CN109646361A - A kind of pet complex biological deodorization spray agent and preparation method thereof - Google Patents
A kind of pet complex biological deodorization spray agent and preparation method thereof Download PDFInfo
- Publication number
- CN109646361A CN109646361A CN201910143893.8A CN201910143893A CN109646361A CN 109646361 A CN109646361 A CN 109646361A CN 201910143893 A CN201910143893 A CN 201910143893A CN 109646361 A CN109646361 A CN 109646361A
- Authority
- CN
- China
- Prior art keywords
- spray agent
- extract
- deodorization spray
- pet
- complex biological
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
Abstract
The present invention relates to it is a kind of suitable for solve dog cat halitosis, body odor, it is just smelly the problems such as pet complex biological deodorization spray agent and preparation method thereof, the deodorization spray agent each component includes yucca extract 5-8% by percentage to the quality, green-tea extract 4-5%, wild marjoram oil extract 6-8%, persimmon extract 4-5%, horseradish extract 4-5%, zinc ricinate 3-4%, emulsifier 5-6%, stabilizer 1-2%, pH adjusting agent 1-2%, surplus are purified water.Deodorization spray agent of the present invention eventually passes through deodorizing effect verifying, confirm that its deodoriging properties is fine, the common foul smell molecule of a variety of pets such as ammonia, hydrogen sulfide, methyl mercaptan, methyl sulfide, dimethyl disulfide can be quickly eliminated in 5 minutes, it can also effectively inhibit and kill pathogenic microorganism simultaneously, the generation of stink can be inhibited from root.
Description
Technical field
The present invention relates to a kind of deodorant, and in particular to a kind of pet complex biological deodorization spray agent and its preparation side
Method.
Background technique
The stink that halitosis, body odor and the excreta fermentation of pet generate is the trouble of each pet fan.Foul smell
Ingredient multiplicity is complicated, so removal difficulty is high, and high concentration foul smell not only influences the quality of the life of pet owner, can also be great
Influence the health of pet and pet owner, for example influence respiratory system, immune system, digestive system, mucous membrane health etc..
The generation of foul smell is largely the growth due to spoilage organisms, has decomposed the carbon in pet fecaluria, in oral cavity, on skin
The organic matters such as hydrate, protein and fat, to supervene the foul smell molecule such as ammonia, hydrogen sulfide, thio-alcohol.So
The key of radical cure foul smell is putrefactivebacterias and the viruses such as killing harmful microorganism, while adsorbing the foul smell in dissolved air again, and
These foul smell molecules are decomposed by biological enzyme and catalyst, to achieve the purpose that eradicate deodorization.
Deodorant type in the market is of all shapes and colors, mainly has physics shielded type deodorant, chemical deodorizing agent, enzyme preparation to remove
Smelly dose, galenical deodorizer, microbiocidal deodorant.These deodorizing methodss all cut both ways, wherein physics shielded type deodorant
It is in the majority, it is main to have the function that cover stink by substances such as essence, and the smell of pet is very sensitive, it is smelly to cover its with perfume
Taste is not permanent and wise method, therefore deodorizing effect is only temporary, and can only treat the symptoms cannot effect a permanent cure, and can only temporarily be covered, no
It can remove and maintain for a long time；Second class is mainly made with chlorine dioxide, hypochlorite, ferrous sulfate etc. for the chemical deodorizing agent of representative
With being exactly oxidation disinfection, deodorization mechanism is predominantly to the desulfurization of odor molecules, oxidation, condensation and addition reaction etc., these sterilizations
Product bactericidal effect is strong, has eradicated putrefactivebacteria, has rooted out the root for generating foul smell, thus the work as deodorant of auxiliary
With, it can effect a permanent cure, but original foul smell cannot remove quickly in air, therefore it is to effect a permanent cure treat the symptoms, while its safety
Property is also very poor；Galenical deodorizer refers to the root from plant, stem, leaf or spends the extract liquor of the oil of middle extraction, juice or medicinal extract by one
Fixed formula compounds, and effective molecule contains chemical activity, bioactivity and conjugated double bond isoreactivity base in plant extracts
Group can react such as acid-base reaction, catalytic oxidation, Lewis Acids and Bases reaction and oxidation also from different smell substances
Original reaction etc., promotes odorant to change original molecular structure, nontoxic, tasteless small molecule is resolved into, to reach deodorization
Purpose can only work to part foul smell molecule, while high expensive if its independent role deodorizing effect is limited；Microorganism removes
Smelly dose using screening obtain deodorizing microorganism construct composite bacteria agent, to some malodor sources being made of perishable organic substance have compared with
Good control action, effect is unobvious in deodorization is likely due to microorganism and can only eliminate one or more of stench chemical combination
Object, if the these types of compound and stench intensity dependence eliminated are very poor, the deodorizing effect of these microbial inoculums will be unobvious.
A kind of pet disinfection is disclosed in Chinese invention patent application CN105724439A disclosed on July 6th, 2016
Bactericidal deodorant, the deodorant include dioctadecyl dimethyl ammonium chloride, double-track suspended self-propelled conveyor, benzalkonium bromide, penta
Dialdehyde, pure plant extracting solution, plants essential oil, distilled water.The deodorant sterilizing deodorizing significant effect, is sprayed on pet cage
Tool, urine, at excrement, or the position aerial spraying to sterilizing deodorizing is needed, the work that disinfection and sterilization can be played, eliminate peculiar smell
With.But the sterilization of the deodorant is because added with chemical disinfection ingredient, secure context cannot be guaranteed, together
When also need dilute after use, so causing inconvenient to use.
Pet deodorizer agent is disclosed in Chinese invention patent application CN108245449A disclosed on July 6th, 2018, it should
Deodorant contains acetic acid linalool, citronellol, benzyl carbinol, parachlorometaxylenol, lauryl methacrylate, cinnamomum camphora extraction
Liquid, polysorbate, citric acid, essence, alcohol, deionized water.The deodorant can be directly sprayed into pet, and deodorizing effect is aobvious
It writes, the duration is long, has biocidal efficacies.But the preparation process of the deodorant is more complicated, leads to that the production cost increases.
In view of the above-mentioned problems, the present invention is specifically proposed.
Summary of the invention
The present invention provides a kind of pet complex biological deodorization spray agents and preparation method thereof, solve market pet and remove
Smelly product deodorizing effect is poor, it is palliative, without bactericidal effect, safety is poor, endanger environment, be at high cost the problems such as, improve
Deodorizing effect improves safety, while cost is also low, is suitable for marketing.
To achieve the above object, the invention provides the following technical scheme:
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality, including yucca extract 5-
8%, green-tea extract 4-5%, wild marjoram oil extract 6-8%, persimmon extract 4-5%, horseradish extract 4-5%, castor oil
Sour zinc 3-4%, emulsifier 5-6%, stabilizer 1-2%, pH adjusting agent 1-2%, surplus are purified water.
