CN109700909A - A kind of preparation method of quick-acting plaster - Google Patents
A kind of preparation method of quick-acting plaster Download PDFInfo
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- CN109700909A CN109700909A CN201910208914.XA CN201910208914A CN109700909A CN 109700909 A CN109700909 A CN 109700909A CN 201910208914 A CN201910208914 A CN 201910208914A CN 109700909 A CN109700909 A CN 109700909A
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Abstract
The present invention relates to plaster preparation technical fields, disclose a kind of preparation method of quick-acting plaster, after the coarse fodder in prescription is smashed, impregnate refluxing extraction with ethyl alcohol, obtain medicinal extract after concentration；Fines in prescription is crushed, fine powder is obtained；Take 5 parts by weight honey heating stirring in the prinsepia utilis royle oil of 2 ~ 3 parts by weight, heating temperature is 100 ~ 120 DEG C, when water content is reduced to 3 ~ 15% in the mixture of heating, the medicinal extract is added into mixture and continues heating stirring, until steam is down to 2% or less stopping heating in mixture, the fine powder is added into mixture to stir evenly, is placed on non-woven rubberized fabric, obtains quick-acting plaster.Quick-acting plaster of the invention are after being affixed on skin, and 5 minutes take effect, remission in half an hour, and effect is rapid.
Description
Technical field
The present invention relates to plaster preparation technical fields, and in particular to a kind of preparation method of quick-acting plaster.
Background technique
Chinese medicine surgical plaster is to coordinate the efficiency for being mutually with drug with traditional Chinese medicine, form multi-flavor medicine
The big compound of object, to play the good result of drug.Plaster is used for fleshy exterior plaster, is affixed on the plaster stimulation nerve endings of body surface,
By reflection, blood vessel is expanded, promotes local blood circulation, improves surrounding tissue nutrition, reaches detumescence, anti-inflammatory and analgesic mesh
's.Drug reaches subcutaneous tissue by Cutaneous permeation in affected part simultaneously, in the relative advantage for locally generating drug concentration, to play
Stronger pharmacological action.After drug break-through skin and mucous membrane, enters body circulation by blood vessel or lymphatic vessel, also can produce systemic
Drug effect.
It is different according to matrix and manufacture craft, current plaster type have lead plaster medicine, rosin cream, adhesive plaster, Goupi Gao, bar
Plaster ointment etc..Traditional plaster is the efficacy component extracted at high temperature in Chinese medicine coarse fodder with vegetable oil, is reached in oil refining process
320 DEG C -360 DEG C of high temperature, such high temperature cause the effective component in Chinese medicine to decompose loss greatly, lead to plant oil extract Chinese medicine
The effective quantity of coarse fodder is limited, thus the plaster content of dispersion produced is also small, causes plaster effect slow, the big discounting of clinical efficacy
Button.Since plaster is at normal temperature at solid-state, plaster drug effect relies on the relatively breast-high scent of drug more, adds Xin Xiang and walks to alter extremely strong draw
Through drug, by infiltrating through skin, the effects of interior transmission from one channel to another network, internal organs, it is wet to play regulating the qi flowing in the channels blood, degrading the channel, cold dispelling, pain of reducing swelling.By
Drug in the barrier action of skin, plaster is difficult to fast strikethrough skin and is absorbed, it is difficult to be rapidly achieved therapeutic effect, together
Sample makes clinical efficacy have a greatly reduced quality.
Summary of the invention
In view of this, this method is without elevated process, by most the present invention provides a kind of preparation method of quick-acting plaster
The active constituent content of the reservation natural drug of limits improves drug in the penetration of skin surface, can reach 5 minutes fastly
The effect that speed works, effect are quick.
