CN110012913A - A kind of compound disinfectant and preparation method thereof - Google Patents
A kind of compound disinfectant and preparation method thereof Download PDFInfo
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- CN110012913A CN110012913A CN201810012954.2A CN201810012954A CN110012913A CN 110012913 A CN110012913 A CN 110012913A CN 201810012954 A CN201810012954 A CN 201810012954A CN 110012913 A CN110012913 A CN 110012913A
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- Prior art keywords
- compound disinfectant
- compound
- solution
- quaternary ammonium
- ammonium salt
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N55/00—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pest Control & Pesticides (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention provides a kind of compound disinfectant and preparation method thereof, it is characterized in that compound disinfectant of the present invention is made of the raw material that following mass concentration matches: compound disinfectant carrier chitosan quaternary ammonium salt: 0.001%~5% (w/w), plant extracts (such as radix scutellariae, aloe, honeysuckle, green tea) mixture: 0.001%~5% (w/w), complex enzyme: 0.001%~5% (w/w), edible salt (such as sodium chloride): 0.001%~1% (w/w), food-grade alkali (such as sodium bicarbonate): 0.001%~2% (w/w), it acts synergistically compound (such as organosilicon quaternary ammonium salt): 0.001%~5% (w/w), surplus is deionized water.Compound disinfectant simple production process of the present invention.It is characterized in that 1. compound disinfectant dosing apparatus of the present invention can be common nontoxic plastics reaction vessel (such as PV) or stainless steel metal container；2. compound disinfectant of the present invention prepares temperature and pressure is room temperature, normal pressure.
Description
Technical field
The present invention relates to a kind of compound disinfectants and preparation method thereof, and in particular to a kind of compound disinfecting formula of liquid and its preparation side
Method.
Background technique
Bacterium is widely present in daily life and articles for daily use, and bacterium is the pathogen of many diseases, including pulmonary tuberculosis,
The diseases such as stranguria syndrome, anthracnose, syphilis, the plague, sand holes are caused by bacterium, produce high risks to human health, because
This develops a kind of safe, potent, lasting, environmental-friendly and harmless, without secondary pollution potent antibacterial agent, to people's
Living environment improvement has great significance.
Current existing disinfectant, such as 84 thimerosals, hypochlorous acid class thimerosal, Disinfection Effect is good, and disinfection speed is fast, but
Available chlorine content is high, so that irritation taste is big；A kind of low molecular n-trimethyl chitosan chloride chelated iodine of patent ZL03112578.6
The preparation method of thimerosal, but which use iodine or iodates, however not excluded that the corrosivity of iodine and its compound in preparation process,
There is it to prepare limitation；Patent CN103041400B discloses a kind of chitosan/gamma-polyglutamic acid for loading antibacterial peptide and compound receives
The preparation method of rice corpuscles, but the patent is solid pharmaceutical preparation, and there is no widely develops to application field；Patent
ZL200710044076.4 eatable disinfection liquid, though raw materials used safety is good, main material neopelex
For oily liquid, and document shows there is micro- toxicity.Develop it is efficient, safe and environment-friendly, degradable and convenient for storage and it is used in everyday
Thimerosal is more advantageous to expansion application field.
Summary of the invention
The present invention provides one kind with chitosan quaternary ammonium salt and plant extract elite (such as radix scutellariae, aloe, honeysuckle, green tea)
Main material, under the proportion of optimization, compounding is multiple with the synergistic effect compound such as organosilicon quaternary ammonium salt with bactericidal bacteriostasis
It is made into the compound disinfectant of broad-spectrum antibacterial sterilization and Fang Mei ﹑ deodorization.
It is raw material that the purpose of the present invention 1, which is using nontoxic substance, develops that safety is good, taste is mildly non-stimulated
Property, efficiently, persistently, the high compound disinfectant of cost performance.
