CN109503238A - A kind of preparation method of the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid - Google Patents
A kind of preparation method of the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid Download PDFInfo
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- CN109503238A CN109503238A CN201811622976.7A CN201811622976A CN109503238A CN 109503238 A CN109503238 A CN 109503238A CN 201811622976 A CN201811622976 A CN 201811622976A CN 109503238 A CN109503238 A CN 109503238A
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- sulfate
- humic acid
- water soluble
- containing high
- activity humic
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- Organic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The present invention provides a kind of preparation method of liquid fertilizer of Water soluble fertilizer containing high-activity humic acid, it is mainly characterized by, high-activity humic acid organic fertilizer 10%-60%, urea 10%-20%, Diammonium phosphate (DAP) 10%-30%, potassium sulfate 10%-30%, magnesium sulfate 1%-5%, zinc sulfate 1%-5%, calcium oxide 1%-5%, ferrous sulfate 1%-5%, boric acid 0.1%-0.5%, ammonium molybdate 0.1%-0.5%, manganese sulfate 0.1%-0.5%, complexing agent 0.1%-4%.It is manufactured by its processing step, has chelated big, middle and trace element and trace element necessary to growing process;Wherein rich in mineral elements and the marine algae Organic nutrient such as mobilizing function humic acid, a variety of amino acid, multi-vitamins and calcium, magnesium, sulphur, iron, zinc, copper, boron, molybdenum, manganese, rare earth.
Description
Technical field
The present invention is a kind of containing high-activity humic acid Water soluble fertilizer liquid fertilizer, especially a kind of to be suitable for drip irrigation and spray irrigation
With a kind of preparation method containing high-activity humic acid Water soluble fertilizer liquid fertilizer of soilless cultivation, soil pouring and foliage spray.
Background technique
China's agricultural chemicals account for leading position in agricultural production in the latest 20 years, ignore arable land planting upper people
Ability to bear, largely apply chemical fertilizer, pesticide, the agricultural chemicals such as hormone.In addition the random discharge of plant gas municipal sewage, causes
Rural Plane Source Pollution is set to enter vicious circle.The quantitative change stress soil of pollutant loses fragile self-purification capacity, soil hardening
Soil fertility declines vigor no longer.According to related data report, Chinese chemical fertilizer usage amount position is at the forefront in the world, the chemical fertilizer in per hectare soil
Dosage is three times of world average level.How to extricate oneself from a plight, general organic fertilizer applies hardened soil, due to " nutritional deficiency disease ",
" lacking bacterium disease ", it is low that organic fertilizer cannot fully decompose conversion fertilizer efficiency.Be a farmer on hardened soil lean on be chemical pesticide protect
Driving convoy has been the fact that can not strive, and microbial activity bacterial manure will turn turtle in face of chemical pesticide.In recent years carry out surveying soil
Rational application of fertilizers only rests on the basis of n p k fertilizer decrement.Such as soil cannot be administered in strict accordance with the principle of balance fertilizing theory
Earth is to be difficult to extricate oneself from a plight in the short time.But food safety cannot wait, " belly " of 1,300,000,000 populations cannot wait.This is flat
Breath arable soil, which is degenerated, walks out the campaign of vicious circle, and Water soluble fertilizer containing high-activity humic acid is certain " the Saviour ".Make a general survey of state
The improvement of inside and outside agroecological environment and the demand of green food safety food, it is indubitable, Water soluble fertilizer containing high-activity humic acid
To there are unlimited wide development space and tempting market prospects.
Summary of the invention
The purpose of the present invention is deficiencies present in view of the above technology, provide a kind of water-soluble solution containing high-activity humic acid
Body method for preparing fertilizer.Big, middle and trace element and trace element necessary to growing process are chelated;Wherein rich in activation
The mineral elements such as function humic acid, a variety of amino acid, multi-vitamins and calcium, magnesium, sulphur, iron, zinc, copper, boron, molybdenum, manganese, rare earth and
Marine algae Organic nutrient.
The object of the present invention is achieved like this, including high-activity humic acid organic fertilizer, urea, Diammonium phosphate (DAP), potassium sulfate,
Magnesium sulfate, zinc sulfate, calcium oxide, ferrous sulfate, boric acid, ammonium molybdate, manganese sulfate, complexing agent.
