CN109463535A - A kind of preparation method and product of the antibacterial calcium-supplementing preparation promoting cray shell - Google Patents
A kind of preparation method and product of the antibacterial calcium-supplementing preparation promoting cray shell Download PDFInfo
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- CN109463535A CN109463535A CN201811390766.XA CN201811390766A CN109463535A CN 109463535 A CN109463535 A CN 109463535A CN 201811390766 A CN201811390766 A CN 201811390766A CN 109463535 A CN109463535 A CN 109463535A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23K20/00—Accessory food factors for animal feeding-stuffs
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- A23K20/105—Aliphatic or alicyclic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/24—Compounds of alkaline earth metals, e.g. magnesium
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/30—Oligoelements
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
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Abstract
The present invention relates to the preparation methods and product of a kind of antibacterial calcium-supplementing preparation for promoting cray shell, for during cray shell, pole need to replenish the calcium, it is in poor health, easily disseminated by bacterial virus, easily stress problem, the compound liquid-phase system of balance and stability is established with microelement, amino acid, multi-vitamins, citric acid in cordate houttuynia, calcium and magnesium etc., prepared product is a kind of antibacterial calcium-supplementing preparation that performance is stable, powerful.
Description
Technical field
The present invention relates to technical field of aquaculture, in particular to a kind of antibacterial calcium-supplementing preparation for promoting cray shell
Preparation method and product.
Background technique
Cray is introduced through Japan to China, from after entering China because its production capacity is strong, nutritive value it is higher and its
Delicious flavour, deep to be pursued by market, market is constantly in the state that supply falls short of demand, and it is far super single to cultivate cray economic benefit
One Rice Cropping or common aquaculture, therefore, domestic cray cultured area is also in tremendous expansion.With the hair of industry
Exhibition, the requirement to cray yield and quality is also higher and higher, also increasingly heavier to the specialty products for being suitable for cray cultivation
Depending on.
Calcium is one of the middle microelement that cray has the call, the variation of cray growthform, the development of organ
With amputation regeneration etc., will be completed by casting off a skin with shell.And it is calcareous be it is crucial, calcium is that cray crust must form portion
Point.Individual size is all in the case that calcium measures satisfaction in cray body, after shell speed, shell success rate and shell
It can increased, improve the disease resistance of cray, the final economic benefit for guaranteeing cultivation.Meanwhile calcium is launched into water body, it can
To increase the calcium content of water body, simultaneously effective promote the flourish of algae, so that water quality is reached fertilizer tender requirement living of feeling well, be feeding
It grows water body and breed variety provides natural production oxygen source and natural resisting stress protection.
Contain 20 kinds of amino acid in cray body, it especially must rich in 8 kinds of human bodies such as lysine, glutamic acid, tryptophans
The amino acid that needs and cannot synthesize, this is also the major reason that human nutrition scholar highly recommends cray.However, cray is wanted
Amino acid abundant is synthesized in vivo to be also required to expend a large amount of energy and nutrition, it therefore, can be direct for cray supplement
The amino acid nutrient being absorbed and utilized just seems particularly necessary, the cray body most weak stage especially after shell.
It meanwhile being the peak period that cray needs calcium during cray shell, and because of its physiological reason, stopping is taken the photograph
Food, the function and vigor of body can be reduced to extremely low degree, simultaneously as lacking the protection of crust, the weak meat of cray
Body portion is highly prone to mechanical damage, therefore and by bacterial disease, viral dip dyeing.
And the product replenished the calcium currently on the market for cray shell, it focuses mostly in the supplement or ammonia of single mineral calcium
The supplement of base acid, and sterilize and solved with antibacterial by chemistry or biological means.There is artificial high, mineral calcium absorption in this mode
The problems such as utilization rate is low.Meanwhile sterilizing antibacterial using chemical means during shell, also easily cause stress reaction, makes
At some side effects.
Therefore, during cray shell, calcium source how is quickly supplemented, energy is replenished in time, sterilizes antibacterial and reduces
Stress, it is always to be difficult to solve the problems, such as in breeding process.
