CN109793261A - A kind of preparation method and application of yellow sunflower extract for tobacco - Google Patents
A kind of preparation method and application of yellow sunflower extract for tobacco Download PDFInfo
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- CN109793261A CN109793261A CN201910091033.4A CN201910091033A CN109793261A CN 109793261 A CN109793261 A CN 109793261A CN 201910091033 A CN201910091033 A CN 201910091033A CN 109793261 A CN109793261 A CN 109793261A
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- extract
- cigarette
- cigarettes
- ambrette
- tobacco
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- 239000000284 extract Substances 0.000 title claims abstract description 82
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 235000003222 Helianthus annuus Nutrition 0.000 title claims abstract 12
- 244000020551 Helianthus annuus Species 0.000 title abstract 3
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 61
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 55
- 241000208125 Nicotiana Species 0.000 claims abstract description 26
- 239000002994 raw material Substances 0.000 claims abstract description 22
- 241000283690 Bos taurus Species 0.000 claims abstract description 14
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 14
- 238000000605 extraction Methods 0.000 claims abstract description 12
- 239000002904 solvent Substances 0.000 claims abstract description 10
- 235000000509 Chenopodium ambrosioides Nutrition 0.000 claims abstract 5
- 244000098897 Chenopodium botrys Species 0.000 claims abstract 5
- 235000005490 Chenopodium botrys Nutrition 0.000 claims abstract 5
- 241000499945 Amaryllis Species 0.000 claims abstract 4
- 238000005096 rolling process Methods 0.000 claims abstract 2
- 239000007788 liquid Substances 0.000 claims description 25
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 18
- 239000012074 organic phase Substances 0.000 claims description 18
- 239000000843 powder Substances 0.000 claims description 16
- 239000000243 solution Substances 0.000 claims description 16
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 10
- 239000007787 solid Substances 0.000 claims description 10
- 238000004108 freeze drying Methods 0.000 claims description 9
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 8
- QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 claims description 8
- 229920006395 saturated elastomer Polymers 0.000 claims description 8
- 238000004821 distillation Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 239000012071 phase Substances 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 5
- AFABGHUZZDYHJO-UHFFFAOYSA-N dimethyl butane Natural products CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 2
- 241000208818 Helianthus Species 0.000 claims 9
- 235000020238 sunflower seed Nutrition 0.000 claims 3
- 244000184734 Pyrus japonica Species 0.000 claims 2
- 244000119298 Emblica officinalis Species 0.000 claims 1
- 235000015489 Emblica officinalis Nutrition 0.000 claims 1
- 241000276699 Seriola Species 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 230000001105 regulatory effect Effects 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical class O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 claims 1
- 235000019505 tobacco product Nutrition 0.000 abstract description 11
- 239000000654 additive Substances 0.000 abstract description 6
- 230000000996 additive effect Effects 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 6
- 239000003795 chemical substances by application Substances 0.000 abstract description 4
- 238000006243 chemical reaction Methods 0.000 abstract description 2
- 239000002798 polar solvent Substances 0.000 abstract 1
- 235000002783 ambrette Nutrition 0.000 description 70
- 244000096712 ambrette Species 0.000 description 70
- 235000019441 ethanol Nutrition 0.000 description 16
- 238000000926 separation method Methods 0.000 description 15
- 239000012266 salt solution Substances 0.000 description 7
- 239000003205 fragrance Substances 0.000 description 6
- 125000003118 aryl group Chemical group 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- 239000010692 aromatic oil Substances 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- -1 glycoside compounds Chemical class 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 150000002596 lactones Chemical class 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
本发明提供一种烟用黄葵提取物的制备方法及其应用，分别以黄葵的果实外皮、干叶、籽为提取原料，以多种极性溶剂为提取剂，分别进行提取反应，将三种提取液去除溶剂按一定比例混溶于乙醇溶液中，得到一种烟用黄葵提取物。将烟用黄葵提取物溶于溶剂中，将其在卷烟生产的烟丝卷制过程中喷洒在烟丝上应用。本发明增加了黄葵新的功效和作用。黄葵提取物作为烟草制品添加剂，效果明显，对开发具有特色风格的“中式卷烟”制品有很好的应用前景。The invention provides a preparation method and application of a yellow sunflower extract for cigarettes. The fruit rind, dried leaves and seeds of the yellow sunflower are used as extraction raw materials, and various polar solvents are used as extracting agents, and the extraction reactions are carried out respectively. The three kinds of extracts are dissolved in ethanol solution by removing the solvent according to a certain proportion to obtain an extract of Ambrosia for cigarettes. Dissolving the extract of Amaryllis for cigarettes in a solvent is sprayed on the cut tobacco during the rolling process of the cut tobacco produced by the cigarette. The present invention increases the efficacy and function of Huang Kui Xin. As an additive to tobacco products, the extract of Amaryllis has obvious effect, and it has a good application prospect for the development of "Chinese cigarette" products with characteristic style.
