CN103844749B - A kind of preparation method of pillow fillings - Google Patents
A kind of preparation method of pillow fillings Download PDFInfo
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- CN103844749B CN103844749B CN201410062700.3A CN201410062700A CN103844749B CN 103844749 B CN103844749 B CN 103844749B CN 201410062700 A CN201410062700 A CN 201410062700A CN 103844749 B CN103844749 B CN 103844749B
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Abstract
The present invention relates to biological technical field; a kind of preparation method of functional health pillow fillings; the method with the seed of maiden cane for base-material; by controlling its moisture, then mix the plant component extracted, dry after then adding chitosan solution process; shitosan is made to form layer protecting film on the base-material adsorbing effective ingredients in plant; microwave treatment, makes the active ingredient slow releasing of plant, thus makes effect of pillow fillings gentle lasting.
Description
Technical field
The invention belongs to biological technical field, relate to pillow fillings preparation method.
Background technology
The health type pillow of the effects such as functional health pillow has referred to certain health-care effect, can play calm nerves, tranquilizing and allaying excitement, protection cervical vertebra.The physiotherapy principle of functional health pillow product can be summarized as two classes: " physical arrangement rehabilitation principle " and " natural plant material for treating principle ".
Physical arrangement rehabilitation principle refers to the shape (hollow pillow) by pillow, and the material (pillow as natural in neck supporting moulding, jade pillow, low resilience are rested the head on) of pillow plays protection cervical vertebra, the effects such as improving water flood comfort level.
Natural plant material for treating principle refers to comes compatibility Chinese medicine or fragrant plant by aromatotherapy or traditional Chinese medical theory, fills pillow with natural plants, utilizes naturally volatilizing of aromatic substance in pillow, plays due health-care effect after being absorbed by the body.Concrete can have tranquilizing and allaying excitement, promoting blood circulation and removing blood stasis, hypotensive, the effects such as Xie Yu of regulating the flow of vital energy.Famous in ancient physician Huatuo, SUN Si miao early have the theory of " Wen Xiang gets rid of illness ", control head, all diseases of neck with medicine-filled pillow.Ming Dynasty's Li Shizhen (1518-1593 A.D.) also once repeatedly mentioned the principle that medicine-filled pillow is cured the disease in Compendium of Material Medica.The draft medicine-filled pillow of high-quality should condense more than all chis of pillow with its medicine perfume (or spice) especially, and its smell is light and quite well, weak for a long time and not, turbid clearly and not, quiet and do not fall apart, loose and do not walk.
At present, market has occurred the seed of many natural plants, root, stem, leaf, flower and fruit etc. fill the pillow of pillow making, in this type of product utilization plant, the volatilization naturally of aromatic substance, plays tranquilizing and allaying excitement, hypotensive, the effects such as Xie Yu of regulating the flow of vital energy.Dark the liking by Chinese Consumer's of this class functional health pillow, occupies larger share in functional health pillow field.Although plant series functional health pillow has many advantages, but, adopt plant directly as the filler of pillow, there are two large shortcomings; One is, the natural evaporation rate of the aromatic substance in natural plants is very fast, high at use initial stage volatile concentrations, produces spread effect on the contrary; In use the concentration of phase and later stage volatile matter declines can affect use effect again.Two are, the seed of natural plants, root, stem, leaf, flower and fruit repeatedly rub and extrude in Long-Time Service process, can cause the historrhexis of plant itself and powdered, unhealthful on the contrary after being inhaled into.If the active ingredient slow releasing of natural plants can be made and avoid directly using the tissue filling of plant itself, will effectively overcome above drawback.
Maiden cane formal name used at school is millet, is grass family Panicum annual herb.A kind of precocity, drought-enduring Fodder and food crop.Round-grained rice person Gu claims Ji, Ji, now claims millet, broom corn millet.Glutinous person's Gu claims broomcorn millet, now claims broomcorn millet, sticky broom corn millet or yellow grain.Its seed size formed is homogeneous, quality is solid, have as pillow filler that gas permeability is good, good fluidity, the features such as fungus resistance is strong, are commonly used for main stuffing, then be aided with the plant components such as chrysanthemum, Cassia occidentalis, selfheal, honeysuckle and lophatherum gracile make functional health pillow.
