CN109329453B - Peony seed oil-containing microcapsule powder suitable for pregnant women and preparation method thereof - Google Patents
Peony seed oil-containing microcapsule powder suitable for pregnant women and preparation method thereof Download PDFInfo
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- CN109329453B CN109329453B CN201811290061.0A CN201811290061A CN109329453B CN 109329453 B CN109329453 B CN 109329453B CN 201811290061 A CN201811290061 A CN 201811290061A CN 109329453 B CN109329453 B CN 109329453B
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Abstract
The invention belongs to the technical field of edible oil processing, and particularly relates to peony seed oil-containing microcapsule powder suitable for women in pregnancy and lactation. The microcapsule powder mainly comprises peony seed oil, algae oil, fish oil, and other nutritional ingredients necessary for pregnant women. The invention combines peony seed oil, fish oil and algae oil through microencapsulation treatment, provides n-3 fatty acid which accords with dietary nutrient recommendation standard of Chinese residents for the pregnancy preparation period and the pregnancy period: nutrient substances such as alpha-linolenic acid, DHA, EPA and the like; in addition, the invention prepares the product form into microcapsule powder, avoids unpleasant mouthfeel brought to pregnant women by fishy smell of fish oil and algae oil, and increases acceptability.
Description
Technical Field
The invention belongs to the technical field of edible oil processing, and particularly relates to peony seed oil-containing microcapsule powder suitable for pregnant women, and a preparation method of the microcapsule powder.
Background
Pregnancy is a complex physiological process, and for the success of pregnancy, the physiological state and body metabolism of pregnant women are greatly adaptively changed so as to meet the growth and development of maternal reproductive organs and fetuses during pregnancy and provide nutrition for postpartum lactation. The quality of the nutritional status during pregnancy has a crucial influence on the health of the fetus from the growth and development to the adult, and the pregnant women have increased energy and various nutrients, especially protein, essential fatty acid, and various trace nutrients such as calcium, iron, folic acid, vitamin A, etc., compared with non-pregnant women.
Because the development speed of the embryo is not smooth in different periods of pregnancy, the physiological state, the metabolic change of the body and the requirement on nutrients of the pregnant woman are different. According to the physiological process and the nutritional requirement characteristics of pregnancy, the dietary guidelines of pregnant women are divided into three parts, namely, the early pregnancy (3 months to 6 months before pregnancy), the early pregnancy (1 week to 12 weeks during pregnancy), the middle pregnancy (13 weeks to 27 weeks during pregnancy) and the late pregnancy (28 weeks during pregnancy to delivery).
From the middle of pregnancy, the fetus enters a fast-growing developmental stage until delivery. Since 20 weeks of pregnancy, the fetal brain cell division is accelerated, which is a key period of fetal brain and retina development, the required amount of phospholipids as structural and functional components of brain cells and retina cells is increased, and the long-chain polyunsaturated fatty acid (i.e., omega-3 fatty acid) on the phospholipids is especially important. Modern life science studies have demonstrated that pregnant women pass through the placenta, and that lying-in women pass through the milk to deliver the ingested alpha-linolenic acid and the metabolites DHA and EPA to the fetus or baby. Therefore, during the period, the pregnant woman and the lying-in woman take enough alpha-linolenic acid, and the brain nerve cells and the optic nerve cells of the fetus or the infant develop well, are more in number and have strong functions. Alpha-linolenic acid can promote the body function and physical development of fetus and infant, especially for the fetus and premature infant with dysplasia, and can promote their function development to reach normal level. World Health Organization (WHO) recommendations: the women in pregnancy and lactation period must take enough alpha-linolenic acid. If pregnant and lying-in women lack of alpha-linolenic acid in vivo, the babies have the symptoms of brain development retardation, intelligence impairment, slow body development, poor eyesight, rough skin and the like.
2013 edition of handbook for reference intake of dietary nutrients for Chinese residents proposes that the suitable intake (AI) of alpha-linolenic acid of pregnant women and lactating women is 0.60% of energy, while the daily intake of the pregnant women is 2700kcal/d, and that the pregnant women and the lactating women are recommended to supplement 1600mg of alpha-linolenic acid daily, which is converted into about 4.5g of peony seed oil per day. The reference intake of DHA is 200mg/d and the reference intake of EPA is 50mg/d, as specified in the quick look manual. The contents of alpha-linolenic acid, DHA and EPA in the peony seed oil solid formula functional food (pregnant and lying-in women formula) strictly execute the dietary guidelines of Chinese residents and the reference intakes of dietary nutrients of Chinese residents.
CN104922230A discloses a peony seed oil soft capsule, which is prepared from the following raw materials in parts by weight:
the preparation method comprises the steps of firstly weighing peony seed oil soft capsules, propyl gallate, linseed oil, fish oil and vitamin E according to the weight parts, uniformly mixing and tempering, and then preparing soft capsule glue solution by using gelatin, glycerol, an opacifier and water. Then pressing and forming to prepare soft capsules, and finally, carrying out hardening, shaping, drying and other treatment steps. The weight parts of the raw materials are as follows: 70-85 parts of peony seed oil, 4-10 parts of propyl gallate, 1-5 parts of linseed oil, 1-5 parts of fish oil, 0.1-0.5 part of vitamin E, 1-5 parts of gelatin, 1-5 parts of glycerol, 1-5 parts of water and 0.1-0.5 part of an opacifier.
The patent discloses a method for preparing a capsule product, which can avoid the fishy smell brought by fish oil when the capsule product is taken orally, but the fishy smell of the fish oil, the fish oil and the algae oil still affect the taste and the feeling of pregnant women through the stomach and the esophagus after the capsule shell is dissolved and the content flows out.
