CN109431832A - One kind containing gold nano-negative ion collagen protein face liquid, facial mask and preparation method thereof - Google Patents
One kind containing gold nano-negative ion collagen protein face liquid, facial mask and preparation method thereof Download PDFInfo
- Publication number
- CN109431832A CN109431832A CN201811602386.8A CN201811602386A CN109431832A CN 109431832 A CN109431832 A CN 109431832A CN 201811602386 A CN201811602386 A CN 201811602386A CN 109431832 A CN109431832 A CN 109431832A
- Authority
- CN
- China
- Prior art keywords
- skin
- negative ion
- collagen
- facial mask
- gold nano
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
- A61K8/355—Quinones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The invention discloses one kind to contain gold nano-negative ion collagen protein face liquid, facial mask and preparation method thereof, the facial mask liquid comprises the following raw materials by weight percent: nanometer gold 0.1-2%, collagen 1-10%, butanediol 5-8%, glycerol 3-6%, Sodium Hyaluronate 2-5%, dimethyl silicone polymer 2-5%, niacinamide 1-3%, vitamin E 2-5%, ubiquinone 1-4%, tripotassium phosphate 0.2-2.5%, essence 1-4%, surplus are water.When facial mask of the invention sticks on skin surface, skin bottom can be also sent to by having the effective component of the functions such as moisturizing, whitening and anti-aging in skin care item, and it is very good with the compatibility of surrounding tissue, skin can be enabled sufficiently to moisten, it profound can more lighten the stain, improve the dim heavy and yellowing phenomenon of skin, the delicate water that shows from inside to outside has moistened the colour of skin, it only needs 30 minutes, quickly enhances Skin Cell vigor, whitening, moisturizing, nutrition and maintenance are carried out to face skin, allow face skin taking on a new look again, soft and smooth water is tender, pale compact, beautiful moving.
Description
Technical field
The present invention relates to a kind of skin care item facial masks, and in particular to one kind contains gold nano-negative ion collagen protein face
Liquid, facial mask and preparation method thereof.
Background technique
A kind of biological polymer substance that collagen is made of fibroblast and fibrocyte, is the master of skin
Ingredient is wanted, collagen accounts for 72% in skin, and 80% is collagen in corium.The distinctive triple-helix structure of collagen, energy
It is effective to lock moisture, a large amount of hydrophilic group is formed because therefore, collagen has extremely strong water storage performance.Meanwhile collagen
In polypeptide can inhibit the activity of tyrosinase, reduce the formation of color spot, and collagen has unique reparation to skin
Effect, combines with the cell tissue of surrounding, effectively facilitates Skin Cell regeneration, repairs the acne print acne scar of epidermis.Collagen
Skin fibr tissue mechanism is also reformed, cell metabolism is promoted, delaying cell aging unfolds fine wrinkles, restores
Skin it is compact and elastic.
Nanometer gold is the nano-scale particle of gold, is in black.Using its minimum structure, can be penetrated into across epidermis
Skin corium promotes neoblast to generate, and skin is made to keep soft, plentiful and flexible, moreover it is possible to play the role of good importing, help
Skin more thoroughly absorbs the nutritional ingredient in skin care item, and plays the effect of tensing aging relaxation skin.
But currently, the generally existing nanometer gold performance of nanometer gold facial mask is unstable, the bad problem of facial mask performance.Together
When, since the composition of raw material in nanometer gold facial mask also affects the performance of facial mask, develop a kind of high performance gold
Nano-negative ion facial mask is of great significance.
Summary of the invention
In view of the deficiencies of the prior art, the object of the present invention is to provide one kind to contain gold nano-negative ion collagen face
Film liquid, facial mask and preparation method thereof, the facial mask have whitening spot-removing, anti-aging, moisturizing water lock, tender skin lightening, balanced grease,
Calmness releives, antianaphylactic effect.