Shitosan (chitosan) is that the chitin (chitin) extensively existed by nature obtains through deacetylation, and chemical name is Chitosan (1-4)-2-amino-B-D glucose.Shitosan has many excellent functional characters and potential using value, and wherein film forming is very noticeable, has been cross-linked to form spacial framework, easy film forming between its molecule, and this film hot strength is large, good toughness, alkaline-resisting and organic solvent-resistant.Therefore shitosan is as a kind of good membranes material, can be widely used at industrial circles such as food, medicine, weaving, chemical industry, papermaking.Shitosan can make various film, as food fresh keeping film, edible film with Preparation of Biodegradable Package Film, be separated filter membrane, waterproof membrane, medical film etc., be more and more subject to people's attention.After shitosan film forming, there is good biocompatibility and permeability, there are important R and D in slow releasing pharmaceutical and targeting medicine and be worth, be commonly used for the carrier of medicament slow release.Medicine carrying membrane has good medicament slow release performance.In the multiple method of administration of clinical treatment, the normal and various medicine compound of shitosan makes transdermal medicine film and the film of administration of swallowing, and reaches the object of protection and slowly-releasing.In addition, shitosan can also suppress the growth of various bacteria with active.A large amount of experiments shows, shitosan has obvious inhibitory action to the bacterium such as Escherichia coli and staphylococcus aureus.According to the study, by infiltrating in cell body, with the cytoplasm of anion in adherent cell body, and there is flocculation and upsetting the normal physiological activity of cell in shitosan, thus the growth of anti-bacteria.Therefore, shitosan is mainly used in the fresh-keeping and anticorrosion of food in field of food industry.
Summary of the invention
The object of the invention is to provide a kind of method and the product of preparing spacetabs type functional health pillow filler with maiden cane seed and shitosan.
The potency uniformity using the seed of plant, root, stem, leaf, flower and fruit etc. directly to exist as the filler of pillow for existing capability health pillow and persistence is poor and the shortcoming of not resistance to use, the present invention adopts that quality is solid, gas permeability is good, good fluidity, the maiden cane seed that fungus resistance is strong is base-material, after drying, make it that there is good water imbibition and oil absorption; The active ingredient in plant is extracted by modern Chinese herbal medicine extraction process of effective component such as water seaoning, the molten methods of alcohol, absorb or adsorption of effective component with dried base-material again, then certain density chitosan solution process is added, after drying, shitosan can having adsorbed active ingredient base-material surface and formed the biomembrane of one deck densification, by having made pillow fillings after microwave sterilization.
The concrete technical scheme of the present invention is as follows:
A kind of preparation method of pillow fillings:
(1) dry maiden cane seed is selected to be pillow base-material;
(2) by chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, one or more mixture of windproof, the bighead atractylodes rhizome, with ethanol or water effective component extracting, concentratedly concentrate is obtained;
(3) concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio, mix, then place 30-60 minute to obtain pillow base-material and concentrate mixture;
(4) chitosan solution is added in pillow base-material and concentrate mixture by the ratio by weight 1:20, mixes;
(5) microwave 20kW heats 6-8 minute; Cooling.
The dry maiden cane seed moisture content of step (1) is lower than 10%.
Step (4) described chitosan solution processes as follows: get the shitosan that deacetylation is greater than 70%, is dissolved in the lactic acid of 10%, and the content of shitosan is 2%, adjusts the pH value of solution to 3.0-6.5 with the NaHCO3 of 0.1Mol/L.
With ethanol or water effective component extracting, concentrate to obtain concentrate.Such as, conventional ethanol or water mild temperature can be adopted to soak, and the mode of filtrate reduced in volume obtains concentrate as medicinal extract or dry powder, and this is routine techniques, no longer superfluous words.
Concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio.If concentrate is medicinal extract, then after mixing with pillow base-material, drying processes again.
Beneficial effect of the present invention:
(1) the present invention is by forming breathable diaphragm with the maiden cane the surface of the seed that shitosan is adsorbing active ingredient of natural plant; aromatic substance in natural plants slowly and is equably discharged; the functional health pillow of filling pillow making with this filler can accomplish that smell is light and quite well; weak for a long time and not, action temperature is with lasting.
