CN109329650A - A kind of filefish feed adsorbent and preparation method thereof improving enteron aisle - Google Patents
A kind of filefish feed adsorbent and preparation method thereof improving enteron aisle Download PDFInfo
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- CN109329650A CN109329650A CN201811194053.6A CN201811194053A CN109329650A CN 109329650 A CN109329650 A CN 109329650A CN 201811194053 A CN201811194053 A CN 201811194053A CN 109329650 A CN109329650 A CN 109329650A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/10—Animal feeding-stuffs obtained by microbiological or biochemical processes
- A23K10/16—Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions
- A23K10/18—Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions of live microorganisms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
- A23K10/22—Animal feeding-stuffs from material of animal origin from fish
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
- A23K20/147—Polymeric derivatives, e.g. peptides or proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
- Y02A40/818—Alternative feeds for fish, e.g. in aquacultures
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Abstract
The invention discloses a kind of filefish feed sorbent preparation methods for improving enteron aisle; include the following steps: for chitosan, mineral oil, sulfuric acid solution to be uniformly mixed, chitin is added and stirs evenly, vacuum is stood; glutaraldehyde stirring is added; filtering is washed, dry; it is put into the tube furnace of nitrogen protection; from room temperature, heat preservation, the cooling filefish feed adsorbent for obtaining improving enteron aisle.The present invention discloses a kind of filefish feed for improving enteron aisle, and raw material includes: 55-83 parts of import peru fish meal, 12-24 parts of peanut powder by weight, 21-30 parts of dry powder of water hyacinth, 14-23 parts of rice chaff, 25-32 parts of leached tea oil slag, 10-18 parts of sesame seed meal, 4-12 parts of Yeast protein, 8-16 parts of locust powder, 1-3 parts of spirulina powder, above-mentioned adsorbent 1-2 parts, 0.5-1.2 parts of mountain flour, 0.4-1 parts of calcium monohydrogen phosphate, 0.1-0.2 parts of probiotics preparation, 1-2 parts of filefish compound premix.
Description
Technical field
The present invention relates to field of feed more particularly to a kind of filefish feed adsorbent for improving enteron aisle and its preparations
Method.
Background technique
Filefish, scientific name river Puffer is many kinds of, there is hundreds of in the world, and Chinese filefish has more than 30, common are yellowfin
Fugu, worm line Fugu, Fugu rubripes, fugu obscurus etc..
Currently, the feed that filefish cultivation uses is difficult to meet filefish enteron aisle demand, feed nutrition loss and water are easily caused
Matter pollution.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of filefish feed adsorbents for improving enteron aisle
And preparation method thereof, absorption property is fabulous, for can effectively clear up filefish enteron aisle in filefish feed；The invention proposes one kind to change
The filefish feed of kind enteron aisle, can effectively increase intestinal beneficial bacterial content, reduce the bacterial content that causes a disease, and it is flat effectively to adjust intestinal flora
Weighing apparatus reduces disease incident, can effectively adjust the immunity function of body, and the digestion and absorption for enhancing filefish is horizontal, improves filefish
Growth performance.
A kind of filefish feed sorbent preparation method improving enteron aisle proposed by the present invention, includes the following steps: shell
Glycan, mineral oil, sulfuric acid solution are uniformly mixed, and chitin is added and stirs evenly, and vacuum is stood, and glutaraldehyde is added and stirs, filtering,
Washing, it is dry, it is put into the tube furnace of nitrogen protection, from room temperature, heat preservation, the cooling filefish feed for obtaining improving enteron aisle is used
Adsorbent.
Preferably, vacuum time of repose is 1-3h, vacuum degree 0.02-0.04MPa.
Preferably, glutaraldehyde is added and stirs 10-16min, whipping temp is 72-80 DEG C.
Preferably, it is put into the tube furnace of nitrogen protection, is warming up to 450- from room temperature with the speed of 0.4-0.9 DEG C/min
600 DEG C, keep the temperature 10-16min.
Preferably, chitosan, mineral oil, sulfuric acid solution, chitin, glutaraldehyde weight ratio be 3.5-8.6:0.12-
0.5:20-34:4-8:0.12-0.18, sulfuric acid solution concentration are 2-2.8mol/L.
A kind of filefish feed adsorbent improving enteron aisle proposed by the present invention, using the filefish feed of above-mentioned improvement enteron aisle
It is made with sorbent preparation method.