Technical scheme is as follows:
The present invention provides a kind of preparation methods of quick-acting plaster, comprising the following steps:
(1) after smashing the coarse fodder in prescription, refluxing extraction is impregnated with ethyl alcohol, obtains medicinal extract after concentration；
(2) fines in prescription is crushed, obtains fine powder；
(3) 5 parts by weight honey heating stirring in the prinsepia utilis royle oil of 2 ~ 3 parts by weight is taken, heating temperature is 100 ~ 120 DEG C, when adding
When water content is reduced to 3 ~ 15% in the mixture of heat, the medicinal extract is added into mixture and continues heating stirring, until mixture
Middle steam is down to 2% or less stopping heating, and the fine powder is added and stirs evenly, is placed on non-woven rubberized fabric, obtains quick-acting plaster；
Wherein, step (1) and step (2) do not have sequencing.
Preferably, the coarse fodder is crushed to partial size less than 1.0cm.
Preferably, the volumetric concentration of step (1) described ethyl alcohol is between 70% ~ 85%.
It is further preferred that the temperature of step (1) described refluxing extraction is 65 ~ 95 DEG C, extraction time is 2 ~ 6 hours.
Preferably, for heating concentration, the medicinal extract being concentrated to get is the 1/4 ~ 1/6 of original volume for step (1) concentration.
Preferably, the smashing partial size of the fines is 40 ~ 120 mesh.
Preferably, for step (3) fine powder when being added, the temperature of mixture is 45 DEG C ~ 65 DEG C.
Preferably, the weight ratio of step (3) medicinal extract and the honey and prinsepia utilis royle oil total weight is 1 ~ 3:10.
Preferably, the weight ratio of step (3) fine powder and the honey and prinsepia utilis royle oil total weight is 1 ~ 5:10.
Compared with the existing technology, the invention has the following advantages that
The present invention provides a kind of preparation methods of quick-acting plaster, comprising the following steps: (1) after the coarse fodder in prescription being smashed,
Refluxing extraction is impregnated with ethyl alcohol, obtains medicinal extract after concentration；(2) fines in prescription is crushed, obtains fine powder；(3) 5 parts by weight are taken
Honey heating stirring in the prinsepia utilis royle oil of 2 ~ 3 parts by weight, heating temperature is 100 ~ 120 DEG C, when aqueous in the mixture of heating
When amount is reduced to 3 ~ 15%, the medicinal extract is added into mixture and continues heating stirring, until steam is down to 2% or less in mixture
Stop heating, the fine powder is added and stirs evenly, is placed on non-woven rubberized fabric, obtains quick-acting plaster.On the one hand, instant effecting ointment of the present invention
The preparation method of medicine does not have elevated process in entire manufacturing process, prepares medicinal extract in such a way that ethyl alcohol impregnates refluxing extraction,
Extracting temperature is low, reduces the loss of effective component in drug, and the active pharmaceutical ingredient remained in plaster to the greatest extent contains
Amount, accelerates plaster onset time, improves the drug effect of plaster.On the other hand, plaster substrate of the invention selects honey and green thorn
The mixture of fruit oil, honey and prinsepia utilis royle oil have extraordinary permeability in skin surface, have greatly accelerated in plaster prescription
Active medicine rapidly go directly lesion, so that fast onset therapeutic effect, reaches quick-acting effects.Quick-acting plaster of the invention are pasting
After skin, 5 minutes take effect, remission in half an hour, 7 days courses for the treatment of.
In preparation method of plaster of the invention, the honey used has effects that sterilization and moisturizing.Prinsepia utilis royle oil is not rich in
Saturated fatty acid, and its composition is close with human sebaceous's class, has extremely strong skin permeability, can play similar with azone
Effect, therefore, plaster of the invention is can reach rapid osmotic skin, fast onset in the case where adding other additives
Effect.Prinsepia utilis royle oil has skin regeneration technique and moisture-keeping function simultaneously, can reduce plaster to skin with honey combination
Stimulation reduces the generation of the allergic phenomenas such as fash, scratchy, blistering.There are also anti-inflammatory effects for prinsepia utilis royle oil, and detumescence is stopped
Bitterly, the plaster of the effects of removing obstruction in channels to relieve pain type can play better control efficiency.