For pregnant women, particularly pregnant women with a strong pregnancy reaction (vomiting reaction) in the early pregnancy period, although the fish oil is a nutrient with fishy smell, the fish oil is very unacceptable for the pregnant women and is easy to cause nausea and vomiting reaction even after being eaten, although the fish oil is beneficial to the health of the pregnant women and the development of fetuses.
Therefore, a healthy oil product which can provide nutrient components required by the pregnant woman and the fetus in the abdomen, make nutrient substances such as alpha-linolenic acid, DHA, EPA, folic acid, iron, calcium and the like meet the dietary standard and make the pregnant woman pleasantly accept needs to be provided.
Disclosure of Invention
In order to solve the technical problems, the invention provides the n-3 fatty acid nutrient-containing microcapsule powder which is prepared by combining three main raw materials of peony seed oil, fish oil and algae oil and utilizing a specific process and is suitable for pregnant women, the microcapsule powder comprehensively benefits the advantages of the peony seed oil, the algae oil and the fish oil, and provides alpha-linolenic acid, DHA, EPA, folic acid, ferrum, calcium, vitamin A and vitamin D which meet dietary standards for the pregnant women and fetuses3The like, and has good taste and no fishy smellIs easy to be accepted by pregnant women.
The invention relates to a peony seed oil-containing microcapsule powder suitable for pregnant women, which solves the technical problems through the following technical scheme:
a microcapsule powder containing peony seed oil suitable for pregnant women mainly comprises edible oil; the edible oil is prepared from the following raw materials in parts by weight:
and (3) peony seed oil: 10-25 parts; algae oil: 0.5-2.5 parts; fish oil: 1-2 parts.
As an improvement of the invention, the microcapsule powder also comprises the following raw materials in parts by weight:
folic acid: 0.001-0.004 portion
Calcium gluconate: 1-3 parts of
Ferrous gluconate: 0.02-0.1 portion
Vitamin A: 0.1-0.25/ten thousand
Vitamin D3: 0.001-0.003/ten thousand
Vitamin B12: 0.10-0.20/ten thousand.
As another improvement of the invention, the microcapsule powder also comprises the following auxiliary materials in parts by weight: perilla extract, sophora flower extract and bamboo leaf extract;
the perilla extract accounts for 0.2-0.6% of the total weight of the edible oil;
the flos Sophorae Immaturus extract accounts for 0.3-0.5% of the total weight of the edible oil;
the bamboo leaf extract accounts for 0.2-0.5% of the total weight of the edible oil.
The peony seed oil-containing microcapsule powder suitable for pregnant women is prepared by the following steps:
(1) preparing the following raw materials in parts by weight:
mixing peony seed oil, algae oil and fish oil uniformly to obtain mixed oil;
(2) adding distilled water into the wall material, and dissolving at 50-70 deg.C;
(3) adding a composite emulsifier into the mixed oil in the step (1), mixing with the wall material in the step (2), shearing, emulsifying and homogenizing to obtain an emulsion;
(4) spray drying, and granulating with fluidized bed to obtain final product.
Preferably, the wall material used in (2) above is specifically: maltodextrin, 2: 10-20 parts of sodium caseinate: 0.5-2 parts of isomaltooligosaccharide: 5-10 parts;
the DE value of maltodextrin is 15-20;
(3) the emulsifier adopted in the method is a compound emulsifier: the emulsifier comprises the following components in parts by weight: mono-diglycerol fatty acid ester: polyglyceryl fatty acid ester ═ 4: 3: 3.
the conditions of shear emulsification are: 6000-7000r/min high-speed shearing emulsification for 15 minutes;
the conditions for homogenization were: homogenizing at 10-25 MPa for 10min
(4) The conditions of spray drying are: the air inlet temperature is 180 ℃, and the air outlet temperature is 70-90 ℃.
More preferably, the preparation method of the peony seed oil-containing microcapsule powder suitable for pregnant women comprises the following steps:
(1) preparing the following raw materials in parts by weight:
taking 15-20 parts of peony seed oil, 1-5 parts of algae oil and 1-2 parts of fish oil, and uniformly mixing to obtain mixed oil;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin, 2: 10-20 parts of sodium caseinate: 0.5-2 parts of isomaltooligosaccharide: 5-10 parts; the parts are by weight;
the DE value of maltodextrin is 15-20;
(3) adding an emulsifier into the mixed oil in the step (1), taking the whole as a core material, shearing and emulsifying the core material and the wall material in the step (2), and homogenizing to obtain an emulsion;
the conditions of shear emulsification are: 6000-7000r/min high-speed shearing emulsification for 15 minutes;
the conditions for homogenization were: homogenizing for 10min under the homogenizing pressure of 10-25 MPa.
The weight ratio of the wall material to the core material is 3: 2;
the emulsifier is a compound emulsifier: the emulsifier comprises a mono-diglycerol fatty acid ester (linolenic acid), a mono-diglycerol fatty acid ester (oleic acid) and a polyglycerol fatty acid ester, wherein the proportion of the three emulsifiers is that the mono-diglycerol fatty acid ester (linolenic acid): mono-diglycerol fatty acid ester (oleic acid): polyglyceryl fatty acid ester ═ 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product.