Preferably, the yucca extract includes saponin, polysaccharide and polyphenol, and wherein saponin content is 10-12%, and polysaccharide contains
Amount is 10-12%, polyphenol content 15-17%.
It preferably, include tea polyphenols in the green-tea extract, wherein the content of tea polyphenols is 20-25%.
It preferably, include Thymol, poly- phenol, perfume Jing Qin phenol, wherein Thymol content in the wild marjoram oil extract
For 10-11%, poly- phenol content be 7-8%, perfume Jing Qin phenol content is 8-10%.
It preferably, include persimmon tannin in the persimmon extract, wherein persimmon tannin content is 15-18%.
Preferably, the horseradish extract includes horseradish peroxidase, and wherein horseradish peroxidase content is 7-
10%.
Preferably, the zinc ricinate is liquid, active constituent content 30-35%.
Preferably, the emulsifier is the mixture of Tween-80, Span-80, and the two proportion is Tween-80:Span-
80=6:4.
Preferably, the stabilizer is the mixture of acetate buffer, lysozyme and glycerol, and the pH adjusting agent is
Citric acid or lactic acid or combinations thereof.
A method of preparing above-mentioned pet complex biological deodorization spray agent, comprising the following steps:
Step 1, a certain amount of purified water is first taken, then sequentially adds yucca extract, green-tea extract, persimmon according to the ratio
Extract, zinc ricinate, stirring dissolves it successively to get solution A after addition；
Step 2, emulsifier is weighed, sequentially adds wild marjoram oil extract, horseradish peroxidase, stabilizer, stirring makes it
Dissolution, up to solution B；
Step 3, solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed
It is 3000-4000 revs/min, mixing time 15-20min obtains the uniform light yellow transparent liquid of color；
Step 4, it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, is finally added
Purified water is to prescribed volume to get deodorization spray agent.
Compared with prior art, beneficial effects of the present invention are as follows:
1, deodorization spray agent of the invention to pet halitosis, body odor, just the malodor molecules in a variety of sources such as smelly all have preferably
Deodorization properties.The main component of these stinks is ammonia, hydrogen sulfide, methyl mercaptan, trimethylamine etc., in deodorization spray agent of the invention
Contained a variety of deodorization ingredients can effectively remove a variety of stinks by a variety of different mechanisms of action such as capture, absorption, decomposition
Molecule is obviously improved odor removal efficient.
2, deodorization spray agent of the invention has sterilization idiocratic, can remove stink from the root.Deodorization spray agent of the invention
Phenolic compound in contained various plants extract all has apparent antibacterial, sterilization, anti-oxidant and antisepsis.
3, deodorization spray agent of the invention be swift in response, odor removal efficient it is high.Deodorization spray agent of the invention can treat the symptoms and effect a permanent cure
Fast deodorization kills bacterium and eliminates virus, and by spray-on process, contained effective component is atomized, the half of space diffusion drop
Diameter≤0.04mm, drop have very big specific surface area, average every mole about tens kilocalories, molten with very big surface energy
The surface of liquid can greatly can not only effectively in absorption air odor molecules, while can also make the solid for the odor molecules being adsorbed
Configuration changes, and weakens the chemical combination key in odor molecules, so that the unstability of odor molecules increases, is easy and other points
Acidic buffer in son and vegetation water chemically reacts, and ultimately produces tasteless, nontoxic substance, eliminates pet in 5 minutes
The stenches such as soiled litter, inhibit mosquitos and flies oviposition, and environment purification reduces disease.
4, deodorization spray agent good deodorization effect of the invention, duration are long.Deodorization spray agent of the invention can be from the root
Inhibit the generation of stink, the deodorization duration is long, and deodorizing effect can maintain 72h or more.
5, deodorization spray agent of the invention is a safe and environment-friendly green product.Selected by deodorization spray agent of the invention
All be nontoxic, harmless, non-stimulated raw material, not ingredients such as spirituosity, essence, can safety for oral deodorizing, body deodorization,
Fecal deodorizing etc., to people, pet and environment all without any harm, can safe and securely for the oral environment of pet, excrement,
The sterilizing deodorizing of abnormal smell of body, cage, bowl, pet hair etc..This product is non-corrosive simultaneously, and non-oxidative can subtract
Light disinfectant, chemical agent etc. endanger pet health, build ecological, nontoxic, faint scent growing environment for humans and animals.
6, deodorization spray agent stability of the invention is strong.Emulsifier contained by deodorization spray agent of the invention, stabilizer can make to match
All components in side can keep dissolved state, and it is stronger not occur characters, the product stability such as layering, precipitating, muddiness.
7, deodorization spray agent product of the invention is easy to use.The sterilization component of the deodorization spray agent be mainly plant extract at
Point, so the deodorization spray agent is not required to dilute, use can be directly sprayed, is used convenient for pet owner and pet doctor.
8, the cost of deodorization spray agent of the invention is low.The deodorization spray agent is plant type deodorization spray agent and biological enzyme type deodorization spray
The combination of agent, while preparation method is simple, cost is relatively low, is suitable for marketing.
9, deodorization spray agent of the invention has a wide range of application.It is smelly that the deodorization spray agent can not only eliminate the various peculiar smell in air
Taste, moreover it is possible to eliminate the peculiar smell that in pet's oral cavity and body generates, while can also restraining and sterilizing bacteria, so the deodorization spray agent applies model
It encloses wider.
Specific embodiment
Below in conjunction with the specific embodiment of the invention, technical solution of the present invention is clearly and completely described, is shown
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Pet of the invention is with yucca extract, green-tea extract, wild marjoram oil extract with complex biological deodorization spray agent
Object, persimmon extract, horseradish extract, zinc ricinate are main active, are aided with emulsifier, stabilizer, and pH value is adjusted
Agent etc., a kind of stabilization being prepared by scientific composition, deodorization and sterilization synchronous high-efficiency, nonirritant, safety easy to use is green
The new type compound biological deodorizing spray of color.Emulsifier is the mixture of Tween-80, Span-80, and the two proportion is Tween-
80:Span-80=6:4, stabilizer are the mixture of acetate buffer, lysozyme and glycerol, and pH adjusting agent is citric acid
Or lactic acid or combinations thereof.
Yucca extract includes saponin, polysaccharide and polyphenol, and wherein saponin content is 10-12%, polyoses content 10-
12%, polyphenol content 15-17%, B50 value < 4mg, B50 value is for measuring rare treasure category yucca extract combination ammonia ability
, the quantity of the rare treasure category yucca extract in conjunction with required for 50% ammonia is measured, the lower this numerical value the better.Yucca is extracted
The foul smell molecules such as ammonia, the hydrogen sulfide that the yucconin in object effectively can combine pet excrement to generate, while it or one kind
Urease inhibitor can effectively inhibit the generation of ammonia from source；Polysaccharide component and ammonia in yucca extract have very strong
Affinity, it is easy to it is in combination, to inhibit the illeffects of ammonia and it is converted into harmless nitride；Yucca extract
In polyphenol have stronger inoxidizability and remove free radical ability.
