DE102016224073A1 - Verbessertes HMF-Herstellungsverfahren - Google Patents

Verbessertes HMF-Herstellungsverfahren Download PDF

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Publication number
DE102016224073A1
DE102016224073A1 DE102016224073.0A DE102016224073A DE102016224073A1 DE 102016224073 A1 DE102016224073 A1 DE 102016224073A1 DE 102016224073 A DE102016224073 A DE 102016224073A DE 102016224073 A1 DE102016224073 A1 DE 102016224073A1
Authority
DE
Germany
Prior art keywords
fructose
hmf
fraction
acid
chromatography
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE102016224073.0A
Other languages
German (de)
English (en)
Inventor
Markwart Kunz
Alireza Haji Begli
Christine Kröner
Wolfgang Wach
Alain-Michel Graf
Wolfgang Kraus
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suedzucker AG
Original Assignee
Suedzucker AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suedzucker AG filed Critical Suedzucker AG
Priority to DE102016224073.0A priority Critical patent/DE102016224073A1/de
Priority to PL17808461T priority patent/PL3548473T3/pl
Priority to US16/465,205 priority patent/US10662167B2/en
Priority to ES17808461T priority patent/ES2852006T3/es
Priority to AU2017367187A priority patent/AU2017367187B2/en
Priority to EA201991342A priority patent/EA037637B1/ru
Priority to HUE17808461A priority patent/HUE053818T2/hu
Priority to CN201780074758.1A priority patent/CN110035999B/zh
Priority to BR112019011367-3A priority patent/BR112019011367B1/pt
Priority to DK17808461.2T priority patent/DK3548473T3/da
Priority to CA3045541A priority patent/CA3045541C/en
Priority to EP17808461.2A priority patent/EP3548473B1/de
Priority to PCT/EP2017/081236 priority patent/WO2018100184A1/de
Priority to JP2019529185A priority patent/JP7042272B2/ja
Publication of DE102016224073A1 publication Critical patent/DE102016224073A1/de
Ceased legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)
  • Saccharide Compounds (AREA)
DE102016224073.0A 2016-12-02 2016-12-02 Verbessertes HMF-Herstellungsverfahren Ceased DE102016224073A1 (de)

Priority Applications (14)

Application Number Priority Date Filing Date Title
DE102016224073.0A DE102016224073A1 (de) 2016-12-02 2016-12-02 Verbessertes HMF-Herstellungsverfahren
PL17808461T PL3548473T3 (pl) 2016-12-02 2017-12-01 Sposób wytwarzania hmf
US16/465,205 US10662167B2 (en) 2016-12-02 2017-12-01 HMF production method
ES17808461T ES2852006T3 (es) 2016-12-02 2017-12-01 Procedimiento de preparación de HMF
AU2017367187A AU2017367187B2 (en) 2016-12-02 2017-12-01 HMF production method
EA201991342A EA037637B1 (ru) 2016-12-02 2017-12-01 Способ получения hmf
HUE17808461A HUE053818T2 (hu) 2016-12-02 2017-12-01 Eljárás HMF elõállítására
CN201780074758.1A CN110035999B (zh) 2016-12-02 2017-12-01 羟甲基糠醛制备方法
BR112019011367-3A BR112019011367B1 (pt) 2016-12-02 2017-12-01 Processo de produção de hmf
DK17808461.2T DK3548473T3 (da) 2016-12-02 2017-12-01 HMF-fremstillingsfremgangsmåde
CA3045541A CA3045541C (en) 2016-12-02 2017-12-01 Hmf production method
EP17808461.2A EP3548473B1 (de) 2016-12-02 2017-12-01 Hmf-herstellungsverfahren
PCT/EP2017/081236 WO2018100184A1 (de) 2016-12-02 2017-12-01 Hmf-herstellungsverfahren
JP2019529185A JP7042272B2 (ja) 2016-12-02 2017-12-01 Ｈｍｆ製造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102016224073.0A DE102016224073A1 (de) 2016-12-02 2016-12-02 Verbessertes HMF-Herstellungsverfahren

Publications (1)

Publication Number Publication Date
DE102016224073A1 true DE102016224073A1 (de) 2018-06-07

Family

ID=60569921

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102016224073.0A Ceased DE102016224073A1 (de) 2016-12-02 2016-12-02 Verbessertes HMF-Herstellungsverfahren

Country Status (13)