Description
Technical field
The application that the present invention relates to natural plant extracts in tobacco product, specifically a kind of cigarette ambrette extract
Preparation method and applications.
Background technique
" Chinese-style cigarette " core competitiveness is to form selling point style, embodies personalized and differentiation, and it is wide to adapt to China
Big consumer's sucks habit and consumer need.Chinese style essence spice for cigarette is Chinese-style cigarette product " soul ", is Chinese style volume
Where the secret that cigarette style characteristic is formed.The scientifically flavoring and casing in cigarette, the personalized style of exactly prominent cigarette product
Important means.Meanwhile in order to improve the safety of smoking, lowering harm and decreasing coking has become an important composition portion of " Chinese-style cigarette "
Point.While reducing coke tar in cigarette, promotes and improve flue gas concentration and fragrance, also only by means of flavoring and casing technology.With
Chinese-style cigarette lowering harm and decreasing coking work go deep into, tobacco flavoring charging show its importance further.
The Chinese style essence spice for cigarette and new technology for constructing independent intellectual property right, extract flavors and fragrances from natural plants,
It allows the theory of health with the refined perfume (or spice) of cigarette, moves towards consumer together, be one of the basic research for developing " Chinese-style cigarette ".
Ambrette has itself unique aromatic style, containing there are many sterols；Also containing there are many glycoside compounds in ambrette leaf；
Containing the lactone substance with characteristic perfume in seed, aromatic oil can be obtained through refining with steam distillation method, is rare advanced tune
Fragrance；Root, leaf are spent and are mostly used as Chinese medicine.The present inventor has found in the course of the research: ambrette seed obtains through refining aromatic oil, yield
It is low, at high cost, limit its application in flavors and fragrances field；Moreover, the aroma component in ambrette other parts also fails to
It is fully utilized.
Summary of the invention
The purpose of the present invention is to the deficiencies in the prior art, provide a kind of cigarette ambrette extract preparation method and
It is applied, and the fruit rinds, cured leaf, seed of ambrette is used to carry out respectively to extract raw material using various polarity solvent as extractant
Reaction is extracted, three kinds of extracting solutions removal solvents are miscible in ethanol solution by a certain percentage, it obtains a kind of cigarette and is extracted with ambrette
Object.
A kind of cigarette preparation method of ambrette extract, includes the following steps:
(1) use ambrette fruit rinds to extract raw material, using ethyl acetate as extractant, extractant and ambrette fruit rinds
Mass ratio be 5~15:1, extracted 1~5 hour at 40~70 DEG C, separate out-feed liquid, the feed liquid after separation is concentrated into medicinal extract shape,
Freeze-drying obtains solid powder A；
(2) use ambrette cured leaf to extract raw material, the ethanol solution for being 50~75% using mass fraction is extracted as extractant
Agent and ambrette cured leaf mass ratio are 10~20:1, are extracted 1~5 hour at 50~90 DEG C, and out-feed liquid is separated, and the feed liquid after separation is dense
It is reduced to medicinal extract shape, obtains ambrette leaf extract；
(3) use ambrette seed for extraction raw material, the mixed solution of saturated salt solution and organic solvent is extractant, passes through steaming
Extraction extraction is evaporated, organic phase is then demultiplex out, the organic phase after separation is concentrated into medicinal extract shape, and freeze-drying obtains solid powder
B；
(4) the extraction product for obtaining step (1), step (2) and step (3) is miscible molten in 70~95% ethyl alcohol in proportion
In liquid to get arrive cigarette of the invention ambrette extract.
Further, saturated salt solution and ambrette seed mass ratio are 15~20:1 in the step (3), organic extractant with
Ambrette seed mass ratio is 2~5:1.
Further, adjust in the step (3) heating temperature make water phase and organic phase to distillate speed equal, extract
Time is 1~5 hour.
Further, the organic solvent in the step (3) is one of pentane, isopentane, ether.
Further, the raw material added in the step (4) according to the mass fraction, wherein solid powder A be 5~40 parts,
Ambrette leaf extract is 30~80 parts, solid powder B is 1~10 part, ethanol solution is 80~300 parts.