The purpose of the present invention 2 considers environmental protection, energy-efficient requirement on the basis of realizing bactericidal, invents
A kind of easy-to-use production technology.Simple production process of the present invention, compound disinfectant reaction temperature are normal pressure, room temperature (15 ~ 35
DEG C), production containers can be rustless steel container, or common plastic containers (such as PV), no particular/special requirement.
The purpose of the present invention 3 is to consider potent, long-acting, synergistic synergistic effect, the compound disinfectant being prepared into
Bactericidal bacteriostasis are strong, action time is lasting, to salmonella, Escherichia coli, golden yellow grape in experiment test 24 hours
Coccus has reached 99.99%.
To achieve the above object, the present invention is formed as follows using following raw material:
Chitosan quaternary ammonium salt: 0.001%~5% (w/w), plant (containing radix scutellariae, aloe, honeysuckle, tea) mixture: 0.001%
~5% (w/w), complex enzyme: 0.001%~5% (w/w), edible salt (such as sodium chloride): 0.001%~1% (w/w),
Dietary alkali (such as sodium bicarbonate): 0.001%~2% (w/w), Synergistic antimicrobial Fungicidal compounds such as organosilicon quaternary ammonium salt:
0.001%~5% (w/w), surplus are deionized water.
Compound disinfectant described in claims 1 is radix scutellariae, aloe, honeysuckle, teas plant extract mixtures.
Plant extracts used in compound disinfectant described in claims 1 is Baical Skullcap root P.E when being main, quality percentage
Content is 0.001%~5% (w/w).
Compound disinfectant plant extracts is aloe extract described in claims 1 when being main, mass percentage
For 0.001%~5% (w/w).
Plant extracts used in compound disinfectant described in claims 1 is Honegsukle flower P.E, mass percentage
For 0.001%~5% (w/w).
Plant extracts used in compound disinfectant described in claims 1 is tea extraction, and mass percentage is
0.001%~5% (w/w).
Plant extracts used in compound disinfectant described in claims 1 is that radix scutellariae, aloe, honeysuckle, tea extraction are mixed
When closing object, mass percentage is 0.001%~5% (w/w).
The enzymatic hydrolysis complex enzyme used of compound disinfectant described in claims 1, mass percentage is 0.001%~
1% (w/w).
Synergistic antimicrobial compound such as organosilicon quaternary ammonium salt used in compound disinfectant described in claims 1, quality percentage
Content is 0.001%~5% (w/w).
Edible salt used in compound disinfectant described in claims 1 (such as sodium chloride), mass percentage are
0.001%~2% (w/w).
Dietary alkali used in compound disinfectant described in claims 1 (such as sodium bicarbonate), mass percentage are
0.001%~2% (w/w).
The compound disinfecting liquid preparing process as described in claims 6 prepare claims, its step are as follows: room temperature or
(15 ~ 35) DEG C are sequentially added the Baical Skullcap root P.E, aloe extract, gold and silver weighed up by formula rate in No.1 plastic containers
After flower extract, tea extraction mixing, the deionized water of 5 times of weight ratios is added, be sufficiently stirred and liquid complex enzyme enzymatic hydrolysis 5 is added
By 8 hours, it is proportionally added into sodium chloride and is sufficiently stirred 10 minutes, be proportionally added into sodium bicarbonate aqueous solution and be sufficiently stirred,
As No.1 solution, that is, plant extracts extracting solution；Chitosan quaternary ammonium salt is weighed by formula rate in No. two plastic containers, while stirring
The deionized water that proper proportion is added in side is mixed, after completely dissolution；It is slowly added into synergistic effect antibacterial such as organosilicone quaternary ammonium salt water
Simultaneously 1 hour as No. two solution is sufficiently stirred in solution, and No.1 solution is compounded by 1:1 mixing into power with two kinds of solution of No. two solution
Compound disinfectant described in sharp claim 1 or 2.Preparation process is detailed in example 1 and 2.
Beneficial effects of the present invention.