(2) the present invention is by extracting the active ingredient of plant, the pillow of directly being filled by the flower of plant, leaf and fruit etc. can be avoided in use to be squeezed and to rub defect that is broken and powdered easily occurs.
(3) the inventive method, shitosan itself has again good antibacterial bacteriostatic effect, and the filler that can make continues to play antibacterial and mouldproof effect in use procedure from now on.
(4) the present invention adopts first shitosan process, then the mode of microwave treatment, has collaborative bacteriostasis, effectively can kill the bacterium in material, have the effects such as good mildew-resistant.
Detailed description of the invention
Embodiment 1
A kind of preparation method of pillow fillings
1. select maiden cane seed to be base-material, by modes such as oven dry, by maiden cane seed drying, make it moisture lower than 10%;
2. chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, windproof, the bighead atractylodes rhizome, second alcohol and water are loaded multipotency by a certain percentage and extract concentration and recovery unit, effective component extracting, and concentrated;
3. will to extract and active ingredient after concentrating joins in dried maiden cane seed in the ratio of 2%-5%, mix in anistree agitator, then place 30-60 minute;
4. get the shitosan that deacetylation is greater than 70%, be dissolved in the lactic acid of 10%, the content of shitosan is 2%, with the NaHCO of 0.1Mol/L
3adjust the pH value of solution to 3.0-6.5;
5. by weight the ratio of 1:20, chitosan solution is added on and has adsorbed in the maiden cane seed of effective ingredients in plant, be uniformly mixed;
6. the maiden cane seed having adsorbed effective ingredients in plant and shitosan is sent into tunnel type micro wave heater (power 20kW), process 6 ~ 8 minutes;
7. collect the maiden cane processed, after cooling, become pillow fillings.
Embodiment 2
1, a preparation method for pillow fillings, comprises the steps:
(1) dry maiden cane seed is selected to be pillow base-material; Dry maiden cane seed moisture content is lower than 10%;
(2) by chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, one or more mixture of windproof, the bighead atractylodes rhizome, with ethanol or water effective component extracting, concentratedly concentrate is obtained;
(3) concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio, mix, then place 30-60 minute to obtain pillow base-material and concentrate mixture;
(4) chitosan solution is added in pillow base-material and concentrate mixture by the ratio by weight 1:20, mixes; Described chitosan solution processes as follows: get the shitosan that deacetylation is greater than 70%, is dissolved in the lactic acid of 10%, and the content of shitosan is 0.5%-2%, adjusts the pH value of solution to 3.0-6.5 with the NaHCO3 of 0.1Mol/L;
(5) microwave 20kW heats 6-8 minute; Cooling, makes pillow inner of pillow filler by the material-filling after process.
Embodiment 3
1, material preparation:
(1) dry maiden cane seed is selected to be pillow base-material;
(2) by chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, one or more mixture of windproof, the bighead atractylodes rhizome, with ethanol or water effective component extracting, concentratedly concentrate is obtained;
(3) concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio, mix, then place 30-60 minute to obtain pillow base-material and concentrate mixture.
2, sterilization mode: shitosan microwave Combined Processing method for disinfection, conventional microwave method for disinfection, be used alone the comparison to bacterium in material (pillow base-material and concentrate mixture), mould and coliform germicidal efficiency and material maximum temperature of shitosan and non-sterilization processing.
3, chitosan solution preparation: get the shitosan 500 grams that deacetylation is greater than 70%, be dissolved in the lactic acid of 10%, the content of shitosan is 2%, with the NaHCO of 0.1Mol/L
3adjust the pH value of solution to 3.0, cumulative volume 100 liters.
4, shitosan process: chitosan solution is added in pillow base-material and concentrate mixture by the ratio by weight 1:20, mixes;
Microwave treatment: microwave 20kW heats 6-8 minute.