Specific embodiment
The present invention provides a kind of preparation methods of quick-acting plaster, comprising the following steps:
(1) after smashing the coarse fodder in prescription, refluxing extraction is impregnated with ethyl alcohol, obtains medicinal extract after concentration；
(2) fines in prescription is crushed, obtains fine powder；
(3) 5 parts by weight honey heating stirring in the prinsepia utilis royle oil of 2 ~ 3 parts by weight is taken, heating temperature is 100 ~ 120 DEG C, when adding
When water content is reduced to 3 ~ 15% in the mixture of heat, the medicinal extract is added into mixture and continues heating stirring, until mixture
Middle steam is down to 2% or less stopping heating, and the fine powder is added into mixture and stirs evenly, is placed on non-woven rubberized fabric, obtains speed
Imitate plaster；
Wherein, step (1) and step (2) do not have sequencing.
The prescription of plaster is not particularly limited in the present invention, the prescription that plaster can be arbitrarily made in this field can be adopted
Plaster is made with method of the invention.Coarse fodder and fines in the present invention are saying well known to the skilled person.Slightly
Material refers to general root, stem and leaf etc. in prescription, and volume is big, quality is hard, containing cellulose is more.Fines refers in prescription
Valuable medicine and aromatic drug, resinous or volatile oil are more.Those skilled in the art can be with according to the Conventional wisdom in this field
Obviously judge the coarse fodder and fines classification in plaster prescription.If containing only coarse fodder in prescription or fines being one of,
Those skilled in the art can production method according to the present invention, corresponding the step of deleting wherein.If being contained only in prescription
Coarse fodder then deletes the step of accordingly making in step (2) and step (3) and fines is added, directly production medicinal extract, with honey and blueness
The mixture of bur oil mixes, and is placed on non-woven rubberized fabric.
In the present invention, after first smashing the coarse fodder in prescription, refluxing extraction is impregnated with ethyl alcohol, obtains medicinal extract after concentration.This
The powder particle diameter of invention coarse fodder is preferably in 1.0cm hereinafter, more preferably 0.2 ~ 0.5cm.Coarse fodder after smashing is soaked in ethanol
Steep refluxing extraction.In the present invention, the volumetric concentration of ethyl alcohol is preferably 70% ~ 85%, and more preferably 75% ~ 80%.In the present invention, reflux
The temperature of extraction is preferably 65 ~ 95 DEG C, and more preferably 70 ~ 85 DEG C.It can guarantee the active constituent in prescription drug at a temperature of this
It can be fully dissolved out, while the active constituent dissolved out is not easily decomposed in ethanol solution, largely retain recovery rate and medicine
Object activity.The extraction time of refluxing extraction of the present invention is preferably 2 ~ 6 hours, and more preferably 4 ~ 5 hours.Longer time returns
The active constituent dissolution rate increase that stream extracts in prescription coarse fodder is no longer obvious.The extracting solution of refluxing extraction is concentrated the present invention
Obtain medicinal extract.The present invention is not particularly limited condensing mode, preferably using heating concentration in the specific embodiment of the invention.Add
Hot temperature is preferably 50 ~ 65 DEG C, is more selected as 60 DEG C.When concentrate is concentrated into the 1/4 ~ 1/6 of original volume, medicinal extract is obtained.
The present invention crushes the fines in prescription, obtains fine powder.The present invention is not particularly limited the grinding particle size of fines,
It is preferred that the smashing partial size of the fines is 40 ~ 120 mesh, more preferably 60 ~ 80 mesh.The type of the fines can be expensive for Moschus etc.
Weight medicine or borneol, camphor, myrrh, olibanum etc. solubility or volatile medicinal material.