In order to make the microcapsule powder richer and more comprehensive in nutrition, the inventor adds a certain proportion of VE and folic acid into the microcapsule powder, so that the microcapsule powder is suitable for pregnant women to eat; the method comprises the following specific steps:
(1) preparing the following raw materials in parts by weight:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil and 0.01-0.07 part of VE, and uniformly mixing to obtain mixed oil;
(2) adding distilled water into the wall material, and dissolving at 60 ℃; the wall material is as follows: maltodextrin, 2: 10-20 parts of sodium caseinate: 0.5-2 parts of isomaltooligosaccharide: 5-10 parts of folic acid and 0.001-0.004 part of folic acid; the DE value of maltodextrin is 15-20;
(3) adding an emulsifier into the mixed oil in the step (1), taking the whole as a core material, shearing and emulsifying the core material and the wall material in the step (2), and homogenizing to obtain an emulsion;
the conditions of shear emulsification are: 6000-7000r/min high-speed shearing emulsification for 15 minutes;
the conditions for homogenization were: homogenizing for 10min under the homogenizing pressure of 10-25 MPa.
The weight ratio of the wall material to the core material is 3: 2;
the emulsifier is a compound emulsifier: the emulsifier comprises a monoglyceride/diglycerol fatty acid ester, a monoglyceride/diglycerol fatty acid ester and a polyglycerol fatty acid ester, wherein the ratio of the three emulsifiers is the monoglyceride/diglycerol fatty acid ester: mono-diglycerol fatty acid ester: polyglyceryl fatty acid ester ═ 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product.
In order to overcome the fishy smell brought by the fish oil and the algae oil in the microcapsule powder, the inventor adds substances capable of eliminating the fishy smell during the preparation of the microcapsule powder, and the added substances have no adverse effect on the bodies of pregnant women or lactating women, and the specific preparation method is as follows:
(1) preparing the following raw materials in parts by weight:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil and 0.01-0.07 part of VE, and uniformly mixing to obtain mixed oil;
adding the perilla extract, the sophora flower extract and the bamboo leaf extract into the mixed oil to obtain a mixture, wherein the adding amounts are respectively as follows:
the perilla extract accounts for 0.2-0.6% of the total weight of the edible oil;
the sophora flower extract accounts for 0.3-0.5% of the total weight of the edible oil;
the bamboo leaf extract accounts for 0.2-0.5% of the total weight of the edible oil;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin, 2: 10-20 parts of sodium caseinate: 0.5-2 parts of isomaltooligosaccharide: 5-10 parts of maltodextrin, wherein the DE value of the maltodextrin is 15-20;
(3) adding an emulsifier into the mixture obtained in the step (1), taking the mixture as a core material, shearing and emulsifying the core material and the wall material obtained in the step (2), and homogenizing to obtain an emulsion;
the conditions of shear emulsification are: 6000-7000r/min high-speed shearing emulsification for 15 minutes;
the conditions for homogenization were: homogenizing for 10min under the homogenizing pressure of 10-25 MPa;
the weight ratio of the wall material to the core material is 3: 2;
the emulsifier is a compound emulsifier: the emulsifier comprises a monoglyceride/diglycerol fatty acid ester, a monoglyceride/diglycerol fatty acid ester and a polyglycerol fatty acid ester, wherein the ratio of the three emulsifiers is the monoglyceride/diglycerol fatty acid ester: mono-diglycerol fatty acid ester: polyglyceryl fatty acid ester ═ 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product.
More preferably, the preparation method of the peony seed oil-containing microcapsule powder suitable for pregnant women comprises the following steps:
(1) preparing the following raw materials in parts by weight:
18 parts of peony seed oil, 4 parts of algae oil, 1.5 parts of fish oil and 0.01-0.07 part of VE, and uniformly mixing to obtain mixed oil;
adding the perilla extract, the sophora flower extract and the bamboo leaf extract into the mixed oil to obtain a mixture, wherein the adding amounts are respectively as follows:
the perilla extract accounts for 0.3% of the total weight of the edible oil;
the sophora flower extract accounts for 0.4% of the total weight of the edible oil;
the bamboo leaf extract accounts for 0.3% of the total weight of the edible oil;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin, 2: 15 parts of sodium caseinate: 1 part of isomaltooligosaccharide: 8 parts of a mixture; DE value of maltodextrin 18;
(3) adding an emulsifier into the mixture obtained in the step (1) as a core material, shearing and emulsifying the core material and the wall material obtained in the step (2), and homogenizing to obtain an emulsion;
the conditions of shear emulsification are: 6500r/min high-speed shearing and emulsifying for 15 min;
the conditions for homogenization were: homogenizing under 20MPa for 10 min;
the weight ratio of the wall material to the core material is 3: 2;
the emulsifier is a compound emulsifier: the emulsifier comprises a monoglyceride/diglycerol fatty acid ester, a monoglyceride/diglycerol fatty acid ester and a polyglycerol fatty acid ester, wherein the ratio of the three emulsifiers is the monoglyceride/diglycerol fatty acid ester: mono-diglycerol fatty acid ester: polyglyceryl fatty acid ester ═ 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product.
The invention has the beneficial effects that the peony seed oil, the fish oil and the algae oil are combined through microencapsulation treatment, so that the nutrient substances such as alpha-linolenic acid, DHA, EPA and the like which meet the dietary standards are provided for pregnant women and fetuses; in addition, the invention prepares the product form into microcapsule powder, avoids unpleasant mouthfeel brought to pregnant women by fishy smell of fish oil and algae oil, and increases acceptability.