The present invention dissolves chitosan in sulfuric acid solution, can coat to chitin, has chitin good
Flexibility, and after glutaraldehyde cross-linking, mutual bond strength is high, finally carbonizes that form hollow carbon micro- by nitrogen protection
Ball, absorption property are fabulous.
A kind of filefish feed improving enteron aisle proposed by the present invention, raw material includes: import peru fish meal 55- by weight
83 parts, 12-24 parts of peanut powder, 21-30 parts of dry powder of water hyacinth, 14-23 parts of rice chaff, 25-32 parts of leached tea oil slag, 10-18 parts of sesame seed meal,
4-12 parts of Yeast protein, 8-16 parts of locust powder, 1-3 parts of spirulina powder, the filefish feed adsorbent 1-2 of above-mentioned improvement enteron aisle
Part, 0.5-1.2 parts of mountain flour, 0.4-1 parts of calcium monohydrogen phosphate, 0.1-0.2 parts of probiotics preparation, 1-2 parts of filefish compound premix.
Preferably, filefish compound premix includes: that methionine, threonine, lysine, glycine betaine, tea polyphenols, apple are more
Phenol, tryptophan, starch.
Preferably, the weight of methionine, threonine, lysine, glycine betaine, tea polyphenols, apple polyphenol, tryptophan, starch
Than for 0.1-0.4:0.2-0.9:0.1-0.5:1-2:0.12-0.43:0.5-0.9:0.1-0.2:10-14.
The present invention is according to the dietary habit and physiological structure of filefish, and science preparation, full of nutrition, disease resistance is strong, uses
Import peru fish meal, peanut powder, dry powder of water hyacinth, rice chaff, leached tea oil slag, sesame seed meal, Yeast protein, locust powder synergistic effect, energy
, cooperation probiotics preparation moderate with protein content is measured, and rationally controls its component and content, intestinal beneficial bacterium can be effectively increased and contained
Amount reduces the bacterial content that causes a disease, effectively adjusting intestinal flora balance, reduces disease incident, can effectively adjust the immunization machine of body
Can, improve the growth performance of filefish；And the filefish feed adsorbent for improving enteron aisle is used to compound with filefish compound premix, it can
The digestion and absorption for utmostly guaranteeing roughage, reduces aquaculture cost, and can safeguard that intestinal microecology balances, and reduces enteron aisle disease
Disease, the digestion and absorption for enhancing filefish is horizontal, improves and supports filefish economic benefit.
Specific embodiment
In the following, technical solution of the present invention is described in detail by specific embodiment.
Embodiment 1
It is a kind of improve enteron aisle filefish feed sorbent preparation method, include the following steps: by 3.5kg chitosan,
0.5kg mineral oil, 20kg concentration are uniformly mixed for 2.8mol/L sulfuric acid solution, and 4kg chitin is added and stirs evenly, vacuum is stood
3h, vacuum degree 0.02MPa are added 0.18kg glutaraldehyde and stir 10min, and whipping temp is 80 DEG C, filters, washs, dry, put
Enter in the tube furnace of nitrogen protection, is warming up to 600 DEG C from room temperature with the speed of 0.4 DEG C/min, keeps the temperature 10min, cooling is changed
The filefish feed adsorbent of kind enteron aisle.
A kind of filefish feed improving enteron aisle, raw material includes: import peru fish meal 83kg, peanut powder 12kg, water hyacinth
Dry powder 30kg, rice chaff 14kg, leached tea oil slag 32kg, sesame seed meal 10kg, Yeast protein 12kg, locust powder 8kg, spirulina powder 3kg, on
State the filefish feed adsorbent 1kg, mountain flour 1.2kg, calcium monohydrogen phosphate 0.4kg for improving enteron aisle, probiotics preparation 0.2kg, filefish
Compound premix 1kg.
Filefish compound premix is by methionine, threonine, lysine, glycine betaine, tea polyphenols, apple polyphenol, tryptophan, shallow lake
Powder is 0.4:0.2:0.5:1:0.43:0.5:0.2:10 composition by weight.
Embodiment 2
It is a kind of improve enteron aisle filefish feed sorbent preparation method, include the following steps: by 8.6kg chitosan,
0.12kg mineral oil, 34kg concentration are uniformly mixed for 2mol/L sulfuric acid solution, and 8kg chitin is added and stirs evenly, vacuum is stood
1h, vacuum degree 0.04MPa are added 0.12kg glutaraldehyde and stir 16min, and whipping temp is 72 DEG C, filters, washs, dry, put
Enter in the tube furnace of nitrogen protection, is warming up to 450 DEG C from room temperature with the speed of 0.9 DEG C/min, keeps the temperature 16min, cooling is changed
The filefish feed adsorbent of kind enteron aisle.