It is characterized in that high-activity humic acid organic fertilizer 10%-60%, urea 10%-20%, Diammonium phosphate (DAP) 10%-30%, potassium sulfate
10%-30%, magnesium sulfate 1%-5%, zinc sulfate 1%-5%, calcium oxide 1%-5%, ferrous sulfate 1%-5%, boric acid 0.1%-0.5%, molybdic acid
Ammonium 0.1%-0.5%, manganese sulfate 0.1%-0.5%, complexing agent 0.1%-4%.
Step 1: element urea 10%-20%, Diammonium phosphate (DAP) 10%-30%, potassium sulfate 10%-30% are crushed to 100 respectively
Mesh is dissolved with water;
Step 2: by middle microelement magnesium sulfate 1%-5%, zinc sulfate 1%-5%, calcium oxide 1%-5%, ferrous sulfate 1%-5%, boric acid
0.1%-0.5%, ammonium molybdate 0.1%-0.5%, manganese sulfate 0.1%-0.5% are crushed to 100 mesh respectively, proportionally mixing for standby use;
Step 3: 20%-50% is contained into high-activity humic acid organic fertilizer and enters reaction kettle, heats 50-85 DEG C, is reacted 30-50 minutes;
Step 4: a great number of elements urea 10%-20%, Diammonium phosphate (DAP) 10%-30%, potassium sulfate after addition crushing is water-soluble in reaction kettle
10%-30%;Middle microelement magnesium sulfate 1%-5%, zinc sulfate 1%-5%, calcium oxide 1%-5%, ferrous sulfate 1%-5%, boron after crushing
Sour 0.1%-0.5%, ammonium molybdate 0.1%-0.5%, manganese sulfate 0.1%-0.5%, complexing agent 0.1%-4% heat 60-95 DEG C, react 40-
60 minutes;
Step 5: material in reactor is cooling, and this product is made in packaging.
The invention has the advantages that providing a kind of liquid fertilizer preparation method of Water soluble fertilizer containing high-activity humic acid.Chelating
Big, middle and trace element and trace element necessary to growing process;Wherein it is rich in mobilizing function humic acid, a variety of amino
The mineral elements such as acid, multi-vitamins and calcium, magnesium, sulphur, iron, zinc, copper, boron, molybdenum, manganese, rare earth and marine algae organic nutrition at
Point.
Specific embodiment
Forms bottom end
Below by specific embodiment, the present invention is described in further detail
Embodiment 1
1) a great number of elements urea 15%, Diammonium phosphate (DAP) 20%, potassium sulfate 10% are crushed to 100 mesh respectively, with material self weight 10%
Water is dissolved;
2) by middle microelement magnesium sulfate 3%, zinc sulfate 3%, calcium oxide 3%, ferrous sulfate 3%, boric acid 0.2%, ammonium molybdate 0.2%,
Manganese sulfate 0.2% is crushed to 100 mesh, mixing for standby use respectively;
3) enter reaction kettle containing high-activity humic acid organic fertilizer for 50%, heat 505 DEG C, react 30 minutes;
4) urea 15%, Diammonium phosphate (DAP) 20%, potassium sulfate 10%, magnesium sulfate 3%, zinc sulfate after addition crushing is water-soluble in reaction kettle
3%, calcium oxide 3%, ferrous sulfate 3%, boric acid 0.2%, ammonium molybdate 0.2%, 0.2% complexing agent 2% of manganese sulfate heat 60 DEG C, reaction 40
Minute, obtained solution are as follows: the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid.