Drawings
FIG. 1 is a physical appearance diagram of microcapsule powder of example 1 of the present invention;
fig. 2 is a three-dimensional picture of the microcapsule powder of example 1 of the present invention after brewing;
fig. 3 is a top view of the microencapsulated powder of example 1 of the present invention after brewing;
FIG. 4 is a photograph of the raw material peony seed oil of the present invention;
FIG. 5 is a photograph of the fish oil as a raw material according to the present invention;
FIG. 6 is a photograph of a raw algal oil according to the present invention.
Detailed Description
The invention will be further described with reference to the accompanying drawings and specific embodiments so that those skilled in the art may better understand the invention, but the invention is not limited thereto.
The manufacturer: tianbao peony biotechnology limited;
and (3) peony seed oil: yao shun peony biotech, Inc.;
algae oil: qingdao Haizyuan Life technologies, Inc.;
fish oil: qingdao Haizyuan Life technologies, Inc.;
wall material: spearmint bioengineering technologies, ltd;
emulsifier: liaoning sea food chemical engineering Co., Ltd;
example 1
The preparation method of the peony seed oil-containing microcapsule powder suitable for pregnant women in the middle pregnancy period (4-7 months of pregnancy) comprises the following steps:
(1) preparing the following raw materials in parts by weight:
18 kg of peony seed oil, 4 kg of algae oil, 1.5 kg of fish oil and 0.04 kg of VE are uniformly mixed to obtain mixed oil;
adding Perilla extract to the mixed oil about 0.072 kg; the weight of the sophora flower extract is about 0.09 kg; the amount of the bamboo leaf extract is about 0.08 kg, and a mixture is obtained;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin (DE value 18)22.2 kg, sodium caseinate: 1.5 kg, isomaltooligosaccharide: 11.8 kg; the amount of distilled water used was 284 kg.
(3) Adding an emulsifier into the mixture obtained in the step (1), taking the mixture as a core material, shearing and emulsifying the core material and the wall material obtained in the step (2), and homogenizing to obtain an emulsion;
the conditions of shear emulsification are: 6500r/min high-speed shearing and emulsifying for 15 min;
the conditions for homogenization were: homogenizing under 20MPa for 10 min;
the weight ratio of the wall material to the core material is about 3: 2;
the emulsifier is a compound emulsifier: the emulsifier comprises a mono-diglycerol fatty acid ester (linolenic acid), a mono-diglycerol fatty acid ester (oleic acid) and a polyglycerol fatty acid ester, wherein the proportion of the three emulsifiers is that the mono-diglycerol fatty acid ester (linolenic acid): mono-diglycerol fatty acid ester (oleic acid): polyglyceryl fatty acid ester ═ 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product. The conditions of the spray drying were: the air inlet temperature is 180 ℃, and the air outlet temperature is 70-90 ℃.
Example 2
The subject to which this embodiment is directed is a pregnant woman in the early stage of pregnancy, i.e. a pregnant woman pregnant for 1-3 months; the preparation method of the peony seed oil-containing microcapsule powder suitable for pregnant women in early pregnancy provided by the embodiment comprises the following steps:
(1) preparing the following raw materials in parts by weight:
18 kg of peony seed oil, 4 kg of algae oil, 1.5 kg of fish oil and 0.05 kg of VE are uniformly mixed to obtain mixed oil;
adding Perilla extract to the mixed oil about 0.075 kg; about 0.095 kg of sophora flower extract; the bamboo leaf extract is about 0.065 kg to obtain a mixture;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin (DE value 18)22.2 kg, sodium caseinate: 1.5 kg, isomaltooligosaccharide: 11.8 kg, then 0.004 kg folic acid is added; the amount of distilled water used was 285 kg.
(3) Adding an emulsifier into the mixed oil in the step (1), taking the whole as a core material, shearing and emulsifying the core material and the wall material in the step (2), and homogenizing to obtain an emulsion;
the conditions of shear emulsification are: 6500r/min high-speed shearing and emulsifying for 15 min;
the conditions for homogenization were: homogenizing under 20MPa for 10 min;
the weight ratio of the wall material to the core material is about 3: 2;
the emulsifier is a compound emulsifier: the emulsifier comprises a mono-diglycerol fatty acid ester (linolenic acid), a mono-diglycerol fatty acid ester (oleic acid) and a polyglycerol fatty acid ester, wherein the proportion of the three emulsifiers is that the mono-diglycerol fatty acid ester (linolenic acid): mono-diglycerol fatty acid ester (oleic acid): polyglyceryl fatty acid ester ═ 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating by fluidized bed to obtain microcapsule powder; the conditions of the spray drying were: the air inlet temperature is 180 ℃, and the air outlet temperature is 70-90 ℃.
Example 3
The subject to which this embodiment is directed is a pregnant woman in the late stage of pregnancy, i.e., pregnant woman from 28 weeks gestation to childbirth; the preparation method of the peony seed oil-containing microcapsule powder suitable for pregnant women in late pregnancy provided by the embodiment comprises the following steps:
(1) preparing the following raw materials in parts by weight:
20 parts of peony seed oil, 4 parts of algae oil, 2 parts of fish oil and 0.07 kg of VE, and uniformly mixing to obtain mixed oil;
adding 0.078 kg of perilla extract, 0.1 kg of sophora flower extract and 0.085 kg of bamboo leaf extract into the mixed oil to obtain a mixture;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin (DE value 15-20): 24.5 kg, sodium caseinate: 1.66 kg, isomaltooligosaccharide: 13 kg; the amount of distilled water used was 156.6 kg.