Honey and prinsepia utilis royle oil are carried out heating stirring by the present invention, the matrix as plaster can guarantee plaster humidity and
Transdermal absorption, bactericidal antiphlogistic shorten the onset time of plaster active drug ingredient, improve curative effect.Type of the present invention to honey
It is not particularly limited, Mel Jujubae, honey of lychee flowers are preferred, and rape honey takes second place.It is preferred with natural honey, commercially available honey in bottle is due to nothing
Method guarantees the purity of honey, should not use.The present invention is not particularly limited the source of prinsepia utilis royle oil, commercially available to buy or according to existing
There is the prepared prinsepia utilis royle oil of the conventional method in technology can be used in the present invention.Honey and prinsepia utilis royle oil in the present invention
Weight ratio be 5:2 ~ 3, can obtain having certain viscosity to be suitable for making the mixture of plaster substrate after agitated heating.This
In invention, the heating temperature of the honey and prinsepia utilis royle oil is 100 ~ 120 DEG C, and more preferably 105 ~ 115 DEG C, Bian Jiare is stirred on side
It mixes, keeps mixture heating temperature uniform.When water content is reduced to 3 ~ 15% in the mixture of heating, institute is added into mixture
It states medicinal extract (if without coarse fodder in prescription, omitting this step) and continues heating stirring, until steam is down to 2% or less and is stopped in mixture
Only heat.In the present invention, the preferably described medicinal extract is 1 ~ 3:10 with the weight ratio of the honey and prinsepia utilis royle oil mixture matrix.Stop
After only heating, when preferred mixture temperature is down to 45 ~ 65 DEG C, more preferably 50 ~ 60 DEG C, it is equal that fine powder stirring is added into mixture
It is even, if in prescription without fine fodder if omit this step.It is preferred that the weight ratio of fine powder and the honey and prinsepia utilis royle oil mixture matrix
For 3 ~ 5:10.The mixture for mixing prescription drug is placed on non-woven rubberized fabric, quick-acting plaster are obtained.
The plaster being prepared using the method for the invention is used honey and prinsepia utilis royle oil in plaster substrate, had
Active pharmaceutical ingredient in prescription can be rapidly entered skin by good percutaneous permeability, reach site of action, improve plaster
Onset time, achieve the effect that fast onset.Honey and prinsepia utilis royle oil are also able to maintain the wettability of skin, sterilize, disappear simultaneously
Inflammation while enhancing plaster drug effect, reduces plaster to the sensibility of skin, improves the safe range that plaster uses, sensitive skin quality
Or the delicate skin such as infant is equally applicable.Due to, without elevated process, greatly reducing prescription Chinese medicine in entire manufacturing process
Activity of the object ingredient in high temperature is lost, and improves the active pharmaceutical ingredient content in plaster, and then ensure that the treatment of plaster
Effect.
Below in conjunction with the embodiment in the present invention, technical solution in the embodiment of the present invention is carried out clearly and completely
Description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on this hair
Embodiment in bright, every other implementation obtained by those of ordinary skill in the art without making creative efforts
Example, shall fall within the protection scope of the present invention.
Below by taking analgesic in the prior art black plaster prescription as an example, illustrate what preparation method of the invention was prepared
Difference of the black plaster that plaster and conventional method obtain on onset time and therapeutic effect.
Analgesic black plaster prescription: Radix Aconiti 10g, Radix Aconiti Kusnezoffii 10g, scorpion 10g, centipede 10g, olibanum 10g, myrrh 10g,
Safflower 10g, dragon's blood 10g, pangolin 10g, lopseed 10g.
Embodiment 1:
The Radix Aconiti in prescription, Radix Aconiti Kusnezoffii, scorpion, centipede, safflower, pangolin, lopseed are smashed to partial size in proportion and existed
For 0.5cm hereinafter, being impregnated at 65 DEG C refluxing extraction 6 hours with 75% ethyl alcohol, obtained ethanol extract heats concentration at 80 DEG C
To the 1/6 of original volume, medicinal extract is obtained.
Olibanum, myrrh, the dragon's blood in prescription are crushed to 80 mesh in proportion, obtain fine powder.
500g honey is taken to mix with 300g prinsepia utilis royle oil, the heating stirring at 100 DEG C, when water content in the mixture of heating
When being reduced to 5%, 100g medicinal extract is added into mixture and continues heating stirring, until steam is down to 2% or less and is stopped in mixture
Heating.When mixture temperature is down to 65 DEG C, 100g fine powder is added into mixture and stirs evenly, is placed on non-woven rubberized fabric, obtains
To quick-acting plaster.