A kind of filefish feed improving enteron aisle, raw material includes: import peru fish meal 55kg, peanut powder 24kg, water hyacinth
Dry powder 21kg, rice chaff 23kg, leached tea oil slag 25kg, sesame seed meal 18kg, Yeast protein 4kg, locust powder 16kg, spirulina powder 1kg, on
State the filefish feed adsorbent 2kg, mountain flour 0.5kg, calcium monohydrogen phosphate 1kg for improving enteron aisle, probiotics preparation 0.1kg, filefish is multiple
Close premix 2kg.
Filefish compound premix is by methionine, threonine, lysine, glycine betaine, tea polyphenols, apple polyphenol, tryptophan, shallow lake
Powder is 0.1:0.9:0.1:2:0.12:0.9:0.1:14 composition by weight.
Embodiment 3
A kind of filefish feed sorbent preparation method improving enteron aisle, includes the following steps: 5kg chitosan, 0.4kg
Mineral oil, 24kg concentration are uniformly mixed for 2.6mol/L sulfuric acid solution, and 5kg chitin is added and stirs evenly, and vacuum stands 2.5h,
Vacuum degree is 0.025MPa, and 0.16kg glutaraldehyde is added and stirs 12min, and whipping temp is 78 DEG C, filters, washs, dry, is put into
In the tube furnace of nitrogen protection, 550 DEG C are warming up to from room temperature with the speed of 0.5 DEG C/min, keeps the temperature 12min, cooling is improved
The filefish feed adsorbent of enteron aisle.
A kind of filefish feed improving enteron aisle, raw material includes: import peru fish meal 80kg, peanut powder 16kg, water hyacinth
Dry powder 28kg, rice chaff 17kg, leached tea oil slag 30kg, sesame seed meal 12kg, Yeast protein 10kg, locust powder 10kg, spirulina powder
2.5kg, filefish feed the adsorbent 1.3kg, mountain flour 1kg, calcium monohydrogen phosphate 0.6kg of above-mentioned improvement enteron aisle, probiotics preparation
0.17kg, filefish compound premix 1.3kg.
Filefish compound premix is by methionine, threonine, lysine, glycine betaine, tea polyphenols, apple polyphenol, tryptophan, shallow lake
Powder is 0.3:0.4:0.4:1.3:0.4:0.6:0.17:11 composition by weight.
Embodiment 4
A kind of filefish feed sorbent preparation method improving enteron aisle, includes the following steps: 7kg chitosan, 0.2kg
Mineral oil, 30kg concentration are uniformly mixed for 2.2mol/L sulfuric acid solution, and 7kg chitin is added and stirs evenly, and vacuum stands 1.5h,
Vacuum degree is 0.035MPa, and 0.14kg glutaraldehyde is added and stirs 14min, and whipping temp is 74 DEG C, filters, washs, dry, is put into
In the tube furnace of nitrogen protection, 500 DEG C are warming up to from room temperature with the speed of 0.7 DEG C/min, keeps the temperature 14min, cooling is improved
The filefish feed adsorbent of enteron aisle.
A kind of filefish feed improving enteron aisle, raw material includes: import peru fish meal 60kg, peanut powder 20kg, water hyacinth
Dry powder 22kg, rice chaff 20kg, leached tea oil slag 28kg, sesame seed meal 16kg, Yeast protein 6kg, locust powder 14kg, spirulina powder 1.5kg,
Filefish feed adsorbent 1.7kg, mountain flour 0.6kg, calcium monohydrogen phosphate 0.8kg, the probiotics preparation 0.13kg of above-mentioned improvement enteron aisle,
Filefish compound premix 1.7kg.
Filefish compound premix is by methionine, threonine, lysine, glycine betaine, tea polyphenols, apple polyphenol, tryptophan, shallow lake
Powder is 0.2:0.8:0.2:1.7:0.2:0.8:0.13:13 composition by weight.
