CN105670834A - Application of camellia seed oil in washing product, washing liquid product and preparation method of washing liquid product - Google Patents
Application of camellia seed oil in washing product, washing liquid product and preparation method of washing liquid product Download PDFInfo
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- CN105670834A CN105670834A CN201610149594.1A CN201610149594A CN105670834A CN 105670834 A CN105670834 A CN 105670834A CN 201610149594 A CN201610149594 A CN 201610149594A CN 105670834 A CN105670834 A CN 105670834A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/008—Polymeric surface-active agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention relates to the field of washing products, in particular to application of camellia seed oil in a washing product and a washing liquid product. The washing liquid product contains camellia seed oil, nonylphenol polyoxyethylene ether, fatty alcohol-polyoxyethylene ether, fatty acyl monoethanolamine/fatty acyl diethanolamine, monosodium maleate, sodium benzoate, pigment and essence. The invention further relates to a preparation method of the washing liquid product. The method includes the step that camellia seed oil, nonylphenol polyoxyethylene ether, fatty alcohol-polyoxyethylene ether, fatty acyl monoethanolamine/fatty acyl diethanolamine, monosodium maleate, sodium benzoate, pigment and essence are evenly mixed with water. The washing liquid product is strong in cleaning effect; the pH value ranges from 6.0 to 8.5, so that the washing liquid product is small in irritation, free of skin irritation and mild in performance; cleaning water consumption can be lowered, so that the use cost for cleaning articles with the washing liquid product is lowered, and great social significance and economic significance are achieved.
Description
Technical field
The invention belongs to cleaning product field, it relates to the application of camellia seed oil in cleaning product, and a kind of liquid detergent goods and its preparation method.
Background technology
Along with the integration of world economy and the development of trade globalization, culture background, state of the art and environmental regulation become three large driving forces of articles for washing globalization development gradually, the whole world articles for washing will tend to variation, but energy-conservation, economize on water, efficient, gentle, easy to use and meet safety and environment protection requirement product will be current and following cleaning product develop main flow direction.
Liquid detergent is the product of the cleaning dirt commonly used of family and greasy dirt, and the performance of its product has influence on the health of the mankind. , it is desired to the characteristic that liquid detergent has safety and environmental protection, clean gentle, foam is soft and fine, rapid decomposition is oily, therefore thus reach fast decontaminating, the effectively thoroughly cleaning and object that do not remain. And in prior art, it may also be useful to liquid detergent can produce a large amount of foams, it is easy to produces the problem of liquid detergent residual, will thoroughly remove, it is necessary to consume a large amount of water, thus adds the cost of cleaning dirt and greasy dirt. And cleaning after terminating, hand skin can become very dry.
Summary of the invention
It is an object of the invention to overcome the defect of the liquid detergent of commercial type, it is provided that a kind of cleaning effect is good, performance is gentle, and can reduce the detergent product of water consumption.
In order to realize above object, first aspect, the present invention provides the application of camellia seed oil in cleaning product.
Second aspect, the present invention provides a kind of liquid detergent goods, and these liquid detergent goods contain camellia seed oil, polyoxyethylene nonylphenol ether, fatty alcohol-polyoxyethylene ether, fatty acyl list and/or two thanomin, toxilic acid list sodium, Sodium Benzoate.
The third aspect, the present invention provides the preparation method of a kind of liquid detergent goods, wherein, the method comprises: camellia seed oil, polyoxyethylene nonylphenol ether, fatty alcohol-polyoxyethylene ether, fatty acyl list and/or two thanomin, toxilic acid list sodium, Sodium Benzoate, pigment and essence are mixed with water.
The detergent product of the present invention liquid detergent provided by the invention, cleaning effect is strong; PH value 6.0-8.5, not skin irritation, performance is gentle; Cleaning water consumption can be reduced, thus reduce the use cost of liquid detergent article-cleaning, there is higher social effect and economic implications.
Other features and advantages of the present invention are described in detail in embodiment part subsequently.
Embodiment
Hereinafter the specific embodiment of the present invention is described in detail. Should be understood that, embodiment described herein, only for instruction and explanation of the present invention, is not limited to the present invention.
Camellia (CAMELLIAJAPONICA), call the making processes also known as thorn apple, sea pomegranate, shallow lake overgrown with wild plants spring, mountain Chinese toon, resistance to winter, Camellia oil such as can be divided into: by being shelled by camellia seed, dry, pulverize, oil expression, filters and just can obtain camellia seed oil (also known as, Camellia oil, tea-seed oil, camellia seed oil). Camellia seed oil is nutritious, have reduce blood pressure, blood fat, prevent and treat heart trouble and vessel softening etc. effect.