Summary of the invention
It is an object of the invention to solve the deficiency of above-mentioned prior art, develop that a kind of promotion cray shell is antibacterial to replenish the calcium
Compound preparation energy is quickly supplemented for the weak phase after cray shell with the supply of calcium source during ensureing cray shell
Amount, while cray exempts from infecting for bacterial disease and virus during preventing and treating shell, and stress not.It is allowed to both increase production
Its disease-resistant antibacterial ability can be enhanced again.
In order to achieve the above object, the invention provides the following technical scheme:
A kind of preparation method of the antibacterial calcium-supplementing preparation of promotion cray shell of the invention, including following preparation step:
Step 1: houttuynia extract is added in reaction kettle, add water and stir and is heated to 40-80 DEG C, it is added in excess
Microelement keeps temperature and stirring, and by the abundant chelatropic reaction of cordate houttuynia, the reaction time is 1-4 hours；
Step 2: excessive amino acid is added in the liquid of step 1, microelement in residue is chelated, reaction temperature is
40-80 DEG C, the reaction time is 1-4 hours；
Step 3: lasting stirring, lemon acid for adjusting pH is added to 6.5-7.5 to 30-40 DEG C in the liquid of cooling step two；
Step 4: the liquid of cooling step three is added multi-vitamins, continues stirring until multi-vitamins whole to room temperature
Dissolution, adding water to weight percentage of each component summation is 100% to get the antibacterial calcium-supplementing preparation for promoting cray shell.
Further, the Extraction solvent of the houttuynia extract is ethyl alcohol, ethyl acetate, petroleum ether or acetone.From fish
The extract extracted in raw meat grass dry powder, wherein rich in objects such as flavones, volatile oil, certain herbaceous plants with big flowers acyl acetaldehyde, laurene, alkaloid, organic acids
Matter is a kind of substance for being widely used in the field of Chinese medicines, has the multiple functions such as clearing heat and detoxicating, lung carbuncle pyemesis.Applied to aquatic products
Aqueous phase system can be stablized, inhibit the growth of coccus, vibrios, cyanobacteria, improve water bottom bacterial diversity and optimize Bacterial community.
Further, the amino acid is contained in compound amino acid possessed by 20 kinds of human bodies and cray body
Compound amino acid, this amino acid contains more carboxyl functional group, can chelate trace element ions in a large amount of, and small molecule
Amino acid is in by cray absorption process, and easily carrying calcium ion etc. is directly entered in cray body.And it is direct for cray
Using and conversion.
Further, the multi-vitamins are vitamin A, 2 kinds in B, E, C, D, K or two or more combination.Combination makes
With multi-vitamins, reduce during cray shell stress.
Further, the middle microelement is calcium, magnesium, iron, manganese, copper, zinc, boron, wherein calcium, magnesium, iron, manganese, copper, zinc
For nitrate state, chlorate state or EDTA state, boron is eight Boratex of borax, boric acid or four water.
Of the invention additionally provides a kind of antibacterial calcium-supplementing preparation for promoting cray shell, is based on above-mentioned preparation method, institute
It states preparation and is prepared from the following ingredients in percentage by composition: houttuynia extract 1-15%, amino acid 5-30%, middle microelement 1-
25%, multi-vitamins 0.1-1.5%, citric acid 0.05-1%, surplus are water；The middle microelement be calcium, magnesium, iron, manganese,
Copper, zinc, boron.
Further, it is prepared from the following ingredients in percentage by composition: houttuynia extract 1-10%, amino acid 5-25%,
Calcium 5-20%, magnesium, iron, manganese, copper, zinc, boron 0.5-5%, multi-vitamins 0.1-1%, citric acid 0.05-0.8% in total, surplus
For water.
Further, it is prepared from the following ingredients in percentage by composition: houttuynia extract 1%, amino acid 5%, calcium 5%,
Magnesium, iron, manganese, copper, zinc, boron in total 0.5%, multi-vitamins 0.1%, citric acid 0.05%, surplus is water.
Further, composition: houttuynia extract 2-8%, amino acid 6-20%, calcium are prepared from the following ingredients in percentage by
10-15%, 1-2%, multi-vitamins 0.2-0.8%, citric acid 0.1-0.5%, surplus are in total for magnesium, iron, manganese, copper, zinc, boron
Water.
Further, composition: houttuynia extract 4-6%, amino acid 8-15%, calcium are prepared from the following ingredients in percentage by
10-13%, magnesium, iron, manganese, copper, zinc, boron 1-1.5%, multi-vitamins 0.3-0.7%, citric acid 0.2-0.5% in total, surplus
For water.