To achieve the goals above, the technical scheme adopted by the invention is that:
One kind containing gold nano-negative ion collagen protein face liquid, comprises the following raw materials by weight percent: nanometer
Gold 0.1-2%, collagen 1-10%, butanediol 5-8%, glycerol 3-6%, Sodium Hyaluronate 2-5%, polydimethylsiloxanes
Alkane 2-5%, niacinamide 1-3%, vitamin E 2-5%, ubiquinone 1-4%, tripotassium phosphate 0.2-2.5%, essence 1-4%, surplus
For water.
Collagen is cow leather collagen, pigskin collagen, pig's feet collagen.
Essence is lavender oil, flavoring rose essence.
Nanometer gold is water-soluble gold nano spheric granules, diameter 10-50nm.
Nanometer gold the preparation method comprises the following steps: 10mg β-CD-g- [PAA-b-PEG] is dissolved in 10mL DMF, list is made
Molecule micella template solution；Then 0.1179g HAuCl is added4Nanometer gold is obtained in 65 DEG C of reaction 10h with ethyl alcohol 2mL
Grain.
The preparation method of multi-arm star block copolymer β-CD-g- [PAA-b-PEG] is with reference to entitled " a kind of water-soluble
The patent of invention of the preparation method and applications of property titania nanoparticles " (application number: CN2017111944528).
Preferably, it containing gold nano-negative ion collagen protein face liquid, comprises the following raw materials by weight percent: receiving
Cream-coloured gold 0.5%, cow leather collagen 2%, butanediol 6%, glycerol 6%, Sodium Hyaluronate 2%, dimethyl silicone polymer
2%, niacinamide 2%, vitamin E 3%, ubiquinone 1%, tripotassium phosphate 0.2%, essence 2%, surplus are water.
A kind of preparation method containing gold nano-negative ion collagen protein face liquid, collagen is added to the water, and is mixed
It closes uniform；Then nanometer gold is added, is uniformly mixed；Add surplus stock, be uniformly mixed to get.
One kind containing gold nano-negative ion collagen protein face, and non-woven cotton facial mask substrate is immersed in facial mask liquid, is made
Contain gold nano-negative ion collagen protein face.
The invention has the advantages that:
1, " penetration theory " " anti-oxidant principle " " assigning principle living " and " synergistic carriers of skin are acted on by nanometer gold
The big principle of principle " four, skin voluntarily generate more collagens to free radical resisting, slow down skin aging after obtaining energy.
Penetration theory: nanometer gold Carrier diameters are less than corneocyte gap 100nm, can transport water-soluble and oiliness
Substance, can penetrate epidermal cell gap, hair follicle and sweat gland easily, take nutrient to skin inner layer, be released effectively active constituent.
Synergistic carriers principle: nanometer gold is anion state, and the nutriment of skin care item is positive ion mode, Ta Menneng
Enough it is closely linked, rapid osmotic to dermal layer of the skin even subcutaneous tissue.
Assign principle living: nanometer gold particle skin permeation can be obviously improved skin firmness, increase skin moisturizing ingredient,
It enables tender whitening skin, water, pigment lightening, fine wrinkles disappearance, skin obtain complete correction, embodies young state.
Anti-oxidant principle: gold has very strong anti-oxidation characteristics, can reduce external environment and in vivo generated mistake
Oxide and free radical, and intracellular SOD content can be increased, it can more reduce internal harmful substance.
2, in raw material of the present invention, collagen is the important constituent of skin, the skin corium for the skin that can go directly, and helps flesh
Skin forms the moisture film of high-moisture, and with the ability that depth water lock and deep layer are nourished, the smooth compact, water of skin surface moisturizes white；
Inside the deep enough skin of aqueous moisturizing ingredient (butanediol, glycerol, Sodium Hyaluronate) energy, reach replenishing water and preserving moisture effect, moist type
Lubricant component (dimethyl silicone polymer) can reinforce soothing effect, improve water lock ability, enhance moisture retention；Skin conditioning agent
(niacinamide, vitamin E, ubiquinone) can releive Lavender Extract, prevent skin allergy, further enhance facial mask antiallergic effect and
Antioxidation.Effect altogether is cooperateed between each ingredient of the present invention, can be reached good moisturizing, whitening and anti-aging and antiallergy and be made
With.