Country Link
US (1) US10662167B2 (https=)
EP (1) EP3548473B1 (https=)
JP (1) JP7042272B2 (https=)
CN (1) CN110035999B (https=)
AU (1) AU2017367187B2 (https=)
BR (1) BR112019011367B1 (https=)
DE (1) DE102016224073A1 (https=)
DK (1) DK3548473T3 (https=)
EA (1) EA037637B1 (https=)
ES (1) ES2852006T3 (https=)
HU (1) HUE053818T2 (https=)
PL (1) PL3548473T3 (https=)
WO (1) WO2018100184A1 (https=)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3402787A4 (en) 2016-01-13 2019-11-27 Stora Enso Oyj PROCESS FOR THE PREPARATION OF 2,5-FURANDIC ACETIC ACID AND INTERMEDIATES AND DERIVATIVES THEREOF
EP3652161A1 (en) 2017-07-12 2020-05-20 Stora Enso Oyj Purified 2,5-furandicarboxylic acid pathway products
FR3076554B1 (fr) * 2018-01-10 2020-09-18 Ifp Energies Now Procede de production de 5-hydroxymethylfurfural
DE102018208510A1 (de) * 2018-05-29 2019-12-05 Südzucker AG Salz- und Säuregemisch-katalysierte HMF-Herstellung
CN113929571A (zh) * 2021-11-23 2022-01-14 常州大学 一种分离纯化乙酰丙酸的方法
CN117756756A (zh) * 2022-09-16 2024-03-26 中科国生(杭州)科技有限公司 一种基于能源植物菊芋制备5-羟甲基糠醛的方法
FR3143605A1 (fr) * 2022-12-14 2024-06-21 IFP Energies Nouvelles Procédé de production de 5-HMF par conversion d’un sirop dans un solvant non aqueux avec extraction de l'eau du sirop en amont de la synthèse
WO2025043536A1 (zh) * 2023-08-30 2025-03-06 乔璞科技股份有限公司 5-羟甲基糠醛的纯化方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3601281A1 (de) * 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
WO2013106136A1 (en) 2012-01-10 2013-07-18 Archer Daniels Midland Company Process for making hmf and hmf derivatives from sugars, with recovery of unreacted sugars suitable for direct fermentation to ethanol
US20150210661A1 (en) * 2014-01-27 2015-07-30 Rennovia, Inc. Conversion of fructose-containing feedstocks to hmf-containing product

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7317116B2 (en) * 2004-12-10 2008-01-08 Archer-Daniels-Midland-Company Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives
DE102004063006A1 (de) 2004-12-22 2006-07-13 Basf Ag Verfahren zur Isolierung von Coenzym Q10
CN101456851B (zh) * 2007-12-12 2012-10-24 中国科学院大连化学物理研究所 一种微波促进制备5-羟甲基糠醛的方法
CN104169263B (zh) * 2011-12-13 2016-06-15 巴斯夫欧洲公司 在蒸汽存在下由己糖溶液制备5-羟甲基糠醛(hmf)
CN103113328A (zh) * 2013-01-12 2013-05-22 塔里木大学 一种以超声催化制备5-羟甲基糠醛的方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3601281A1 (de) * 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
EP0230250B1 (de) 1986-01-17 1991-04-03 Südzucker Aktiengesellschaft Mannheim/Ochsenfurt Verfahren zur Herstellung von 5-Hydroxymethylfurfural einschliesslich eines kristallinen Produktes unter ausschliesslicher Verwendung von Wasser als Lösungsmittel
WO2013106136A1 (en) 2012-01-10 2013-07-18 Archer Daniels Midland Company Process for making hmf and hmf derivatives from sugars, with recovery of unreacted sugars suitable for direct fermentation to ethanol
US20140315262A1 (en) * 2012-01-10 2014-10-23 Archer Daniels Midland Company Process for making hmf and hmf derivatives from sugars, with recovery of unreacted sugars suitable for direct fermentation to ethanol
US20150210661A1 (en) * 2014-01-27 2015-07-30 Rennovia, Inc. Conversion of fructose-containing feedstocks to hmf-containing product
WO2015113060A2 (en) 2014-01-27 2015-07-30 Rennovia, Inc. Conversion of fructose-containing feedstocks to hmf-containing product

Also Published As

Publication number Publication date
JP2020511405A (ja) 2020-04-16
AU2017367187A1 (en) 2019-06-20
CA3045541A1 (en) 2018-06-07
DK3548473T3 (da) 2021-02-01
EA201991342A1 (ru) 2019-10-31
US20200002300A1 (en) 2020-01-02
EP3548473A1 (de) 2019-10-09
US10662167B2 (en) 2020-05-26
BR112019011367B1 (pt) 2022-12-27
AU2017367187B2 (en) 2021-02-25
EA037637B1 (ru) 2021-04-23
PL3548473T3 (pl) 2021-05-31
CN110035999B (zh) 2025-08-26
WO2018100184A1 (de) 2018-06-07
EP3548473B1 (de) 2020-11-18
ES2852006T3 (es) 2021-09-10
CN110035999A (zh) 2019-07-19
HUE053818T2 (hu) 2021-07-28
BR112019011367A2 (pt) 2019-10-15
JP7042272B2 (ja) 2022-03-25

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Representative=s name: GLEISS GROSSE SCHRELL UND PARTNER MBB PATENTAN, DE

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