CN109734077A - A kind of heavy duty detergent graphene production equipment based on microwave method - Google Patents

Abstract

The heavy duty detergent graphene production equipment based on microwave method that the present invention relates to a kind of, including reacting furnace, controller, sealing block, microwave emitter, supporting plate, vibrating mechanism, placement mechanism and two lifting assemblies, vibrating mechanism includes fixed plate, first motor, turntable, translate component and two vibration components, vibration component includes translational block, reciprocal unit and vibrating mass, placement mechanism includes placing ware, cover board and several fixation kits, fixation kit includes fixed ring, drag hook and spring, the heavy duty detergent graphene production equipment based on microwave method makes supporting plate that placement ware be driven to vibrate up and down by vibrating mechanism, it is uniformly layered on and is placed in ware convenient for graphite particle, absorb microwave energy, improve graphene production efficiency, moreover, graphene is concentrated on placing in ware by placement mechanism, convenient for the collection of graphene, it is set to improve Standby practicability.

Description

A kind of heavy duty detergent graphene production equipment based on microwave method

Technical field

The present invention relates to new material production equipment field, in particular to a kind of heavy duty detergent graphene production based on microwave method Equipment.

Background technique

Graphene is the carbon atomic layer of monoatomic thickness, is that carbon atom is only with the thickness that solid SP2 hydbridized carbon atoms are formed The hexaplanar of single layer atom is arranged in the single layer two dimensional crystal of honeycomb lattice.Graphene has excellent optics, electricity, mechanics Characteristic, it is with important application prospects in terms of materialogy, micro-nano technology, the energy, biomedicine and medicine, it is artificial It is a kind of future revolutionary material.

Graphene can be made by microwave method, to graphite particle irradiating microwaves, so that graphite particle absorbs the energy of microwave After redox reaction occurs, that is, when producing obtained graphene, but producing graphene using microwave, due to graphite particle heap Product together, so that can not be absorbed into microwave energy inside graphite particle heap, leads to the waste of graphite particle raw material, reduces simultaneously Formation efficiency, moreover, using graphene made from microwave since fluffy degree is very high, lighter weight, in production process, stone Black alkene is easy to fly upward in reactor, brings trouble puzzlement to the collection of graphene, it is raw to thereby reduce existing graphene Produce the practicability of equipment.

Summary of the invention

The technical problem to be solved by the present invention is for overcome the deficiencies in the prior art, provide a kind of based on microwave method Heavy duty detergent graphene production equipment.

The technical solution adopted by the present invention to solve the technical problems is: a kind of heavy duty detergent graphene based on microwave method is raw Produce equipment, including reacting furnace, controller, sealing block, microwave emitter, supporting plate, vibrating mechanism, placement mechanism and two lifting groups Part, the controller are fixed on reacting furnace, and PLC is equipped in the controller, and the sealing block lid is located at the opening of reacting furnace Place, the microwave emitter are fixed on the lower section of sealing block, and the placement mechanism, supporting plate and vibrating mechanism are successively set from top to down It sets in the inside of reacting furnace, two lifting assemblies are located at the two sides of sealing block, and the lifting assembly and sealing block transmission connect It connects, the microwave emitter is electrically connected with PLC；

The vibrating mechanism includes fixed plate, first motor, turntable, translation component and two vibration components, the fixation Plate is fixed in reacting furnace, and the first motor is fixed on the top of fixed plate, and the first motor is electrically connected with PLC, described First motor and turntable are sequentially connected, and the vibration component includes translational block, reciprocal unit and vibrating mass, the translational block against In the top of turntable, the translation component and translational block are sequentially connected, and the top of translational block is arranged in the reciprocal unit, described Reciprocal unit and vibrating mass are sequentially connected, and the vibrating mass is resisted against the lower section of supporting plate；

The placement mechanism includes placing ware, cover board and several fixation kits, the top placed ware and supporting plate is arranged in, The cover plate lid is located at the opening for placing ware, and the fixation kit is circumferentially evenly distributed on the periphery for placing ware, the fixation Component includes fixed ring, drag hook and spring, and the fixed ring is fixed on the lower section of cover board, and the drag hook is arranged in fixed ring, One end of the spring is connect with drag hook, and the other end of the spring is connect with supporting plate, and the spring is in compressive state, described The making material of cover board is pyroceram, is equipped with several sliding rails in the reacting furnace, the sliding rail is circumferentially evenly distributed on instead It answers on the inner wall of furnace, the shape of the sliding rail is U-shaped, and the both ends of the sliding rail are fixed on the inner wall of reacting furnace, the supporting plate It is arranged on the slide rail.