(3) Adding an emulsifier into the mixture obtained in the step (1), taking the mixture as a core material, shearing and emulsifying the core material and the wall material obtained in the step (2), and homogenizing to obtain an emulsion;
the conditions of shear emulsification are: shearing and emulsifying at 7000r/min for 15 min;
the conditions for homogenization were: homogenizing for 10min under the homogenizing pressure of 10-25 MPa;
the weight ratio of the wall material to the core material is 3: 2;
the emulsifier is a compound emulsifier: the emulsifier comprises a mono-diglycerol fatty acid ester (linolenic acid), a mono-diglycerol fatty acid ester (oleic acid) and a polyglycerol fatty acid ester, wherein the proportion of the three emulsifiers is that the mono-diglycerol fatty acid ester (linolenic acid): mono-diglycerol fatty acid ester (oleic acid): polyglyceryl fatty acid ester ═ 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product. The conditions of the spray drying were: the air inlet temperature is 180 ℃, and the air outlet temperature is 70-90 ℃.
Comparative experiment:
the inventor performs the following comparative experiments when selecting the auxiliary material components:
comparative example 1
(1) Preparing the following raw materials in parts by weight:
18 kg of peony seed oil, 4 kg of algae oil, 1.5 kg of fish oil and 0.05 kg of VE are uniformly mixed to obtain mixed oil;
comparative example 2
The difference from example 1 is that only one plant extract is added, and the rest is the same as example 1;
adding the perilla extract into the mixed oil, wherein the adding amount is as follows: 0.242 kg;
comparative example 3
The difference from comparative example 2 is that the plant extract was replaced with sophora flower extract, which was added in the following amounts: 0.242 kg;
comparative example 4
The difference from comparative example 2 is that the plant extract was replaced with bamboo leaf extract, which was added in the following amounts: 0.242 kg;
comparative example 5
The difference from the example 1 is that the perilla extract and the sophora flower extract are added into the mixed oil, and the adding amount is as follows: perilla extract 0.112 kg; 0.13 kg of sophora flower extract; the rest is completely the same as the embodiment 1;
comparative example 6
The difference from the example 1 is that the sophora flower extract and the bamboo leaf extract are added into the mixed oil, and the adding amount is as follows: 0.126 kg of sophora flower extract; 0.116 kg of bamboo leaf extract; the rest is exactly the same as in example 1.
Comparative example 7
The difference from example 1 is that perilla extract and bamboo leaf extract are added to the mixed oil in the following amounts: perilla extract 0.117 kg, bamboo leaf extract 0.125 kg; the rest is completely the same as the embodiment 1;
with respect to the products of examples 1 to 3 and comparative examples 1 to 7, the present inventors conducted the following test experiments:
the peroxide value is determined according to GB/T5538-:
the raw materials of the product are detected by high performance liquid chromatography (three main substances with fishy smell are selected), and the data are as follows:
table 1 table of the results of measuring the content of the main fishy smell substances in the examples and comparative examples
As can be seen from the data in the above table, the comparative example 1, which is not added with any plant extract, has stronger fishy smell and higher oxidation resistance, which indicates that the plant extract used in the present invention has a more significant effect on removing the fishy smell and the plant extract used in the present invention also has a very significant effect on the oxidation resistance of the microcapsule powder.
As can be seen from comparative examples 2-4, a single plant extract, which had some effect on fishy smell removal or oxidation resistance, but the overall effect was not as good as that of examples 1-3; the reason is that the perilla extract, the sophora flower extract and the bamboo leaf extract all have antioxidant effects, and the perilla extract and the sophora flower extract have obvious effects on removing fishy smell; the principle of removing fishy smell of the two is as follows: the fish oil is very easy to oxidize during storage, carbides and other fishy components generated by automatic oxidation of omega-3 unsaturated fatty acids, such as 2, 4-decadienal, 2, 4, 7-decatrienal and the like, are putrefactive during storage of the fish oil due to action of microorganisms or enzymes or automatic oxidation of lipids, and the fish oil also contains oxidized trimethylamine, which is degraded under the combined action of the microorganisms and the enzymes to generate trimethylamine and dimethylamine, wherein the pure trimethylamine has only ammonia smell and is not existed in many fresh fishes, but the content of the stored fish oil is high, and the pure trimethylamine is subjected to action of the microorganisms or the enzymes or automatic oxidation of fish oil lipids and generates strong fishy smell together with delta-2 aminopentanoic acid, hexahydropyridine and the like.
Therefore, the plant extract, the perilla extract, the sophora flower extract and the bamboo leaf extract are added, the oxidation resistance of the three extracts is stronger and far exceeds that of antioxidants such as VC, and fishy smell components such as carbides generated by automatic oxidation of omega-3 unsaturated fatty acids are prevented from being generated by oxidation of fish oil in the storage process; the purple perilla extract and the bamboo leaf extract have the remarkable effects of bacteriostasis, and the bamboo leaf extract can inhibit the generation of microorganisms in the fish oil in the storage process, prevent trimethylamine in the fish oil from being influenced by the microorganisms and generate strong fishy smell together with delta-2 aminovaleric acid, hexahydropyridine and the like; therefore, the purpose of inhibiting the fishy smell is achieved, meanwhile, the perilla extract and the sophora flower extract contain aromatic substances and can cover or shield the fishy smell, so that the addition of the three plant extracts has a good effect on removing the fishy smell;
in addition, the added perilla extract has high safety, the perilla is a medicinal and edible raw material, has the miscarriage prevention effect and does not harm pregnant women; the sophora flower extract has high safety and strong oxidation resistance, and can remove fishy smell in the microcapsule powder by synergistic action with the perilla extract. Although the mint extract also has a certain fishy smell removing effect, the mint extract is not suitable for pregnant women and has an anti-early pregnancy effect, so that not any plant extract is suitable for pregnant women. Safety is a primary consideration when selecting plant extracts, followed by a fishy smell-removing effect; the raw materials adopted by the invention have higher safety, and the dosage of the raw materials is very small, thereby having no adverse effect on the body of the pregnant woman.