The discovery that the present inventor is surprising in the process of research, by camellia seed oil being added in liquid detergent goods, and select and polyoxyethylene nonylphenol ether, fatty alcohol-polyoxyethylene ether, fatty acyl list and/or two thanomin, toxilic acid list sodium and Sodium Benzoate with the use of, prepared liquid detergent goods foam is fine and smooth, there is stronger cleaning capacity, easily rinse, can effectively save water resources, and performance gentleness does not hinder hand, thus completes the present invention.
Based on above discovery, first aspect, the present invention provides the application of camellia seed oil in cleaning product.
Preferably, described cleaning product is kitchen cleaning product, it is more preferable to be liquid detergent.
According to the present invention, described camellia seed oil is by preparing voluntarily, it is also possible to commercially available, such as, purchased from perfect (China) company limited.
Second aspect, present invention also offers a kind of liquid detergent goods, and these liquid detergent goods contain camellia seed oil, polyoxyethylene nonylphenol ether, fatty alcohol-polyoxyethylene ether, fatty acyl list and/or two thanomin, toxilic acid list sodium, Sodium Benzoate.
Although various components matching as above being used and can realizing good synergy, but the present inventor finds, when the liquid detergent goods based on 100 weight parts, the content of described camellia seed oil is 1-10 weight %, the content of described polyoxyethylene nonylphenol ether be 5-20 weight %, content to be the content of 1-5 weight %, described fatty acyl list and/or two thanomin the be 0.5-5 weight % of described fatty alcohol-polyoxyethylene ether, described toxilic acid list sodium content be content when being 0.01-0.5 weight % of 1-5 weight %, described Sodium Benzoate; Preferred further, when the liquid detergent goods based on 100 weight parts, the content of described camellia seed oil is 3-8 weight %, the content of described polyoxyethylene nonylphenol ether be 8-15 weight %, content to be the content of 2-4 weight %, described fatty acyl list and/or two thanomin the be 1-3 weight % of described fatty alcohol-polyoxyethylene ether, described toxilic acid list sodium content be content when being 0.05-0.3 weight % of 2-4 weight %, described Sodium Benzoate, the performance of the liquid detergent goods obtained can be promoted further.
According to the present invention, also containing pigment and essence in described detergent product. Preferably, based on the liquid detergent goods of 100 weight parts, the content of described pigment is 0.005-0.03 weight %, the content of described essence is 0.1-0.5 weight %, preferred further, the content of described pigment is 0.008-0.015 weight %, and the content of described essence is 0.2-0.4 weight %.
According in the present invention, described essence can be the various essence that this area routine uses, it optionally can add according to actual demand, such as, described essence can be one or more in green cucumber essence, rose compound, osmanthus flower fragrance, peach flavor, lemon flavour, flavoring pineapple essence and cream jasmin france.
Such as, according to, in the present invention, described pigment can be the various pigments that this area routine uses, and it optionally can add according to actual demand, and, described pigment can be one or more in anthocyanidin, carotenoid, xenthophylls and Lyeopene.
According to the present invention, generally, also containing the water of surplus in described liquid detergent goods, also, taking the gross weight of liquid detergent as 100 parts by weight, water and as above composition sum are 100 weight parts.
According to the present invention, preferably simultaneously containing the two thanomin of fatty acyl monoethanolamine and fatty acyl in described liquid detergent goods, and preferred further, the content of fatty acyl monoethanolamine and the two thanomin of fatty acyl is than being 1:0.5-1.5.
The third aspect, the invention also discloses the preparation method of a kind of liquid detergent goods, wherein, the method comprises: camellia seed oil, polyoxyethylene nonylphenol ether, fatty alcohol-polyoxyethylene ether, fatty acyl list and/or two thanomin, toxilic acid list sodium, Sodium Benzoate, pigment and essence are mixed with water.
According to the present invention, although each composition as above and water being mixed the liquid detergent goods that can either obtain the present invention, but the present inventor finds, carries out the preparation of liquid detergent goods according to following mode, and stability, the detergency ability of products obtained therefrom are more superior.
Concrete, first water and fatty acyl list and/or two thanomin and polyoxyethylene nonylphenol ether are mixed, add toxilic acid list sodium and fatty alcohol-polyoxyethylene ether afterwards again, when stirring, this mixed system is heated, preferably, in the process of heating, supplement the moisture lost due to evaporation. Condition the present invention of described heating not too much restriction by the present invention, as long as being conducive to the mixing of each several part, it is preferable that, described heating carries out when 40-55 DEG C.