Preferably, the lifting in order to realize sealing block, the lifting assembly includes side plate and cylinder, the cylinder of the cylinder Body is fixed on reacting furnace vertically upward, and the side plate is fixedly connected with sealing block, and the top of the gas bar of the cylinder is fixed on The lower section of side plate, the cylinder are electrically connected with PLC.

Preferably, in order to guarantee that sealing performance, the shape of the bottom end of the sealing block are circular cone cylindricality, the sealing block The outer diameter of one end of close reacting furnace be less than the internal diameter of reacting furnace, the outer diameter of the other end of the seal pipe is greater than reacting furnace Internal diameter.

Preferably, the translation component includes the second motor and two translation units, institute in order to drive translational block mobile It states the second motor to be electrically connected with PLC, the translation unit and vibration component correspond, and the translation unit includes bearing and silk Bar, second motor and bearing are each attached to the top of turntable, and one end transmission connection of second motor and screw rod is described The other end of screw rod is arranged in bearing, and the translational block is set on screw rod, and the translational block is set with the junction of screw rod Have and the matched screw thread of screw rod.

Preferably, the lower section of the turntable is equipped with several supporting blocks, the supporting block for the rotation of Auxiliary support turntable It is circumferentially evenly distributed on the periphery of first motor, the lower section of the supporting block is equipped with recess, and ball is equipped in the recess, described Recess matches with ball, and the centre of sphere of the ball is located in recess, and the ball is resisted against in fixed plate.

Preferably, the reciprocating movement in order to realize vibrating mass, the reciprocal unit includes third motor, drive disk, drive Lever, driving frame and two connecting rods, the third motor are fixed on the top of translational block, and the third motor is electrically connected with PLC, The third motor and drive disk are sequentially connected, and the drive rod is fixed on the separate the center point of drive disk, the drive rod position In the inside of driving frame, the driving frame is fixedly connected by connecting rod with vibrating mass.

Preferably, the steady movement in order to realize driving frame, the both ends of the driving frame are equipped with slip ring and slide bar, described Slip ring is set on slide bar, and the slip ring is fixedly connected with driving frame, and the slide bar is fixed on the top of translational block.

Preferably, placing the placement location of ware for the ease of regulation, the placement mechanism further includes positioning ring, described fixed Position ring is fixed on the top of supporting plate, and the internal diameter of one end of the separate supporting plate of the positioning ring is greater than the outer diameter for placing ware.

Preferably, in order to guarantee reaction safety, the bottom of the side of the reacting furnace is equipped with air inlet pipe, the air inlet pipe It is inside equipped with the first valve, the top of the other side of the reacting furnace is equipped with escape pipe, is equipped with the second valve, institute in the escape pipe It states the first valve and the second valve is electrically connected with PLC.

Preferably, in order to further ensure that reaction safety, the lower section of the sealing block is equipped with oxygen concentration instrument, the oxygen Gas concentration instrument is electrically connected with PLC.

Made the invention has the advantages that being somebody's turn to do the heavy duty detergent graphene production equipment based on microwave method by vibrating mechanism Supporting plate, which drives, places ware up-down vibration, is uniformly layered on and is placed in ware convenient for graphite particle, absorb microwave energy, it is raw to improve graphene Efficiency is produced, moreover, concentrates on placing in ware by graphene by placement mechanism, convenient for the collection of graphene, to improve The practicability of equipment.

Detailed description of the invention

Present invention will be further explained below with reference to the attached drawings and examples.