Green-tea extract includes tea polyphenols, and wherein the content of tea polyphenols is 20-25%, the tea polyphenols pair in green-tea extract
Stink odor methyl mercaptan (the CH that oral microorganism generates3SH) there is good elimination effect.Wild marjoram oil extract includes in hundred
Fragrant phenol, poly- phenol, perfume Jing Qin phenol, wherein Thymol content is 10-11%, poly- phenol content is 7-8%, perfume Jing Qin phenol content is 8-
10%.Persimmon extract includes persimmon tannin, and wherein persimmon tannin content is 15-18%, the persimmon tannin in persimmon extract
Be a kind of polyphenols, with good antioxidant activity, there is stronger deodorizing performance, to trimethylamine deodorizing performance compared with
By force.And Thymol contained in wild marjoram oil extract, poly- phenol, perfume Jing Qin phenol etc., the polyhydric phenols structure energy in persimmon tannin
It reacts with protein, polysaccharide and alkaloid etc., so that its physical and chemical behavior is changed, so having in terms of Antimicrobial
Its unique advantage.
Horseradish extract includes horseradish peroxidase, and wherein horseradish peroxidase content is 7-10%, and horseradish extracts
Horseradish peroxidase in object has removal effect to 12 kinds of odor causing substances, and horseradish peroxidase can completely remove phenols
Odorant, deodorizing effect can maintain 72h or more, and horseradish peroxidase also has volatile fatty acid and preferably goes
Except effect.Zinc ricinate is liquid, active constituent content 30-35%, and zinc ricinate great advantage is through skin, mouth
And the absorption toxicity of respiratory tract is low, safe and reliable, it can effectively eliminate main stink odor ammonia, hydrogen sulfide and organic
Sulfide, it will be apparent that reduce odor strength.The preparation method of deodorization spray agent of the invention the following steps are included:
Step 1, a certain amount of purified water is first taken, then sequentially adds yucca extract, green-tea extract, persimmon according to the ratio
Extract, zinc ricinate, stirring dissolves it successively to get solution A after addition；
Step 2, emulsifier is weighed, sequentially adds wild marjoram oil extract, horseradish peroxidase, stabilizer, stirring makes it
Dissolution, up to solution B；
Step 3, solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed
It is 3000-4000 revs/min, mixing time 15-20min obtains the uniform light yellow transparent liquid of color；
Step 4, it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, is finally added
Purified water is to prescribed volume to get deodorization spray agent.
The deodorization spray agent good deodorization effect that is prepared by above-mentioned preparation method, duration are long, and character is stablized.In order into one
Step understands the present invention, below with reference to embodiment to pet provided by the invention complex biological deodorization spray agent and preparation method thereof
It is specifically described.
Embodiment 1
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality:
Preparation method, comprising the following steps:
(1) a certain amount of purified water is first taken, yucca extract, green-tea extract, persimmon extract, castor oil are sequentially added
Sour zinc, stirring dissolves it successively stand-by to get solution A after addition；
(2) emulsifier is weighed again, sequentially adds following raw material: wild marjoram oil extract, horseradish peroxidase, stabilizer,
And stir that dissolve it successively stand-by to get solution B；
(3) solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
3000 revs/min, mixing time 20min, obtain the uniform light yellow transparent liquid of color；
(4) it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water to 1L to get deodorization spray agent.
Embodiment 2
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality:
Preparation method, comprising the following steps:
(1) a certain amount of purified water is first taken, yucca extract, green-tea extract, persimmon extract, castor oil are sequentially added
Sour zinc, stirring dissolves it successively stand-by to get solution A after addition；
(2) emulsifier is weighed again, sequentially adds following raw material: wild marjoram oil extract, horseradish peroxidase, stabilizer,
And stir that dissolve it successively stand-by to get solution B；
(3) solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
4000 revs/min, mixing time 15min, obtain the uniform light yellow transparent liquid of color；
(4) it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water to 1L to get deodorization spray agent.
Embodiment 3
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality:
Preparation method, comprising the following steps:
(1) a certain amount of purified water is first taken, yucca extract, green-tea extract, persimmon extract, castor oil are sequentially added
Sour zinc, stirring dissolves it successively stand-by to get solution A after addition；
(2) emulsifier is weighed again, sequentially adds following raw material: wild marjoram oil extract, horseradish peroxidase, stabilizer,
And stir that dissolve it successively stand-by to get solution B；
(3) solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
3500 revs/min, mixing time 20min, obtain the uniform light yellow transparent liquid of color；
(4) it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water to 1L to get deodorization spray agent.
Embodiment 4
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality:
Preparation method, comprising the following steps:
(1) a certain amount of purified water is first taken, yucca extract, green-tea extract, persimmon extract, castor oil are sequentially added
Sour zinc, stirring dissolves it successively stand-by to get solution A after addition；
(2) emulsifier is weighed again, sequentially adds following raw material: wild marjoram oil extract, horseradish peroxidase, stabilizer,
And stir that dissolve it successively stand-by to get solution B；
(3) solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
4000 revs/min, mixing time 20min, obtain the uniform light yellow transparent liquid of color；
(4) it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water to 1L to get deodorization spray agent.
Embodiment 5
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality:
Preparation method, comprising the following steps:
(1) a certain amount of purified water is first taken, yucca extract, green-tea extract, persimmon extract, castor oil are sequentially added
Sour zinc, stirring dissolves it successively stand-by to get solution A after addition；
(2) emulsifier is weighed again, sequentially adds following raw material: wild marjoram oil extract, horseradish peroxidase, stabilizer,
And stir that dissolve it successively stand-by to get solution B；
(3) solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
3300 revs/min, mixing time 20min, obtain the uniform light yellow transparent liquid of color；
(4) it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water to 1L to get deodorization spray agent.
Embodiment 6
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality:
Preparation method, comprising the following steps:
(1) a certain amount of purified water is first taken, yucca extract, green-tea extract, persimmon extract, castor oil are sequentially added
Sour zinc, stirring dissolves it successively stand-by to get solution A after addition；
(2) emulsifier is weighed again, sequentially adds following raw material: wild marjoram oil extract, horseradish peroxidase, stabilizer,
And stir that dissolve it successively stand-by to get solution B；
(3) solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
3800 revs/min, mixing time 17min, obtain the uniform light yellow transparent liquid of color；
(4) it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water to 1L to get deodorization spray agent.
Embodiment 7
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality:
Preparation method, comprising the following steps:
(1) a certain amount of purified water is first taken, yucca extract, green-tea extract, persimmon extract, castor oil are sequentially added
Sour zinc, stirring dissolves it successively stand-by to get solution A after addition；
(2) emulsifier is weighed again, sequentially adds following raw material: wild marjoram oil extract, horseradish peroxidase, stabilizer,
And stir that dissolve it successively stand-by to get solution B；
(3) solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
3500 revs/min, mixing time 18min, obtain the uniform light yellow transparent liquid of color；
(4) it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water to 1L to get deodorization spray agent.
