CN109566658A - A kind of Medical antiseptic solution and preparation method thereof - Google Patents
A kind of Medical antiseptic solution and preparation method thereof Download PDFInfo
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- CN109566658A CN109566658A CN201811439883.0A CN201811439883A CN109566658A CN 109566658 A CN109566658 A CN 109566658A CN 201811439883 A CN201811439883 A CN 201811439883A CN 109566658 A CN109566658 A CN 109566658A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/12—Iodine, e.g. iodophors; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- Wood Science & Technology (AREA)
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- Natural Medicines & Medicinal Plants (AREA)
- Environmental Sciences (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
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- Pest Control & Pesticides (AREA)
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- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of Medical antiseptic solutions and preparation method thereof；Medical antiseptic solution includes the raw material of following parts by weight: 16-20 parts of honeysuckle, to 10-14 parts of leaf woods, 8-12 parts of stone sunshade, cut trailing plants 7-11 parts of summer, 4-8 parts of Artemisia spharocephala, 2-6 parts of potassium iodide, 1-5 parts of denseleaf crazyweed herb；The present invention using natural material honeysuckle, to leaf woods, stone sunshade, cut Xia Luo, Artemisia spharocephala and denseleaf crazyweed herb and potassium iodide be added and be prepared through above-mentioned technique, the Medical antiseptic solution bactericidal effect of preparation is good, human body is stimulated small, it has no toxic side effect, and preparation process is simple, it is easily industrialized production, production cost is low.
Description
Technical field
The present invention relates to a kind of thimerosal, specifically a kind of Medical antiseptic solution and preparation method thereof.
Background technique
Medical Devices, which refer to, is used alone or in combination the instrument in human body, equipment, utensil, material or other articles,
It also include required software.Medical Devices are medical treatment, scientific research, teaching, mechanism, the most basic element of clinical speciality work, that is, are wrapped
Professional medical equipment is included, also includes domestic medical device.Medical Devices are easily adhered with contacts such as bacterial viruses certain for a long time
Germ, more directly with the equipment of human contact, for prevent germ in equipment infect medical staff need to its into
Row periodically disinfection, because general device volume is larger, now mostly uses thimerosal to carry out disinfection.
Existing Medical antiseptic solution to using chemical industry synthesis, pollute larger by when production, and has certain thorn to human body
Swash property, use is dangerous, not strong to the killing performance of germ although strong to common bacteria sterilizing ability.
Summary of the invention
The purpose of the present invention is to provide a kind of Medical antiseptic solutions and preparation method thereof, to solve to mention in above-mentioned background technique
Out the problem of.
To achieve the above object, the invention provides the following technical scheme:
A kind of Medical antiseptic solution, the raw material including following parts by weight: 16-20 parts of honeysuckle, to 10-14 parts of leaf woods, stone
8-12 parts of sunshade cuts trailing plants 7-11 parts of summer, 4-8 parts of Artemisia spharocephala, 2-6 parts of potassium iodide, 1-5 parts of denseleaf crazyweed herb.
As a further solution of the present invention: the raw material including following parts by weight: 17-19 parts of honeysuckle, to leaf woods 11-
13 parts, 9-11 parts of stone sunshade, cut trailing plants 8-10 parts of summer, 5-7 parts of Artemisia spharocephala, 3-5 parts of potassium iodide, 2-4 parts of denseleaf crazyweed herb.
As a further solution of the present invention: the raw material including following parts by weight: 18 parts of honeysuckle, to 12 parts of leaf woods,
10 parts of stone sunshade cuts 9 parts of summer trailing plants, 6 parts of Artemisia spharocephala, 4 parts of potassium iodide, 3 parts of denseleaf crazyweed herb.
The pharmacological property of the used raw medicinal material of the present invention is as follows:
Honeysuckle, alias honeysuckle flowers, aigret mandarin duck flower, golden flower, honeysuckle flower, honeysuckle etc. have clearing heat and detoxicating, anti-inflammatory detumescence effect,
With resisting pathogenic microbes, antitoxin, anti-inflammatory, promotion inflammatory cell phagocytic function effect.
To leaf woods, alias baseline ginseng, Rui ginseng, there is desinsection, detoxicating functions.
Stone sunshade, alias stone lion, mountain brain root, has heat-clearing, detoxicating functions.
Xia Luo is cut, alias camellia field has effects that removing damp-heat, purging fire for removing toxin.
Artemisia spharocephala, alias seed wormwood artemisia have the Xiaoyan San stasis of blood, qi-regulating disinsection efficiency.
Denseleaf crazyweed herb, alias are put on flesh wheatgrass, watermifoil whin, have effects that it is clearing heat and detoxicating, detumescence hemostasis, control influenza.