It can be seen from comparative examples 5-7 that the three plant extracts used in the present invention have synergistic effect, and when the three extracts are combined, the fishy smell removing effect and the antioxidant effect are obviously better than those of the combination of the two plant extracts with the same addition amount.
Example 4
With respect to the quality of the microcapsule powders obtained in examples 1 to 3, the present inventors carried out the following examination:
(1) quality evaluation
a. Sense organ
And evaluating the sensory properties of the powder oil and fat such as color, smell, tissue state and the like by using a sensory evaluation method.
b. Physical and chemical properties
The physicochemical indexes of the powdered oil, such as water content, density, solubility, stacking angle, oil content, surface oil content, embedding efficiency, particle size distribution, etc., are analyzed.
c. Microstructure
Spreading the sample on a sample table adhered with double-sided adhesive tape, blowing off redundant powder, spraying gold powder on the surface of the sample by using an ion sputtering device, and observing the microstructure of the product by using a scanning electron microscope. The accelerating voltage is 1KV, and the amplification factor is 300-1000 times.
d. Reconstituted emulsion
Weighing 25g of powder oil product into a 250mL beaker, adding 200mL of hot water at the temperature of 70-80 ℃, stirring, fully dissolving, dispersing, and observing the dissolution condition, color and uniformity of the recovered emulsion; the surface has no conjunctiva, layering and particle wall hanging; the emulsion was analyzed for particle size distribution.
(2) Evaluation of storage stability
Storage at a.20 ℃
The powdered oil is sealed and placed in a constant temperature incubator, and the temperature in the incubator is 20 ℃. The oil content of the surface of the powdered oil and fat, the embedding efficiency and the granularity of the recovered emulsion are detected at certain time intervals within the storage period of 6 months, and the acid value, the peroxide value and the fatty acid composition of the oil and fat are detected.
b. Accelerated storage test
The accelerated storage test was carried out in an oven at 60 ℃ and the powdered oil and core oil were stored in an oven at 60 ℃ for 30 days. The oxidation stability index OSI and peroxide number of the oil and fat were measured separately.
c. Shelf life prediction
The powdered oil was stored at 20 ℃, 40 ℃, 50 ℃ and 60 ℃ respectively, and the peroxide value of the sample was measured at each storage temperature to predict the shelf life of the product.
(3) Index analysis
a. Melting Point of oil and fat samples
The sliding melting point was determined by the open capillary method. And (3) completely drying the grease sample, melting, soaking at least 3 capillaries into the sample, raising the grease to a height of 10mm, and immediately cooling the sample until the grease is solidified. And (3) placing the glass tube in a refrigerator at 4-10 ℃ for 16h, taking out the capillary tube, fixing the capillary tube on a thermometer by using a rubber band, and enabling the lower end to be parallel to the mercury column. The thermometer was hung in a beaker of clean distilled water with the lower end of the thermometer submerged below the liquid level. Adjusting the initial temperature of the water bath to be 8-10 ℃ lower than the sliding melting point, stirring the water bath to heat the water bath for 1 ℃/min, and cooling to 0.5 ℃/min when the temperature is close to the melting point. The temperature was continued until the fat column rose, and the temperature at which each fat column rose was observed and the average value was calculated.
b. Emulsion stability of emulsions
Keeping the emulsion in a constant temperature water bath at 60 deg.C for 30min, and centrifuging the tube in a centrifuge for 15min (4500 r/min). The liquid was taken out to observe the delamination, and the total height (H) of the liquid and the height (H1) of the non-delamination were recorded. Calculating the stability value of the emulsion according to the following formula;
c. oil content of powdery oil and fat
Chloroform-methanol extraction method is adopted. A3 g sample (m) was taken and dissolved in 12mL of water. Adding 15mL of chloroform and 30mL of methanol, and uniformly mixing; then, 15mL of chloroform and 15mL of distilled water were added thereto and mixed for 30 seconds. The solution is transferred to a centrifuge tube, 3000r/min and centrifuged for 10 min. The lower chloroform solution 10mL was pipetted into a constant weight round bottom flask (m1), the chloroform was removed by rotary evaporation, and the solution was dried to a constant weight and weighed (m 2). The formula for oil content is as follows:
d. surface oil content and embedding efficiency (MEE) of powdery oil
Accurately weighing a sample with the mass (m) of 2-3G in a triangular flask, accurately leaching for 1min by using 40mL of petroleum ether with the temperature of 30-60 ℃ under slight stirring, immediately performing suction filtration by using a G3 sand core funnel, washing filter residue for 40s by using 25mL of petroleum ether, immediately performing suction filtration, recovering the petroleum ether in filtrate, and drying at 65 ℃ to constant weight to obtain the mass (m1) of surface grease; calculating the surface oil content and the embedding efficiency;
e. and (3) particle size analysis: the particle size of the emulsion is measured by a laser particle size analyzer in a wet method, and the particle size of the powdered oil particles is measured by a dry method
f. Water content: according to the GB5497-1985 method, drying is carried out for 2-3 h at 105 ℃, and constant weight weighing is carried out
g. Density: pouring the powdered oil into a graduated measuring cylinder, and calculating the weight of the powdered oil per unit volume
h. Solubility of powdery oil: dissolving the sample in water at 25-30 ℃, centrifuging, measuring the mass of the precipitate, and calculating the solubility of the powdered oil
i. Angle of stack: measuring the angle of natural accumulation by taking a certain amount of product
j. Fatty acid composition: fatty acid composition analysis reference
k. Oxidation stability index OSI: according to GB/T21121-2007
Peroxide number: according to GB/T5538-2005
m. acid value: according to GB/T5530-2005.
