CN109575802A - A kind of chafing dish sterilizing deodoring of natural component is spraying and preparation method thereof - Google Patents

A kind of chafing dish sterilizing deodoring of natural component is spraying and preparation method thereof Download PDF

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Publication number
CN109575802A
CN109575802A CN201811276668.3A CN201811276668A CN109575802A CN 109575802 A CN109575802 A CN 109575802A CN 201811276668 A CN201811276668 A CN 201811276668A CN 109575802 A CN109575802 A CN 109575802A
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China
Prior art keywords
chafing dish
spraying
preparation
under conditions
slowly added
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Pending
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CN201811276668.3A
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Chinese (zh)
Inventor
乔丽君
胡衎
陈巧玲
刘玲玲
刘�文
赵学成
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Anhui Kai Wei Biological Technology Co Ltd
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Anhui Kai Wei Biological Technology Co Ltd
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Priority to CN201811276668.3A priority Critical patent/CN109575802A/en
Publication of CN109575802A publication Critical patent/CN109575802A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02Amines; Quaternary ammonium compounds
    • A01N33/12Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/14Paints containing biocides, e.g. fungicides, insecticides or pesticides
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Chemical & Material Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Environmental Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Mycology (AREA)
  • Materials Engineering (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Organic Chemistry (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Pest Control & Pesticides (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

It is spraying that the present invention provides a kind of chafing dish sterilizing deodorings of natural component, including following parts by weight material: soapberry extract 0.010-5.000%, sorbitan mono-oleic acid ester 0.010-5.000%, solubilizer 0.010-5.000%, dehydrated alcohol 0.010-5.000%, chlorocarbon base dimethyl-benzyl amine 0.010-0.200%, Phenoxyethanol 0.010-1.000%, lemon 0.010-1.000% purifies water surplus.The present invention needs to study for chafing dish volatile flavor substance, and the chafing dish sterilizing deodoring for preparing a kind of natural component is spraying, efficiently solves the problem that fragrance covers the hardly possible that eliminates the unusual smell with chemisorption.