Embodiment 5
A kind of filefish feed sorbent preparation method improving enteron aisle, includes the following steps: 6kg chitosan, 0.3kg
Mineral oil, 27kg concentration are uniformly mixed for 2.4mol/L sulfuric acid solution, and 6kg chitin is added and stirs evenly, vacuum stands 2h, very
Reciprocal of duty cycle is 0.03MPa, and 0.15kg glutaraldehyde is added and stirs 13min, and whipping temp is 76 DEG C, filters, washs, dry, is put into nitrogen
In the tube furnace of gas shielded, 520 DEG C are warming up to from room temperature with the speed of 0.6 DEG C/min, keeps the temperature 13min, it is cooling to obtain improving intestines
The filefish feed adsorbent in road.
A kind of filefish feed improving enteron aisle, raw material includes: import peru fish meal 70kg, peanut powder 18kg, water hyacinth
Dry powder 25kg, rice chaff 18kg, leached tea oil slag 29kg, sesame seed meal 14kg, Yeast protein 8kg, locust powder 12kg, spirulina powder 2kg, on
State the filefish feed adsorbent 1.5kg, mountain flour 0.8kg, calcium monohydrogen phosphate 0.7kg for improving enteron aisle, probiotics preparation 0.15kg, river
Globefish compound premix 1.5kg.
Filefish compound premix is by methionine, threonine, lysine, glycine betaine, tea polyphenols, apple polyphenol, tryptophan, shallow lake
Powder is 0.25:0.6:0.3:1.5:0.3:0.7:0.15:12 composition by weight.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (9)
1. a kind of filefish feed sorbent preparation method for improving enteron aisle, which comprises the steps of: gather shell
Sugar, mineral oil, sulfuric acid solution are uniformly mixed, and chitin is added and stirs evenly, and vacuum is stood, and glutaraldehyde stirring is added, and filtering is washed
It washs, it is dry, it is put into the tube furnace of nitrogen protection, from room temperature, heat preservation, the cooling filefish feed for obtaining improving enteron aisle is inhaled
Attached dose.
2. improving the filefish feed sorbent preparation method of enteron aisle according to claim 1, which is characterized in that vacuum is stood
Time is 1-3h, vacuum degree 0.02-0.04MPa.
3. the filefish feed sorbent preparation method according to claim 1 or claim 2 for improving enteron aisle, which is characterized in that be added
Glutaraldehyde stirs 10-16min, and whipping temp is 72-80 DEG C.
4. any one of -3 filefish feed sorbent preparation method for improving enteron aisle according to claim 1, which is characterized in that
It is put into the tube furnace of nitrogen protection, is warming up to 450-600 DEG C from room temperature with the speed of 0.4-0.9 DEG C/min, keeps the temperature 10-
16min。
5. any one of -4 filefish feed sorbent preparation method for improving enteron aisle according to claim 1, which is characterized in that
Chitosan, mineral oil, sulfuric acid solution, chitin, glutaraldehyde weight ratio be 3.5-8.6:0.12-0.5:20-34:4-8:
0.12-0.18, sulfuric acid solution concentration are 2-2.8mol/L.
6. a kind of filefish feed adsorbent for improving enteron aisle, which is characterized in that using any one of the claim 1-4 improvement
The filefish feed of enteron aisle is made with sorbent preparation method.
7. a kind of filefish feed for improving enteron aisle, which is characterized in that its raw material includes: import peru fish meal 55-83 by weight
Part, 12-24 parts of peanut powder, 21-30 parts of dry powder of water hyacinth, 14-23 parts of rice chaff, 25-32 parts of leached tea oil slag, 10-18 parts of sesame seed meal, ferment
Female albumen 4-12 parts, 8-16 parts of locust powder, 1-3 parts of spirulina powder, the filefish feed for improving enteron aisle as claimed in claim 6 is inhaled
Attached dose 1-2 parts, 0.5-1.2 parts of mountain flour, 0.4-1 parts of calcium monohydrogen phosphate, 0.1-0.2 parts of probiotics preparation, filefish compound premix 1-2
Part.
8. improving the filefish feed of enteron aisle according to claim 7, which is characterized in that filefish compound premix includes: egg ammonia
Acid, threonine, lysine, glycine betaine, tea polyphenols, apple polyphenol, tryptophan, starch.
9. improving the filefish feed of enteron aisle according to claim 8, which is characterized in that methionine, threonine, lysine, sweet tea
Dish alkali, tea polyphenols, apple polyphenol, tryptophan, starch weight ratio be 0.1-0.4:0.2-0.9:0.1-0.5:1-2:0.12-
0.43:0.5-0.9:0.1-0.2:10-14.
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Application publication date: 20190215 |