The preparation method of a kind of antibacterial calcium-supplementing preparation promoting cray shell provided by the invention, for cray shell
Period, pole need to replenish the calcium, in poor health, easily be disseminated by bacterial virus, easily stress problem, with micro in cordate houttuynia, calcium and magnesium etc.
Element, amino acid, multi-vitamins, citric acid establish the compound liquid-phase system of balance and stability, and prepared product is a kind of
Performance is stablized, and powerful antibacterial calcium-supplementing preparation has the advantage that
1, utilize in microelement each ingredient of cordate houttuynia is sufficiently chelated, after preventing cordate houttuynia from entering water body by heavy metal from
Son is chelated and is inactivated, and is enhanced stability and lasting effect of the cordate houttuynia in water body, is enhanced its antibacterial sterilizing function；
2, the middle microelement based on calcium is sufficiently chelated using amino acid, so that cray is absorbing amino acid, fastly
While speed supplement energy, microelement in supplement makes element ion easily absorb easy transport；
3, the present invention will replenish the calcium, supplement energy, it is antibacterial disinfection, prevent stress four big function together as one, greatly reduce
The cost of labor that field uses, and application security is significantly improved.
4, the energy supply during cray shell can be effectively improved, calcium source supplement has and promotes cray shell, reduces
Soft-shell disease reduces bacterial disease incidence, increases the monomer multiple efficacies such as again.
Detailed description of the invention
Fig. 1 is a kind of preparation method flow chart for the antibacterial calcium-supplementing preparation for promoting cray shell in the present invention.
Specific embodiment
Below in conjunction with attached drawing of the invention, technical solution of the present invention is clearly and completely described.Based on this hair
Embodiment in bright, every other implementation obtained by those of ordinary skill in the art without making creative efforts
Example, shall fall within the protection scope of the present invention.
Embodiment 1
As shown in Figure 1,20kg houttuynia extract is added in reaction kettle, adds water to 600kg and stirs and be heated to 80 DEG C,
It being added 60kg calcium (pure), each 2kg of microelement (pure) in magnesium, iron, manganese, copper, zinc, boron etc. keeps 80 DEG C of temperature and stirring,
By the abundant chelatropic reaction of cordate houttuynia, the reaction time is 1 hour.
200kg amino acid is added in aforesaid liquid, maintains 80 DEG C of reaction temperatures, the reaction time is 1 hour.Persistently stir
It mixes, lemon acid for adjusting pH is added to 6.5-7.5 to 30 DEG C in cooling aforesaid liquid.
To room temperature multi-vitamins 1.5kg is added, wherein vitamin A, each 500g of C, K, lasting stirring in the cooling liquid for preparing
It is all dissolved to multi-vitamins.Add water to 1000kg finally to get the antibacterial preparation replenished the calcium of cray shell is promoted.
Gained promotes the antibacterial each main ingredient content of preparation replenished the calcium of cray shell are as follows: cordate houttuynia 2%, amino acid
20%, calcium 6%, magnesium 0.2%, iron, manganese, copper, zinc, boron in total 1%, multi-vitamins 0.15%.
Embodiment 2
15kg houttuynia extract is added in reaction kettle, 500kg is added water to and stirs and be heated to 60 DEG C, addition 80kg calcium
(pure), each 5kg of microelement (pure) in magnesium, iron, manganese, copper, zinc, boron etc., keeps 60 DEG C of temperature and stirring, cordate houttuynia is filled
Divide chelatropic reaction, the reaction time is 2 hours.
240kg amino acid is added in aforesaid liquid, maintains 60 DEG C of reaction temperatures, the reaction time is 2 hours.Persistently stir
It mixes, lemon acid for adjusting pH is added to 6.5-7.5 to 30 DEG C in cooling aforesaid liquid.
To room temperature multi-vitamins 2.0kg is added, wherein vitamin B, each 500g of A, C, K, are persistently stirred in the cooling liquid for preparing
It mixes to multi-vitamins and all dissolves.Add water to 1000kg finally to get the antibacterial preparation replenished the calcium of cray shell is promoted.