Preferred further, homogenization treatment is carried out after stirring heating again when 40-60 DEG C, wherein, described homogenization treatment can complete in clarifixator. Add Sodium Benzoate after homogeneous, it is cooled to 30-40 DEG C, then add pigment and essence. Wherein, the temperature of described homogenization treatment is higher than the temperature of system after cooling. Speed the present invention of described cooling also has no particular limits, such as, it is possible to be Temperature fall.
According to the present invention, in order to improve the described mildness preparing liquid detergent goods further, it is preferable that the pH value of mixed system is adjusted to 6.0-8.5. The reagent regulated for pH value can be all ingredients that this area routine uses, such as, it is possible to be citric acid.
According to the present invention, in order to improve the stability of final resulting product further, it is preferable that, the system after adjust ph is filtered. Described filtration preferably carries out under 170-230 object aperture.
According to the present invention, the consumption of each composition as above is described in detail in second aspect, and in order to avoid unnecessary repetition, the present invention does not repeat them here.
According to the present invention, the selection of described essence and pigment can carry out according to description as above, and the present invention is also no longer described in detail at this.
The specific embodiment of the present invention below will be described in detail.
In following examples and comparative example,
Described camellia seed oil is purchased from perfect (China) company limited.
Embodiment 1-5 and comparative example 1-4
For illustration of detergent product and its preparation method
(1) according to each composition in table 1 and consumption, water, fatty acyl monoethanolamine, the two thanomin of fatty acyl and polyoxyethylene nonylphenol ether are uniformly mixed, then toxilic acid list sodium, cocoanut fatty acid diethanolamide and fatty alcohol-polyoxyethylene ether is added, mixture is heated at 50 DEG C and stirs, make mixing of materials even; Supplement the moisture of evaporation after the heating.
(2) by step (1) gained material homogeneous at 50 DEG C, Sodium Benzoate is then added.
(3) temperature of system is naturally cooled to 35 DEG C, add pigment and essence, it may also be useful to pH value is adjusted to 7 by citric acid, use 200 order filtered through gauze afterwards, obtain liquid detergent finished product.
Table 1
Comparative example 5
For illustration of makeup removing oil compositions and its preparation method of ginseng ratio
Liquid detergent is prepared according to the method for embodiment 1, the difference is that, each composition is directly mixed, then heats at 50 DEG C and stir, afterwards homogeneous at 50 DEG C, then pH value is adjusted to 7, use 200 order filtered through gauze afterwards, obtain liquid detergent finished product.
Comparative example 6
For illustration of makeup removing oil compositions and its preparation method of ginseng ratio
Liquid detergent is prepared according to the method for embodiment 1, the difference is that, the addition sequence of Sodium Benzoate and fatty acyl monoethanolamine, the two thanomin of fatty acyl and polyoxyethylene nonylphenol ether is exchanged.
Test case 1
(1) estimation of stability
Respectively get the liquid detergent goods of 10g embodiment 1-5 and comparative example 1-6, and be placed in incubation at room temperature case separately, the circulation of 40 DEG C of insulation cans and-10 DEG C-40 DEG C become temperature case, then its stability carry out the observation of 6 months, and whether the whether layering of main detection product, there is precipitation. Observations is shown in following table 2.
Table 2
(2) irritation test, supersensitivity are tested
Hair is cut at small white mouse 8 backs, smears respectively by the makeup removing oil of preparation in embodiment 1-5 and comparative example 1-6 in cutting plucked position, and no painting position does not compare, and result does not all have pungency and anaphylaxis.
Test case 2
Choose 110 experimenters, it is equally divided into 11 groups, often organize 10 people, experimenter has been carried out the survey of the effect of the cleaning effect of the liquid detergent about embodiment 1-5 and comparative example 1-6, mildness and water saving ability. Use effect described in 5 level evaluations, assessed value (5 grades) is averaged and is shown in following table 3. Wherein, 5: very effective; 4: effective a little; 3: moderate; 2: almost there is no effect; 1: there is no effect.
Table 3
By the result in upper table 3 it may be seen that the detergent product of the present invention liquid detergent provided by the invention, cleaning effect is strong; Performance gentleness not skin irritation; Cleaning water consumption can be reduced, thus reduce the use cost of liquid detergent article-cleaning, there is higher social effect and economic implications.
Below the preferred embodiment of the present invention is described in detail; but, the detail that the present invention is not limited in above-mentioned enforcement mode, within the scope of the technical conceive of the present invention; the technical scheme of the present invention can being carried out multiple simple variant, these simple variant all belong to protection scope of the present invention.