Develop the mild sterilization bacteriostat of a kind of strong bacteriostasis, safe and efficient, persistent, property.
The compound disinfectant that the present invention develops divides the laboratory 10 of staphylococcus aureus, Escherichia coli, salmonella
Clock, 30 minutes, 4 hours, 10 hours, 24 hours tracking and testings show compound disinfectant of the present invention to Staphylococcus aureus
Bacterium, Escherichia coli, salmonella bactericidal and bacteriostatic effect are fast and lasting, are kept at sterilizing rate 99.99%.
The present invention is directed under energy-saving and environment-friendly theory, production equipment is simple, working condition is room temperature, normal pressure, without heating,
Pressurization.
The present invention is under the optimum proportioning of various components, to there is certain persistent sterilization bacteriostat.
Case is embodied.
Embodiment 1.
At room temperature (15 ~ 35) DEG C, two lidded container 10L rigid plastics reactors (PV material)；Number is No.1 reaction
Container, No. two reaction vessels.
The Baical Skullcap root P.E weighed up, aloe extract, Honegsukle flower P.E, tea extraction are sequentially added by formula rate
After mixing, the deionized water of 15 times of weight ratios is added, be sufficiently stirred and be added liquid complex enzyme digest 5 to 8 hours, in proportion plus
Enter sodium chloride and be sufficiently stirred 10 minutes, is proportionally added into sodium bicarbonate aqueous solution and is sufficiently stirred, deionized water sufficiently dissolves
It is extracted afterwards for No.1 solution, that is, plant extracts.
Chitosan quaternary ammonium salt is weighed by formula rate in No. two plastic containers, the deionization of proper proportion is added while stirring
Water is slowly added into the synergistic effect antibacterial such as organosilicon quaternary ammonium salt aqueous solution and abundant of recipe requirements proportion after completely dissolution
Stirring 1 hour is No. two solution.
No.1 solution is compounded by 1:1 mixing into compound described in claims 1 or 2 with two kinds of solution of No. two solution to disappear
Venom.Above-mentioned No.1 solution is compounded with No. two solution mixing, is discharged.
Embodiment 2.
At room temperature (15 ~ 35) DEG C, two lidded container 10L stainless steel reactors；Number be No.1 reaction vessel, No. two it is anti-
Answer container.
The Baical Skullcap root P.E weighed up, aloe extract, Honegsukle flower P.E, tea extraction are sequentially added by formula rate
After mixing, the deionized water of 15 times of weight ratios is added, be sufficiently stirred and be added liquid complex enzyme digest 5 to 8 hours, in proportion plus
Enter sodium chloride and be sufficiently stirred 10 minutes, is proportionally added into sodium bicarbonate aqueous solution and is sufficiently stirred, deionized water sufficiently dissolves
It is extracted afterwards for No.1 solution, that is, plant extracts.
Chitosan quaternary ammonium salt is weighed by formula rate in No. two plastic containers, the deionization of proper proportion is added while stirring
Water is slowly added into the synergistic effect antibacterial such as organosilicon quaternary ammonium salt aqueous solution and abundant of recipe requirements proportion after completely dissolution
Stirring 1 hour is No. two solution.
No.1 solution is compounded by 1:1 mixing into compound described in claims 1 or 2 with two kinds of solution of No. two solution to disappear
Venom.Above-mentioned No.1 solution is compounded with No. two solution mixing, is discharged.
Claims (6)
1. a kind of compound disinfectant and preparation method thereof, it is characterised in that: be made of the raw material that following mass concentration matches:
Chitosan quaternary ammonium salt: 0.001%~5% (w/w)
Radix scutellariae, aloe, honeysuckle, tea mixture: 0.001%~5% (w/w)
Complex enzyme: 0.001%~5% (w/w)
Edible salt (such as sodium chloride): 0.001%~1% (w/w)
Dietary alkali (such as sodium bicarbonate): 0.001%~2% (w/w)
Synergistic antimicrobial Fungicidal compounds such as organosilicon quaternary ammonium salt: 0.001%~5% (w/w)
Surplus is deionized water.