Description

A kind of chafing dish sterilizing deodoring of natural component is spraying and preparation method thereof
Technical field
The present invention relates to household chemicals technical fields, and in particular to a kind of chafing dish sterilizing deodoring of natural component it is spraying and Preparation method.
Background technique
A kind of characteristic traditional food mode of the chafing dish as Sichuan-chongqing Region, because its special mouthfeel and fragrance are each by the whole nation The favor of the more and more consumers in ground.Convenient and efficient possessed by chafing dining, Popular Characteristic is continued saying it with interest by consumers. When weather cold, chafing dish is even more the first choice of numerous consumers, still, eats up and remains the chafing dish for being difficult to remove on clothing after chafing dish Taste.
The method of common removal chafing dish taste is first is that laundry, however winter apparel is thick and heavy does not change clothes easily;Second is that sprinkling Perfume, this is a kind of smell encapsulation method, and chafing dish taste can only be temporarily blanked, after volatilizing perfume or aroma fades, chafing dish taste Still exist.Because chafing dish taste remains on clothing and is difficult to the problem removed, to increase Gu of the consumer when selection is had dinner Consider, weakens the competitiveness of chafing dining industry.
The special flavor that chafing dish generates during rinsing and cooking material be mainly derived from soup halogen in chafing dish bottom flavorings, grease and The effect of fragrance.Through each researchers the study found that the either red oil the bottom of a pan, three delicacies the bottom of a pan either clear soup the bottom of a pan etc., master Wanting volatile flavor substance is mainly that alcohols, hydro carbons etc. are prepared so needing to be studied for chafing dish volatile flavor substance A kind of chafing dish sterilizing deodoring of natural component is spraying out.
Summary of the invention
It is spraying and preparation method thereof the object of the present invention is to provide a kind of chafing dish sterilizing deodoring of natural component, it is prepared Chafing dish sterilizing deodoring can efficiently solve that fragrance is covered and chemisorption eliminates the unusual smell difficult problem by spraying.
The present invention solves above-mentioned technical problem using following technical scheme:
A kind of chafing dish sterilizing deodoring of natural component is spraying, including following parts by weight material:
Further, the solubilizer is one of Cremophor RH40 and alkyl phenol polyoxyethylene ether 10 or two Kind.
The spraying preparation method of the chafing dish sterilizing deodoring of this natural component, which is characterized in that mainly comprise the steps that
(1) lemon, solubilizer and sorbitan mono-oleic acid ester are mixed under constant temperature conditions;
(2) it is stirred after being slowly added to dehydrated alcohol into the mixed solution of step (1);
(3) soapberry extract, chlorocarbon base dimethyl-benzyl amine, Phenoxyethanol are added into the mixed solution of step (2) It is stirred with after purified water;PH adjusting agent is added, solution ph is adjusted to 6.50-8.00, arrives one kind after the completion of preparation The chafing dish sterilizing deodoring of natural component is spraying.
Further, whipping temp is 30-35 DEG C, mixing speed 400-800rpm in the step (1), mixing time For 0.5-2.0h.
Further, mixing speed is 400-800rpm, mixing time 20-40min in the step (2).
Further, mixing speed is 400-800rpm, mixing time 1-3h in the step (3).Further, institute Stating the mode/means being added in step (3) includes: to be slowly added to purified water under conditions of the stirring of 600rmp revolving speed and stir 20min;Soapberry extract is slowly added under conditions of the stirring of 600rmp revolving speed and stirs 40min;It is stirred in 600rmp revolving speed It is slowly added to chlorocarbon base dimethyl-benzyl amine under conditions of mixing and stirs 30min;Under conditions of the stirring of 600rmp revolving speed slowly Phenoxyethanol is added and stirs 30min.
Further, pH adjusting agent is disodium hydrogen phosphate dodecahydrate and sodium dihydrogen phosphate dihydrate in the step (3).
The present invention has the advantages that
A kind of chafing dish sterilizing deodoring of natural component provided by the invention is spraying, and this natural taste removal is spraying from soapberry It extracts, chafing dish taste removal rate is 78.40-94.80%, has and efficiently removes chafing dish taste effect;It can be done directly on clothing, it is molten Liquid system pH is 6.50-8.00, and stability is good, nonirritant to skin and respiratory tract, is a kind of natural to clothing without damageability Chafing dish sterilizing deodoring it is spraying.
Specific embodiment
The present invention will be further described With reference to embodiment, following embodiment be intended to illustrate invention without It is limitation of the invention further.
Embodiment 1
A kind of chafing dish sterilizing deodoring of natural component of the present invention is spraying, including following parts by weight material:
The spraying preparation method of the chafing dish sterilizing deodoring of this natural component, comprising the following steps:
(1) by lemon, sorbitan mono-oleic acid ester and Cremophor RH40,30 DEG C of constant temperature, it is in revolving speed It is lower under conditions of 400rpm to stir 0.5h;
(2) stop constant temperature, be slowly added to dehydrated alcohol under conditions of the stirring of 400rmp revolving speed and stir 20 min;
(3) purified water is slowly added under conditions of 400rmp revolving speed stirs and stir 10min;It is stirred in 400 rmp revolving speeds It is slowly added to soapberry extract under conditions of mixing and stirs 20min;Chlorine is slowly added under conditions of the stirring of 400rmp revolving speed Alkyl dimethyl-benzyl amine simultaneously stirs 20min;Phenoxyethanol is slowly added under conditions of the stirring of 400rmp revolving speed and is stirred 10min;
(4) it is first slowly added to disodium hydrogen phosphate dodecahydrate under conditions of 400rmp revolving speed stirs, is slow added into two Hypophosphite monohydrate sodium dihydrogen, control pH are 6.50, to get spraying to a kind of chafing dish sterilizing deodoring of natural component after the completion of preparation.
Embodiment 2
A kind of chafing dish sterilizing deodoring of natural component of the present invention is spraying, including following parts by weight material:
The spraying preparation method of the chafing dish sterilizing deodoring of this natural component, comprising the following steps:
(1) by lemon, sorbitan mono-oleic acid ester and Cremophor RH40,30 DEG C of constant temperature, it is in revolving speed It is lower under conditions of 600rpm to stir 1h;
(2) stop constant temperature, be slowly added to dehydrated alcohol under conditions of the stirring of 600rmp revolving speed and stir 30 min;
(3) purified water is slowly added under conditions of 600rmp revolving speed stirs and stir 20min;It is stirred in 600 rmp revolving speeds It is slowly added to soapberry extract under conditions of mixing and stirs 40min;Chlorine is slowly added under conditions of the stirring of 600rmp revolving speed Alkyl dimethyl-benzyl amine simultaneously stirs 30min;Phenoxyethanol is slowly added under conditions of the stirring of 600rmp revolving speed and is stirred 30min;
(4) it is first slowly added to disodium hydrogen phosphate dodecahydrate under conditions of 400rmp revolving speed stirs, is slow added into two Hypophosphite monohydrate sodium dihydrogen, control pH are 7.10, to get spraying to a kind of chafing dish sterilizing deodoring of natural component after the completion of preparation.
Embodiment 3
A kind of chafing dish sterilizing deodoring of natural component of the present invention is spraying, including following parts by weight material:
The spraying preparation method of the chafing dish sterilizing deodoring of this natural component, comprising the following steps:
(1) by lemon, sorbitan mono-oleic acid ester and Cremophor RH40,30 DEG C of constant temperature, it is in revolving speed It is lower under conditions of 600rpm to stir 1h;
(2) stop constant temperature, be slowly added to dehydrated alcohol under conditions of the stirring of 600rmp revolving speed and stir 30 min;
(3) purified water is slowly added under conditions of 600rmp revolving speed stirs and stir 20min;It is stirred in 600 rmp revolving speeds It is slowly added to soapberry extract under conditions of mixing and stirs 40min;Chlorine is slowly added under conditions of the stirring of 600rmp revolving speed Alkyl dimethyl-benzyl amine simultaneously stirs 30min;Phenoxyethanol is slowly added under conditions of the stirring of 600rmp revolving speed and is stirred 30min;
(4) it is first slowly added to disodium hydrogen phosphate dodecahydrate under conditions of 400rmp revolving speed stirs, is slow added into two Hypophosphite monohydrate sodium dihydrogen, control pH are 7.30, to get spraying to a kind of chafing dish sterilizing deodoring of natural component after the completion of preparation.
Embodiment 4
A kind of chafing dish sterilizing deodoring of natural component of the present invention is spraying, including following parts by weight material:
The spraying preparation method of the chafing dish sterilizing deodoring of this natural component, comprising the following steps:
(1) by lemon, sorbitan mono-oleic acid ester and Cremophor RH40,30 DEG C of constant temperature, it is in revolving speed It is lower under conditions of 600rpm to stir 1h;
(2) stop constant temperature, be slowly added to dehydrated alcohol under conditions of the stirring of 600rmp revolving speed and stir 30 min;
(3) purified water is slowly added under conditions of 600rmp revolving speed stirs and stir 20min;It is stirred in 600 rmp revolving speeds It is slowly added to soapberry extract under conditions of mixing and stirs 40min;Chlorine is slowly added under conditions of the stirring of 600rmp revolving speed Alkyl dimethyl-benzyl amine simultaneously stirs 30min;Phenoxyethanol is slowly added under conditions of the stirring of 600rmp revolving speed and is stirred 30min;
(4) it is first slowly added to disodium hydrogen phosphate dodecahydrate under conditions of 400rmp revolving speed stirs, is slow added into two Hypophosphite monohydrate sodium dihydrogen, control pH are 7.50, to get spraying to a kind of chafing dish sterilizing deodoring of natural component after the completion of preparation.
Embodiment 5
A kind of chafing dish sterilizing deodoring of natural component of the present invention is spraying, including following parts by weight material:
The spraying preparation method of the chafing dish sterilizing deodoring of this natural component, comprising the following steps:
(1) by lemon, sorbitan mono-oleic acid ester and alkyl phenol polyoxyethylene ether 10,35 DEG C of constant temperature, it is in revolving speed It is lower under conditions of 800rpm to stir 2h;
(2) stop constant temperature, be slowly added to dehydrated alcohol under conditions of the stirring of 800rmp revolving speed and stir 40 min;
(3) purified water is slowly added under conditions of 600rmp revolving speed stirs and stir 40min;It is stirred in 600 rmp revolving speeds It is slowly added to soapberry extract under conditions of mixing and stirs 60min;Chlorine is slowly added under conditions of the stirring of 600rmp revolving speed Alkyl dimethyl-benzyl amine simultaneously stirs 40min;Phenoxyethanol is slowly added under conditions of the stirring of 600rmp revolving speed and is stirred 40min;
(4) it is first slowly added to disodium hydrogen phosphate dodecahydrate under conditions of 400rmp revolving speed stirs, is slow added into two Hypophosphite monohydrate sodium dihydrogen, control pH are 8.00, to get spraying to a kind of chafing dish sterilizing deodoring of natural component after the completion of preparation.
The content of each raw material used in above-described embodiment and the information of manufacturer are as follows:
Soapberry extract: a Japanese ball company;Sorbitan mono-oleic acid ester: content: 99%, the limited public affairs of Yongtai chemical industry Department;Cremophor RH40: content: 99%, Shandong You Suo Chemical Industry Science Co., Ltd;Dehydrated alcohol: content: 99.7%, Sinopharm Chemical Reagent Co., Ltd.;Chlorocarbon base dimethyl-benzyl amine: content: 95%, Shanghai Mike's woods biochemical technology is limited Company;Phenoxyethanol: content: 99%, Linyi City Lv Sen Chemical Co., Ltd.;Lemon: the new natural plants of Ji'an City China have Limit company;Sodium dihydrogen phosphate dihydrate: Sinopharm Chemical Reagent Co., Ltd. analyzes pure;Disodium hydrogen phosphate dodecahydrate: state Chemical reagent Co., Ltd, medicine group analyzes pure;Alkyl phenol polyoxyethylene ether 10: content: 99%, the green gloomy chemical industry of Linyi City is limited Company;
Other commercially available raw materials with identical parameters also can achieve equivalent effect.
It is as follows that taste removal test is carried out by spraying for chafing dish sterilizing deodoring preparation-obtained in embodiment:
Material: electromagnetic oven cooker is a set of;Fish out (mellowness) beef tallow basic flavouring for chafing dish 150g in seabed;10*10cm tests cotton;Originally Water;Purified water;The taste removal component sample to be tested of various concentration is contained in identical spray bottle;
Build chafing dish taste removal simulation model:
(1) seabed is added in electromagnetic oven pan and fishes out (mellowness) beef tallow basic flavouring for chafing dish 150g, then 1.5L is added originally to pot Water is boiled with high firepower value;
(2) above the pot at 20cm, according to the position that vapor dissipates, 10*10cm experiment cotton is spread, with moderate heat force value Constantly boiling 90min;
(3) experiment cotton is removed, taste removal sample is pressed 2 times on experiment cotton with Sprayable, weight about 0.4g makes Eliminating smell agent interacts with chafing dish taste.
Set blank control for the suction taste cotton not dealt with, negative control is set as with the cotton of purifying water process, The aqueous solution of the soapberry extract of variant mass percent concentration acts on chafing dish peculiar smell, carries out chafing dish taste removal test.Table 1 Assessment experts are selected by condition of euosmia, men and women is each according to 6 grades of representations of stench intensity for 6 grades of representations of stench intensity 5 people carry out odor strength sensory evaluation.
Smell-removing rate %=(peculiar smell intensity ratings value after 5- taste removal)/5*100.
Table 1: 6 grades of representations of stench intensity
Table 2 respectively is listed in peculiar smell degree scoring after acting on except chafing dish peculiar smell except chafing dish taste sample;
Table 2: the taste removal scoring and smell-removing rate of chafing dish taste sample are respectively removed
As seen from the above table, the smell grading system of blank control group is 5 points, smell-removing rate 0%;Negative control group average air Taste grading system is 3.90 points, smell-removing rate 22.00%;Test sample A effective concentration is 2.10%, and average oder levels are commented It is divided into 1.08 points, smell-removing rate 78.40%;Test sample B effective concentration is 4.80%, and average smell grade scoring is 0.26 point, smell-removing rate 94.80%;The result shows that the concentration of active principle is higher, except chafing dish taste effect is better.
Finally, it should be noted that above embodiments are only to illustrate the present invention and not limit technology described in the invention Scheme;Those skilled in the art should understand that still can modify to the present invention or equivalent replacement;And all are not It is detached from the technical solution and its improvement of the spirit and scope of the present invention, should all be covered within the scope of the claims of the present invention.