It should be noted that in addition, each the concrete technology feature described in above-mentioned embodiment, when not contradiction, it is possible to combined by any suitable mode. In order to avoid unnecessary repetition, various possible array mode is illustrated by the present invention no longer separately.
In addition, can also carrying out arbitrary combination between the various different enforcement mode of the present invention, as long as it does not run counter to the thought of the present invention, it should be considered as content disclosed in this invention equally.
Claims (10)
1. the application of camellia seed oil in cleaning product.
2. application according to claim 1, wherein, described cleaning product is kitchen cleaning product, it is preferable to liquid detergent.
3. liquid detergent goods, these liquid detergent goods contain camellia seed oil, polyoxyethylene nonylphenol ether, fatty alcohol-polyoxyethylene ether, fatty acyl monoethanolamine and/or fatty acyl two thanomin, toxilic acid list sodium, Sodium Benzoate.
4. liquid detergent goods according to claim 3, wherein, based on the liquid detergent goods of 100 weight parts, the content of described camellia seed oil is 1-10 weight %, the content of described polyoxyethylene nonylphenol ether is 5-20 weight %, and the content of described fatty alcohol-polyoxyethylene ether is 1-5 weight %, and the content of described fatty acyl monoethanolamine and/or the two thanomin of fatty acyl is 0.5-5 weight %, the content of described toxilic acid list sodium is 1-5 weight %, and the content of described Sodium Benzoate is 0.01-0.5 weight %.
5. liquid detergent goods according to claim 3, wherein, based on the liquid detergent goods of 100 weight parts, the content of described camellia seed oil is 3-8 weight %, the content of described polyoxyethylene nonylphenol ether is 8-15 weight %, and the content of described fatty alcohol-polyoxyethylene ether is 2-4 weight %, and the content of described fatty acyl monoethanolamine and/or the two thanomin of fatty acyl is 1-3 weight %, the content of described toxilic acid list sodium is 2-4 weight %, and the content of described Sodium Benzoate is 0.05-0.3 weight %.
According to liquid detergent goods described in any one in claim 3-5, wherein, 6. also containing water, pigment and essence in described liquid detergent goods.
7. the preparation method of liquid detergent goods, it is characterized in that, the method comprises: two to camellia seed oil, polyoxyethylene nonylphenol ether, fatty alcohol-polyoxyethylene ether, fatty acyl monoethanolamine and/or fatty acyl thanomin, toxilic acid list sodium, Sodium Benzoate, pigment and essence are mixed with water.
8. method according to claim 7, wherein, the method comprises:
(1) first two to water, fatty acyl monoethanolamine and/or fatty acyl thanomin is mixed with polyoxyethylene nonylphenol ether, then add toxilic acid list sodium and fatty alcohol-polyoxyethylene ether, mixture is heated at 40-55 DEG C and stirs, make mixing of materials even;
(2) by step (1) gained material homogeneous at 40-60 DEG C, and material after homogeneous adds Sodium Benzoate;
(3) step (2) gained material is cooled to 30-40 DEG C, adds pigment and essence.
9. method according to claim 8, wherein, in step (3), regulates the pH to 6.0-8.5 of described material.
10. method according to claim 8 or claim 9, wherein, the method also comprises the step being undertaken step (3) gained material filtering.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610149594.1A CN105670834A (en) | 2016-03-16 | 2016-03-16 | Application of camellia seed oil in washing product, washing liquid product and preparation method of washing liquid product |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610149594.1A CN105670834A (en) | 2016-03-16 | 2016-03-16 | Application of camellia seed oil in washing product, washing liquid product and preparation method of washing liquid product |
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| CN105670834A true CN105670834A (en) | 2016-06-15 |
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| CN201610149594.1A Pending CN105670834A (en) | 2016-03-16 | 2016-03-16 | Application of camellia seed oil in washing product, washing liquid product and preparation method of washing liquid product |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106957746A (en) * | 2017-03-07 | 2017-07-18 | 广州小蜜蜂生物科技有限公司 | Baby's pro-skin plant liquid detergent |
| CN109735395A (en) * | 2019-02-27 | 2019-05-10 | 福建果宝生物科技有限公司 | A kind of cleaning solution of edible plant extract |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106957746A (en) * | 2017-03-07 | 2017-07-18 | 广州小蜜蜂生物科技有限公司 | Baby's pro-skin plant liquid detergent |
| CN109735395A (en) * | 2019-02-27 | 2019-05-10 | 福建果宝生物科技有限公司 | A kind of cleaning solution of edible plant extract |
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Application publication date: 20160615 |