Fig. 1 is the structural schematic diagram of the heavy duty detergent graphene production equipment of the invention based on microwave method；

Fig. 2 is the structural schematic diagram of the vibrating mechanism of the heavy duty detergent graphene production equipment of the invention based on microwave method；

Fig. 3 is the structural schematic diagram of the vibration component of the heavy duty detergent graphene production equipment of the invention based on microwave method；

Fig. 4 is the portion the A enlarged drawing of Fig. 1；

In figure: 1. reacting furnaces, 2. controllers, 3. microwave emitters, 4. supporting plates, 5. fixed plates, 6. first motors, 7. turns Disk, 8. placement wares, 9. cover boards, 10. fixed rings, 11. drag hooks, 12. springs, 13. sliding rails, 14. side plates, 15. cylinders, 16. second Motor, 17. bearings, 18. screw rods, 19. supporting blocks, 20. balls, 21. third motors, 22. drive disks, 23. drive rods, 24. drive Dynamic frame, 25. connecting rods, 26. slip rings, 27. slide bars, 28. positioning rings, 29. air inlet pipe, 30. escape pipes, 31. oxygen concentration instrument, 32. Sealing block, 33. translational blocks, 34. vibrating mass.

Specific embodiment

In conjunction with the accompanying drawings, the present invention is further explained in detail.These attached drawings are simplified schematic diagram, only with Illustration illustrates basic structure of the invention, therefore it only shows the composition relevant to the invention.

As shown in Figure 1, a kind of heavy duty detergent graphene production equipment based on microwave method, including it is reacting furnace 1, controller 2, close Envelope block 32, microwave emitter 3, supporting plate 4, vibrating mechanism, placement mechanism and two lifting assemblies, the controller 2 are fixed on instead It answers on furnace 1, PLC is equipped in the controller 2, the sealing block 32 covers the opening for being located at reacting furnace 1, the microwave emitter 3 are fixed on the lower section of sealing block 32, and the placement mechanism, supporting plate 4 and vibrating mechanism are successively set on reacting furnace 1 from top to down Inside, two lifting assemblies are located at the two sides of sealing block 32, and the lifting assembly and sealing block 32 are sequentially connected, described micro- Wave launcher 3 is electrically connected with PLC；

For the production equipment when preparing graphene, user operates equipment operation by controller 2, is driven by lifting assembly close Envelope block 32 moves up, so that placement mechanism to be placed on to the top of supporting plate 4, then lifting group after the opening of reacting furnace 1 is opened Part drives sealing block 32 to move down, and blocks reacting furnace 1, and then PLC controls microwave emitter 3 and runs, into placement mechanism Graphite particle emits microwave and reacts after graphite particle absorbs microwave energy and generate graphene, utilizes the vibration of 4 lower section of supporting plate Motivation structure drives supporting plate 4 to be vibrated, so that graphite particle is evenly distributed in placement mechanism, is convenient for uniform pickup microwave energy Amount improves the formation efficiency of graphene so that reaction is uniformly.

As shown in Fig. 2, the vibrating mechanism includes fixed plate 5, first motor 6, turntable 7, translation component and two vibrations Component, the fixed plate 5 are fixed in reacting furnace 1, and the first motor 6 is fixed on the top of fixed plate 5, the first motor 6 are electrically connected with PLC, and the first motor 6 is sequentially connected with turntable 7, the vibration component include translational block 33, reciprocal unit and Vibrating mass 34, the translational block 33 are resisted against the top of turntable 7, and the translation component and translational block 33 are sequentially connected, described past The top of translational block 33 is arranged in multiple unit, and the reciprocal unit and vibrating mass 34 are sequentially connected, and the vibrating mass 34 is resisted against The lower section of supporting plate 4；

When vibrating mechanism is run, PLC controls first motor 6 and starts, and drives turntable 7 to rotate, so that the vibration group of 7 row of turntable Part is rotated along the axis of turntable 7, is vibrated from different positions to supporting plate 4, while translating component starting, drives translational block 33 is mobile, changes the axial line distance of vibration component and turntable 7, so that vibration is more uniformly, in 4 vibration processes of supporting plate, edge About 13 sliding rail move back and forth, and when vibration component is run, PLC controls reciprocal unit starting, drives on vibrating mass 34 Lower movement, realizes the reciprocating movement of supporting plate 4, is uniformly laid with convenient for the graphite particle shake in placement mechanism, is convenient for graphite Grain uniform pickup microwave energy.