Embodiment 8
A kind of pet complex biological deodorization spray agent, each component by percentage to the quality:
Preparation method, comprising the following steps:
(1) a certain amount of purified water is first taken, yucca extract, green-tea extract, persimmon extract, castor oil are sequentially added
Sour zinc, stirring dissolves it successively stand-by to get solution A after addition；
(2) emulsifier is weighed again, sequentially adds following raw material: wild marjoram oil extract, horseradish peroxidase, stabilizer,
And stir that dissolve it successively stand-by to get solution B；
(3) solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
3000 revs/min, mixing time 15min, obtain the uniform light yellow transparent liquid of color；
(4) it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water to 1L to get deodorization spray agent.
Test example 1
The visual examination of deodorization spray agent is tested, and checks the appearance of deodorization spray agent, if uniformly, whether there is or not layering or precipitatings.
The no less than original of 500ml is taken after the deodorization spray agent of 1~embodiment of embodiment 8 is sufficiently shaken up in original packing container
Liquid therefrom takes 100ml deodorization spray agent stoste to be put in 100ml tool plug graduated cylinder, after placing for 24 hours at 15~35 DEG C, according to " China
People's republic's veterinary drug allusion quotation " liquid appearance check criteria, observe the appearance of deodorization spray agent stoste.
The visual examination test result of deodorization spray agent is as shown in table 1, seen from table 1,1~embodiment of embodiment, 8 deodorization spray
The appearance character of agent meets the visual examination standard of liquid uniformly and without layering and precipitating.
The visual examination result of the different Example formulations of table 1
Test example 2
The pH value of deodorization spray agent investigates test, detects the pH value of deodorization spray agent stoste.
A certain amount of deodorization spray agent is taken after the deodorization spray agent of 1~embodiment of embodiment 8 is sufficiently shaken up in original packing container
Stoste with the pH value of pH meter test deodorization spray agent stoste, is accurate to 0.1pH unit, tries at room temperature (25 DEG C ± 2 DEG C)
Test that the results are shown in Table 2, as can be seen from Table 2, the pH of the deodorization spray agent stoste of 1~embodiment of embodiment 8 is between 6.5~7.5,
It is neutrality, use is safe, and it is non-corrosive, oral cavity, body, environment sprinkling can be used safely in.
The pH value testing result of the different Example formulations of table 2
Test example 3
The high and low temperature stability test of deodorization spray agent is seen whether by deodorization spray agent sample after high temperature, low-temperature treatment
There is phenomena such as layering and precipitating.
The test method of thimble test is that deodorization spray agent is poured into 50ml tool plug graduated cylinder to 50ml scale, after jumping a queue
It being put into 60 ± 2 DEG C of water bath with thermostatic control, the water surface should be higher than that scale 20mm, after 6h, take out, it is to be restored to observe appearance to after room temperature,
The results are shown in Table 3.
Low-temperature stability test test method will through the unconverted sample of hot test (new sample need to separately be taken by such as changing),
It is put into -5 ± 2 DEG C of refrigerators and keeps 2h, take out, to its spontaneous recovery to room temperature, observe appearance, the results are shown in Table 3.
Seen from table 3, the deodorization spray agent sample of 1~embodiment of embodiment 8 character under high temperature and cryogenic conditions it is stable,
Uniformly, not stratified, and nodeless mesh or Precipitation.
The high and low temperature stability change test result of the different Example formulations of table 3
Test example 4
The deodorizing effect testing experiment of deodorization spray agent is come by the deodorizing effect to the common several foul smell molecules of pet
Evaluate the deodorizing effect of each deodorization spray agent formula of 1~embodiment of embodiment 8.
Test reagent used in the deodorizing effect testing experiment of deodorization spray agent be ammonium hydroxide, hydrogen sulfide, methyl mercaptan, methyl sulfide,
Dimethyl disulfide.Test apparatus used in the deodorizing effect testing experiment of deodorization spray agent be ammonia, hydrogen sulfide gas detection pipe,
HP5840A gas chromatograph, 5.5L vial, syringe.
1, foul smell instrumental method
The ammonia, hydrogen sulfide and 3 kinds of organic sulfur compounds for preparing various concentration respectively in 5.5L vial, are absorbed with boric acid
Fixed ammonia assessment deodorizing effect, with headspace gas chromatography assessment deodorization spray agent to hydrogen sulfide, methyl mercaptan, methyl sulfide, diformazan
Disulfide dispels effect.GC conditions: column DB-1,40 DEG C of column temperature, 250 DEG C of verifier, carries ammonia by 170 DEG C of injector temperature
The gases such as gas (60ml/min), using hydrogen as fuel, pressure 1kg/cm2, air-breathing, pressure 1.5kg/cm2.Weigh 0.01g sample
Product are dissolved in the ml headspace bottle of 1ml water, and a certain amount of odorous substance is injected in sealing, and indwelling 1h draws 1ml static headspace gas sample introduction.Measurement is made
With the concentration of gas each before and after 1h, its elimination factor is calculated, tests while doing blank control group (purified water).
As shown in table 4 to the deodorizing effect of single foul smell molecule, as shown in Table 4, deodorization spray agent of the invention can effectively, fastly
Removal ammonia, hydrogen sulfide, methyl mercaptan, methyl sulfide, the foul smell such as dimethyl disulfide of speed, make the elimination of this 5 kinds single foul smell molecules
Rate is attained by 85% or more.
The different Example formulations of table 4 are to 5 kinds of individual deodorizing effects of foul smell
2, Olfactive evaluation method
The mixed gas that ammonia, hydrogen sulfide, methyl mercaptan, methyl sulfide and dimethyl disulfide are prepared in bottle, with six grades of foul smell
Intensity representation (is shown in Table 5), engages 5 trained and qualified odor strengths smelt the person of distinguishing and measure elimination front and back, asks it average
Value, while calculating its elimination factor.
5 kinds of foul smell are mixed, the deodorization of Artificial Olfactory evaluation assessment assessment 1~embodiment of the embodiment of the present invention 8 is passed through
The deodorizing effect of spray, using purified water as control experiment, the results are shown in Table 6, as can be seen from Table 6, this deodorization spray agent
Deodorizing effect is splendid, can also reach 85% or more for the elimination factor ratio of compound foul smell molecule.
Foul smell degree table of the table 5 according to smell
The different Example formulations of table 6 mix the deodorizing effect table of foul smell to 5 kinds
Test example 5
The security test of deodorization spray agent is tested, and is tried by acute toxicity test, subacute toxicity test, dermal toxicity
It tests, animal eyes combination film irritant test, human skin local stimulation test, to evaluate each deodorization spray agent of 1~embodiment of embodiment 8
The safety of formula.