Embodiment 2
1) a great number of elements urea 150%, Diammonium phosphate (DAP) 200%, potassium sulfate 100% are crushed to 100 mesh respectively, with material self weight 10%
Water dissolved;
2) by middle microelement magnesium sulfate 20%, zinc sulfate 20%, calcium oxide 20%, ferrous sulfate 15%, boric acid 0.2%, ammonium molybdate
0.2%, manganese sulfate 0.2% is crushed to 100 mesh, mixing for standby use respectively;
3) enter reaction kettle containing high-activity humic acid organic fertilizer for 50%, heat 505 DEG C, react 30 minutes;
4) urea 150%, Diammonium phosphate (DAP) 200%, potassium sulfate 100%, magnesium sulfate 20%, sulfuric acid after addition crushing is water-soluble in reaction kettle
Zinc 20%, calcium oxide 20%, ferrous sulfate 15%, boric acid 0.2%, ammonium molybdate 0.2%, manganese sulfate 0.2%, complexing agent 2% heat 70 DEG C,
Reaction 45 minutes, obtained solution are as follows: the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid.
Embodiment 3
1) a great number of elements urea 100%, Diammonium phosphate (DAP) 300%, potassium sulfate 200% are crushed to 100 mesh respectively, with material self weight 10%
Water dissolved;
2) by middle microelement magnesium sulfate 30%, zinc sulfate 20%, calcium oxide 20%, ferrous sulfate 10%, boric acid 0.2%, ammonium molybdate
0.2%, manganese sulfate 0.2% is crushed to 100 mesh, mixing for standby use respectively;
3) enter reaction kettle containing high-activity humic acid organic fertilizer for 50%, heat 505 DEG C, react 30 minutes;
4) urea 100%, Diammonium phosphate (DAP) 300%, potassium sulfate 200%, magnesium sulfate 30%, sulfuric acid after addition crushing is water-soluble in reaction kettle
Zinc 20%, calcium oxide 20%, ferrous sulfate 10%, boric acid 0.2%, ammonium molybdate 0.2%, manganese sulfate 0.2%, complexing agent 2%, heating 75
DEG C, it reacts 50 minutes, obtained solution are as follows: the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid.
Claims (9)
1. a kind of preparation method of the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid, characterized in that be made of following quality feeds:
High-activity humic acid organic fertilizer 10%-60%, urea 10%-20%, Diammonium phosphate (DAP) 10%-30%, potassium sulfate 10%-30%, magnesium sulfate 1%-
5%, zinc sulfate 1%-5%, calcium oxide 1%-5%, ferrous sulfate 1%-5%, boric acid 0.1%-0.5%, ammonium molybdate 0.1%-0.5%, manganese sulfate
0.1%-0.5%, complexing agent 0.1%-4%,
Step 1: a great number of elements urea 10%-20%, Diammonium phosphate (DAP) 10%-30%, potassium sulfate 10%-30% are crushed to 100 respectively
Mesh is dissolved with water;
Step 2: by middle microelement magnesium sulfate 1%-5%, zinc sulfate 1%-5%, calcium oxide 1%-5%, ferrous sulfate 1%-5%, boric acid
0.1%-0.5%, ammonium molybdate 0.1%-0.5%, manganese sulfate 0.1%-0.5% are crushed to 100 mesh respectively, proportionally mixing for standby use;
Step 3: 20%-50% is contained into high-activity humic acid organic fertilizer and enters reaction kettle, heats 50-85 DEG C, is reacted 30-50 minutes;
Step 4: a great number of elements urea 10%-20%, Diammonium phosphate (DAP) 10%-30%, potassium sulfate after addition crushing is water-soluble in reaction kettle
10%-30%;Middle microelement magnesium sulfate 1%-5%, zinc sulfate 1%-5%, calcium oxide 1%-5%, ferrous sulfate 1%-5%, boron after crushing
Sour 0.1%-0.5%, ammonium molybdate 0.1%-0.5%, manganese sulfate 0.1%-0.5%, complexing agent 0.1%-4% heat 60-95 DEG C, react 40-
60 minutes;
Step 5: material in reactor is cooling, and the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid is made in packaging.
2. a kind of preparation method of liquid fertilizer of Water soluble fertilizer containing high-activity humic acid according to claim 1, characterized in that
Urea described in step 1, Diammonium phosphate (DAP), potassium sulfate object feed-weight ratio 5%-10% dissolved in purified water.
3. a kind of preparation method of liquid fertilizer of Water soluble fertilizer containing high-activity humic acid according to claim 1, characterized in that
Middle microelement magnesium sulfate described in step 2, zinc sulfate, calcium oxide, ferrous sulfate, boric acid, ammonium molybdate, manganese sulfate mixing
Ratio are as follows: 1-5:1-5:1-5:1-5:1-0.5:1-0.5:1-0.5.