(4) Analysis of fatty acid composition
And (3) measuring by using a gas chromatograph:
chromatographic conditions are as follows:
chromatographic column with stuffing of cyanopropyl aryl polysiloxane capillary column of 100m length, 0.25mm inside diameter and 0.2 micron thickness; or a column of equivalent performance.
A hydrogen Flame Ionization Detector (FID), wherein the detector temperature is 300 ℃, the sample inlet temperature is 250 ℃, the carrier gas has the split ratio of 10:1, the sample injection amount is 1.0 mu L, and the temperature programming conditions are as follows:
TABLE 2 temperature programmed conditions
| Rate of temperature rise (. degree. C./min) | Temperature (. degree.C.) | Retention time (min) |
| - | 120 | 0 |
| 10 | 175 | 10 |
| 5 | 210 | 5 |
| 5 | 230 | 5 |
As can be seen from the table above, the fatty acid composition of the peony seed oil solid formula functional food is basically consistent with that of the raw oil, and the unsaturated fatty acid content is 90 percent
Table 3 table of characteristics of products in examples 1 to 3
The content of the alpha-linolenic acid, DHA and EPA is basically consistent before and after embedding, which shows that the fatty acid composition in the crude oil is not damaged and the process parameters are reasonable under the spray drying process condition.
Table 4 fatty acid analysis of products in examples 1-3
Through the data analysis and comparison in the above tables, it can be concluded that the microcapsule powder of the present invention has the advantages of: the accompanying drawings 4-6 are pictures of the raw materials of the invention, and compared with the raw material edible oil, the product of the invention has the advantages that the pregnant women do not need to eat or drink various nutritional oil products one by one, and only one bag or one cup of the microcapsule powder of the invention needs to be brewed to obtain the nutritional substances such as alpha-linolenic acid, DHA, EPA and the like required by the diet, which brings great convenience for the pregnant women; the invention also solves the problem that the fish oil and the algae oil bring unpleasant acceptance to the pregnant women, and the auxiliary material raw material, namely the plant extract, is added, so that the microcapsule powder can play an effective antioxidation role, and the fishy smell can be removed, thereby enabling the pregnant women to enjoy the acceptance.
Example 5
The subject to which this embodiment is directed is a pregnant woman in late pregnancy, i.e., a pregnant woman in 5-30 weeks of pregnancy; the preparation method of the peony seed oil-containing microcapsule powder suitable for pregnant women in late pregnancy provided by the embodiment comprises the following steps:
(1) preparing the following raw materials in parts by weight:
20 parts of peony seed oil, 4 parts of algae oil, 2 parts of fish oil and 0.07 kg of VE, and uniformly mixing to obtain mixed oil;
adding 0.078 kg of perilla extract, 0.1 kg of sophora flower extract and 0.085 kg of bamboo leaf extract into the mixed oil to obtain a mixture;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin (DE value 15-20): 24.5 kg, sodium caseinate: 1.66 kg, isomaltooligosaccharide: 13 kg; the amount of distilled water used was 156.6 kg.
(3) Adding an emulsifier into the mixture obtained in the step (1), taking the mixture as a core material, shearing and emulsifying the core material and the wall material obtained in the step (2), and homogenizing to obtain an emulsion; adding folic acid to the emulsion: 0.001-0.004 kg, calcium gluconate: 1-3 kg, ferrous gluconate: 0.02-0.1 kg, vitamin a: 0.3/ten thousand, vitamin D3: 0.002/ten thousand vitamin B12: 0.15/ten thousand;
the conditions of shear emulsification are: shearing and emulsifying at 7000r/min for 15 min;
the conditions for homogenization were: homogenizing for 10min under the homogenizing pressure of 10-25 MPa;
the weight ratio of the wall material to the core material is 3: 2;
the emulsifier is a compound emulsifier: the emulsifier comprises a mono-diglycerol fatty acid ester (linolenic acid), a mono-diglycerol fatty acid ester (oleic acid) and a polyglycerol fatty acid ester, wherein the proportion of the three emulsifiers is that the mono-diglycerol fatty acid ester (linolenic acid): mono-diglycerol fatty acid ester (oleic acid): polyglyceryl fatty acid ester ═ 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product. The conditions of the spray drying were: the air inlet temperature is 180 ℃, and the air outlet temperature is 80 ℃.
Claims (7)
1. The peony seed oil-containing microcapsule powder suitable for pregnant women is characterized by mainly comprising edible oil and auxiliary raw materials; the edible oil is prepared from the following raw materials in parts by weight: and (3) peony seed oil: 10-25 parts; algae oil: 0.5-2.5 parts; fish oil: 1-2 parts; the auxiliary materials comprise the following raw materials: perilla extract, sophora flower extract and bamboo leaf extract;
the perilla extract accounts for 0.2-0.6% of the total weight of the mixed oil;
the sophora flower extract accounts for 0.3-0.5% of the total weight of the mixed oil;
the bamboo leaf extract accounts for 0.2-0.5% of the total weight of the mixed oil.