Gained promotes the antibacterial each main ingredient content of preparation replenished the calcium of cray shell are as follows: cordate houttuynia 1.5%, amino acid
24%, calcium 8%, magnesium 0.5%, iron, manganese, copper, zinc, boron in total 2.5%, multi-vitamins 0.2%.
Embodiment 3
30kg houttuynia extract is added in reaction kettle, 400kg is added water to and stirs and be heated to 55 DEG C, addition 120kg
Calcium (pure), each 1kg of microelement (pure) in magnesium, iron, manganese, copper, zinc, boron etc., keeps 55 DEG C of temperature and stirring, by cordate houttuynia
Abundant chelatropic reaction, reaction time are 3 hours.
160kg amino acid is added in aforesaid liquid, maintains 55 DEG C of reaction temperatures, the reaction time is 3 hours.Persistently stir
It mixes, lemon acid for adjusting pH is added to 6.5-7.5 to 30 DEG C in cooling aforesaid liquid.
The cooling liquid for preparing is added multi-vitamins 2.5kg, wherein vitamin B, each 500g of A, C, K, E, continues to room temperature
Stirring is all dissolved to multi-vitamins.Add water to 1000kg finally to get the antibacterial preparation replenished the calcium of cray shell is promoted.
Gained promotes the antibacterial each main ingredient content of preparation replenished the calcium of cray shell are as follows: cordate houttuynia 3%, amino acid
16%, calcium 12%, magnesium 0.1%, iron, manganese, copper, zinc, boron in total 0.5%, multi-vitamins 0.25%.
Experimental example
The antibacterial preparation replenished the calcium of obtained promotion cray shell to embodiment 1-3 is subjected to field trial, totally 4 500
㎡ little Chi, wherein in 4-6 month of three little Chi in cray shell early period and peak period, use sample one obtained by embodiment in every 15 days
Secondary, each dosage is 1kg/ mus, and totally 4 times, the 4th little Chi is control, uses nontraditional amino acid and calcium powder.It is used in last time
Later the 15th day, every little Chi caught 100 at random, detected average monomer weight, the rotten tail rate of gill rot, crust abnormal rate, sampling observation knot
Fruit is as shown in table 1 below.
Table 1
| Average monomer weight (g) | The rotten tail rate (only) of gill rot | Crust abnormal rate (only) | |
| Embodiment 1 | 42.5 | 0 | 2 |
| Embodiment 2 | 39.8 | 2 | 0 |
| Embodiment 3 | 40.2 | 1 | 0 |
| Control group | 30.7 | 7 | 8 |
It can be seen that using the antibacterial preparation replenished the calcium of cray shell prepared by the present invention, compared with conventional formulation, monomer
Have again and significantly improve, while the rotten tail rate of gill rot, crust abnormal rate are remarkably decreased.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of preparation method for the antibacterial calcium-supplementing preparation for promoting cray shell, which is characterized in that including following preparation step:
Step 1: houttuynia extract is added in reaction kettle, add water and stir and is heated to 40-80 DEG C, it is added micro in excess
Element keeps temperature and stirring, and by the abundant chelatropic reaction of cordate houttuynia, the reaction time is 1-4 hours；
Step 2: excessive amino acid is added in the liquid of step 1, and microelement in chelating residue, reaction temperature 40-80
DEG C, the reaction time is 1-4 hours；
Step 3: lasting stirring, lemon acid for adjusting pH is added to 6.5-7.5 to 30-40 DEG C in the liquid of cooling step two；
Step 4: the liquid of cooling step three is added multi-vitamins, it is all molten to continue stirring until multi-vitamins to room temperature
Solution, adding water to weight percentage of each component summation is 100% to get the antibacterial calcium-supplementing preparation for promoting cray shell.
2. a kind of preparation method of antibacterial calcium-supplementing preparation for promoting cray shell according to claim 1, feature exist
In the Extraction solvent of the houttuynia extract is ethyl alcohol, ethyl acetate, petroleum ether or acetone.
3. a kind of preparation method of antibacterial calcium-supplementing preparation for promoting cray shell according to claim 1, feature exist
In the amino acid is compound amino acid possessed by 20 kinds of human bodies.
4. a kind of preparation method of antibacterial calcium-supplementing preparation for promoting cray shell according to claim 1, feature exist
In, multi-vitamins be vitamin A, 2 kinds or two or more combination in B, E, C, D, K.
