CN109457482A - A kind of coffee carbon keeps warm the preparation method of super soft trousering and its super soft finishing agent - Google Patents

A kind of coffee carbon keeps warm the preparation method of super soft trousering and its super soft finishing agent Download PDF

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Publication number
CN109457482A
CN109457482A CN201811300255.4A CN201811300255A CN109457482A CN 109457482 A CN109457482 A CN 109457482A CN 201811300255 A CN201811300255 A CN 201811300255A CN 109457482 A CN109457482 A CN 109457482A
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China
Prior art keywords
super soft
yarn
trousering
coffee carbon
finishing agent
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CN201811300255.4A
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CN109457482B (en
Inventor
胡海龙
胡哲
刘宇术
陆国荣
王建江
周辉
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Zhejiang Shiyada Textile Co.,Ltd.
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Zhejiang Shi Yada Textile Co Ltd
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    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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    • D03D13/008—Woven fabrics characterised by the special disposition of the warp or weft threads, e.g. with curved weft threads, with discontinuous warp threads, with diagonal warp or weft characterised by weave density or surface weight
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Abstract

The application provides the preparation method that a kind of coffee carbon keeps warm super soft trousering and its super soft finishing agent, belongs to textile finishing technical field.Using double-layered structure's structure, by warp thread and weft weaving, the warp thread selects the tencel of 16-32s, weft yarn selects three kinds of yarns: A yarn is that R70/JC30 is bifilar, B yarn is C+70D, and C yarn is 60/40 coffee carbon of 16-30s/tencel G100, and weft yarn A, B, C are weaved by the circulation that puts in order of B, C, A, B, A, C, B, A, A, and it is located at coffee carbon fiber in fabric inner layer, then through dyeing and finishing technology.The application is applied to the processing of the fabrics such as trousering, has many advantages, such as that skin-friendly and comfort are good, reduces electrostatic, realizes two-color effect.