3, when facial mask of the invention sticks on skin surface, there is the effective of the functions such as moisturizing, whitening and anti-aging in skin care item
Ingredient can also be sent to skin bottom, and very good with the compatibility of surrounding tissue, and skin can be enabled sufficiently to moisten, more can be profound
Lighten the stain, dim heavy and yellowing phenomenon, the delicate water that shows from inside to outside for improving skin have moistened the colour of skin, only need 30 points
Clock quickly enhances Skin Cell vigor, carries out whitening, moisturizing, nutrition and maintenance to face skin, face skin is allowed to shine again
Brilliance, soft and smooth water is tender, pale compact, beautiful moving.
Detailed description of the invention
Fig. 1 is the XRD spectrum of nanometer gold particle made from the embodiment of the present invention 1.
Fig. 2 is the transmission electron microscope picture of nanometer gold particle made from the embodiment of the present invention 1.
Specific embodiment
Specific embodiments of the present invention will be described in further detail with reference to embodiments.
Embodiment 1
Nanometer gold the preparation method comprises the following steps: 10mg β-CD-g- [PAA-b-PEG] is dissolved in 10mL DMF, list is made
Molecule micella template solution；Then 0.1179g HAuCl is added4Nanometer gold is obtained in 65 DEG C of reaction 10h with ethyl alcohol 2mL
Grain.
Fig. 1 be preparation particle XRD diagram, through with JCPDF card check analysis, 2 θ be 38.20 °, 44.40 °,
At 64.50 °, 77.50 °, there are 4 diffraction maximums, is the characteristic diffraction peak of gold, (111), (200), (220), (222) four
Crystal face is corresponding with the crystal face of gold of face-centred cubic structure respectively, it is possible thereby to determine that the granular product of preparation is elemental gold.
Fig. 2 is the transmission electron microscope picture for preparing nanogold particle.Nanogold is spheric granules it can be seen from transmission electron microscope picture
Shape, average diameter 12nm, good dispersion do not occur agglomeration.
Embodiment 2
One kind containing gold nano-negative ion collagen protein face liquid, comprises the following raw materials by weight percent: nanometer
Gold 0.5%, cow leather collagen 2%, butanediol 6%, glycerol 6%, Sodium Hyaluronate 2%, dimethyl silicone polymer 2%,
Niacinamide 2%, vitamin E 3%, ubiquinone 1%, tripotassium phosphate 0.2%, lavender oil 2%, surplus are water.
Preparation method is, comprising the following steps:
(1) cow leather collagen is added to the water, is uniformly mixed, collagen aqueous solution is made；
(2) nanometer gold is added in collagen aqueous solution, is heated to 60 DEG C, stirs；
(3) butanediol, glycerol, Sodium Hyaluronate, dimethyl silicone polymer are added in the mixed liquor of step (2), stirring
Cooling；40 DEG C are cooled to, niacinamide, vitamin E, ubiquinone is added, is sufficiently mixed, stirs evenly, be cooled to 30 DEG C, add phosphorus
Sour tripotassium, lavender oil, be sufficiently mixed, stir evenly to get.
Embodiment 3
One kind containing gold nano-negative ion collagen protein face liquid, comprises the following raw materials by weight percent: nanometer
Gold 0.1%, pig's feet collagen protein 10 %, butanediol 5%, glycerol 3%, Sodium Hyaluronate 5%, dimethyl silicone polymer 5%,
Niacinamide 3%, vitamin E 2%, ubiquinone 4%, tripotassium phosphate 2.5%, flavoring rose essence 2.5%, surplus are water.
Preparation method is the same as embodiment 2.
Embodiment 4
One kind containing gold nano-negative ion collagen protein face liquid, comprises the following raw materials by weight percent: nanometer
Gold 1%, cow leather collagen 5%, butanediol 7%, glycerol 4%, Sodium Hyaluronate 4%, dimethyl silicone polymer 3%, cigarette
Amide 1%, vitamin E 2%, ubiquinone 1%, tripotassium phosphate 1%, lavender oil 4%, surplus are water.