Embodiment 2
The Radix Aconiti in prescription, Radix Aconiti Kusnezoffii, scorpion, centipede, safflower, pangolin, lopseed are smashed to partial size in proportion and existed
0.3cm with 85% ethyl alcohol at 90 DEG C hereinafter, impregnated refluxing extraction 2.5 hours, obtained ethanol extract heats dense at 90 DEG C
It is reduced to the 1/4 of original volume, obtains medicinal extract.
Olibanum, myrrh, the dragon's blood in prescription are crushed to 60 mesh in proportion, obtain fine powder.
500g honey is taken to mix with 200g prinsepia utilis royle oil, the heating stirring at 110 DEG C, when water content in the mixture of heating
When being reduced to 10%, 150g medicinal extract is added into mixture and continues heating stirring, until steam is down to 2% or less and is stopped in mixture
Heating.When mixture temperature is down to 45 DEG C, 200g fine powder is added into mixture and stirs evenly, is placed on non-woven rubberized fabric, obtains
To quick-acting plaster.
Embodiment 3
The Radix Aconiti in prescription, Radix Aconiti Kusnezoffii, scorpion, centipede, safflower, pangolin, lopseed are smashed to partial size in proportion and existed
For 0.2cm hereinafter, being impregnated at 75 DEG C refluxing extraction 4 hours with 80% ethyl alcohol, obtained ethanol extract heats concentration at 80 DEG C
To the 1/5 of original volume, medicinal extract is obtained.
Olibanum, myrrh, the dragon's blood in prescription are crushed to 100 mesh in proportion, obtain fine powder.
500g honey is taken to mix with 100g prinsepia utilis royle oil, the heating stirring at 115 DEG C, when water content in the mixture of heating
When being reduced to 15%, 180g medicinal extract is added into mixture and continues heating stirring, until steam is down to 2% or less and is stopped in mixture
Heating.When mixture temperature is down to 50 DEG C, 250g fine powder is added into mixture and stirs evenly, is placed on non-woven rubberized fabric, obtains
To quick-acting plaster.
Comparative example 1
For embodiment 3, prinsepia utilis royle oil is not added during making quick-acting plaster, directly does base with 600g honey
Matter, production method is the same as embodiment 3.
Comparative example 2
Honey in embodiment 3 is substituted for rosin, other steps are same as Example 3.
Comparative example 3
Conventional black plaster preparation method (not using honey and prinsepia utilis royle oil as matrix)
4 liang of sesame oil, 3 liang of tung oil, 3 liang of cottonseed oil, 4 liang of yellow lead.Sesame oil, tung oil, cottonseed oil are poured into pot, 40-80 is heated to
After DEG C, Radix Aconiti, Radix Aconiti Kusnezoffii, scorpion, centipede, safflower, pangolin, lopseed are poured into oil and decocted, to pharmaceutical presentations in deep
Brown, inside are degree compared with yellow, and oil temperature about at 200-250 DEG C or so, is filtered from fire cooling.Then medicine oil is answered into pot, it is first small
High fire does not stop to stir after fire.After dropping into a bead, immediately by pot from fire, when oil being waited to be down to 200-250 degree or so, lower yellow lead is ceaselessly
Agitation.Old tender test is done within about 3-5 minutes after lower pellet, turning off stove cools down in place, and then by olibanum, myrrh, dragon's blood, fine powder, which is cooked, to be stirred
It is even.Then plaster is poured into and is got ready in cold water, impregnated 3-7 days, change 1-2 releasing fire-toxin of water daily, can be sticked and be collected.
The analgesic plaster prepared is affixed on affected part, changes within seven days a medicine.