Description

A kind of coffee carbon keeps warm the preparation method of super soft trousering and its super soft finishing agent
Technical field
It keeps warm the preparation method of super soft trousering and its super soft finishing agent this application involves a kind of coffee carbon, belongs to textile finishing Technical field.
Background technique
In recent years, people are higher and higher to the functional requirements of textile, and the product of unification has been unable to satisfy people day The demand that benefit increases.With the prevalence of environmental protection and low-carbon, there is a kind of novel environment friendly coffee prepared using coffee grounds as raw material Carbon yarn.With good spinnability, while there are the characteristics such as smelly eliminating, heating, quick-drying, have far infrared, anion, heat accumulation, The functions such as warming, are very suitable to light and thin type autumn and winter clothes, and can suitably reduce air-conditioner temperature, reduce energy consumption.It is close several Year, consumer has a preference for frivolous, warming, comfortable, environment-friendly plus material, especially in the selection of pant fabric, Wo Men in autumn and winter Improve that original autumn and winter pant fabric is frivolous, warming aspect, is also studied at the super soft aspect of wearing comfort, be prepared for one The super soft finishing agent of kind, is used on this fabric, finally develops a kind of frivolous, warming, comfortable, super soft coffee carbon trousering, tool There is very vast market prospect.
Summary of the invention
In view of this, the purpose of the application first aspect is, a kind of coffee carbon is provided and is kept warm super soft trousering.This coffee carbon Heat accumulation thermal, the health properties for the super soft trousering figure processing coffee carbon that keeps warm, and it is elastic, two-color effect can reach by dyeing, There is particularly preferred skin-friendly and comfort after grabbing cropping, super soft arrangement.
To achieve the above object, the technical solution that the application takes is as follows:
A kind of coffee carbon keeps warm super soft trousering, which is the double-layered structure's structure formed by warp thread and weft weaving, is wrapped Fabric surface layer and fabric inner layer are included, the warp thread selects the tencel of 16-32s, and weft yarn selection A yarn, B yarn, three kinds: A yarn of C yarn are R70/JC30 is bifilar, B yarn be C+70D cotton packet spandex yarn, C yarn be coffee carbon/tencel G100, weft yarn A, B, C by B, C, A, B, A, C, B, A, A circulation weaving, is located at coffee carbon fiber in fabric inner layer.
During trousering provided herein is constituted, warp thread selects the tencel of 16-32s, and bright in color is soft, weft yarn Three kinds of yarns are selected, A yarn is that R70/JC30 is bifilar, i.e. viscose glue/combed cotton double strand yarn of 20-30s；B yarn is C+70D, that is, 20-30s Cotton packet spandex yarn；C yarn be 60/40 coffee carbon of 16-30s/tencel G100, weft yarn A, B, C put in order by B, C, A, B, A, C, the weaving of B, A, A circulation, this arrangement mode are conducive to coffee carbon yarn weaving in fabric inner layer, and it is warming to play it to greatest extent Performance；Institutional framework selects double-layered structure；Coffee carbon fiber design in fabric inner layer, after by grabbing shearing technology, fabric inner layer Villous layer, the rich reality of feel carry out final finishing by dedicated super soft finishing agent, and gained fabric has good heat accumulation thermal function Air-conditioner temperature can be suitably reduced in winter with super soft comfort, reduce energy consumption.
Further, as preferred:
The face weave technological parameter: through close: (60-90) piece/inch；Filling density: (110-130) piece/inch；Always through root Number: 5400-6000 root；Porter selects No. 65；Denting amplitude 205-210cm；650-750 revs/min of speed of weaving；Warp thread with Weft yarn A, C institutional framework is Three Up Three Down, and warp thread and weft yarn B institutional framework are fabric tissue are as follows: 1/1+3/3 is bis- one on the other Layer.
It further include having dyeing and finishing technology after the face weave, dyeing and finishing technology parameter are as follows: enzyme desizing-dyeing-pre-setting-is grabbed The super soft arrangement of cropping-- finished product sizing, the above-mentioned specific process parameter being related to are as follows:
Starch desizing enzyme LS-3:2-3g/L, temperature: 50-60 DEG C, time 20min, bath raio: 1:5；
Dyeing: active Nary Blue BET, 1.5% (owf) salt: 15-30g/L, color fixing agent: 5-10g/L, temperature: 50- 60 DEG C, time 30-60min, bath raio: 1:20；
Grab shearing technology: cylinder revolving speed 80-100r/min, tension 15-20N, ball woll number 2-5 times, cropping edge of a knife knife away from 0.5-0.8mm, cropping number 3-5 times；
Super soft arrangement: super soft finishing agent: 30-50g/L, nip pressure: 4.0-6.0MPa, pick-up: 80-85%, speed 12-15m/min, temperature: 185-195 DEG C.
The coffee carbon that above scheme provides keeps warm super soft trousering, and selecting coffee grounds is the novel environment friendly coffee carbon of raw material preparation Yarn has the functions such as far infrared, anion, heat accumulation, warming, by above-mentioned organizational structure design, grabs shearing technology etc. for face The thermal property of material plays to the limit, its coffee carbon keeps warm thermal resistance >=0.0560 ㎡/W of super soft trousering after tested, Crow Value >=0.40, heat preservation rate >=52% have good warmth retention property, hence it is evident that improve original autumn and winter pant fabric in warming and thickness The deficiency of aspect, after super soft arrangement have particularly preferred skin-friendly and comfort, can satisfy in recent years consumer in the autumn Frivolous, warming, comfortable, in terms of environment-friendly plus material the demand of winter seasonal bias, and air-conditioner temperature can be suitably reduced, it reduces the energy and disappears Consumption.