Preparation method is the same as embodiment 2.
Embodiment 5
One kind containing gold nano-negative ion collagen protein face liquid, comprises the following raw materials by weight percent: nanometer
Gold 2%, pigskin collagen 4%, butanediol 8%, glycerol 5%, Sodium Hyaluronate 5%, dimethyl silicone polymer 4%, cigarette
Amide 1%, vitamin E 5%, ubiquinone 1%, tripotassium phosphate 2%, flavoring rose essence 3%, surplus are water.
Preparation method is the same as embodiment 2.
Embodiment 6
One kind containing gold nano-negative ion collagen protein face, preparation method are as follows: immerses non-woven cotton facial mask substrate
In the facial mask liquid of embodiment 2, it is made and contains gold nano-negative ion collagen protein face.
Control group 1
The facial mask liquid ingredient of 1 facial mask of control group does not add nanometer gold, remaining ingredient is same as Example 2.
Control group 2
The facial mask liquid ingredient of 2 facial mask of control group does not add collagen, remaining ingredient is same as Example 2.
Control group 3
The facial mask liquid of 3 facial mask of control group, comprises the following raw materials by weight percent: nanometer gold 2%, pigskin collagen egg
White 4%, allantoin 0.3%, triethanolamine 0.2%, xanthan gum 0.5%, carbomer 0.4%, dipotassium glycyrrhizinate 0.5%, lecithin
Rouge 5%, Phenoxyethanol 6%, vitamin B5 0.6%, surplus are water.
Measure of merit:
1, facial mask performance of keeping humidity is tested:
The women for selecting four age brackets carries out performance of keeping humidity survey to the facial mask of the embodiment of the present invention 6 and control group 1-3
Examination, four age brackets distinguish 18-25 years old, 25-32 years old, 33-40 years old, 40-47 years old, and each age bracket picks out 100 women, often
A age bracket picks out 25 at random, and totally 100 women are divided into one group to four age brackets, and totally 4 groups, facial mask is made with moisture content of skin
For judgment criteria, facial mask is pasted on facial 30min at 9 points at night, is tested and 7 points of the next morning having applied in half an hour
It gets up test data, as a result see the table below.
| Group | Moisture content of skin before face mask film | Face mask film half an hour moisture content of skin | Next day gets up moisture content of skin |
| Embodiment 6 | 32.6% | 58.2% | 48.3% |
| Control group 1 | 31.2% | 45.8% | 32.5% |
| Control group 2 | 33.5% | 41.7% | 34.6% |
| Control group 3 | 30.9% | 49.9% | 41.5% |
These results suggest that the present invention contains the moisturizings such as nanometer gold and collagen, water lock ingredient, in facial mask liquid
After other material combinations, effect altogether is cooperateed with, the application effect of facial mask is can be improved, improves moisturizing, the water lock effect of facial mask.
2, facial mask Whitening, spot performance test
Selection there are it is obscure it is unglazed, pore is coarse, has acne print, 18-48 year old women of color spot, to facial mask progress whitening it is light
Spot performance is tested, and is divided into 4 groups, and every group of 100 people stick the facial mask of embodiment 6 and control group 1-3, by mask sheet respectively
It is removed after spreading on facial 30min, sticks once, continuously stick 90 days before sleep daily, the skin for observing tested women absorbs journey
Degree and improvement situation, as a result see the table below.
These results suggest that the present invention contains other raw materials in the ingredients, with facial mask liquid such as nanometer gold and collagen
After combination, effect altogether is cooperateed with, can be improved the application effect of facial mask, improves the whitening of facial mask, light spot effect.
3, facial mask smoothing wrinkle performance test
Selecting skin, there are 35-48 years old women of obvious wrinkle, carry out smoothing wrinkle performance and are tested, are divided into 4 groups, often
100 people of group, remove after facial mask is pasted on facial 30min, stick once, continuously stick 90 days before sleep daily, observe tested
The wrinkle of skin of women improves situation, as a result see the table below.