A kind of preparation method of Medical antiseptic solution, comprising the following steps:
(1) it is dried after cleaning honeysuckle and Artemisia spharocephala, the soaking in Chinese liquor 25-35d of 2-4 times of its gross mass is added, filtered
Obtain filtrate A and filter residue；
(2) by filter residue with to leaf woods, stone sunshade, cut Xia Luo and denseleaf crazyweed herb is dried, crushed into hybrid particles, mixing is added
The medicinal alcohol of 6-10 times of grain is heated to 85-95 DEG C, insulated and stirred 2-4h under agitation, crosses 200 meshes and obtains liquor B；
(3) filtrate A is mixed with liquor B, 40-60 DEG C is heated under stirring condition, potassium iodide, insulated and stirred 20- is added
40min, up to Medical antiseptic solution after cooling.
As a further solution of the present invention: white wine degree is 50-60 degree in the step (1).
As a further solution of the present invention: hybrid particles partial size is 100-200 μm in the step (2), mixing speed
For 200-400rpm.
As a further solution of the present invention: crossing 200 meshes in the step (2) and obtain liquor B.
As a further solution of the present invention: mixing speed is 100-200rpm in the step (3).
Compared with prior art, the beneficial effects of the present invention are: using natural material honeysuckle, to leaf woods, stone sunshade, cut
Xia Luo, Artemisia spharocephala and denseleaf crazyweed herb are simultaneously added potassium iodide and are prepared through above-mentioned technique, and the Medical antiseptic solution bactericidal effect of preparation is good,
It is small to human body stimulation, it has no toxic side effect, and preparation process is simple, it is easy to accomplish industrialized production, production cost are low.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of Medical antiseptic solution, the raw material including following parts by weight: 16 parts of honeysuckle, to 10 parts of leaf woods, stone sunshade 8
Part cuts 7 parts of summer trailing plants, 4 parts of Artemisia spharocephala, 2 parts of potassium iodide, 1 part of denseleaf crazyweed herb.
A kind of preparation method of Medical antiseptic solution, comprising the following steps:
(1) it is dried after cleaning honeysuckle and Artemisia spharocephala, the soaking in Chinese liquor 25d that 2 times of degrees of its gross mass are 50 degree is added,
Filter to get filtrate A and filter residue；
(2) by filter residue with to leaf woods, stone sunshade, cut Xia Luo and denseleaf crazyweed herb is dried, crushed into the mixing that partial size is 100 μm
6 times of hybrid particles of medicinal alcohol is added in grain, and 85 DEG C, insulated and stirred 2h are heated under the stirring condition of 200rpm, crosses 200
Mesh obtains liquor B；
(3) filtrate A is mixed with liquor B, 40 DEG C is heated under the stirring condition of 100rpm, potassium iodide, heat preservation is added
20min is stirred, up to Medical antiseptic solution after cooling.
Embodiment 2
A kind of Medical antiseptic solution, the raw material including following parts by weight: 17 parts of honeysuckle, to 11 parts of leaf woods, stone sunshade 9
Part cuts 8 parts of summer trailing plants, 5 parts of Artemisia spharocephala, 3 parts of potassium iodide, 2 parts of denseleaf crazyweed herb.
A kind of preparation method of Medical antiseptic solution, comprising the following steps:
(1) it is dried after cleaning honeysuckle and Artemisia spharocephala, the soaking in Chinese liquor that 2.5 times of degrees of its gross mass are 53 degree is added
28d, filter to get filtrate A and filter residue；
(2) by filter residue with to leaf woods, stone sunshade, cut Xia Luo and denseleaf crazyweed herb is dried, crushed into the mixing that partial size is 125 μm
Grain is added 7 times of hybrid particles of medicinal alcohol, 88 DEG C, insulated and stirred 2.5h is heated under the stirring condition of 250rpm, mistake
200 meshes obtain liquor B；
(3) filtrate A is mixed with liquor B, 45 DEG C is heated under the stirring condition of 125rpm, potassium iodide, heat preservation is added
25min is stirred, up to Medical antiseptic solution after cooling.
Embodiment 3
A kind of Medical antiseptic solution, the raw material including following parts by weight: 18 parts of honeysuckle, to 12 parts of leaf woods, stone sunshade 10
Part cuts 9 parts of summer trailing plants, 6 parts of Artemisia spharocephala, 4 parts of potassium iodide, 3 parts of denseleaf crazyweed herb.