5, according to after the process of following table different condition, national standard method (GB 4789.2-2010 pressed by different sample; GB4789.3-2010 and GB 4789.15-2010) measure total number of bacteria, coliform and fungi count, and measure the maximum temperature of material.
| Filler (maiden cane) | Total number of bacteria (cfu/g) | Coliform (MPN) | Fungi count (cfu/g) | Material maximum temperature |
| Non-sterilization | 159000 | 1100 | 3560 | 20℃ |
| Independent shitosan (consumption 10%, 6 minutes time) | 125300 | 870 | 2943 | 20℃ |
| Independent microwave treatment (power 20kw, time 6 minutes) | 1860 | 59 | 311 | 96℃ |
| First microwave (power 20kw, time 6 minutes)+shitosan process again (consumption 10%) | 1528 | 46 | 269 | 96℃ |
| First shitosan (consumption 10%)+microwave treatment (power 20kw, time 6 minutes) again | 102 | Do not detect | Do not detect | 85℃ |
Conclusion: first shitosan process, in microwave treatment, has collaborative bacteriostasis, better than shitosan process antibacterial action after independent shitosan, microwave, first microwave.
Claims (2)
1. a preparation method for pillow fillings, is characterized in that comprising the steps: that (1) selects dry maiden cane seed to be pillow base-material; (2) by chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, one or more mixture of windproof, the bighead atractylodes rhizome, with ethanol or water effective component extracting, concentratedly concentrate is obtained; (3) concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio, mix, then place 30-60 minute to obtain pillow base-material and concentrate mixture; (4) chitosan solution is added in pillow base-material and concentrate mixture by the ratio by weight 1:20, mixes; (5) microwave 20kW heats 6-8 minute; Cooling;
Step (4) described chitosan solution processes as follows: get the shitosan that deacetylation is greater than 70%, is dissolved in the lactic acid of 10%, and the content of shitosan is 0.5%-2%, adjusts the pH value of solution to 3.0-6.5 with the NaHCO3 of 0.1mol/L.
2. preparation method according to claim 1, is characterized in that the dry maiden cane seed moisture content of step (1) is lower than 10%.
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| CN201410062700.3A CN103844749B (en) | 2014-02-25 | 2014-02-25 | A kind of preparation method of pillow fillings |
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| CN201410062700.3A CN103844749B (en) | 2014-02-25 | 2014-02-25 | A kind of preparation method of pillow fillings |
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| CN103844749A CN103844749A (en) | 2014-06-11 |
| CN103844749B true CN103844749B (en) | 2015-10-28 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104799642B (en) * | 2015-05-09 | 2016-02-24 | 福建农林大学 | A kind of medicine is healed pillow with neck and preparation method thereof |
| CN105231740A (en) * | 2015-10-23 | 2016-01-13 | 李景超 | Pillow filled with plant seeds |
| CN108185750A (en) * | 2017-12-05 | 2018-06-22 | 重庆帕特企业管理咨询有限公司 | A kind of health taxad pillow and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2290264Y (en) * | 1996-05-22 | 1998-09-09 | 马君渭 | Baby's health pillow |
| CN101264254A (en) * | 2007-03-15 | 2008-09-17 | 朱建良 | Medicaments for silkworm excrement vein relaxing pillow and pillow made of the same and manufacturing method of the pillow |
| CN101361920A (en) * | 2008-08-25 | 2009-02-11 | 李富祥 | Traditional Chinese medicine combination of hypotension tranquilization pillow inner |
| CN101991319A (en) * | 2009-08-20 | 2011-03-30 | 安徽奥来新能源有限公司 | Novel Chinese medicament-plant health care pillow |
| CN102327011A (en) * | 2010-07-13 | 2012-01-25 | 江苏宝缦卧室用品有限公司 | Health-care traditional Chinese medicinal pillow |
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2014
- 2014-02-25 CN CN201410062700.3A patent/CN103844749B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2290264Y (en) * | 1996-05-22 | 1998-09-09 | 马君渭 | Baby's health pillow |
| CN101264254A (en) * | 2007-03-15 | 2008-09-17 | 朱建良 | Medicaments for silkworm excrement vein relaxing pillow and pillow made of the same and manufacturing method of the pillow |
| CN101361920A (en) * | 2008-08-25 | 2009-02-11 | 李富祥 | Traditional Chinese medicine combination of hypotension tranquilization pillow inner |
| CN101991319A (en) * | 2009-08-20 | 2011-03-30 | 安徽奥来新能源有限公司 | Novel Chinese medicament-plant health care pillow |
| CN102327011A (en) * | 2010-07-13 | 2012-01-25 | 江苏宝缦卧室用品有限公司 | Health-care traditional Chinese medicinal pillow |
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