Cigarette is added with ambrette extract according to mass ratio 0.01%~0.05% for a kind of application of cigarette ambrette extract
Into the pipe tobacco of cigarette.
Further, cigarette ambrette extract is added in the pipe tobacco of cigarette according to mass ratio 0.02%~0.04%.
Further, cigarette is added to the specific steps of pipe tobacco with ambrette extract are as follows: be dissolved in ambrette extract cigarette molten
In agent, it will be sprayed on pipe tobacco, then evaporate molten during the pipe tobacco of production of cigarettes rolls dissolved with the solvent of ambrette extract
Agent.
Further, the solvent is the ethyl alcohol that mass concentration is 95%.
The present invention shows the ambrette extract of addition in tobacco product suction by a series of experimental studies of smokeing panel test
Can effectively flavouring, and fragrance is abundant；And ambrette extract can also impart to the unique aromatic of tobacco product and note；And
While improving tobacco product mouthfeel, it can be avoided and the negative effect such as introduce miscellaneous gas, increase irritation.
Invention increases ambrette new effects and effect.For ambrette extract as additive of tobacco product, effect is obvious,
There is " Chinese-style cigarette " product of distinctive style to have good application prospect exploitation.
Specific embodiment
Below in conjunction with specific embodiment, the technical solution in the present invention is clearly and completely described.
Embodiment 1
1. use ambrette fruit rinds to extract raw material, using ethyl acetate as extractant, extractant and ambrette fruit rinds
Mass ratio is 5, is extracted 5 hours at 40 DEG C, and out-feed liquid is separated, and the feed liquid after separation is concentrated into medicinal extract shape, and freeze-drying is consolidated
Body powder.
2. use ambrette cured leaf to extract raw material, using 75% ethanol solution as extractant, extractant and ambrette cured leaf quality
It than being 20, is extracted 1 hour at 60 DEG C, separates out-feed liquid, the feed liquid after separation is concentrated into medicinal extract shape.
3. using ambrette seed to extract raw material, saturated salt solution and ether are extractant, and Simultaneous distillation extracts, and are satisfied
It is 15 with saline solution and ambrette seed mass ratio, ether and ambrette seed mass ratio are 2, and adjusting heating temperature makes water phase and organic phase
It is equal to distillate speed, extracts 1 hour, isolates organic phase, the organic phase after separation is concentrated into medicinal extract shape, and freeze-drying is consolidated
Body powder.
4. according to the mass fraction, product 1 is 5 parts, product 2 is 80 parts, product 3 is 1 part, 70% ethanol solution is 200 parts,
It is miscible to get arrive cigarette of the invention ambrette extract.The extract can be used for additive of tobacco product.
Embodiment 2
1. use ambrette fruit rinds to extract raw material, using ethyl acetate as extractant, extractant and ambrette fruit rinds
Mass ratio is 15, is extracted 1 hour at 70 DEG C, and out-feed liquid is separated, and the feed liquid after separation is concentrated into medicinal extract shape, and freeze-drying is consolidated
Body powder.
2. use ambrette cured leaf to extract raw material, using 50% ethanol solution as extractant, extractant and ambrette cured leaf quality
It than being 15, is extracted 3 hours at 75 DEG C, separates out-feed liquid, the feed liquid after separation is concentrated into medicinal extract shape.
3. using ambrette seed to extract raw material, saturated salt solution and pentane are extractant, and Simultaneous distillation extracts, and are satisfied
It is 20 with saline solution and ambrette seed mass ratio, pentane and ambrette seed mass ratio are 5, and adjusting heating temperature makes water phase and organic phase
It is equal to distillate speed, extracts 5 hours, isolates organic phase, the organic phase after separation is concentrated into medicinal extract shape, and freeze-drying is consolidated
Body powder.
4. in parts by mass, product 1 is 10 parts, product 2 is 40 parts, product 3 is 10 parts, 80% ethanol solution is 150 parts,
It is miscible to get arrive cigarette of the invention ambrette extract.The extract can be used for additive of tobacco product.
Embodiment 3
1. use ambrette fruit rinds to extract raw material, using ethyl acetate as extractant, extractant and ambrette fruit rinds
Mass ratio is 12, is extracted 2 hours at 55 DEG C, and out-feed liquid is separated, and the feed liquid after separation is concentrated into medicinal extract shape, and freeze-drying is consolidated
Body powder.
2. use ambrette cured leaf to extract raw material, using 60% ethanol solution as extractant, extractant and ambrette cured leaf quality
It than being 10, is extracted 2 hours at 85 DEG C, separates out-feed liquid, the feed liquid after separation is concentrated into medicinal extract shape.