1, test material and subjects
Test material: acute toxicity test is mixed with cod-liver oil (vitamin A containing 1500U, 500U vitamin D/g) deodorization spray agent
Suspension；Mixed fodder of the subacute test containing 0.5% deodorization spray agent；The glycerol of 25% deodorization spray agent of skin toxicology test
Suspension；The cod-liver oil suspension of 5% deodorization spray agent of eye conjunctiva irritant test；Human skin irritant test is sprayed with 15% deodorization
Agent vaseline mixture.
Subjects: acute toxicity test is with wistar female rats 40, and subacute toxicity test is with wistar rat
40 (male, female fifty-fifty), dermal toxicity and irritant test are with Female guinea pigs 15, and eye conjunctiva irritant test is with cavy, rabbit
Each 10, human skin local stimulation test asks between twenty and fifty each 5 participation of healthy men and women.
2, acute toxicity test
According to the deodorization spray agent of gastric infusion 6.8g/kg and 8g/kg embodiment 1 in trial test, animal all deposit by work.It will examination
It tests dosage and is set to 9.0g/kg deodorization spray agent, i.e. 5~8mL cod-liver oil suspension.Control-animal gives equivalent cod-liver oil.Prohibit before test
Ate for 1 night, perfusion in the 2nd day, later, observe animal ordinary circumstance and it is living deposit situation, animal broken end work was killed in the 8th day, take lung,
Liver, kidney, observe histomorphological changes under an optical microscope.It lives after killing animal, lung, the heart, liver, kidney and blood is taken (to divide immediately
From serum) it is respectively put into the beaker of 25ml, addition nitric acid 5ml, perchloric acid 2ml, after nitrification, use atomic absorption spectrometry
Zn content.
During test, 9.0g/kg weight stomach-filling experimental group and control rats each 20, none is dead, it is possible thereby to agree
Its fixed LD50It is worth (median lethal dose) far away from 9.0g/kg or more, since gastric capacity is limited, it is difficult to obtain LD50Specific value.
Experimental group and control animals breathe after stomach-filling all to be accelerated than originally, did not liked activity, continued 1 day or so, herein
Period appetite is declined.After a week, experimental group weight increases to 216.3g by the average 178.4g before testing, average to increase
21.2%；Control group increases to 217.8g by the 182.6g before testing, and averagely increases by 19.3%, two groups of statistical procedures without significant
Difference, see Table 7 for details.
Histomorphological liver cell, sinusoid, sinusoid wall, cortex, the medullary substance of kidney；Alveolar wall of lungs etc. is not
See that specific pathologies change.
After a week, animal main organs and serum Zn content are substantially close, and statistical procedures are without marked difference, explanation for stomach-filling
No zinc accumulation, see Table 8 for details.
The acute toxicity tests of 2~embodiment of embodiment 8 are identical as the acute toxicity tests of embodiment 1, this
It is no longer repeated at place.
7 acute toxicity test the weight of animals situation of change (g) of table
N=20
Zn content (ug/g) in 8 acute toxicity test internal organs of table and serum
N=10 (m ± SD) * unit umol/L
3, subacute toxicity test
Experimental animal is randomly divided into two groups of experiment and control, is raised in 4 cages respectively.Experimental animal, which is fed, contains 0.5%
The normal diet of 1 deodorization spray agent of embodiment, control feed normal diet, arbitrarily drink water.Monthly claim a weight, is used after 3 months
2.2% yellow Jackets intraperitoneal injection of anesthesia (1m1 or so) abdominal incision, abdomen active, take lung, liver, nephridial tissue at venesection,
A part does routine pathology inspection, observes histomorphological changes, separately takes a part for zinc-content determination in tissue.
During the experiment of 90d, two groups of animals all deposit by work, and weight gain, the results are shown in Table 9, can be seen by table 9
Out, experimental group weight gain in 3 months 96.9%, control group weight gain 87.2%, two groups without significant difference.
Histomorphological liver cell, sinusoid, sinusoid wall, cortex, the medullary substance of kidney；Alveolar wall of lungs etc. is not
See that specific pathologies change.Histomorphological is the result shows that experimental group and control group compare lung, liver, renal pathology change
Without significant difference.
The results are shown in Table 10 for subacute toxicity test animal main organs zinc-content determination, as shown in Table 10, animal
Main organs Zn content is substantially close, and statistical procedures illustrate no zinc accumulation without marked difference.
The subacute toxicity test result phase of the subacute toxicity test result of 2~embodiment of embodiment 8 and embodiment 1
Together, it is no longer repeated herein.
9 subacute toxicity test animal situation of change of table
N=40 (M ± SD) P > 0.5
Zn content (ug/g) in 10 experimental animal main organs of table
N=10 (M ± SD) P > 0.2
4, skin toxicology test
Cavy is cut short back before test to become mildewed, coats depilatory agent (10% vulcanized sodium and Arabic gum are made into), 5-7min
Shaving afterwards is observed for 24 hours after flushing, is selected without obvious red and swollen and skin injury cavy as subjects.Just with guinea pig back
Middle line is boundary, and two sides are respectively trial zone and check plot, respectively about 6cm2, trial zone applies the deodorization spray agent of 25% embodiment 1 formula
Glycerol (1:1 aqua) is applied 1 time, continuous 5d daily with covering skin and undercoat as degree.Control applies 50% glycerol aqua, sees day by day
Examining epidermis, whether there is or not red and swollen spots etc..Broken end work in 6th day is killed, and is taken two area's skin normal dyeings respectively, is seen under an optical microscope
Examine histomorphological changes.
Embodiment 1 be formulated deodorization spray agent coating after 5d's observation indicate that, trial zone and check plot skin surface are equal
It there are no any apparent irritation and red, swollen, spot equivalent damage.Two groups of animal skins of light microscopic undertissue morphological observation
Belong to normal skin.
The skin toxicology test result of 2~embodiment of embodiment 8 and the skin toxicology test result of embodiment 1 are identical, this
It is no longer repeated at place.
5, animal eyes combination film irritant test
It drips the deodorization spray agent cod-liver oil suspension 2 that 5% embodiment 1 is formulated to rabbit or cavy left eye to drip, right eye only drips fish
Liver oil 2 drips, after drop immediately, 10min, 30min, l h and 4h observation eye conjunctiva whether there is or not it is congested, shed tears situations such as.
Embodiment 1 be formulated deodorization spray agent through animal eyes combination film irritant test the result shows that, have 2 medication eyes in rabbit
With 1 control eye, there is slight mucous hyperemia in 30min after putting medicine, restore normal immediately, is showed no after cavy eyespot medicine obvious
Stimulate the reaction.
The animal eyes combination film irritant test result of 2~embodiment of embodiment 8 film in conjunction with the animal eyes of embodiment 1 stimulates
Test result is essentially identical, and it is no longer repeated herein.
6, human skin local stimulation test
The petroleum jelly cream for preparing the formula deodorization spray agent containing 15% embodiment 1, is coated on the side skin of forearm of subject, uses
Oilpaper, which covers, to be bound up with gauze, and 1 time a day, continuous 5d, control only applies petroleum jelly cream, observes the stimulation to skin.