2. compound disinfectant as claimed in claim 1, it is characterized in that the botanical extract Scutellaria, aloe, honeysuckle,
Teas extraction mixture.
3. compound disinfectant as claimed in claim 1, it is characterized in that it is complex enzyme that the enzymatic hydrolysis is used.
4. compound disinfectant as claimed in claim 1, it is characterized in that the plant enzymolysis post-processing is sodium chloride with salt,
It is sodium bicarbonate that post-processing, which is digested, with alkali.
5. a kind of preparation process of compound disinfectant as claimed in claim 1, its step are as follows: weighing radix scutellariae by formula and mentions
It takes object, aloe extract, Honegsukle flower P.E, tea extraction, liquid complex enzyme, sodium chloride, sodium bicarbonate to mix and is dissolved in
After ionized water, as No.1 solution, that is, plant extracts extracting solution；Chitosan quaternary ammonium salt is weighed by formula, organosilicon quaternary ammonium salt is molten
In deionized water be No. two solution, No.1 solution and two kinds of solution of No. two solution mixed by 1:1 compound form claims 1 or
Compound disinfectant described in 2.
6. preparation process is detailed in example 1 and 2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810012954.2A CN110012913A (en) | 2018-01-06 | 2018-01-06 | A kind of compound disinfectant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810012954.2A CN110012913A (en) | 2018-01-06 | 2018-01-06 | A kind of compound disinfectant and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN110012913A true CN110012913A (en) | 2019-07-16 |
Family
ID=67187297
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810012954.2A Pending CN110012913A (en) | 2018-01-06 | 2018-01-06 | A kind of compound disinfectant and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110692634A (en) * | 2019-10-22 | 2020-01-17 | 河北首优医药科技有限公司 | Compound o-phthalaldehyde disinfectant and preparation process thereof |
| CN111280185A (en) * | 2020-03-24 | 2020-06-16 | 青海大学 | Anti-virus disinfectant and preparation method thereof |
| CN112262846A (en) * | 2020-11-13 | 2021-01-26 | 中国科学院武汉病毒研究所 | Object surface disinfectant for high-grade biosafety laboratory and preparation method thereof |
| CN113080207A (en) * | 2021-04-15 | 2021-07-09 | 宁波保税区华萌生物科技有限公司 | Process for preparing disinfectant |
| CN113712042A (en) * | 2021-05-24 | 2021-11-30 | 常州崇高纳米材料有限公司 | Multifunctional persistent antibacterial composition and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104904753A (en) * | 2015-07-01 | 2015-09-16 | 荆永正 | Efficient disinfectant and preparation method thereof |
-
2018
- 2018-01-06 CN CN201810012954.2A patent/CN110012913A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104904753A (en) * | 2015-07-01 | 2015-09-16 | 荆永正 | Efficient disinfectant and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110692634A (en) * | 2019-10-22 | 2020-01-17 | 河北首优医药科技有限公司 | Compound o-phthalaldehyde disinfectant and preparation process thereof |
| CN111280185A (en) * | 2020-03-24 | 2020-06-16 | 青海大学 | Anti-virus disinfectant and preparation method thereof |
| CN112262846A (en) * | 2020-11-13 | 2021-01-26 | 中国科学院武汉病毒研究所 | Object surface disinfectant for high-grade biosafety laboratory and preparation method thereof |
| CN113080207A (en) * | 2021-04-15 | 2021-07-09 | 宁波保税区华萌生物科技有限公司 | Process for preparing disinfectant |
| CN113712042A (en) * | 2021-05-24 | 2021-11-30 | 常州崇高纳米材料有限公司 | Multifunctional persistent antibacterial composition and preparation method thereof |
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Application publication date: 20190716 |