A kind of preparation method of Medical antiseptic solution, comprising the following steps:
(1) it is dried after cleaning honeysuckle and Artemisia spharocephala, the soaking in Chinese liquor 30d that 3 times of degrees of its gross mass are 55 degree is added,
Filter to get filtrate A and filter residue；
(2) by filter residue with to leaf woods, stone sunshade, cut Xia Luo and denseleaf crazyweed herb is dried, crushed into the mixing that partial size is 150 μm
8 times of hybrid particles of medicinal alcohol is added in grain, and 90 DEG C, insulated and stirred 3h are heated under the stirring condition of 300rpm, crosses 200
Mesh obtains liquor B；
(3) filtrate A is mixed with liquor B, 50 DEG C is heated under the stirring condition of 150rpm, potassium iodide, heat preservation is added
30min is stirred, up to Medical antiseptic solution after cooling.
Embodiment 4
A kind of Medical antiseptic solution, the raw material including following parts by weight: 19 parts of honeysuckle, to 13 parts of leaf woods, stone sunshade 11
Part cuts 10 parts of summer trailing plants, 7 parts of Artemisia spharocephala, 5 parts of potassium iodide, 4 parts of denseleaf crazyweed herb.
A kind of preparation method of Medical antiseptic solution, comprising the following steps:
(1) it is dried after cleaning honeysuckle and Artemisia spharocephala, the soaking in Chinese liquor that 3.5 times of degrees of its gross mass are 58 degree is added
32d, filter to get filtrate A and filter residue；
(2) by filter residue with to leaf woods, stone sunshade, cut Xia Luo and denseleaf crazyweed herb is dried, crushed into the mixing that partial size is 175 μm
Grain is added 9 times of hybrid particles of medicinal alcohol, 82 DEG C, insulated and stirred 3.5h is heated under the stirring condition of 350rpm, mistake
200 meshes obtain liquor B；
(3) filtrate A is mixed with liquor B, 55 DEG C is heated under the stirring condition of 180rpm, potassium iodide, heat preservation is added
35min is stirred, up to Medical antiseptic solution after cooling.
Embodiment 5
A kind of Medical antiseptic solution, the raw material including following parts by weight: 20 parts of honeysuckle, to 14 parts of leaf woods, stone sunshade 12
Part cuts 11 parts of summer trailing plants, 8 parts of Artemisia spharocephala, 6 parts of potassium iodide, 5 parts of denseleaf crazyweed herb.
A kind of preparation method of Medical antiseptic solution, comprising the following steps:
(1) it is dried after cleaning honeysuckle and Artemisia spharocephala, the soaking in Chinese liquor 35d that 4 times of degrees of its gross mass are 60 degree is added,
Filter to get filtrate A and filter residue；
(2) by filter residue with to leaf woods, stone sunshade, cut Xia Luo and denseleaf crazyweed herb is dried, crushed into the mixing that partial size is 200 μm
10 times of hybrid particles of medicinal alcohol is added in grain, and 95 DEG C, insulated and stirred 4h are heated under the stirring condition of 400rpm, crosses 200
Mesh obtains liquor B；
(3) filtrate A is mixed with liquor B, 60 DEG C is heated under the stirring condition of 200rpm, potassium iodide, heat preservation is added
40min is stirred, up to Medical antiseptic solution after cooling.
Comparative example 1
In addition to being free of Artemisia spharocephala in raw material, other preparation processes and embodiment 3 are consistent.
Comparative example 2
In addition to being free of denseleaf crazyweed herb in raw material, other preparation processes and embodiment 3 are consistent.
Comparative example 3
In addition to being free of Artemisia spharocephala and denseleaf crazyweed herb in raw material, other preparation processes and embodiment 3 are consistent.
Comparative example 4
Raw material and embodiment 3 are consistent, when preparation by honeysuckle, Artemisia spharocephala, to leaf woods, stone sunshade, cut Xia Luo and denseleaf crazyweed herb
The hybrid particles that partial size is 150 μm are dried, crushed into, 8 times of hybrid particles of medicinal alcohol are added, in the stirring condition of 300rpm
Under be heated to 90 DEG C, insulated and stirred 3h, cross 200 meshes and obtain filtrate, then temperature adjustment adds to 50 DEG C under the stirring condition of 150rpm
Enter potassium iodide, insulated and stirred 30min, up to Medical antiseptic solution after cooling.
Comparative example 5
Using commercially available Medical antiseptic solution as comparative example 5.
Experimental example 1
Sterilization ability test is carried out to Medical antiseptic solution prepared by embodiment 1-5 and comparative example 1-5, is trained in ten same specifications
It supports and cultivates the congener germ of equal amount (including equivalent influenza virus, hemolytic streptococcus, staphylococcus aureus and lung on ware
Scorching coccus), the Medical antiseptic solution for respectively corresponding addition equivalent embodiment 1-5 and comparative example 1-5 preparation kills germ, and
Killing rate is detected, testing result is shown in Table 1.