As shown in figure 4, the placement mechanism includes placing ware 8, cover board 9 and several fixation kits, the placement ware 8 is arranged In the top of supporting plate 4, the cover board 9 covers the opening for being located at and placing ware 8, and the fixation kit is circumferentially evenly distributed on placement ware 8 periphery, the fixation kit include fixed ring 10, drag hook 11 and spring 12, and the fixed ring 10 is fixed under cover board 9 Side, the drag hook 11 are arranged in fixed ring 10, and one end of the spring 12 is connect with drag hook 11, the other end of the spring 12 It is connect with supporting plate 4, the spring 12 is in compressive state, and the making material of the cover board 9 is pyroceram, the reacting furnace Several sliding rails 13 are equipped in 1, the sliding rail 13 is circumferential to be evenly distributed on the inner wall of reacting furnace 1, and the shape of the sliding rail 13 is U The both ends of shape, the sliding rail 13 are fixed on the inner wall of reacting furnace 1, and the supporting plate 4 is set on sliding rail 13.

Graphite particle is placed on after placing 8 inside of ware, placement ware 8 is put in the top of supporting plate 4, then covers cover board 9, It is detached from 4 vibration processes cover plate 9 of supporting plate in order to avoid placing ware 8 and places the top of ware 8, by each fixation kit by cover board 9 are resisted against 8 top of placement ware, pull spring 12, so that drag hook 11 catches on the fixed ring 10 for being fixed on 9 lower section of cover board, thus will Cover board 9 is fixed on the top for placing ware 8, and cover board 9 selects pyroceram to be made, and on the one hand can bear the high temperature of reaction, separately On the one hand can also instant microwave pass through cover board 9 and transfer energy to the graphite particle placed in ware 8, meanwhile, cover board 9 can also be to putting It sets ware 8 to be sealed, the lighter graphene for avoiding reaction from generating waves inside reacting furnace 1, so that graphene concentrates on putting It sets in ware 8, when after the reaction was completed, drag hook 11 is removed from fixed ring 10, takes away and place ware 8, remove cover board 9, can obtain The graphene inside ware 8 is placed, to facilitate the collection of graphene.

Preferably, the lifting in order to realize sealing block 32, the lifting assembly includes side plate 14 and cylinder 15, the gas The cylinder body of cylinder 15 is fixed on vertically upward on reacting furnace 1, and the side plate 14 is fixedly connected with sealing block 32, the gas of the cylinder 15 The top of bar is fixed on the lower section of side plate 14, and the cylinder 15 is electrically connected with PLC.

PLC controls cylinder 15 and starts, the intracorporal air pressure of cylinder of adjustable displacements of cylinders 15, so that the gas bar of cylinder 15 is with cylinder body Pressure change and move, and then drive 14 lifting moving of side plate, since side plate 14 is fixedly connected with sealing block 32, thus reality The lifting of sealing block 32 is showed.

Preferably, in order to guarantee that sealing performance, the shape of the bottom end of the sealing block 32 are circular cone cylindricality, the sealing The outer diameter of one end of the close reacting furnace 1 of block 32 is less than the internal diameter of reacting furnace 1, and the outer diameter of the other end of the seal pipe is greater than anti- Answer the internal diameter of furnace 1.

One end of the close reacting furnace 1 of sealing block 32 uses the cylindrical design of circular cone, is conducive to sealing block 32 and moves down When, the bottom of sealing block 32 is protruded into reacting furnace 1, continues to move down with sealing block 32, the circular conical surface of sealing block 32 supports On the inner wall for leaning against the top in reacting furnace 1, the sealing to reacting furnace 1 is realized.

As shown in Fig. 2, the translation component includes the second motor 16 and two translation units, second motor 16 with PLC electrical connection, the translation unit and vibration component correspond, and the translation unit includes bearing 17 and screw rod 18, described Second motor 16 and bearing 17 are each attached to the top of turntable 7, and one end of second motor 16 and screw rod 18 is sequentially connected, institute State screw rod 18 the other end be arranged in bearing 17, the translational block 33 is set on screw rod 18, the translational block 33 with silk The junction of bar 18 is equipped with and the matched screw thread of screw rod 18.