Plaster prepared by embodiment 3, comparative example 1 ~ 3 is average respectively, and for treating pain patients, (cervical spondylosis, bruise are frustrated
Wound, arthralgia or strain wound), therapeutic effect is as follows:
The analgesic plaster effect of 1 distinct methods of table preparation
| Onset time | Analgesic time | Allergy rate | It is efficient | |
| Embodiment 3 | 2 ~ 5 minutes | In half an hour | 0 | 100% |
| Comparative example 1 | 30 ~ 60 minutes | 2 ~ 4 hours | 2% | 96% |
| Comparative example 2 | 20 ~ 45 minutes | 1 ~ 3 hour | 3% | 95% |
| Comparative example 3 | 2 ~ 5 hours | > 24 hours | 24% | 90% |
It can be seen from Table 1 that the plaster being prepared using method of the invention, since plaster substrate is using honey and green thorn
Fruit oil, plaster drug can fast strikethrough skin, reach site of action, can work in 2 ~ 5 minutes, analgesic is reached in half an hour
Effect, it is efficient higher, and without allergic phenomena.Only use honey as plaster substrate in comparative example 1, compared with embodiment 3 action when
Between and analgesic time it is long, effective percentage is declined, and has fraction people allergic phenomena occur.Comparative example 2 is in the mistake for preparing plaster
Honey is replaced with into rosin in journey, the honey of effect and comparative example 1 is slightly poor, but difference is not obvious.Comparative example 3 is conventional method
The black plaster being prepared.Due to using high temperature in preparation process, effect of drugs is poor.Be added in preparation process yellow lead at
Point, and that added with the medicament conducive to Medicated Permeation, the long action time of plaster does not work slow, it is larger to the irritation of skin,
The people that allergic phenomena occurs in skin is more, erious adverse reaction.
Above embodiment, which is intended to illustrate the present invention, to be realized or use for professional and technical personnel in the field, to above-mentioned
Embodiment, which is modified, will be readily apparent to those skilled in the art, therefore the present invention includes but is not limited to
Above embodiment, it is any to meet the claims or specification description, meet with principles disclosed herein and novelty,
The method of inventive features, technique, product, fall within the scope of protection of the present invention.
Claims (9)
1. a kind of preparation method of quick-acting plaster, comprising the following steps:
After coarse fodder in prescription is smashed, refluxing extraction is impregnated with ethyl alcohol, obtains medicinal extract after concentration；
Fines in prescription is crushed, fine powder is obtained；
5 parts by weight honey heating stirring in the prinsepia utilis royle oil of 2 ~ 3 parts by weight is taken, heating temperature is 100 ~ 120 DEG C, when heating
When water content is reduced to 3 ~ 15% in mixture, the medicinal extract is added into mixture and continues heating stirring, until water in mixture
Vapour is down to 2% or less stopping heating, and the fine powder is added into mixture and stirs evenly, is placed on non-woven rubberized fabric, obtains instant effecting ointment
Medicine；
Wherein, step (1) and step (2) do not have sequencing.
2. preparation method according to claim 1, which is characterized in that the coarse fodder is crushed to partial size less than 1.0cm.
3. preparation method according to claim 1, which is characterized in that the volumetric concentration of step (1) described ethyl alcohol 70% ~
Between 85%.
4. preparation method according to claim 1 or 3, which is characterized in that the temperature of step (1) described refluxing extraction is 65
~ 95 DEG C, extraction time is 2 ~ 6 hours.
5. preparation method according to claim 1, which is characterized in that step (1) concentration is heating concentration, is concentrated to give
The medicinal extract arrived is the 1/4 ~ 1/6 of original volume.
6. preparation method according to claim 1, which is characterized in that the smashing partial size of the fines is 40 ~ 120 mesh.
7. preparation method according to claim 1, which is characterized in that step (3) fine powder be added when, mixture
Temperature is 45 DEG C ~ 65 DEG C.
8. preparation method according to claim 1, which is characterized in that step (3) medicinal extract and the honey and green thorn
The weight ratio of fruit oil total weight is 1 ~ 3:10.
9. preparation method according to claim 1, which is characterized in that step (3) fine powder and the honey and green thorn
The weight ratio of fruit oil total weight is 1 ~ 5:10.
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| CN201910208914.XA CN109700909A (en) | 2019-03-19 | 2019-03-19 | A kind of preparation method of quick-acting plaster |
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Application publication date: 20190503 |