The second aspect purpose of the application is, prepares a kind of super soft finishing agent, improves the comfort property of fabric, reduces Electrostatic, and finally improve fabric class.
The above-mentioned super soft finishing agent of one kind, by weight percentage, which includes:
The preparation method of above-mentioned super soft finishing agent, comprising the following steps:
(1) accurately weigh parts by weight cyclohexyl secondary amino group silicone, isomerous tridecanol polyoxyethylene ether be placed in it is completely dry In the dry three-necked flask with thermometer；
(2) agitating device is loaded onto, starts blender, is started to warm up after mixing evenly to 50-60 DEG C, then be sequentially added into meter The double heptyl esters of measured octamethylcyclotetrasiloxane, hexamethyldisiloxane, phthalic acid, HYDROXY PROPYL METHYLCELLULOSE and positive fourth Alcohol, constant temperature stir 45-60min；
(3) system temperature is down to room temperature, measured dodecyl sodium sulfate and deionized water high-speed stirred 30min is added After discharge to get super soft finishing agent.
Above-mentioned cyclohexyl secondary amino group silicone can have an effect with hydroxyl, the carboxyl of fiber surface etc., firmly be adsorbed on On fiber, so that the confficient of static friction between fiber declines, it is soft smooth, fabric whiteness, water imbibition are not influenced, and are used for There is durable, soft gloss on fabric；Octamethylcyclotetrasiloxane, hexamethyldisiloxane all have good soft for fabric Soft, slickness, molecular size range is different, has particularly preferred soft synergistic effect for fabric after mixing.Hydroxypropyl first Base cellulose makes auxiliary agent have high surface activity, the transparency high after mixing with n-butanol proper proportion, performance is stablized, solubility Greatly, and the advantages of good film-forming property, the endurance quality for being conducive to its auxiliary agent improves；Isomerous tridecanol polyoxyethylene ether contains polyether chain Forging has good hydrophily, can play the role of accelerating auxiliary agent dissolution, the advantageous used additives of stability for increasing auxiliary agent make With easy operability in the process；Dodecyl sodium sulfate has good permeability, and addition can improve auxiliary agent moment infiltration Permeability energy, can be avoided processing speed it is too fast caused by roll banding.Above-mentioned several auxiliary agents can according to special ratios dosage compounding It displays one's respective advantages and there is good synergistic effect, superior, fine and smooth sense enhances, is yellow the super soft finishing agent of preparation with flexibility Become smaller, moment is hydrophilic, has many advantages, such as antistatic property.
The super soft finishing agent that aforesaid way is prepared is applied on velvet coffee carbon trousering for the super soft finishing agent of O/W type, Sense of touch is smooth super soft, can be obviously improved the comfort property of fabric, reduces electrostatic, has touching compared with the finishing agent of other identity functions Feel the advantages that smooth super soft, solubility property is good, stability is good, small, antistatic property is good on fabric whiteness or dyefastness influence, this After fabric is collated, feel is up to 5 grades, stiffness≤1.2/cm, confficient of static friction≤0.2.
The present invention is described in further detail With reference to embodiment, but protection scope of the present invention is unlimited In this.
Detailed description of the invention
Fig. 1 is that the application coffee carbon keeps warm super soft trousering weave structure figure；
Fig. 2 is that the application coffee carbon keeps warm super soft trousering bilayer schematic cross-section.
Figure label: 2-1. fabric surface layer；2-2. fabric inner layer.
Specific embodiment
Embodiment 1
A kind of coffee carbon of the present embodiment keeps warm super soft trousering, and warp thread selects the tencel of 20s, and bright in color is soft, latitude Yarn selects three kinds of yarns, and A yarn is R70/JC30 30/2, i.e. viscose glue/combed cotton double strand yarn of 30s；B yarn is C20+70D, that is, 20s Cotton packet spandex yarn；C yarn is 60/40 coffee carbon of 16s/tencel G100；Weft yarn A, B, C are arranged as shown in Figure 1, this arrangement side Formula is conducive to coffee carbon yarn weaving in fabric inner layer 2-2, plays its thermal property to greatest extent；Institutional framework is selected double-deck Tissue, as shown in connection with fig. 2, coffee carbon fiber design in fabric inner layer 2-2, after by grabbing shearing technology, on fabric inner layer 2-2 Tapetum is formed, the rich reality of feel carries out final finishing by dedicated super soft finishing agent, and gained fabric has good heat accumulation thermal Function and super soft comfort can suitably reduce air-conditioner temperature in winter, reduce energy consumption.
Face weave technological parameter: weft density: 66 pieces/inch * 119 pieces/inch；Total quantity of warps: 5400；Porter is selected 65#；Denting amplitude 208.9cm；700 revs/min of speed of weaving；Warp thread and weft yarn A, C institutional framework are Three Up Three Down, warp thread with Weft yarn B institutional framework is fabric tissue one on the other are as follows: 1/1+3/3 is double-deck.
Shell-fabric dyeing and finishing process parameter: enzyme desizing-dyeing-pre-setting-grabs the super soft arrangement of cropping-- finished product sizing, the tool being related to Body technology parameter is as follows:
Starch desizing enzyme LS-3:2-3g/L temperature: 55 DEG C of time 20min bath raioes: 1:5；
Dyeing: active Nary Blue BET 1.5% (owf) salt: 20g/L color fixing agent: 10g/L temperature: 60 DEG C of times: 40min bath raio: 1:20；
Grab shearing technology: cylinder revolving speed 85r/min, tension 15N, ball woll number 3 times, cropping edge of a knife knife is cut away from 0.5mm Hair number 4 times；
Super soft finishing technique: super soft finishing agent: 45g/L, nip pressure: 4.5MPa pick-up: 83%, speed 12m/min, Temperature: 190 DEG C；
Super soft finishing agent involved in above-mentioned super soft finishing technique, including following each component by weight percentage:
The preparation method of above-mentioned super soft finishing agent, comprising the following steps:
(1) accurately weigh parts by weight cyclohexyl secondary amino group silicone, isomerous tridecanol polyoxyethylene ether be placed in it is completely dry In the dry three-necked flask with thermometer；
(2) agitating device is loaded onto, starts blender, is started to warm up after mixing evenly to 56 DEG C, then be sequentially added into metering Good octamethylcyclotetrasiloxane, hexamethyldisiloxane, the double heptyl esters of phthalic acid, HYDROXY PROPYL METHYLCELLULOSE and positive fourth Alcohol, constant temperature stir 55min；
(3) system temperature is down to room temperature, measured dodecyl sodium sulfate and deionized water high-speed stirred 30min is added After discharge to get super soft finishing agent.
Coffee carbon trousering (the calling sample 1 in the following text) test result prepared with above-mentioned technique is as shown in table 1.
The testing result summary sheet of 1 sample 1 of table
As it can be seen from table 1 designed trousering have very good warmth retention property, thermal resistance, clo value test result compared with Conventional trousering is larger, and heat transfer coefficient is low, and for heat preservation rate up to 52%, more conventional trousering is higher by 20%-30%.Its softness test knot In fruit, for feel up to 5 grades, stiffness is lower, and confficient of static friction is very low, and softness is fabulous.
Embodiment 2
The present embodiment coffee carbon keeps warm super soft trousering, and warp thread selects the tencel of 21s, and bright in color is soft, weft yarn choosing With three kinds of yarns, A yarn is R70/JC30 45/2, i.e. viscose glue/combed cotton double strand yarn of 45s；B yarn is the cotton of C20+70D, that is, 20s Packet spandex yarn；C yarn is 60/40 coffee carbon of 16s/tencel G100 weft yarn A, B, C arrangement as shown in Figure 1, this arrangement mode has Conducive to coffee carbon yarn weaving in fabric inner layer, its thermal property is played to greatest extent；Institutional framework selects double-layered structure, sees figure Shown in 2, coffee carbon fiber design in fabric inner layer 2-2, after by grabbing shearing technology, fabric inner layer villous layer, the rich reality of feel, Final finishing is carried out by dedicated super soft finishing agent, gained fabric has the function of good heat accumulation thermal and super soft comfort, Air-conditioner temperature can be suitably reduced in winter, reduce energy consumption.
Face weave technological parameter: weft density: 72 pieces/inch * 125 pieces/inch；Total quantity of warps: 5800；Porter is selected 65#；Denting amplitude 210cm；720 revs/min of speed of weaving；Warp thread and weft yarn A, C institutional framework are Three Up Three Down, warp thread and latitude Yarn B institutional framework is fabric tissue one on the other are as follows: 1/1+3/3 is double-deck.
Shell-fabric dyeing and finishing process parameter: enzyme desizing-dyeing-pre-setting-grabs the super soft arrangement of cropping-- finished product sizing,
Starch desizing enzyme LS-3:3g/L temperature: 55 DEG C of time 20min bath raioes: 1:5；
Dyeing: active Nary Blue BET 1.5% (owf) salt: 20g/L color fixing agent: 10g/L temperature: 60 DEG C of times 40min bath raio: 1:20；
Grab cropping: cylinder revolving speed 80r/min, tension 18N, ball woll number 4 times, cropping edge of a knife knife is away from 0.6mm, cropping number 5 times；
Super soft arrangement: super soft finishing agent: 40g/L, nip pressure: 4.2MPa pick-up: 85%, speed 15m/min, temperature Degree: 190 DEG C.
Super soft finishing agent involved in above-mentioned super soft finishing technique, including following each component by weight percentage:
A kind of preparation method of super soft finishing agent, comprising the following steps:
(1) accurately weigh parts by weight cyclohexyl secondary amino group silicone, isomerous tridecanol polyoxyethylene ether be placed in it is completely dry In the dry three-necked flask with thermometer；
(2) agitating device is loaded onto, starts blender, is started to warm up after mixing evenly to 56 DEG C, then be sequentially added into metering Good octamethylcyclotetrasiloxane, hexamethyldisiloxane, the double heptyl esters of phthalic acid, HYDROXY PROPYL METHYLCELLULOSE and positive fourth Alcohol, constant temperature stir 55min；
(3) system temperature is down to room temperature, measured dodecyl sodium sulfate and deionized water high-speed stirred 30min is added After discharge to get super soft finishing agent.
Coffee carbon trousering (the calling sample 2 in the following text) test result prepared with above-mentioned technique is as shown in table 2.
The testing result summary sheet of 2 sample 2 of table
From table 2 it can be seen that designed trousering has good warmth retention property, thermal resistance, clo value test result are more normal Rule trousering is larger, and heat transfer coefficient is low, and for heat preservation rate up to 58%, more conventional trousering is higher by 20%-30%.Its softness test result In, for feel up to 5 grades, stiffness is lower, and confficient of static friction is very low, and softness is fabulous.