PLC controls the starting of the second motor 16, drives the screw rod 18 in the translation unit of two sides in the supporting role of bearing 17 Lower rotation, screw rod 18 passes through threaded function in translational block 33, so that translational block 33 is moved along the axis direction of screw rod 18 It is dynamic.

Preferably, the lower section of the turntable 7 is equipped with several supporting blocks 19, the branch for the rotation of Auxiliary support turntable 7 The circumferential periphery for being evenly distributed on first motor 6 of bracer 19, the lower section of the supporting block 19 are equipped with recess, are equipped in the recess Ball 20, the recess match with ball 20, and the centre of sphere of the ball 20 is located in recess, and the ball 20 is resisted against fixation On plate 5.First motor 6 drives in 7 rotary course of turntable, the lower section of turntable 7, by supporting block 19 and ball 20 to turntable 7 into Row support, prevents turntable 7 from tilting, while in the recess of supporting block 19, ball 20 can roll in fixed plate 5, reduce Turntable 7 rotates suffered friction.

As shown in figure 3, the reciprocal unit includes third motor 21, drive disk 22, drive rod 23, drives frame 24 and two Connecting rod 25, the third motor 21 are fixed on the top of translational block 33, and the third motor 21 is electrically connected with PLC, the third Motor 21 and drive disk 22 are sequentially connected, and the drive rod 23 is fixed on the separate the center point of drive disk 22, the drive rod 23 Positioned at the inside of driving frame 24, the driving frame 24 is fixedly connected by connecting rod 25 with vibrating mass 34.

PLC controls third motor 21 and starts, and drives drive disk 22 to rotate, so that axis of the drive rod 23 along drive disk 22 It moves in a circle, drive rod 23 acts on the inner wall of driving frame 24, so that driving frame 24 drives vibrating mass 34 by connecting rod 25 It is moved back and forth up and down.

Preferably, the steady movement in order to realize driving frame 24, the both ends of the driving frame 24 are equipped with slip ring 26 and slide Bar 27, the slip ring 26 are set on slide bar 27, and the slip ring 26 is fixedly connected with driving frame 24, and the slide bar 27 is fixed on flat Move the top of block 33.While driving frame 24 that slip ring 26 is driven to carry out lifting moving, slip ring 26 is slided along the axis of slide bar 27, Since slide bar 27 is fixed in translational block 33, to realize the steady movement of driving frame 24.

Preferably, placing the placement location of ware 8 for the ease of regulation, the placement mechanism further includes positioning ring 28, institute The top that positioning ring 28 is fixed on supporting plate 4 is stated, the internal diameter of one end of the separate supporting plate 4 of the positioning ring 28, which is greater than, places ware 8 Outer diameter.Facilitate the placement location of regulation placement ware 8, while the separate supporting plate 4 of positioning ring 28 using the positioning ring 28 of fixed position The internal diameter of one end be greater than the outer diameter for placing ware 8, be put into the inside of fixed ring 10 convenient for placing ware 8.

Preferably, in order to guarantee reaction safety, the bottom of the side of the reacting furnace 1 is equipped with air inlet pipe 29, it is described into The first valve is equipped in tracheae 29, the top of the other side of the reacting furnace 1 is equipped with escape pipe 30, is equipped in the escape pipe 30 Second valve, first valve and the second valve are electrically connected with PLC.Before the reaction, PLC controls the first valve and the second valve Door is opened, and is passed through inert gas into reacting furnace 1 using air inlet pipe 29, the oxygen in reacting furnace 1 is discharged from escape pipe 30, The first valve and the second valve are then shut, so that reaction carries out in inert gas, and then keeps preparing for graphene safer Reliably.

Preferably, in order to further ensure that reaction safety, the lower section of the sealing block 32 is equipped with oxygen concentration instrument 31, institute Oxygen concentration instrument 31 is stated to be electrically connected with PLC.The oxygen concentration in reacting furnace 1 is detected using oxygen concentration instrument 31, and by concentration numbers According to PLC is passed to, after being passed through inert gas into reacting furnace 1, PLC detects the variation of oxygen concentration data, when concentration value drops After a certain range, PLC controls the first valve and the second valve is closed, to make to guarantee in reacting furnace 1 full of inert gas The safety of reaction carries out.

