CN110035999B - 羟甲基糠醛制备方法 - Google Patents

羟甲基糠醛制备方法

Info

Publication number
CN110035999B
CN110035999B CN201780074758.1A CN201780074758A CN110035999B CN 110035999 B CN110035999 B CN 110035999B CN 201780074758 A CN201780074758 A CN 201780074758A CN 110035999 B CN110035999 B CN 110035999B
Authority
CN
China
Prior art keywords
fructose
fraction
acid
hmf
product mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201780074758.1A
Other languages
English (en)
Chinese (zh)
Other versions
CN110035999A (zh
Inventor
马克瓦德·金茨
阿里-礼萨·哈吉·贝格力
C·克勒内
沃尔夫冈·瓦赫
A-M·格拉夫
W·克劳斯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suedzucker AG
Original Assignee
Suedzucker AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suedzucker AG filed Critical Suedzucker AG
Publication of CN110035999A publication Critical patent/CN110035999A/zh
Application granted granted Critical
Publication of CN110035999B publication Critical patent/CN110035999B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)
  • Saccharide Compounds (AREA)
CN201780074758.1A 2016-12-02 2017-12-01 羟甲基糠醛制备方法 Active CN110035999B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102016224073.0A DE102016224073A1 (de) 2016-12-02 2016-12-02 Verbessertes HMF-Herstellungsverfahren
DE102016224073.0 2016-12-02
PCT/EP2017/081236 WO2018100184A1 (de) 2016-12-02 2017-12-01 Hmf-herstellungsverfahren

Publications (2)

Publication Number Publication Date
CN110035999A CN110035999A (zh) 2019-07-19
CN110035999B true CN110035999B (zh) 2025-08-26

Family

ID=60569921

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201780074758.1A Active CN110035999B (zh) 2016-12-02 2017-12-01 羟甲基糠醛制备方法

Country Status (13)

Country Link
US (1) US10662167B2 (https=)
EP (1) EP3548473B1 (https=)
JP (1) JP7042272B2 (https=)
CN (1) CN110035999B (https=)
AU (1) AU2017367187B2 (https=)
BR (1) BR112019011367B1 (https=)
DE (1) DE102016224073A1 (https=)
DK (1) DK3548473T3 (https=)
EA (1) EA037637B1 (https=)
ES (1) ES2852006T3 (https=)
HU (1) HUE053818T2 (https=)
PL (1) PL3548473T3 (https=)
WO (1) WO2018100184A1 (https=)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3402787A4 (en) 2016-01-13 2019-11-27 Stora Enso Oyj PROCESS FOR THE PREPARATION OF 2,5-FURANDIC ACETIC ACID AND INTERMEDIATES AND DERIVATIVES THEREOF
EP3652161A1 (en) 2017-07-12 2020-05-20 Stora Enso Oyj Purified 2,5-furandicarboxylic acid pathway products
FR3076554B1 (fr) * 2018-01-10 2020-09-18 Ifp Energies Now Procede de production de 5-hydroxymethylfurfural
DE102018208510A1 (de) * 2018-05-29 2019-12-05 Südzucker AG Salz- und Säuregemisch-katalysierte HMF-Herstellung
CN113929571A (zh) * 2021-11-23 2022-01-14 常州大学 一种分离纯化乙酰丙酸的方法
CN117756756A (zh) * 2022-09-16 2024-03-26 中科国生(杭州)科技有限公司 一种基于能源植物菊芋制备5-羟甲基糠醛的方法
FR3143605A1 (fr) * 2022-12-14 2024-06-21 IFP Energies Nouvelles Procédé de production de 5-HMF par conversion d’un sirop dans un solvant non aqueux avec extraction de l'eau du sirop en amont de la synthèse
WO2025043536A1 (zh) * 2023-08-30 2025-03-06 乔璞科技股份有限公司 5-羟甲基糠醛的纯化方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104053649A (zh) * 2012-01-10 2014-09-17 阿彻丹尼尔斯米德兰德公司 从糖类制备hmf和hmf衍生物同时回收适合于直接发酵为乙醇的未反应糖类的方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3601281A1 (de) * 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
US7317116B2 (en) * 2004-12-10 2008-01-08 Archer-Daniels-Midland-Company Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives
DE102004063006A1 (de) 2004-12-22 2006-07-13 Basf Ag Verfahren zur Isolierung von Coenzym Q10
CN101456851B (zh) * 2007-12-12 2012-10-24 中国科学院大连化学物理研究所 一种微波促进制备5-羟甲基糠醛的方法
CN104169263B (zh) * 2011-12-13 2016-06-15 巴斯夫欧洲公司 在蒸汽存在下由己糖溶液制备5-羟甲基糠醛(hmf)
CN103113328A (zh) * 2013-01-12 2013-05-22 塔里木大学 一种以超声催化制备5-羟甲基糠醛的方法
EA201691459A1 (ru) * 2014-01-27 2016-12-30 Ренновия Инк. Преобразование фруктозосодержащего исходного сырья в hmf-содержащий продукт

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104053649A (zh) * 2012-01-10 2014-09-17 阿彻丹尼尔斯米德兰德公司 从糖类制备hmf和hmf衍生物同时回收适合于直接发酵为乙醇的未反应糖类的方法

Also Published As

Publication number Publication date
JP2020511405A (ja) 2020-04-16
AU2017367187A1 (en) 2019-06-20
CA3045541A1 (en) 2018-06-07
DK3548473T3 (da) 2021-02-01
EA201991342A1 (ru) 2019-10-31
US20200002300A1 (en) 2020-01-02
EP3548473A1 (de) 2019-10-09
US10662167B2 (en) 2020-05-26
BR112019011367B1 (pt) 2022-12-27
AU2017367187B2 (en) 2021-02-25
EA037637B1 (ru) 2021-04-23
PL3548473T3 (pl) 2021-05-31
WO2018100184A1 (de) 2018-06-07
EP3548473B1 (de) 2020-11-18
ES2852006T3 (es) 2021-09-10
CN110035999A (zh) 2019-07-19
HUE053818T2 (hu) 2021-07-28
DE102016224073A1 (de) 2018-06-07
BR112019011367A2 (pt) 2019-10-15
JP7042272B2 (ja) 2022-03-25

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