Claims (5)

  1. The super soft trousering 1. a kind of coffee carbon keeps warm, it is characterised in that: the trousering is the bilayer formed by warp thread and weft weaving Institutional framework, including fabric surface layer and fabric inner layer, the warp thread select the tencel of 16-32s, and weft yarn selects A yarn, B yarn, C yarn Three kinds: A yarn is that R70/JC30 is bifilar, and B yarn is C+70D cotton packet spandex yarn, and C yarn is coffee carbon/tencel G100, and weft yarn A, B, C are pressed B, C, A, B, A, C, B, A, A circulation weaving, is located at coffee carbon fiber in fabric inner layer.
  2. The super soft trousering 2. a kind of coffee carbon as described in claim 1 keeps warm, which is characterized in that the warp thread and weft weaving are joined Number are as follows: through close: (60-90) piece/inch；Filling density: (110-130) piece/inch；Total quantity of warps: 5400-6000 root；Porter is selected No. 65；Denting amplitude 205-210cm；650-750 revs/min of speed of weaving；Warp thread and weft yarn A, C institutional framework are three on three Under, warp thread and weft yarn B institutional framework are fabric tissue one on the other are as follows: 1/1+3/3 is double-deck.
  3. The super soft trousering 3. a kind of coffee carbon as claimed in claim 1 or 2 keeps warm, which is characterized in that the face weave finishes Dyeing and finishing, dyeing and finishing technology parameter have also been carried out afterwards are as follows: enzyme desizing-dyeing-pre-setting-grabs the super soft arrangement of cropping-- finished product sizing, In,
    Starch desizing enzyme LS-3:2-3g/L, temperature: 50-60 DEG C, time 20min, bath raio: 1:5；
    Dyeing: active Nary Blue BET:1.5% (owf), salt: 15-30g/L, color fixing agent: 5-10g/L, temperature: 50-60 DEG C, the time: 30-60min, bath raio: 1:20；
    Grab cropping: cylinder revolving speed 80-100r/min, tension 15-20N, ball woll number 2-5 times, cropping edge of a knife knife is away from 0.5- 0.8mm, cropping number 3-5 times, grabbing cropping makes tapetum occur on fabric inner layer；
    Super soft arrangement: super soft finishing agent: 30-50g/L, nip pressure: 4.0-6.0MPa pick-up: 80-85%, speed 12- 15m/min, temperature: 185-195 DEG C.
  4. 4. a kind of preparation method of super soft finishing agent, which is characterized in that by weight percentage, the super soft finishing agent include with Lower component:
  5. 5. a kind of preparation method of super soft finishing agent as claimed in claim 4, which comprises the following steps:
    (1) the cyclohexyl secondary amino group silicone and isomerous tridecanol polyoxyethylene ether for weighing parts by weight are warming up to after mixing evenly 50-60℃；
    (2) octamethylcyclotetrasiloxane measured, hexamethyldisiloxane, phthalic acid double heptyl esters, hydroxyl are sequentially added into Propyl methocel and n-butanol, constant temperature stir 45-60min；
    (3) system temperature is down to room temperature, discharging is after measured dodecyl sodium sulfate and deionized water stirring is added to get super Soft finishing agent.
CN201811300255.4A 2018-11-02 2018-11-02 Coffee carbon warm-keeping super-soft trousers material and preparation method of super-soft finishing agent thereof Active CN109457482B (en)

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CN113930963B (en) * 2021-10-29 2024-02-13 达利(中国)有限公司 Preparation method of real silk warm fabric finished by nano coffee carbon material

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