3. using ambrette seed to extract raw material, saturated salt solution and isopentane are extractant, and Simultaneous distillation extracts,
Saturated salt solution and ambrette seed mass ratio are 18, and isopentane and ambrette seed mass ratio are 3, and adjusting heating temperature makes water phase and organic
Phase to distillate speed equal, extract 4 hours, isolate organic phase, the organic phase after separation is concentrated into medicinal extract shape, is freeze-dried
To solid powder.
4. in parts by mass, wherein product 1 is 25 parts, product 2 is 55 parts, product 3 is 5 parts, 90% ethanol solution is 80
Part, it is miscible to get arrive cigarette of the invention ambrette extract.The extract can be used for additive of tobacco product.
Embodiment 4
1. use ambrette fruit rinds to extract raw material, using ethyl acetate as extractant, extractant and ambrette fruit rinds
Mass ratio is 10, is extracted 4 hours at 45 DEG C, and out-feed liquid is separated, and the feed liquid after separation is concentrated into medicinal extract shape, and freeze-drying is consolidated
Body powder.
2. use ambrette cured leaf to extract raw material, using 65% ethanol solution as extractant, extractant and ambrette cured leaf quality
It than being 12, is extracted 2 hours at 90 DEG C, separates out-feed liquid, the feed liquid after separation is concentrated into medicinal extract shape.
3. using ambrette seed to extract raw material, saturated salt solution and ether are extractant, and Simultaneous distillation extracts, and are satisfied
Be 20 with saline solution and ambrette seed mass ratio, organic extractant and ambrette seed mass ratio are 3.5, adjust heating temperature make water phase and
Organic phase to distillate speed equal, extract 3 hours, isolate organic phase, the organic phase after separation is concentrated into medicinal extract shape, and freezing is dry
It is dry to obtain solid powder.
4. in parts by mass, wherein product 1 is 40 parts, product 2 is 30 parts, product 3 is 8 parts, 95% ethanol solution is 300
Part, it is miscible to get arrive cigarette of the invention ambrette extract.The extract can be used for additive of tobacco product.
Using the cigarette ambrette extract that above method preparation is added in the pipe tobacco to cigarette
Pipe tobacco is added with ambrette extract in cigarette during the pipe tobacco of production of cigarettes rolls.The ambrette being added into pipe tobacco
Extract accounts for the 0.03% of pipe tobacco weight.Specific method is first ambrette extract to be dissolved in the ethyl alcohol that mass concentration is 95%,
Diluted Alcohol dissolved with ambrette extract is uniformly sprayed on pipe tobacco, subsequent ethanol evaporation is fallen.Pipe tobacco rolls into inspection through cigarette machine
Sample cigarette.
Effect experiment in cigarette smoke
40 grams two parts of finished cut tobacco balanced at 22 DEG C ± 1 DEG C of temperature and relative humidity (RH) 60% ± 2% are taken, are pressed
The 0.04% of its quality weighs cigarette ambrette extract, after the dilution of 95% ethyl alcohol, is equably sprayed on pipe tobacco with larynx jet pipe,
Flavoring and non-aromatic tobacco sample are placed in the climatic chamber of 22 DEG C ± 1 DEG C of temperature and RH60% ± 2% and balance 48 hours, use
It fills out cigarette device and cigarette is made in the pipe tobacco of flavoring and non-flavoring respectively, then balance 48 is small under 22 DEG C ± 1 DEG C and RH60% ± 2%
When, ask cigarette sensory evaluating smoking group to be smoked panel test.
The personnel that smoke panel test unanimously think the ambrette extract being added in tobacco product suction can effectively flavouring, and fragrance is rich
It is rich；And ambrette extract can also impart to the unique aromatic of cigarette and note.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Belong to those skilled in the art in the technical scope disclosed by the present invention, any changes or substitutions that can be easily thought of, all answers
It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.
Claims (9)
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| CN201910091033.4A CN109793261B (en) | 2019-01-30 | 2019-01-30 | A kind of preparation method and application of yellow sunflower extract for tobacco |
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| CN201910091033.4A CN109793261B (en) | 2019-01-30 | 2019-01-30 | A kind of preparation method and application of yellow sunflower extract for tobacco |
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ID=66559313
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2019
- 2019-01-30 CN CN201910091033.4A patent/CN109793261B/en active Active
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| CN102757865A (en) * | 2011-04-25 | 2012-10-31 | 湖北中烟工业有限责任公司 | Carum carvi and dried ginger composite extract and purpose thereof as tobacco product additive |
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