These results suggest that the present invention contains other raw materials in the ingredients, with facial mask liquid such as nanometer gold and collagen
After combination, effect altogether is cooperateed with, the application effect of facial mask is can be improved, improves smoothing wrinkle, the anti-aging effects of facial mask.
Claims (8)
1. one kind contains gold nano-negative ion collagen protein face liquid, which is characterized in that by the raw material of following weight percent
Composition: nanometer gold 0.1-2%, collagen 1-10%, butanediol 5-8%, glycerol 3-6%, Sodium Hyaluronate 2-5%, gather
Dimethyl siloxane 2-5%, niacinamide 1-3%, vitamin E 2-5%, ubiquinone 1-4%, tripotassium phosphate 0.2-2.5%, essence
1-4%, surplus are water.
2. according to claim 1 contain gold nano-negative ion collagen protein face liquid, which is characterized in that the glue
Former albumen is cow leather collagen, pigskin collagen, pig's feet collagen.
3. according to claim 1 contain gold nano-negative ion collagen protein face liquid, which is characterized in that the perfume (or spice)
Essence is lavender oil, flavoring rose essence.
4. according to claim 1 contain gold nano-negative ion collagen protein face liquid, which is characterized in that described receives
Cream-coloured gold is water-soluble gold nano spheric granules, diameter 10-50nm.
5. according to claim 1 contain gold nano-negative ion collagen protein face liquid, which is characterized in that described receives
Cream-coloured gold the preparation method comprises the following steps: 10mg β-CD-g- [PAA-b-PEG] is dissolved in 10mL DMF, unimolecular micelle mould is made
Plate solution；Then 0.1179g HAuCl is added4Nanometer gold particle is obtained in 65 DEG C of reaction 10h with ethyl alcohol 2mL.
6. according to claim 1 contain gold nano-negative ion collagen protein face liquid, which is characterized in that it is preferred,
Comprise the following raw materials by weight percent: nanometer gold 0.5%, cow leather collagen 2%, butanediol 6%, glycerol 6%, thoroughly
Bright matter acid sodium 2%, dimethyl silicone polymer 2%, niacinamide 2%, vitamin E 3%, ubiquinone 1%, tripotassium phosphate 0.2%, perfume
Essence 2%, surplus is water.
7. a kind of preparation side as claimed in any one of claims 1 to 6 containing gold nano-negative ion collagen protein face liquid
Method, which is characterized in that collagen is added to the water, is uniformly mixed；Then nanometer gold is added, is uniformly mixed；It adds surplus
Remaining raw material, be uniformly mixed to get.
8. one kind contains gold nano-negative ion collagen protein face, which is characterized in that non-woven cotton facial mask substrate is immersed right
It is required that being made in the described in any item facial mask liquids of 1-6 and containing gold nano-negative ion collagen protein face.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811602386.8A CN109431832A (en) | 2018-12-26 | 2018-12-26 | One kind containing gold nano-negative ion collagen protein face liquid, facial mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811602386.8A CN109431832A (en) | 2018-12-26 | 2018-12-26 | One kind containing gold nano-negative ion collagen protein face liquid, facial mask and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109431832A true CN109431832A (en) | 2019-03-08 |
Family
ID=65537509
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811602386.8A Withdrawn CN109431832A (en) | 2018-12-26 | 2018-12-26 | One kind containing gold nano-negative ion collagen protein face liquid, facial mask and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109431832A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110787073A (en) * | 2019-11-21 | 2020-02-14 | 嘉汶化妆品(东莞)有限公司 | Gold anti-aging repairing skin-tendering mask essence and preparation method thereof |
| CN113057932A (en) * | 2021-03-19 | 2021-07-02 | 李雪云 | Collagen skin care product for improving skin wrinkles |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106880580A (en) * | 2017-02-28 | 2017-06-23 | 广州诚予化妆品有限公司 | A kind of nm of gold repairs facial mask and its production technology |