4. according to a kind of preparation method of the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid described in claim 1, characterized in that step
Contain in high-activity humic acid organic fertilizer described in rapid three, activated humic acid content >=7%, the content of organic matter >=25%.
5. according to a kind of preparation method of the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid described in claim 1, characterized in that step
Complexing agent described in rapid four is ethylenediamine tetraacetic acid (EDTA), 1,2-diaminocyclohexane tetraacetic acid, ethoxy second diammonium triacetic acid, proportion are as follows: 7:
1:0.5。
6. a kind of preparation method of liquid fertilizer of Water soluble fertilizer containing high-activity humic acid according to claim 1, characterized in that
Urea described in step 1, Diammonium phosphate (DAP), potassium sulfate object feed-weight ratio 5%-10% dissolved in purified water.
7. a kind of preparation method of liquid fertilizer of Water soluble fertilizer containing high-activity humic acid according to claim 1, characterized in that
Middle microelement magnesium sulfate described in step 2, zinc sulfate, calcium oxide, ferrous sulfate, boric acid, ammonium molybdate, manganese sulfate mixing
Ratio are as follows: 1-5:1-5:1-5:1-5:1-0.5:1-0.5:1-0.5.
8. according to a kind of preparation method of the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid described in claim 1, characterized in that step
Contain in high-activity humic acid organic fertilizer described in rapid three, activated humic acid content >=7%, the content of organic matter >=25%.
9. according to a kind of preparation method of the liquid fertilizer of Water soluble fertilizer containing high-activity humic acid described in claim 1, characterized in that step
Complexing agent described in rapid four is ethylenediamine tetraacetic acid (EDTA), 1,2-diaminocyclohexane tetraacetic acid, ethoxy second diammonium triacetic acid, proportion are as follows: 7:
1:0.5。
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110156518A (en) * | 2019-06-05 | 2019-08-23 | 中农中能生物科技有限公司 | A kind of plant gene cell fertilizer |
CN110550988A (en) * | 2019-09-23 | 2019-12-10 | 张梓榆 | Complexing product of mineral humic acid and inorganic salt fertilizer and preparation method thereof |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1110672A (en) * | 1995-02-22 | 1995-10-25 | 高美施活性液肥(石家庄)有限公司 | Active liquid fertilizer and its production method |
CN1401616A (en) * | 2002-07-24 | 2003-03-12 | 通辽绿阳科技开发有限公司 | Liquid multi-nutrient element humic acid fertilizer and preparing process thereof |
CN103539575A (en) * | 2013-11-08 | 2014-01-29 | 南开大学 | Development method of special efficient fulvic acid liquid compound fertilizer for potatoes |
CN107827580A (en) * | 2017-11-27 | 2018-03-23 | 贵阳开磷化肥有限公司 | A kind of fertilizer containing humic acid water-soluble and preparation method thereof |
-
2018
- 2018-12-28 CN CN201811622976.7A patent/CN109503238A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1110672A (en) * | 1995-02-22 | 1995-10-25 | 高美施活性液肥(石家庄)有限公司 | Active liquid fertilizer and its production method |
CN1401616A (en) * | 2002-07-24 | 2003-03-12 | 通辽绿阳科技开发有限公司 | Liquid multi-nutrient element humic acid fertilizer and preparing process thereof |
CN103539575A (en) * | 2013-11-08 | 2014-01-29 | 南开大学 | Development method of special efficient fulvic acid liquid compound fertilizer for potatoes |
CN107827580A (en) * | 2017-11-27 | 2018-03-23 | 贵阳开磷化肥有限公司 | A kind of fertilizer containing humic acid water-soluble and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110156518A (en) * | 2019-06-05 | 2019-08-23 | 中农中能生物科技有限公司 | A kind of plant gene cell fertilizer |
CN110550988A (en) * | 2019-09-23 | 2019-12-10 | 张梓榆 | Complexing product of mineral humic acid and inorganic salt fertilizer and preparation method thereof |
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