1 sterilization ability test result of table
| Project | Sterilization rate (%) |
| Embodiment 1 | 95.8 |
| Embodiment 2 | 96.2 |
| Embodiment 3 | 96.6 |
| Embodiment 4 | 96.3 |
| Embodiment 5 | 96.0 |
| Comparative example 1 | 89.8 |
| Comparative example 2 | 84.7 |
| Comparative example 3 | 72.9 |
| Comparative example 4 | 94.8 |
| Comparative example 5 | 88.2 |
The thimerosal sterilization rate of 1-5 of embodiment of the present invention preparation is apparently higher than existing product comparison as can be seen from Table 1
Example 5, sterilization rate improve about 9%, and comparative example 1 and comparative example 2 reduce Artemisia spharocephala and denseleaf crazyweed herb in raw material respectively in the feed,
It can be seen that there is synergistic effect using Artemisia spharocephala and denseleaf crazyweed herb simultaneously compared with comparative example, hence it is evident that improve sterilization rate, have
Substantive distinguishing features outstanding and significant progressive.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of Medical antiseptic solution, which is characterized in that the raw material including following parts by weight: 16-20 parts of honeysuckle, to leaf woods
10-14 parts, 8-12 parts of stone sunshade, cut trailing plants 7-11 parts of summer, 4-8 parts of Artemisia spharocephala, 2-6 parts of potassium iodide, 1-5 parts of denseleaf crazyweed herb.
2. Medical antiseptic solution according to claim 1, which is characterized in that the raw material including following parts by weight: honeysuckle
17-19 parts, to 11-13 parts of leaf woods, 9-11 parts of stone sunshade, cut trailing plants 8-10 parts of summer, 5-7 parts of Artemisia spharocephala, 3-5 parts of potassium iodide, chicken tail feather
It is 2-4 parts careless.
3. Medical antiseptic solution according to claim 1, which is characterized in that the raw material including following parts by weight: honeysuckle
18 parts, to 12 parts of leaf woods, 10 parts of stone sunshade, cut 9 parts of summer trailing plants, 6 parts of Artemisia spharocephala, 4 parts of potassium iodide, 3 parts of denseleaf crazyweed herb.
4. a kind of preparation method of Medical antiseptic solution a method according to any one of claims 1-3, which is characterized in that including following step
It is rapid:
(1) it is dried after cleaning honeysuckle and Artemisia spharocephala, the soaking in Chinese liquor 25-35d of 2-4 times of its gross mass is added, filter to obtain filter
Liquid A and filter residue；
(2) by filter residue with to leaf woods, stone sunshade, cut Xia Luo and denseleaf crazyweed herb is dried, crushed into hybrid particles, hybrid particles 6- is added
10 times of medicinal alcohol is heated to 85-95 DEG C, insulated and stirred 2-4h under agitation, crosses 200 meshes and obtains liquor B；
(3) filtrate A is mixed with liquor B, 40-60 DEG C is heated under stirring condition, potassium iodide, insulated and stirred 20- is added
40min, up to Medical antiseptic solution after cooling.
5. the preparation method of Medical antiseptic solution as claimed in claim 4, which is characterized in that white wine degree in the step (1)
For 50-60 degree.
6. the preparation method of Medical antiseptic solution as claimed in claim 4, which is characterized in that hybrid particles in the step (2)
Partial size is 100-200 μm, mixing speed 200-400rpm.
7. the preparation method of Medical antiseptic solution as claimed in claim 4, which is characterized in that mixing speed in the step (3)
For 100-200rpm.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110278968A (en) * | 2019-05-13 | 2019-09-27 | 李汝新 | A kind of manufacturing method of clinical care disinfectant |
Citations (2)
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|---|---|---|---|---|
| CN103585271A (en) * | 2013-10-17 | 2014-02-19 | 青岛昊源环境工程技术有限公司 | Anti-bacterial disinfectant |
| CN104116683A (en) * | 2014-08-12 | 2014-10-29 | 李娜 | Disinfectant hand sanitizer and application thereof |
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2018
- 2018-11-29 CN CN201811439883.0A patent/CN109566658A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103585271A (en) * | 2013-10-17 | 2014-02-19 | 青岛昊源环境工程技术有限公司 | Anti-bacterial disinfectant |
| CN104116683A (en) * | 2014-08-12 | 2014-10-29 | 李娜 | Disinfectant hand sanitizer and application thereof |
Non-Patent Citations (1)
| Title |
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| 贺延龄: "《环境微生物学》", 30 April 2001, 中国轻工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110278968A (en) * | 2019-05-13 | 2019-09-27 | 李汝新 | A kind of manufacturing method of clinical care disinfectant |
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