| CN107900376A (en) * | 2017-11-24 | 2018-04-13 | 洛阳量子纳米科技有限公司 | A kind of preparation method of water-soluble silver nano particle |
-
2018
- 2018-12-26 CN CN201811602386.8A patent/CN109431832A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106880580A (en) * | 2017-02-28 | 2017-06-23 | 广州诚予化妆品有限公司 | A kind of nm of gold repairs facial mask and its production technology |
| CN107900376A (en) * | 2017-11-24 | 2018-04-13 | 洛阳量子纳米科技有限公司 | A kind of preparation method of water-soluble silver nano particle |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110787073A (en) * | 2019-11-21 | 2020-02-14 | 嘉汶化妆品(东莞)有限公司 | Gold anti-aging repairing skin-tendering mask essence and preparation method thereof |
| CN113057932A (en) * | 2021-03-19 | 2021-07-02 | 李雪云 | Collagen skin care product for improving skin wrinkles |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106109296B (en) | A kind of moisturizing essence lotion and preparation method thereof | |
| US10682257B2 (en) | Biological fiber composite dressing | |
| CN101926741B (en) | Skin refinishing essence and skin care product with same | |
| CN105342882B (en) | A kind of compound moisturizing stoste of more effects and its application process | |
| WO2007078056A1 (en) | Cosmetic composition containing algae extract for effect on improving the skin complexion | |
| CN109431832A (en) | One kind containing gold nano-negative ion collagen protein face liquid, facial mask and preparation method thereof | |
| CN108403483A (en) | It is a kind of element face frost and its preparation process | |
| CN107320431A (en) | A kind of skin whitening, moisturizing face cream and its preparation technology | |
| CN109125116A (en) | A kind of U.S. face jelly lipstick of transparent color and preparation method thereof | |
| CN107582445A (en) | A kind of moisture-retention gel facial mask and preparation method thereof | |
| CN108348441A (en) | The lip for containing natural ceramide and rose hip oil as active ingredient protects the composition that applies some make up | |
| CN106109391B (en) | A kind of potent moisture retention water and preparation method thereof | |
| CN105686971A (en) | Polyamino acid gel and preparation method and application thereof | |
| CN109820807A (en) | A kind of moisturizing restorative facial cream and preparation method thereof | |
| JP7329588B2 (en) | A color cosmetic composition containing a color base reacted with a low-temperature, high-pressure enzyme and an extract | |
| CN109453047A (en) | A kind of gold nano-negative ion collagen protein face liquid of water lock moisturizing, facial mask and preparation method thereof | |
| CN109125211A (en) | A kind of anti-ageing activating essence of whitening and preparation method thereof | |
| CN107802576A (en) | A kind of natural animal-plant cell replenishers and preparation method thereof | |
| CN100358488C (en) | Whitening crystal invisual face film for activating skin and production thereof | |
| CN116785202A (en) | Multiple skin care essence with suspended grease and preparation method thereof | |
| EP4257116A1 (en) | Method for producing spicule coated with active ingredient for skin improvement and diamond, and diamond spicule cosmetic composition comprising same | |
| CN108653143A (en) | A kind of facial treatment essence liquid | |
| BR112012006726B1 (en) | method of treating a semi-manufactured leather or imitation leather product and items resulting therefrom | |
| CN109431831A (en) | A kind of gold nano-negative ion facial mask liquid of Whitening, spot, facial mask and preparation method thereof | |
| CN112675071A (en) | Wool keratin freeze-dried mask and preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20190628 Address after: 450000 Henan Province Zhengzhou High-tech Industrial Development Zone No. 11 Changchun Road Henan National University Science and Technology Park Incubation Building B 17-storey southwest and northwest households Applicant after: Henan Kedou New Materials Research Institute Co., Ltd. Address before: 471000 F1 Floor, Yanhuang Science Park, 333 West Kaiyuan Avenue, Luolong District, Luoyang City, Henan Province Applicant before: Luoyang quantum nanotechnology Co., Ltd. |
|
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190308 |