Claims (8)

1. a kind of chafing dish sterilizing deodoring of natural component is spraying, which is characterized in that including following parts by weight material:
2. a kind of chafing dish sterilizing deodoring of natural component according to claim 1 is spraying, which is characterized in that the solubilizer For one or both of Cremophor RH40 and alkyl phenol polyoxyethylene ether 10.
3. such as a kind of preparation method that the chafing dish sterilizing deodoring of natural component is spraying claimed in claims 1-2, which is characterized in that It mainly comprises the steps that
(1) lemon, solubilizer and sorbitan mono-oleic acid ester are mixed under constant temperature conditions;
(2) it is stirred after being slowly added to dehydrated alcohol into the mixed solution of step (1);
(3) soapberry extract, chlorocarbon base dimethyl-benzyl amine, Phenoxyethanol and pure are added into the mixed solution of step (2) It is stirred after changing water;PH adjusting agent is added, solution ph is adjusted to 6.50-8.00, to get natural to one kind after the completion of preparation The chafing dish sterilizing deodoring of ingredient is spraying.
4. preparation method according to claim 3, which is characterized in that whipping temp is 30-35 DEG C in the step (1), Mixing speed is 400-800rpm, mixing time 0.5-2.0h.
5. preparation method according to claim 3, which is characterized in that mixing speed is 400- in the step (2) 800rpm, mixing time 20-40min.
6. preparation method according to claim 3, which is characterized in that mixing speed is 400- in the step (3) 800rpm, mixing time 1-3h.
7. preparation method according to claim 3, which is characterized in that the mode/means packet being added in the step (3) It includes: being slowly added to purified water under conditions of the stirring of 600rmp revolving speed and stir 20min;Under conditions of the stirring of 600rmp revolving speed It is slowly added to soapberry extract and stirs 40min;Chlorocarbon base dimethyl is slowly added under conditions of the stirring of 600rmp revolving speed Benzene methanamine simultaneously stirs 30min;Phenoxyethanol is slowly added under conditions of the stirring of 600rmp revolving speed and stirs 30min.
8. preparation method according to claim 3, which is characterized in that pH adjusting agent is 12 hydrations in the step (3) Disodium hydrogen phosphate and sodium dihydrogen phosphate dihydrate.
CN201811276668.3A 2018-10-30 2018-10-30 A kind of chafing dish sterilizing deodoring of natural component is spraying and preparation method thereof Pending CN109575802A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1970089A (en) * 2006-12-04 2007-05-30 张涉 Deodorant spray and its preparing method
US9149550B2 (en) * 2012-10-02 2015-10-06 Innovasource, Llc Air and fabric freshener
CN104971446A (en) * 2015-07-15 2015-10-14 黄国杰 Air purification device used by fireman

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1970089A (en) * 2006-12-04 2007-05-30 张涉 Deodorant spray and its preparing method
US9149550B2 (en) * 2012-10-02 2015-10-06 Innovasource, Llc Air and fabric freshener
CN104971446A (en) * 2015-07-15 2015-10-14 黄国杰 Air purification device used by fireman

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
廖文胜等: "《宾馆与家用洗涤剂配方设计》", 31 January 2000, 中国轻工业出版社 *

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