2. The method for preparing the peony seed oil-containing microcapsule powder suitable for pregnant women according to claim 1, comprising the steps of:
(1) preparing raw materials:
mixing peony seed oil, algae oil and fish oil uniformly to obtain mixed oil; adding the perilla extract, the sophora flower extract and the bamboo leaf extract into the mixed oil to obtain a mixture;
(2) adding distilled water into the wall material, and dissolving at 50-70 deg.C;
(3) adding a composite emulsifier into the mixture in the step (1), mixing with the wall material in the step (2), shearing, emulsifying and homogenizing to obtain an emulsion;
(4) spray drying, and granulating with fluidized bed to obtain final product.
3. The method for preparing the peony seed oil-containing microcapsule powder suitable for pregnant women according to claim 2, wherein the peony seed oil-containing microcapsule powder is prepared by the following steps:
(2) the wall material adopted in the method is specifically as follows: maltodextrin, 2: 10-20 parts of sodium caseinate: 0.5-2 parts of isomaltooligosaccharide: 5-10 parts; the DE value of maltodextrin is 15-20.
4. The method for preparing the peony seed oil-containing microcapsule powder suitable for pregnant women according to claim 2, wherein the peony seed oil-containing microcapsule powder is prepared by the following steps:
(3) the emulsifier adopted in the method is a compound emulsifier: mono-diglycerol linolenate, mono-diglycerol oleate, polyglyceryl fatty acid ester; the weight ratio of the three emulsifiers is that the mono-diglycerol linolenic acid ester: mono-diglycerol oleate: polyglyceryl fatty acid ester = 4: 3: 3; the conditions of shear emulsification are: 6000-7000r/min high-speed shearing emulsification for 15 minutes; the conditions for homogenization were: homogenizing for 10min under the homogenizing pressure of 10-25 MPa.
5. The method for preparing the peony seed oil-containing microcapsule powder suitable for pregnant women according to claim 2, wherein the peony seed oil-containing microcapsule powder is prepared by the following steps:
(4) the conditions of spray drying are: the air inlet temperature is 180 ℃, and the air outlet temperature is 70-90 ℃.
6. The method for preparing the peony seed oil-containing microcapsule powder suitable for pregnant women according to claim 1, comprising the steps of:
(1) preparing the following raw materials in parts by weight:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil and 0.01-0.07 part of VE, and uniformly mixing to obtain mixed oil; adding the perilla extract, the sophora flower extract and the bamboo leaf extract into the mixed oil to obtain a mixture, wherein the adding amounts are respectively as follows:
the perilla extract accounts for 0.2-0.6% of the total weight of the mixed oil;
the sophora flower extract accounts for 0.3-0.5% of the total weight of the mixed oil;
the bamboo leaf extract accounts for 0.2-0.5% of the total weight of the mixed oil;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin, 2: 10-20 parts of sodium caseinate: 0.5-2 parts of isomaltooligosaccharide: 5-10 parts; the DE value of maltodextrin is 15-20;
(3) adding an emulsifier into the mixture obtained in the step (1), taking the mixture as a core material, shearing and emulsifying the core material and the wall material obtained in the step (2), and homogenizing to obtain an emulsion; the conditions of shear emulsification are: 6000-7000r/min high-speed shearing emulsification for 15 minutes; the conditions for homogenization were: homogenizing for 10min under the homogenizing pressure of 10-25 MPa; the weight ratio of the wall material to the core material is 3: 2; the emulsifier is a compound emulsifier: mono-diglycerol linolenate, mono-diglycerol oleate, polyglyceryl fatty acid ester; the proportion of the three emulsifiers is that mono-diglycerol linolenic acid ester: mono-diglycerol oleate: polyglyceryl fatty acid ester = 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product.
7. The method for preparing the peony seed oil-containing microcapsule powder suitable for pregnant women according to claim 1, comprising the steps of:
(1) preparing the following raw materials in parts by weight:
18 parts of peony seed oil, 4 parts of algae oil, 1.5 parts of fish oil and 0.01-0.07 part of VE, and uniformly mixing to obtain mixed oil; adding the perilla extract, the sophora flower extract and the bamboo leaf extract into the mixed oil to obtain a mixture, wherein the adding amounts are respectively as follows:
the perilla extract accounts for 0.3% of the total weight of the mixed oil;
the flos Sophorae Immaturus extract accounts for 0.4% of the total weight of the mixed oil;
the bamboo leaf extract accounts for 0.3% of the total weight of the mixed oil;
(2) adding wall materials into distilled water, and dissolving at 60 ℃; the wall material is as follows: maltodextrin, 2: 15 parts of sodium caseinate: 1 part of isomaltooligosaccharide: 8 parts of a mixture; DE value of maltodextrin 18;
(3) adding an emulsifier into the mixture obtained in the step (1), taking the mixture as a core material, shearing and emulsifying the core material and the wall material obtained in the step (2), and homogenizing to obtain an emulsion; the conditions of shear emulsification are: 6500r/min high-speed shearing and emulsifying for 15 min; the conditions for homogenization were: homogenizing under 20MPa for 10 min; the weight ratio of the wall material to the core material is 3: 2; the emulsifier is a compound emulsifier: mono-diglycerol linolenate, mono-diglycerol oleate, polyglyceryl fatty acid ester; the proportion of the three emulsifiers is that mono-diglycerol linolenic acid ester: mono-diglycerol oleate: polyglyceryl fatty acid ester = 4: 3: 3, the dosage of the composite material is 0.3 percent of the total weight of the wall material and the core material;
(4) spray drying, and granulating with fluidized bed to obtain final product.
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