Embodiment 1 be formulated deodorization spray agent through human skin local stimulation test as a result, it has been found that, 10 subjects are in coating
Occur altogether on 3 person in the process 5 times it is transient it is rubescent, itch, the reaction such as small rash, wherein test side 3 times, control side 2 times,
Have no significant difference.
The human skin local stimulation of the human skin local stimulation test result and embodiment 1 of 2~embodiment of embodiment 8
Test result is essentially identical, and it is no longer repeated herein.
According to result above as it can be seen that as a kind of pet external application articles, 1~embodiment of embodiment 8 selected by us is each
Formulation product safety is fabulous, pierces through acute toxicity test, subacute toxicity test, skin toxicology test, animal eyes combination film
The verification experimental verifications such as test, human skin local stimulation test are swashed, to pet eyes, skin, oral cavity etc. almost without toxicity, safety
Splendid, pet can lick safely and lick.
Test example 6
Deodorization spray agent is to dog factory scene deodorizing effect testing experiment.Shandong large-scale dog factory is chosen in this test, in air duct slats
The winter of part difference detects the verifying each deodorization spray agent formula of 1~embodiment of embodiment 8 to the deodorizing effect of dog factory by instrument.
10 kennels are chosen in this large-scale dog factory, are detected after five minutes with portable ammonia before deodorization with deodorization
Instrument carries out colony house ammonia on-site test, and specific method is to simultaneously close off each door and window within 2 hours before testing, respectively the 3 of every kennel
A different distributions point, height of 0.9 meter away from ground carry out the detection of ammonia value, and are averaged.
Test result is as shown in table 11, and as shown in Table 11, respectively formula deodorization spray agent is existing to dog factory for 1~embodiment of embodiment 8
Field deodorizing effect is fine, can quickly eliminate ammonia after five minutes in effect, drop ammonia percentage reach 75% or more, make in kennel
Air is effectively purified, and reduces the generation of respiratory disease, and the drop ammonia deodorizing effect of deodorization spray agent of the present invention is better than city
The similar deodorization spray agent in field.
The different Example formulations of table 11 are to dog factory deodorizing effect test result
Test example 7
Deodorization spray agent is to dog factory scene sterilizing testing experiment.Shandong large-scale dog factory is chosen in this test, and verifying is implemented
Killing effect of each deodorization spray agent formula of 1~embodiment of example 8 to dog factory surface natural bacteria.
1, test reagent and material
Phosphate buffer (PBS, 0.03mol/L, pH 7.2), dilution (PBS solution containing 0.1% Tween 80), nothing
Bacterium cotton swab, dimension board (being prepared with stainless steel material, there are the spaces of 5.0cm × 5.0cm as sampling sites in center) and battalion
Support agar medium.
2, test method
(1) wall surface is taken at random, and demarcating 3 pieces of areas with dimension board is respectively 25cm2Block, one for sterilize before sampling,
One sterilizes sampling for deodorization spray agent for chemical disinfection post-sampling, one.
(2) purified water is sparged into sample region, then bedewed sterile cotton swab in the test tube of dilution containing 5ml, to one
Block swabing sampling, it is vertical and horizontal each 8 times round-trip.After sampling, cotton swab sampling end is cut in a manner of sterile working and is tried into former dilution
In pipe, 20s or rapping 80 times are shaken, after doing appropriate dilution, as negative control group sample.
(3) sample region will be sparged after the dilution of chemosterilant by specification dosage to carry out disinfection, then by sterile cotton swab
Son bedews in the test tube of dilution containing 5ml, vertical and horizontal each 8 times round-trip to a block swabing sampling.After sampling, with sterile working side
Formula cuts cotton swab sampling end in former dilution test tube, shakes 20s or rapping 80 times, after doing appropriate dilution, as positive right
According to a group sample.
(4) deodorization spray agent Direct spraying is subjected to deodorization and disinfection in sample region, then dilutes sterile cotton swab in containing 5ml
It is bedewed in liquid test tube, it is vertical and horizontal each 8 times round-trip to deodorization and disinfection block swabing sampling.After sampling, by cotton swab in a manner of sterile working
Sub-sampling end is cut original and is released in liquid test tube, and electronic vortex mixer shakes 20s or rapping 80 times, as deodorization and disinfection group sample.
(5) by positive controls, negative control group and deodorization and disinfection group sample, every part of absorption 1.0ml, with agar tilt-pour process
It is inoculated with plate, each sample is inoculated with 2 plates, puts and cultivate 48h in 37 DEG C of insulating boxs, observes final result.
(6) it calculates and kills logarithm
Test is repeated 3 times, and calculates the colony counts (cfu) of each group, and is scaled logarithm (N), is then calculated as follows
Kill logarithm:
Kill logarithm (No)-experimental group viable bacteria concentration logarithm of logarithm (KL)=control group mean viable concentration
(Nx)
Test is repeated 3 times, and positive controls should have more bacterial growth, and feminine gender answers asepsis growth to group, sterilizes sample
Logarithm >=1 is averagely killed, it is qualified that disinfection can be judged to.
3, test result
Deodorization spray agent is as shown in table 12 to the test result of dog factory scene sterilizing testing experiment, as shown in Table 12, real
Applying 1~embodiment of example 8, respectively formula deodorization spray agent is fine to dog factory scene disinfection effect, and it is big that each group averagely kills logarithm
In be equal to 1, it is similar to positive controls (chemosterilant) effect.We are it can be concluded that 1~embodiment of embodiment 8 is each as a result,
Deodorization spray agent is formulated while deodorization, moreover it is possible to which efficient sterilization is asked so as to solve stink inherently, from source
Topic.
The different Example formulations of table 12 are to dog factory scene sterilizing test result
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of pet complex biological deodorization spray agent, which is characterized in that by percentage to the quality, including yucca mentions each component
Take object 5-8%, green-tea extract 4-5%, wild marjoram oil extract 6-8%, persimmon extract 4-5%, horseradish extract 4-5%,
Zinc ricinate 3-4%, emulsifier 5-6%, stabilizer 1-2%, pH adjusting agent 1-2%, surplus are purified water.
2. pet according to claim 1 complex biological deodorization spray agent, which is characterized in that the yucca extract packet
Saponin, polysaccharide and polyphenol are included, wherein saponin content is 10-12%, polyoses content 10-12%, polyphenol content 15-17%.
3. pet according to claim 1 complex biological deodorization spray agent, which is characterized in that the green-tea extract packet
Tea polyphenols are included, wherein the content of tea polyphenols is 20-25%.
4. pet according to claim 1 complex biological deodorization spray agent, which is characterized in that the wild marjoram oil extract
Including Thymol, poly- phenol, perfume Jing Qin phenol, wherein Thymol content is 10-11%, poly- phenol content is 7-8%, perfume Jing Qin phenol
Content is 8-10%.
