medium temperature frit 3.9%, high expansion frit
1.1%, quartz 25%, kaolin 12%, calcined alumina 9.5%.
3. the ground coat enamel being rapidly fired to as described in claim 1 suitable for glazed tile, it is characterised in that: pressed in the medium temperature frit
Mass percent meter SiO2Content is 60~75%, Al2O3Content is 2~10%.
4. the ground coat enamel being rapidly fired to as described in claim 1 suitable for glazed tile, which is characterized in that it further include auxiliary material, it is described
Each component and its to account for ground coat enamel material mass percentage as follows: zirconium silicate 5~15% in auxiliary material, sodium carboxymethylcellulose 0.1~
0.25%, sodium tripolyphosphate 0.25~0.5%.
5. a kind of glazed tile, it is characterised in that: including idiosome, overglaze, and such as described in any item ground coat enamels of Claims 1 to 4.
6. glazed tile as claimed in claim 5, which is characterized in that the overglaze includes glaze material and overglaze auxiliary material, the face
Glaze includes following component by mass percentage: potassium feldspar 15~20%, albite 13~18%, dolomite 3~8%, silicon ash
Stone 5~8%, burning talcum 1~3%, barium carbonate 3~10%, calcining zinc oxide 2~6%, water-washed kaoline 5~12%, quartz 1~5%,
Calcined alumina 2~4%, high temperature Matt frit 26~32%；The overglaze auxiliary material includes sodium carboxymethylcellulose and tripolyphosphate
Sodium, the carboxymethylcellulosodium sodium content account for the 0.1~0.15% of glaze material quality, and the tripolyphosphate sodium content accounts for glaze material
The 0.25~0.4% of quality.
7. glazed tile as claimed in claim 6, which is characterized in that calcium oxide mass percent 4~8%, oxygen in the glaze material
Change barium mass percent 3~5%, magnesia mass percent 1.5~2.5%.
8. such as the preparation method of the described in any item glazed tiles of claim 5~7, which is characterized in that firstly, idiosome is formed dry
It is dry, to drying after the surface of green body apply ground coat enamel, apply overglaze to the surface for applying ground coat enamel again after dry, enter roller-way after dry
Kiln is burnt into 20~35min at 1000~1240 DEG C of firing temperature, obtains glazed tile.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910445824.2A CN110330229A (en) | 2019-05-27 | 2019-05-27 | A kind of ground coat enamel being rapidly fired to suitable for glazed tile, glazed tile and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910445824.2A CN110330229A (en) | 2019-05-27 | 2019-05-27 | A kind of ground coat enamel being rapidly fired to suitable for glazed tile, glazed tile and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111792949A (en) * | 2020-07-08 | 2020-10-20 | 佛山市东鹏陶瓷有限公司 | Ceramic glazed tile and preparation method thereof |
| CN112110750A (en) * | 2020-08-03 | 2020-12-22 | 湖北杭瑞陶瓷有限责任公司 | Super-white polished porcelain marble and preparation method thereof |
| CN112266171A (en) * | 2020-11-02 | 2021-01-26 | 广东百强陶瓷有限公司 | Marble ceramic tile glaze capable of meeting rapid firing of wide roller kiln |
| CN114349522A (en) * | 2021-12-23 | 2022-04-15 | 贵州贵安新区百隆陶业有限公司 | Formula and production process of medium and high aluminum brick |
| CN115504671A (en) * | 2022-10-12 | 2022-12-23 | 佛山市东鹏陶瓷有限公司 | High-temperature wear-resistant transparent glaze as well as preparation method and application thereof |
| CN116375505A (en) * | 2023-04-14 | 2023-07-04 | 佛山市陶莹新型材料有限公司 | Luminous ceramic material and preparation method thereof |
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