5. a kind of preparation method of antibacterial calcium-supplementing preparation for promoting cray shell according to claim 1, feature exist
In the middle microelement is calcium, magnesium, iron, manganese, copper, zinc, boron, wherein calcium, magnesium, iron, manganese, copper, zinc are nitrate state, chlorination
Salt state or EDTA state, boron are eight Boratex of borax, boric acid or four water.
6. a kind of antibacterial calcium-supplementing preparation for promoting cray shell, which is characterized in that based on such as any one of claim 1-5 institute
The preparation method stated, the preparation are prepared from the following ingredients in percentage by composition: houttuynia extract 1-15%, amino acid 5-
30%, middle microelement 1-25%, multi-vitamins 0.1-1.5%, citric acid 0.05-1%, surplus is water；It is micro in described
Element is calcium, magnesium, iron, manganese, copper, zinc, boron.
7. a kind of antibacterial calcium-supplementing preparation for promoting cray shell according to claim 6, which is characterized in that by following heavy
The component for measuring percentage is constituted: houttuynia extract 1-10%, amino acid 5-25%, calcium 5-20%, magnesium, iron, manganese, copper, zinc, boron
0.5-5% in total, multi-vitamins 0.1-1%, citric acid 0.05-0.8%, surplus are water.
8. a kind of antibacterial calcium-supplementing preparation for promoting cray shell according to claim 7, which is characterized in that by following heavy
The component for measuring percentage is constituted: houttuynia extract 1%, amino acid 5%, calcium 5%, magnesium, iron, manganese, copper, zinc, boron are in total
0.5%, multi-vitamins 0.1%, citric acid 0.05%, surplus is water.
9. a kind of antibacterial calcium-supplementing preparation for promoting cray shell according to claim 7, which is characterized in that by following heavy
The component for measuring percentage is constituted: houttuynia extract 2-8%, amino acid 6-20%, calcium 10-15%, magnesium, iron, manganese, copper, zinc, boron
1-2% in total, multi-vitamins 0.2-0.8%, citric acid 0.1-0.5%, surplus are water.
10. a kind of antibacterial calcium-supplementing preparation for promoting cray shell according to claim 9, which is characterized in that by following
The component of weight percent is constituted: houttuynia extract 4-6%, amino acid 8-15%, calcium 10-13%, magnesium, iron, manganese, copper, zinc,
1-1.5%, multi-vitamins 0.3-0.7%, citric acid 0.2-0.5%, surplus are water to boron in total.
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| CN201811390766.XA CN109463535A (en) | 2018-11-21 | 2018-11-21 | A kind of preparation method and product of the antibacterial calcium-supplementing preparation promoting cray shell |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102144724A (en) * | 2010-02-08 | 2011-08-10 | 上海朝翔生物技术有限公司 | Preparation method of heartleaf houttuynia herb extract feed additive |
| CN106333140A (en) * | 2016-08-26 | 2017-01-18 | 湖南金欧农业科技有限公司 | Crawfish unshelling hormone |
| CN107535401A (en) * | 2017-10-27 | 2018-01-05 | 宿松县东求水产开发有限公司 | A kind of method of replenishing the calcium of cray |
| CN107981097A (en) * | 2017-11-25 | 2018-05-04 | 广州智龙生物科技有限公司 | Promote the nutrient and its preparation and application of aquatic crustacean health |
-
2018
- 2018-11-21 CN CN201811390766.XA patent/CN109463535A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102144724A (en) * | 2010-02-08 | 2011-08-10 | 上海朝翔生物技术有限公司 | Preparation method of heartleaf houttuynia herb extract feed additive |
| CN106333140A (en) * | 2016-08-26 | 2017-01-18 | 湖南金欧农业科技有限公司 | Crawfish unshelling hormone |
| CN107535401A (en) * | 2017-10-27 | 2018-01-05 | 宿松县东求水产开发有限公司 | A kind of method of replenishing the calcium of cray |
| CN107981097A (en) * | 2017-11-25 | 2018-05-04 | 广州智龙生物科技有限公司 | Promote the nutrient and its preparation and application of aquatic crustacean health |
Non-Patent Citations (1)
| Title |
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| 周德生: "《实用临床中西药合用解读》", 30 November 2016, 山西科学技术出版社 * |
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