When preparing graphene using the production equipment, lifting assembly drives sealing block 32 to move up, and graphite particle is put It sets after placing in ware 8, ware 8 will be placed and be placed on supporting plate 4, cover board 9 is fixed on to the top for placing ware 8 using fixation kit, It is flown upward after avoiding graphene from generating to placing outside ware 8, after then lifting assembly drive sealing block 32 blocks reacting furnace 1, microwave Transmitter 3 emits microwave to graphite particle, so that graphite particle, which reacts, generates graphene, using first motor 6 with turn Vibration component on disk 7 is moved to the different location of 4 lower section of supporting plate, and the position of vibration component is adjusted by translation component, makes It obtains vibration component to vibrate the different location of supporting plate 4, guarantees that graphite particle is uniformly laid on and place in ware 8, uniform pickup Microwave energy, to improve the production efficiency of graphene, after completion of the reaction, sealing block 32 is moved up, and is removed and is placed ware 8, due to Prevent graphene from flying upward using sealing cover, so that the graphene generated is made to concentrate on placing in ware 8, convenient for the collection of graphene, To improve the practicability of equipment.

Compared with prior art, it is somebody's turn to do the heavy duty detergent graphene production equipment based on microwave method and supporting plate is made by vibrating mechanism 4 drive placement ware 8 to vibrate up and down, and are uniformly layered on and are placed in ware 8 convenient for graphite particle, absorb microwave energy, improve graphene life Efficiency is produced, moreover, concentrates on placing in ware 8 by graphene by placement mechanism, convenient for the collection of graphene, to improve The practicability of equipment.

Taking the above-mentioned ideal embodiment according to the present invention as inspiration, through the above description, relevant staff is complete Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention Property range is not limited to the contents of the specification, it is necessary to which the technical scope thereof is determined according to the scope of the claim.

Claims (10)

1. a kind of heavy duty detergent graphene production equipment based on microwave method, which is characterized in that including reacting furnace (1), controller (2), sealing block (32), microwave emitter (3), supporting plate (4), vibrating mechanism, placement mechanism and two lifting assemblies, the control Device (2) is fixed on reacting furnace (1), and PLC is equipped in the controller (2), and sealing block (32) lid is located at reacting furnace (1) Opening, the microwave emitter (3) are fixed on the lower section of sealing block (32), the placement mechanism, supporting plate (4) and vibrating mechanism It is successively set on the inside of reacting furnace (1) from top to down, two lifting assemblies are located at the two sides of sealing block (32), the liter Part of coming down to a lower group is sequentially connected with sealing block (32), and the microwave emitter (3) is electrically connected with PLC；

The vibrating mechanism includes fixed plate (5), first motor (6), turntable (7), translates component and two vibration components, described Fixed plate (5) is fixed in reacting furnace (1), and the first motor (6) is fixed on the top of fixed plate (5), the first motor (6) it is electrically connected with PLC, the first motor (6) and turntable (7) are sequentially connected, and the vibration component includes translational block (33), past Multiple unit and vibrating mass (34), the translational block (33) are resisted against the top of turntable (7), the translation component and translational block (33) Transmission connection, in the top of translational block (33), the reciprocal unit and vibrating mass (34) are sequentially connected for the reciprocal unit setting, The vibrating mass (34) is resisted against the lower section of supporting plate (4)；

The placement mechanism includes placing ware (8), cover board (9) and several fixation kits, and the placement ware (8) is arranged in supporting plate (4) top, cover board (9) lid are located at the opening for placing ware (8), and the fixation kit is circumferentially evenly distributed on placement ware (8) periphery, the fixation kit include fixed ring (10), drag hook (11) and spring (12), and the fixed ring (10) is fixed on The lower section of cover board (9), the drag hook (11) are arranged on fixed ring (10), and one end and drag hook (11) of the spring (12) are even It connects, the other end of the spring (12) is connect with supporting plate (4), and the spring (12) is in compressive state, the system of the cover board (9) Making material is pyroceram, is equipped with several sliding rails (13) in the reacting furnace (1), the sliding rail (13) is circumferentially evenly distributed on On the inner wall of reacting furnace (1), the shape of the sliding rail (13) is U-shaped, and the both ends of the sliding rail (13) are fixed on reacting furnace (1) On inner wall, the supporting plate (4) is set on sliding rail (13).