5. pet according to claim 1 complex biological deodorization spray agent, which is characterized in that the persimmon extract packet
Persimmon tannin is included, wherein persimmon tannin content is 15-18%.
6. pet according to claim 1 complex biological deodorization spray agent, which is characterized in that the horseradish extract packet
Horseradish peroxidase is included, wherein horseradish peroxidase content is 7-10%.
7. the complex biological deodorization spray agent of pet described in any one according to claim 1, which is characterized in that the castor-oil plant
Zinc oleate is liquid, active constituent content 30-35%.
8. pet according to claim 1 complex biological deodorization spray agent, which is characterized in that the emulsifier is
The mixture of Tween-80, Span-80, the two proportion are Tween-80:Span-80=6:4.
9. pet according to claim 1 complex biological deodorization spray agent, which is characterized in that the stabilizer is acetic acid
The mixture of salt buffer, lysozyme and glycerol, the pH adjusting agent are citric acid or lactic acid or combinations thereof.
10. a kind of method for preparing any pet complex biological deodorization spray agent of claim 1-9, feature exist
In, comprising the following steps:
Step 1, a certain amount of purified water is first taken, then sequentially adds yucca extract, green-tea extract according to the ratio, persimmon extracts
Object, zinc ricinate, stirring dissolves it successively to get solution A after addition；
Step 2, emulsifier is weighed, wild marjoram oil extract, horseradish peroxidase are sequentially added, stabilizer stirs to dissolve,
Up to solution B；
Step 3, solution B and solution A are poured into high shear homogeneous vacuum mixing mulser and is stirred, mixing speed is
3000-4000 revs/min, mixing time 15-20min, obtain the uniform light yellow transparent liquid of color；
Step 4, it is 6.5-7.5 that pH adjusting agent, which is added, and adjusts solution A and mixed liquor to the pH value of solution B, finally adds purifying
Water is to prescribed volume to get deodorization spray agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910143893.8A CN109646361B (en) | 2019-02-27 | 2019-02-27 | Composite biological deodorization spray for pets and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910143893.8A CN109646361B (en) | 2019-02-27 | 2019-02-27 | Composite biological deodorization spray for pets and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109646361A true CN109646361A (en) | 2019-04-19 |
| CN109646361B CN109646361B (en) | 2022-03-29 |
Family
ID=66123708
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910143893.8A Active CN109646361B (en) | 2019-02-27 | 2019-02-27 | Composite biological deodorization spray for pets and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109646361B (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111214420A (en) * | 2020-03-16 | 2020-06-02 | 厦门汇承药业有限公司 | Preparation method of deodorant spray for pets |
| CN111804136A (en) * | 2020-06-17 | 2020-10-23 | 深圳职业技术学院 | Formaldehyde scavenging agent and preparation method thereof |
| CN112315842A (en) * | 2020-10-27 | 2021-02-05 | 杭州宠趣生物科技有限公司 | Dog and cat oral care spray containing lysozyme and preparation method thereof |
| CN112616860A (en) * | 2020-12-18 | 2021-04-09 | 合肥中龙神力动物药业有限公司 | Pet environment disinfection and deodorization solution and preparation method and application thereof |
| CN112972282A (en) * | 2021-02-08 | 2021-06-18 | 石远琳 | Natural deodorant and preparation method and application thereof |
| CN113117500A (en) * | 2019-12-30 | 2021-07-16 | 广东铭康香精香料有限公司 | Composition with peculiar smell removing effect, preparation method and application thereof |
| CN114042373A (en) * | 2021-10-15 | 2022-02-15 | 苏州市易柯露环保科技有限公司 | Novel efficient plant deodorant and preparation method thereof |
| CN114767556A (en) * | 2022-03-31 | 2022-07-22 | 河北登尚科技有限公司 | Pet deodorant |
| CN114831137A (en) * | 2022-05-24 | 2022-08-02 | 湖南普泰尔环境股份有限公司 | Deodorant with antibacterial effect |
| CN115227609A (en) * | 2022-05-12 | 2022-10-25 | 胡银艳 | Pet plant extract deodorization spray |
| CN115428863A (en) * | 2022-09-13 | 2022-12-06 | 广东尚爱嘉宠营养科技有限公司 | Pet nutritional meat particles and preparation method thereof |
| CN116407939A (en) * | 2023-04-14 | 2023-07-11 | 广东鹏炜精细化工有限公司 | Preparation method and application of natural plant composite biological enzyme deodorizing spray |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004242516A (en) * | 2003-02-12 | 2004-09-02 | Johnson Trading Kk | Deodorant for pet |
| CN103384526A (en) * | 2011-01-24 | 2013-11-06 | 巴斯夫欧洲公司 | Oral health improving compositions |
| CN104039338A (en) * | 2011-11-03 | 2014-09-10 | 纽约市哥伦比亚大学理事会 | Botanical Antimicrobial Composition |
| CN104957399A (en) * | 2015-06-08 | 2015-10-07 | 宁波希诺亚海洋生物科技有限公司 | Pet deodorizing tablet and preparation method thereof |
| CN106914128A (en) * | 2017-04-28 | 2017-07-04 | 中林山水（北京）生态科技股份有限公司 | A kind of biological deodorant and preparation method thereof |
| CN107362655A (en) * | 2017-08-17 | 2017-11-21 | 广州崃克保化工有限公司 | A kind of environment-friendly water-based eliminating smell agent and its application |
| CN108546317A (en) * | 2017-12-25 | 2018-09-18 | 宜兴丹森科技有限公司 | Super absorbent resin deodorant composition with plant odour-proof component |
| CN108840535A (en) * | 2018-06-30 | 2018-11-20 | 贵州织金丰金农业科技发展有限公司 | A kind of bacteria agent of feces of livestock and poultry deodorization |
-
2019
- 2019-02-27 CN CN201910143893.8A patent/CN109646361B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004242516A (en) * | 2003-02-12 | 2004-09-02 | Johnson Trading Kk | Deodorant for pet |
| CN103384526A (en) * | 2011-01-24 | 2013-11-06 | 巴斯夫欧洲公司 | Oral health improving compositions |
| CN104039338A (en) * | 2011-11-03 | 2014-09-10 | 纽约市哥伦比亚大学理事会 | Botanical Antimicrobial Composition |
| CN104957399A (en) * | 2015-06-08 | 2015-10-07 | 宁波希诺亚海洋生物科技有限公司 | Pet deodorizing tablet and preparation method thereof |
| CN106914128A (en) * | 2017-04-28 | 2017-07-04 | 中林山水（北京）生态科技股份有限公司 | A kind of biological deodorant and preparation method thereof |
| CN107362655A (en) * | 2017-08-17 | 2017-11-21 | 广州崃克保化工有限公司 | A kind of environment-friendly water-based eliminating smell agent and its application |