2. the heavy duty detergent graphene production equipment based on microwave method as described in claim 1, which is characterized in that the lifting group Part includes side plate (14) and cylinder (15), and the cylinder body of the cylinder (15) is fixed on vertically upward on reacting furnace (1), the side plate (14) it is fixedly connected with sealing block (32), the top of the gas bar of the cylinder (15) is fixed on the lower section of side plate (14), the gas Cylinder (15) is electrically connected with PLC.

3. the heavy duty detergent graphene production equipment based on microwave method as described in claim 1, which is characterized in that the sealing block (32) shape of bottom end is circular cone cylindricality, and the outer diameter of one end of the close reacting furnace (1) of the sealing block (32) is less than reaction The internal diameter of furnace (1), the outer diameter of the other end of the seal pipe are greater than the internal diameter of reacting furnace (1).

4. the heavy duty detergent graphene production equipment based on microwave method as described in claim 1, which is characterized in that the translation group Part includes the second motor (16) and two translation units, and second motor (16) is electrically connected with PLC, the translation unit and vibration Dynamic component corresponds, and the translation unit includes bearing (17) and screw rod (18), second motor (16) and bearing (17) It is each attached to the top of turntable (7), second motor (16) and the one end of screw rod (18) are sequentially connected, the screw rod (18) In the bearing (17), the translational block (33) is set on screw rod (18) for other end setting, the translational block (33) and screw rod (18) junction is equipped with and screw rod (18) matched screw thread.

5. the heavy duty detergent graphene production equipment based on microwave method as described in claim 1, which is characterized in that the turntable (7) lower section is equipped with several supporting blocks (19), and the supporting block (19) is circumferentially evenly distributed on the periphery of first motor (6), institute The lower section for stating supporting block (19) is equipped with recess, is equipped with ball (20) in the recess, the recess matches with ball (20), institute The centre of sphere for stating ball (20) is located in recess, and the ball (20) is resisted against on fixed plate (5).

6. the heavy duty detergent graphene production equipment based on microwave method as described in claim 1, which is characterized in that the reciprocal list Member includes third motor (21), drive disk (22), drive rod (23), driving frame (24) and two connecting rods (25), the third electricity Machine (21) is fixed on the top of translational block (33), and the third motor (21) is electrically connected with PLC, the third motor (21) and drive Moving plate (22) transmission connection, the drive rod (23) are fixed on the separate the center point of drive disk (22), drive rod (23) position In the inside of driving frame (24), the driving frame (24) is fixedly connected by connecting rod (25) with vibrating mass (34).

7. the heavy duty detergent graphene production equipment based on microwave method as claimed in claim 6, which is characterized in that the driving frame (24) both ends are equipped with slip ring (26) and slide bar (27), and the slip ring (26) is set on slide bar (27), the slip ring (26) and Driving frame (24) is fixedly connected, and the slide bar (27) is fixed on the top of translational block (33).

8. the heavy duty detergent graphene production equipment based on microwave method as described in claim 1, which is characterized in that the placement machine Structure further includes positioning ring (28), and the positioning ring (28) is fixed on the top of supporting plate (4), the separate supporting plate of the positioning ring (28) (4) internal diameter of one end is greater than the outer diameter for placing ware (8).

9. the heavy duty detergent graphene production equipment based on microwave method as described in claim 1, which is characterized in that the reacting furnace (1) bottom of side is equipped with air inlet pipe (29), is equipped with the first valve in the air inlet pipe (29), the reacting furnace (1) it is another The top of side is equipped with escape pipe (30), and the second valve, first valve and the second valve are equipped in the escape pipe (30) It is electrically connected with PLC.

10. the heavy duty detergent graphene production equipment based on microwave method as described in claim 1, which is characterized in that the sealing The lower section of block (32) is equipped with oxygen concentration instrument (31), and the oxygen concentration instrument (31) is electrically connected with PLC.