| CN108546317A (en) * | 2017-12-25 | 2018-09-18 | 宜兴丹森科技有限公司 | Super absorbent resin deodorant composition with plant odour-proof component |
| CN108840535A (en) * | 2018-06-30 | 2018-11-20 | 贵州织金丰金农业科技发展有限公司 | A kind of bacteria agent of feces of livestock and poultry deodorization |
Non-Patent Citations (6)
| Title |
|---|
| 中国材料研究学会等: "《中国战略性新兴产业 新材料 环境工程材料》", 30 November 2018, 中国铁道出版社 * |
| 余有本等: "《茶学专业实践教学指导》", 30 October 2017, 西北农林科技大学出版社 * |
| 派锐宠物用品: "《https://mp.weixin.qq.com/s/339x03YyaztKiCnDi_KTvQ》", 26 June 2018 * |
| 王建新等: "《化妆品植物原料大全》", 30 June 2012, 中国纺织出版社 * |
| 裘炳毅等: "《现代化妆品科学与技术 中》", 31 March 2016, 中国轻工业出版社 * |
| 辛国贤等: ""柿子单宁提取新工艺及对5类臭味化合物脱臭性能分析"", 《中国食品学报》 * |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113117500A (en) * | 2019-12-30 | 2021-07-16 | 广东铭康香精香料有限公司 | Composition with peculiar smell removing effect, preparation method and application thereof |
| CN111214420A (en) * | 2020-03-16 | 2020-06-02 | 厦门汇承药业有限公司 | Preparation method of deodorant spray for pets |
| CN111804136A (en) * | 2020-06-17 | 2020-10-23 | 深圳职业技术学院 | Formaldehyde scavenging agent and preparation method thereof |
| CN112315842A (en) * | 2020-10-27 | 2021-02-05 | 杭州宠趣生物科技有限公司 | Dog and cat oral care spray containing lysozyme and preparation method thereof |
| CN112616860A (en) * | 2020-12-18 | 2021-04-09 | 合肥中龙神力动物药业有限公司 | Pet environment disinfection and deodorization solution and preparation method and application thereof |
| CN112972282A (en) * | 2021-02-08 | 2021-06-18 | 石远琳 | Natural deodorant and preparation method and application thereof |
| CN114042373A (en) * | 2021-10-15 | 2022-02-15 | 苏州市易柯露环保科技有限公司 | Novel efficient plant deodorant and preparation method thereof |
| CN114767556A (en) * | 2022-03-31 | 2022-07-22 | 河北登尚科技有限公司 | Pet deodorant |
| CN115227609A (en) * | 2022-05-12 | 2022-10-25 | 胡银艳 | Pet plant extract deodorization spray |
| CN114831137A (en) * | 2022-05-24 | 2022-08-02 | 湖南普泰尔环境股份有限公司 | Deodorant with antibacterial effect |
| CN114831137B (en) * | 2022-05-24 | 2023-06-16 | 湖南普泰尔环境股份有限公司 | Deodorant with antibacterial effect |
| CN115428863A (en) * | 2022-09-13 | 2022-12-06 | 广东尚爱嘉宠营养科技有限公司 | Pet nutritional meat particles and preparation method thereof |
| CN116407939A (en) * | 2023-04-14 | 2023-07-11 | 广东鹏炜精细化工有限公司 | Preparation method and application of natural plant composite biological enzyme deodorizing spray |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109646361B (en) | 2022-03-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109646361A (en) | A kind of pet complex biological deodorization spray agent and preparation method thereof | |
| KR100817296B1 (en) | Stable automatic disinfection system | |
| CN109316536A (en) | A kind of skin mucosa disinfecting agent and preparation method thereof | |
| CN109260927A (en) | A kind of deodorization taste removal concentrate composition of the oil of another name for containing Chinese juniper and preparation method thereof | |
| CN109432470A (en) | A kind of footgear deodorant compositions and preparation method thereof containing Caulis Sacchari sinensis extract | |
| CN107518012A (en) | A kind of efficient mosquito repelling Chinese medicine compound prescription essential oil | |
| CN108371724A (en) | A kind of deodorizing sterilizing air cleaning agent of the flower extract containing ginger | |
| CN109805038A (en) | A kind of Australia tea tree essential oil disinfection agent and its preparation method and application | |
| CN111249173A (en) | Deodorizing and purifying concentrated solution and preparation method and application thereof | |
| CN110637839A (en) | Jasmine flower mosquito repellent with nerve calming and sleep aiding effects and preparation method thereof | |
| KR101622305B1 (en) | Disinfectant making air fresh and preparation method and use thereof | |
| CN1210069C (en) | Air freshener | |
| JP2004509636A (en) | Water-based disinfectant / disinfectant for food | |
| CN106726871A (en) | Sweet wormwood mosquito-expelling and antipruritic floral water and preparation method thereof | |
| CN111543442A (en) | Composite sterilization liquid based on traditional Chinese medicine volatile oil and preparation method thereof | |
| CN110859194B (en) | Compound mosquito-repelling essential oil, application and mosquito repellent | |
| CN104815096B (en) | A kind of nanometer composite skin disinfection emulsion and preparation method thereof | |
| CN105031701A (en) | Environmentally-friendly plant source deodorant | |
| CN112807259B (en) | Safe and nontoxic mosquito-repellent composition and preparation method and application thereof | |
| CN110250227A (en) | A kind of pet dog deodorizing sterilizing composition and preparation method thereof | |
| CN111437288A (en) | Atomized molecular iodine disinfectant and application thereof | |
| CN112494388A (en) | Nonalcoholic spray for repelling mosquitoes and relieving itching and preparation method thereof | |
| CN109984153A (en) | A kind of multi-functional plant essential mosquito repellent | |
| CN107343865B (en) | Compound volatile oil and preparation method and application thereof | |
| CN116784354A (en) | Fumigating type air degerming agent compounded by plant extraction essential oil and preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information |
Address after: 262200 no.195 Shungeng Road, Zhucheng City, Weifang City, Shandong Province Applicant after: SHANDONG SINDER TECHNOLOGY Co.,Ltd. Applicant after: SHANDONG CHONGZHIYOUPIN PET FOOD Co.,Ltd. Address before: 262200 no.195 Shungeng Road, Zhucheng City, Weifang City, Shandong Province Applicant before: SHANDONG SINDER TECHNOLOGY Co.,Ltd. Applicant before: SHANDONG XINDE PET FOOD Co.,Ltd. |
|
| CB02 | Change of applicant information | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20220228 Address after: 262200 no.195 Shungeng Road, Zhucheng City, Weifang City, Shandong Province Applicant after: SHANDONG SINDER TECHNOLOGY Co.,Ltd. Applicant after: SHANDONG CHONGZHIYOUPIN PET FOOD Co.,Ltd. Applicant after: Shandong Zhuzi Biotechnology Co.,Ltd. Address before: 262200 no.195 Shungeng Road, Zhucheng City, Weifang City, Shandong Province Applicant before: SHANDONG SINDER TECHNOLOGY Co.,Ltd. Applicant before: SHANDONG CHONGZHIYOUPIN PET FOOD Co.,Ltd. |
|
| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |