CN109329453A - A kind of microcapsule powder and preparation method containing peony seed oil suitable for pregnant woman - Google Patents
A kind of microcapsule powder and preparation method containing peony seed oil suitable for pregnant woman Download PDFInfo
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- CN109329453A CN109329453A CN201811290061.0A CN201811290061A CN109329453A CN 109329453 A CN109329453 A CN 109329453A CN 201811290061 A CN201811290061 A CN 201811290061A CN 109329453 A CN109329453 A CN 109329453A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
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Abstract
The invention belongs to edible oil processing technique fields, and in particular to a kind of microcapsule powder containing peony seed oil eaten suitable for standby pregnant phase and pregnant food in one's mouth phase women.The microcapsule powder mainly includes following raw material: other nutritional ingredients necessary to peony seed oil, algae oil, fish oil and pregnant woman.The present invention is handled by microencapsulation, and peony seed oil, fish oil and algae oil three are combined, the n-3 fatty acid for meeting Chinese residents diet nutrient proposed standard: the nutriments such as alpha-linolenic acid, DHA, EPA is provided for standby pregnant phase, pregnancy period；In addition, the form of product is prepared into microcapsule powder by the present invention, the smelling of fish of fish oil and algae oil is avoided to mouthfeel not pleasant brought by pregnant woman, increases acceptable degree.
Description
Technical field
Invention belongs to edible oil processing technique field, and in particular to a kind of micro-capsule containing peony seed oil suitable for pregnant woman
Powder further relates to the preparation method of above-mentioned microcapsule powder.
Background technique
Gestation is a complicated physiology course, for the success of gestation, the physiological status and organism metabolism of pregnant women
Biggish adaptive change has occurred, to meet the growth and development of pregnancy period maternal genital official and fetus, and for postpartum milk secretion into
Support deposit in field headquarters.The superiority and inferiority of maternal weight gain situation is to embryo growth and development until the health after adult will generate vital shadow
It rings, compared with non-pregnant women, pregnant women increased the requirement of energy and various nutrients, especially albumen
The lot of trace nutrient such as matter, essential fatty acid and calcium, iron, folic acid, vitamin A.
Since the rate of development of pregnancy different times embryo is obstructed, the physiological status of pregnant woman, metabolic alterations of body and right
The demand of nutrient is also different.By the physiology course and nutritional need feature of gestation, diet for pregnant woman guide is divided into pregnant early period (before pregnant
3 months~6 months), pregnant early stage (pregnant 1 week~12 weeks) and it is pregnant in (pregnant 13 weeks~27 weeks), latter stage (pregnant 28 weeks~childbirth) three
Point.
Since second trimester, fetus enters the fast-growth puberty, until childbirth.From pregnant 20 weeks, fetal brain cell division
Accelerate to accelerate, is the critical period of fetal brain and retinal development, as brain cell and retina cell's structure and function ingredient
Phosphatide requirement increase, and long-chain polyunsaturated fatty acid, that is, omega-fatty acid on phosphatide is then particularly important.It is modern
Life science confirms that pregnant woman then passes through milk for the alpha-linolenic acid of intake and metabolin DHA and EPA by placenta, puerpera
Send fetus or baby to.Therefore, in the cranial nerve that this period is pregnant, puerpera takes in enough alpha-linolenic acids, fetus or baby
Cell and optic cell are developed, number is more, function is strong.Alpha-linolenic acid can also promote tire, babies function and body hair
It educates, especially to hypogenetic fetus and premature, their physiogeny can be promoted to reach normal level.World health group
Knit (WHO) suggestion: the gestational period, lactating female must take in enough alpha-linolenic acids.If lacking alpha-linolenic acid in pregnant and lying-in women's body,
So baby's there will be brain growths slow, intellectual impairment, body development slowly, have defective vision, the symptoms such as pachylosis.
It is proposed in 2013 editions " Dietary Reference Intakes of Chinese Residents quick checking handbook ", pregnant woman, wet nurse's alpha-linolenic acid
Suitable intake (AI) be the 0.60% of energy, and the daily ingestion of energy of pregnant woman is 2700kcal/d, it is proposed that pregnant and lying-in women day mend
Filling alpha-linolenic acid 1600mg is advisable, and convert needs 4.5g or so for peony seed oil daily.It is provided in quick checking handbook, the reference of DHA is taken the photograph
Entering amount is 200mg/d, and the Dietary reference intakes of EPA are 50mg/d.Peony seed oil solid formulation functional food (pregnant and lying-in women's formula)
The equal strict implement Chinese residents dietary guidelines of content and " Chinese residents diet nutrient reference of middle alpha-linolenic acid, DHA, EPA
Intake ".
CN104922230A discloses a kind of Peony-seed-oil soft capsule, the Peony-seed-oil soft capsule by following parts by weight original
Material is made:
Preparation conventionally carry out, first by Peony-seed-oil soft capsule, propylgallate, linseed oil, fish oil and
Vitamin E is weighed according to parts by weight, and mixing is quenched uniformly, then, prepares soft capsule glue by gelatin, glycerol, opacifier and water
Liquid.Soft capsule is made in the type of being then pressed into, finally, passing through the processing steps such as hardening sizing, dry.The parts by weight of each raw material
Number is as follows: 70~85 parts of peony seed oil, 4~10 parts of propylgallate, 1~5 part of linseed oil, 1~5 part of fish oil, vitamin
E0.1~0.5 part, 1~5 part of gelatin, 1~5 part of glycerol, 1~5 part of water and 0.1~0.5 part of opacifier.
What the patent disclosed is a kind of capsule product production method, though fish oil bring fishy smell when being avoided that oral,
Stomach, capsule shells dissolution are reached after edible, content flows out, and the fishy smell of the ingredients such as fish oil, algae oil still can pass through stomach, esophagus shadow
Ring the sense of taste and feeling of pregnant woman.
For pregnant woman of the early stage especially pregnant for pregnant woman with strong pregnancy reaction (morning sickness is reacted), eats and have fishy smell
The nutriment of youngster, though being conducive to pregnant woman herself's health and development of fetus, for pregnant woman, the smelling of fish of fish oil is extremely
It is difficult to receive, is also easy to cause nausea and vomiting reaction after even eating.
Accordingly, it is desirable to provide it is a kind of he or she and foetus can be provided for pregnant woman needed for nutritional ingredient, make α-Asia
The nutriments such as numb acid, DHA, EPA, folic acid, iron, calcium meet dietary standard, and can make the healthy oil product of the receiving of pregnant woman's pleasure.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of by these three masters of peony seed oil, fish oil and algae oil
It wants raw material to combine, and prepares the micro- of the obtained fatty acid nutrient containing n-3 suitable for pregnant woman using specific technique
It the advantages of capsule powder, microcapsule powder synthesis has been conducive to peony seed oil, algae oil and fish oil, provides for pregnant woman and fetus and meets diet mark
Alpha-linolenic acid, the DHA, EPA, folic acid, iron, calcium, vitamin A, vitamin D of standard3Equal nutriments, and its mouthfeel is good, no raw meat
Taste is easy to be received by pregnant woman.
The microcapsule powder containing peony seed oil that the present invention is suitable for pregnant woman is more than being solved by following technical solutions
The technical issues of:
A kind of microcapsule powder containing peony seed oil suitable for pregnant woman, which mainly includes edible oils；Edible oil
Class is the raw material of following parts by weight:
Peony seed oil: 10-25 parts；Algae oil: 0.5-2.5 parts；Fish oil: 1-2 parts.
As an improvement of the present invention, which further includes the raw material of following parts by weight:
Folic acid: 0.001-0.004 parts
Calcium gluconate: 1-3 parts
Ferrous gluconate: 0.02-0.1 parts
Vitamin A: 0.1-0.25/ ten thousand
Vitamine D3: 0.001-0.003/ ten thousand
Vitamin B12: 0.10-0.20/ ten thousand.
Improve as another kind of the invention, which further includes the auxiliary material raw material of following parts by weight: purple perilla extracts
Object, Flos Sophorae extract, bamboo extractive；
Extractive of perilla accounts for the 0.2-0.6% of edible oil gross weight；
Flos Sophorae extract accounts for the 0.3-0.5% of edible oil gross weight；
Bamboo extractive accounts for the 0.2-0.5% of edible oil gross weight.
A kind of above-mentioned microcapsule powder containing peony seed oil suitable for pregnant woman, be by following steps method preparation and
At:
(1) prepare each raw material by following weight part ratio:
Peony seed oil, algae oil, fish oil are taken, is uniformly mixed, obtains miscella；
(2) distilled water is added in wall material, is dissolved at 50-70 DEG C；
(3) compound emulsifying agent is added in the miscella in (1), then is mixed with the wall material in (2), emulsification pretreatment,
Matter obtains emulsion；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
Preferably, wall material employed in above-mentioned (2) specifically: maltodextrin: 10-20 parts, casein sodium: 0.5-
2 parts, oligoisomaltose: 5-10 parts；
The DE value 15-20 of maltodextrin；
(3) emulsifier employed in is compound emulsifying agent: single diglycerine fatty acid ester, gathers single diglycerine fatty acid ester
Fatty acid glyceride, the weight proportion of three kinds of emulsifiers are single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglycerol ester
Fat acid esters=4:3:3.
The condition of emulsification pretreatment is: 6000-7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min
(4) in, the condition of spray drying is: inlet air temperature is 180 DEG C, and leaving air temp is 70~90 DEG C.
It is furthermore preferred that a kind of preparation method of above-mentioned microcapsule powder containing peony seed oil suitable for pregnant woman, including with
Under step:
(1) prepare each raw material by following weight part ratio:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil are taken, is uniformly mixed, obtains miscella；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin: 10-20 parts, casein sodium:
0.5-2 parts, oligoisomaltose: 5-10 parts；The above number is parts by weight；
The DE value 15-20 of maltodextrin；
(3) it is added in the miscella in step (1) after emulsifier and integrally shears cream as the wall material in core material, with (2)
Change, homogeneous obtains emulsion；
The condition of emulsification pretreatment is: 6000-7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min.
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester (linolenic acid), is gathered at single diglycerine fatty acid ester (oleic acid)
Fatty acid glyceride, the proportion of three kinds of emulsifiers are single diglycerine fatty acid ester (linolenic acid): single diglycerine fatty acid ester (oil
Acid): polyglyceryl fatty acid ester=4:3:3., dosage is the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
In order to keep above-mentioned microcapsule powder nutrition richer and comprehensive, the present inventor joined centainly in above-mentioned microcapsule powder
The VE and folic acid of ratio, are adapted to pregnant woman；Specific step is as follows:
(1) prepare each raw material by following weight part ratio:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil, are uniformly mixed, obtain miscella by VE0.01-0.07 parts；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin: 10-20 parts, casein sodium:
0.5-2 parts, oligoisomaltose: 5-10 parts, 0.001-0.004 parts of folic acid；The DE value 15-20 of maltodextrin；
(3) it is added in the miscella in step (1) after emulsifier and integrally shears cream as the wall material in core material, with (2)
Change, homogeneous obtains emulsion；
The condition of emulsification pretreatment is: 6000-7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min.
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester, single diglycerine fatty acid ester, polyglyceryl fatty acid ester,
The proportion of three kinds of emulsifiers is single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglyceryl fatty acid ester=4:3:3,
Dosage is the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
In order to overcome microcapsule powder smelling of fish as brought by fish oil and algae oil, the present inventor's addition when preparing microcapsule powder
The substance of the smelling of fish can be eliminated, and the substance added has no adverse effects for pregnant woman's either breast feeding women body, specifically
The preparation method is as follows:
(1) prepare each raw material by following weight part ratio:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil, are uniformly mixed, obtain miscella by VE0.01-0.07 parts；
Extractive of perilla, Flos Sophorae extract, bamboo extractive are added in miscella, obtains mixture, additional amount difference
Are as follows:
Extractive of perilla accounts for the 0.2~0.6% of edible oil gross weight；
Flos Sophorae extract accounts for the 0.3~0.5% of edible oil gross weight；
Bamboo extractive accounts for the 0.2~0.5% of edible oil gross weight；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin: 10-20 parts, casein sodium:
0.5-2 parts, oligoisomaltose: 5-10 parts,；The DE value 15-20 of maltodextrin；
(3) it is added in the mixture in step (1) after emulsifier and integrally shears cream as the wall material in core material, with (2)
Change, homogeneous obtains emulsion；
The condition of emulsification pretreatment is: 6000-7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester, single diglycerine fatty acid ester, polyglyceryl fatty acid ester,
The proportion of three kinds of emulsifiers is single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglyceryl fatty acid ester=4:3:3,
Dosage is the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
It is furthermore preferred that being suitable for the preparation method of the microcapsule powder containing peony seed oil of pregnant woman, include the following steps:
(1) prepare each raw material by following weight part ratio:
18 parts of peony seed oil, 4 parts of algae oil, 1.5 parts of fish oil, are uniformly mixed, obtain miscella by VE0.01-0.07 parts；
Extractive of perilla, Flos Sophorae extract, bamboo extractive are added in miscella, obtains mixture, additional amount difference
Are as follows:
Extractive of perilla accounts for the 0.3% of edible oil gross weight；
Flos Sophorae extract accounts for the 0.4% of edible oil gross weight；
Bamboo extractive accounts for the 0.3% of edible oil gross weight；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin: 15 parts, casein sodium: 1 part,
Oligoisomaltose: 8 parts；The DE value 18 of maltodextrin；
(3) emulsifier is added in the mixture in step (1) as the wall material emulsification pretreatment in core material, with (2),
Matter obtains emulsion；
The condition of emulsification pretreatment is: 6500r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure 20MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester, single diglycerine fatty acid ester, polyglyceryl fatty acid ester,
The proportion of three kinds of emulsifiers is single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglyceryl fatty acid ester=4:3:3,
Dosage is the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
The beneficial effects of the present invention are the present invention is handled by microencapsulation, by peony seed oil, fish oil and algae oil three's phase
In conjunction with providing the nutriments such as the alpha-linolenic acid for meeting dietary standard, DHA, EPA for pregnant woman and fetus；In addition, of the invention
The form of product is prepared into microcapsule powder, is avoided since fish oil and the smelling of fish of algae oil are to mouth not pleasant brought by pregnant woman
Sense, increases acceptable degree.
Detailed description of the invention
Fig. 1 is the outside drawing in kind of the microcapsule powder of the embodiment of the present invention 1；
Fig. 2 is the stereotome after the brewing of microcapsule powder of the embodiment of the present invention 1；
Fig. 3 is the top view after the brewing of microcapsule powder of the embodiment of the present invention 1；
Fig. 4 is the photo of raw material peony seed oil of the invention；
Fig. 5 is the photo of raw material fish oil of the invention；
Fig. 6 is the photo of raw material algae oil of the invention.
Specific embodiment
Next with reference to the accompanying drawings and detailed description the present invention will be further explained, so as to the technology of this field
Personnel know more about the present invention, but do not limit the present invention with this.
Manufacturer: Tian Bao tree peony Biotechnology Co., Ltd
Peony seed oil: Yao and Shun tree peony Biotechnology Co., Ltd；
Algae oil: the Qingdao source Hai Zhi Life Science Co., Ltd；
Fish oil: the Qingdao source Hai Zhi Life Science Co., Ltd；
Wall material: Heze Big Tree Bioengineering Technology Co., Ltd.；
Emulsifier: Liaoning Ke Hai Food Chemistry Engineering Co., Ltd；
Embodiment 1
The preparation method of the microcapsule powder containing peony seed oil suitable for second trimester (pregnant 4-7 months) pregnant woman, including it is following
The step of:
(1) prepare each raw material by following weight part ratio:
18 kilograms of peony seed oil, 4 kilograms of algae oil, 1.5 kilograms of fish oil, are uniformly mixed, obtain miscella by VE0.04 kilograms；
It is about 0.072 kilogram that extractive of perilla is added in miscella；Flos Sophorae extract is about 0.09 kilogram；The leaf of bamboo extracts
Object is about 0.08 kilogram, obtains mixture；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: 22.2 kilograms of maltodextrin (its DE value 18), junket
Protein acid sodium: 1.5 kilograms, oligoisomaltose: 11.8 kilograms；The dosage of distilled water is 284 kilograms.
(3) it is added in the mixture in step (1) after emulsifier and integrally shears cream as the wall material in core material, with (2)
Change, homogeneous obtains emulsion；
The condition of emulsification pretreatment is: 6500r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure 20MPa, homogeneous 10min；
The weight ratio of wall material and core material is about 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester (linolenic acid), is gathered at single diglycerine fatty acid ester (oleic acid)
Fatty acid glyceride, the proportion of three kinds of emulsifiers are single diglycerine fatty acid ester (linolenic acid): single diglycerine fatty acid ester (oil
Acid): polyglyceryl fatty acid ester=4:3:3, dosage are the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.The condition of spray drying is: inlet air temperature
It is 180 DEG C, leaving air temp is 70~90 DEG C.
Embodiment 2
The targeted object of the present embodiment is the pregnant woman of pregnant early stage, i.e. the pregnant woman of pregnancy 1-3 months；The present embodiment is provided
The microcapsule powder containing peony seed oil for being applicable in pregnant early stage pregnant woman, preparation method is as follows:
(1) prepare each raw material by following weight part ratio:
18 kilograms of peony seed oil, 4 kilograms of algae oil, 1.5 kilograms of fish oil, are uniformly mixed, obtain miscella by VE0.05 kilograms；
It is about 0.075 kilogram that extractive of perilla is added in miscella；Flos Sophorae extract is about 0.095 kilogram；The leaf of bamboo mentions
Taking object is about 0.065 kilogram, obtains mixture；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: 22.2 kilograms of maltodextrin (its DE value 18), junket
Protein acid sodium: 1.5 kilograms, oligoisomaltose: 11.8 kilograms, 0.004 kilogram of folic acid is then added；The dosage of distilled water is
285 kilograms.
(3) it is added in the miscella in step (1) after emulsifier and integrally shears cream as the wall material in core material, with (2)
Change, homogeneous obtains emulsion；
The condition of emulsification pretreatment is: 6500r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure 20MPa, homogeneous 10min；
The weight ratio of wall material and core material is about 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester (linolenic acid), is gathered at single diglycerine fatty acid ester (oleic acid)
Fatty acid glyceride, the proportion of three kinds of emulsifiers are single diglycerine fatty acid ester (linolenic acid): single diglycerine fatty acid ester (oil
Acid): polyglyceryl fatty acid ester=4:3:3, dosage are the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder；The condition of spray drying is: inlet air temperature
It is 180 DEG C, leaving air temp is 70~90 DEG C.
Embodiment 3
The targeted object of the present embodiment is the pregnant woman in pregnant advanced stage, i.e., the pregnant woman of pregnant 28 weeks~childbirth phase；The present embodiment institute
The edible microcapsule powder containing peony seed oil of the applicable iii trimester pregnancies provided, preparation method are as follows:
(1) prepare each raw material by following weight part ratio:
20 parts of peony seed oil, 4 parts of algae oil, 2 parts, VE0.07 kilograms of fish oil are uniformly mixed, obtain miscella；
0.078 kilogram of extractive of perilla, 0.1 kilogram of Flos Sophorae extract, 0.085 bamboo extractive are added in miscella,
Obtain mixture；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin (DE value 15-20): 24.5 kilograms,
Casein sodium: 1.66 kilograms, oligoisomaltose: 13 kilograms；The dosage of distilled water is 156.6 kilograms.
(3) it is added in the mixture in step (1) after emulsifier and integrally shears cream as the wall material in core material, with (2)
Change, homogeneous obtains emulsion；
The condition of emulsification pretreatment is: 7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester (linolenic acid), is gathered at single diglycerine fatty acid ester (oleic acid)
Fatty acid glyceride, the proportion of three kinds of emulsifiers are single diglycerine fatty acid ester (linolenic acid): single diglycerine fatty acid ester (oil
Acid): polyglyceryl fatty acid ester=4:3:3, dosage are the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.The condition of spray drying is: inlet air temperature
It is 180 DEG C, leaving air temp is 70~90 DEG C.
Comparative experiments:
The present inventor did following comparative experiments when selecting adjunct ingredient:
Comparative example 1
(1) prepare each raw material by following weight part ratio:
18 kilograms of peony seed oil, 4 kilograms of algae oil, 1.5 kilograms of fish oil, are uniformly mixed, obtain miscella by VE0.05 kilograms；
Comparative example 2
It is with the difference of embodiment 1, be simply added into a Plant Extracts, remaining is same as Example 1；
Extractive of perilla, additional amount are added in miscella are as follows: 0.242 kilogram；
Comparative example 3
It is with the difference of comparative example 2, plant extracts is replaced with into Flos Sophorae extract, additional amount are as follows: 0.242 thousand
Gram；
Comparative example 4
It is with the difference of comparative example 2, plant extracts is replaced with into bamboo extractive, additional amount are as follows: 0.242 thousand
Gram；
Comparative example 5
It is with the difference of embodiment 1, extractive of perilla, Flos Sophorae extract, additional amount is added in miscella are as follows: is purple
0.112 kilogram of extract of Soviet Union；0.13 kilogram of Flos Sophorae extract；Remaining is identical with embodiment 1；
Comparative example 6
It is with the difference of embodiment 1, Flos Sophorae extract, bamboo extractive, additional amount are as follows: Chinese scholartree is added in miscella
0.126 kilogram of flower extract；0.116 kilogram of bamboo extractive；Remaining is identical with embodiment 1.
Comparative example 7
It is with the difference of embodiment 1, extractive of perilla and bamboo extractive, additional amount is added in miscella are as follows:
0.117 kilogram of extractive of perilla, 0.125 kilogram of bamboo extractive；Remaining is identical with embodiment 1；
About the product in embodiment 1-3 and comparative example 1-7, the present inventor has made following test experience:
Peroxide value is measured according to GB/T 5538-2005, specific as follows:
Products material is detected and (has chosen three kinds of main substances with bad smell) by high performance liquid chromatography,
Data are as follows:
Main fishy smell content of material testing result table in 1 embodiment of table and comparative example
It can be seen that by the data in above table and any plant extracts be not added in comparative example 1, fishy smell is still
It is denseer, and anti-oxidant value is higher, and it is more significant that this illustrates that plant extracts of the present invention plays removal fishy smell
Effect, in addition plant extracts of the present invention also plays the inoxidizability of microcapsule powder in the work of highly significant
With.
As can be seen that single plant extracts from comparative example 2-4, for removal fishy smell or it is anti-oxidant have it is certain
Effect, but its general effect is not so good as embodiment 1-3；This is because extractive of perilla, Flos Sophorae extract in the present invention,
Bamboo extractive all has oxidation resistant effect, and extractive of perilla and Flos Sophorae extract for deodorization effect than more significant；
The principle of the two deodorization is: fish oil easily aoxidizes during having storage, the carbonization that omega-3 unsaturated fatty acid autoxidation generates
The fishy smell ingredient such as object, such as 2,4- decadienal, 2,4, the 7- last of the ten Heavenly stems, three olefine aldehydr etc., during fish oil storage, microorganism or enzyme
Effect or lipid autoxidation will also result in the corruption of fish oil, and also contain trimethylamine oxide in fish oil, which can be micro-
Degradation generates trimethylamine under the collective effect of biology and enzyme and dimethylamine, pure trimethylamine only have ammonia taste, many fresh
In fish and it is not present, but but content is higher in the fish oil of storage, pure trimethylamine is during storage by microorganism
Or the effect of enzyme either fish oil lipid autoxidation, it is coexisted with δ -2 aminovaleric acid, hexahydropyridine etc. and produces stronger raw meat
The olfactory of taste.
Therefore, present invention adds plant extracts, extractive of perilla, Flos Sophorae extract and bamboo extractive, three's
Inoxidizability is relatively strong, considerably beyond antioxidants such as VC, prevents fish oil from aoxidizing during storage and generates fishy smell ingredient, than
The carbide generated such as omega-3 unsaturated fatty acid autoxidation；One obvious action of extractive of perilla and bamboo extractive
It is that there is antibacterial effect, bamboo extractive can inhibit fish oil to generate microorganism during storage, prevent three in fish oil
Methylamine is coexisted with δ -2 aminovaleric acid, hexahydropyridine etc. and generates the strong smelling of fish by microbial action；To reach inhibition
The purpose of the smelling of fish, meanwhile, extractive of perilla, Flos Sophorae extract itself contain aroma substance, can cover or cover fishlike smell
Youngster, therefore the addition of these three plant extracts have good effect for the removal of fishlike smell；
In addition the extractive of perilla that the present invention is added, highly-safe, purple perilla is a kind of two kinds of medicine food of raw material,
Body has the function of miscarriage prevention, and extract is also safe from harm for pregnant woman；Flos Sophorae extract, highly-safe, inoxidizability is strong,
And it acts synergistically with extractive of perilla, can remove the smelling of fish in microcapsule powder.Although being equally plant extracts, peppermint is mentioned
Take object that can also play the role of a degree of deodorization, but mint extract is not suitable for pregnant woman, with Robust speaker feature
Effect, therefore not any plant extracts is adapted to pregnant woman.It is primarily to examine safely when selecting plant extracts
The factor of worry, followed by remove the effect of fishy smell；Materials safety of the present invention is all higher, and its dosage is very
It is few, undesirable effect will not be generated to the body of pregnant woman.
From can be seen that three Plant Extracts used in the present invention in comparative example 5-7, there is synergistic effect, when three
When person combines, deodorization effect and antioxidant effect will be significantly better than the combinations of two Plant Extracts of identical additive amount.
Embodiment 4
The quality of the microcapsule powder obtained in embodiment 1-3, present inventor has performed following inspections:
(1) quality evaluation
A. sense organ
The sensory properties such as color, smell, structural state with subjective appreciation method evaluation powdered oil.
B. physicochemical character
To the moisture content of powdered oil, density, solubility, stocking angle, oil content, surface oil content, embedding efficiency, partial size
The physical and chemical indexes such as distribution are analyzed.
C. microstructure
Sample is sprinkling upon on the sample stage for posting double-sided adhesive, excessive powder is blown away, is sprayed with ion sputtering device in sample surfaces
Bronze is applied, with the microstructure of scanning electron microscope observation product.Acceleration voltage is 1KV, and amplification factor is 300~1000
Times.
D. emulsion is restored
25g powdered oil product is weighed in 250mL beaker, 70~80 DEG C of temperature of hot water 200mL is added, stirs, fill
Dissolution, dispersion, observation is divided to restore emulsion dissolution situation, color, if uniformly；Surface whether there is or not conjunctiva, layering, whether there is or not particle extensions
Wall；Analyze the size distribution of emulsion.
(2) storage stability is evaluated
DEG C a.20 stored at
Powdered oil sealing is put in constant incubator, 20 DEG C of the temperature inside the box.In 6 months Storage periods, with certain
Time interval, detect the surface oil content of powdered oil, embedding efficiency, the granularity for restoring emulsion, and to wherein grease
Acid value, peroxide value and fatty acid composition are detected.
B. accelerate storage test
Acceleration storage test is carried out in 60 DEG C of baking oven, and powdered oil and core material grease are stored in 60 DEG C of baking oven
30 days.The Oxidative Stability Index OSI and peroxide value of grease are measured respectively.
C. forecasting shelf life
Powdered oil is stored at 20 DEG C, 40 DEG C, 50 DEG C and 60 DEG C respectively, measures the mistake of sample under each storage temperature
Oxidation number predicts the shelf life of product.
(3) index analysis
A. the fusing point of oil sample
Slip point is measured using open capillary method.Melt after oil sample is completely dried, takes at least 3 capillaries
It immerses in sample, grease is made to be raised to 10mm eminence, cool down sample at once until solidification.16h is placed in 4~10 DEG C of refrigerator
Afterwards, it takes out capillary to be fixed on it on thermometer with rubber band, and low side is made to be parallel to mercury.Thermometer is hung over and is equipped with
In the beaker of clean distilled water, below the low side immersed in liquid level of thermometer.The initial temperature of water-bath is adjusted, slip point 8 is lower than
~10 DEG C, agitation water-bath makes 1 DEG C/min of warming-in-water, is down to 0.5 DEG C/min when close to melting temperature.It is continuously heating to fatty column
Rise, observes temperature when each fatty column rises, and calculate average value.
B. the emulsion stability of emulsion
By emulsion in 60 DEG C of waters bath with thermostatic control constant temperature 30min, by centrifuge tube be put into centrifuge centrifugation 15min (4500r/
min).Observation delamination is taken out, liquid total height (H) and non-layer height (H1) is recorded.The cream is calculated according to following equation
The stability value of shape liquid；
C. the oil content of powdered oil
Using chloroform-methanol extraction method.3g sample (m) is taken, the dissolution of 12mL water is added.15mL chloroform and 30mL first is added
Alcohol mixes；15mL chloroform and 15mL distilled water are added, 30s is mixed.Above-mentioned solution is transferred in centrifuge tube, 3000r/
Min is centrifuged 10min.Lower layer chloroformic solution 10mL is pipetted in the round-bottomed flask (m1) of constant weight with pipette, rotary evaporation removal
Chloroform weighs (m2) after drying constant weight.The formula of oil content is as follows:
D. the surface oil content of powdered oil, embedding efficiency (MEE)
Accurately weighing quality (m) is 2~3g sample in triangular flask, with 30~60 DEG C of petroleum ethers of 40mL in gentle agitation
Lower accurate extraction 1min, is filtered with G3 sand core funnel immediately, with 25mL petroleum ether filter residue 40s, is filtered immediately, recycle filtrate
In petroleum ether, the quality (m1) of 65 DEG C of drying to constant weight surface greases；Gauging surface oil content and embedding efficiency；
E. grain size analysis: the partial size of emulsion carries out wet process measurement, the partial size of powdered oil particle using laser particle analyzer
It is measured using dry method
F. moisture content: referring to GB5497-1985 method, 105 DEG C of 2~3h of drying, constant weight weighing
G. density: powdered oil is poured into graduated cylinder with a scale, the weight of unit of account volume powdered oil
H. powdered oil solubility: sample being dissolved in 25~30 DEG C of water, is centrifuged, and sediment quality is measured, and is calculated
The solubility of powdered oil out
I. stocking angle: the angle of a certain amount of products measure natural packing is taken
J. fatty acid forms: fatty acid compositional analysis bibliography
K. Oxidative Stability Index OSI: according to GB/T 21121-2007
L. peroxide value: according to GB/T5538-2005
M. acid value: according to GB/T5530-2005.
(4) analysis of fatty acid composition
Using gas chromatograph for determination:
Chromatographic condition:
Chromatographic column: filler is the capillary column of cyanogen propyl aryl polysiloxane, column length 100m, internal diameter 0.25mm, film thickness 0.2
μm；Or the chromatographic column of equal performance.
Flame ionization ditector (FID), 300 DEG C of detector temperature, 250 DEG C of injector temperature, carrier gas, split ratio
10:1,1.0 μ L of sample volume, temperature programming condition are as follows:
2 temperature programming condition of table
| Heating rate (DEG C/min) | Temperature (DEG C) | Retention time (min) |
| - | 120 | 0 |
| 10 | 175 | 10 |
| 5 | 210 | 5 |
| 5 | 230 | 5 |
As can be seen from the above table, the fatty acid composition and feedstock oil basic one of peony seed oil solid for mulation functional food
It causes, unsaturated fatty acid content is 90%
Product characteristic table in 3 embodiment 1-3 of table
More than, alpha-linolenic acid, the content embedding front and back of DHA, EPA are almost the same, under the conditions of illustrating this drying process with atomizing,
Fatty acid composition is not destroyed in crude oil, and technological parameter is reasonable.
Product fatty acid analysis in 4 example 1-3 of table
By the analysis of data in above table and compare, it can be deduced that conclusion, microcapsule powder in the present invention its advantage is that:
Attached drawing 4-6 is the picture of raw material of the invention, and product of the invention is relative to raw material edible oil, its advantage is that another without pregnant woman
One eats or drinks various nutrition oil products, it is thus only necessary to which brewing a packet or one glass of microcapsule powder of the invention can be obtained needed for diet
Alpha-linolenic acid, the nutriments such as DHA, EPA, this brings great convenience to the edible of pregnant woman；And the present invention also solves
As fish oil and algae oil to brought by pregnant woman cannot happiness receive the problem of, the present invention is added that auxiliary material raw material --- plant mentions
Object is taken, effective antioxidation can be played to microcapsule powder, and the smelling of fish can also be removed, make the receiving of pregnant woman's pleasure.
Embodiment 5
The targeted object of the present embodiment is the pregnant woman in pregnant advanced stage, i.e., pregnant 5 weeks~30 weeks pregnant woman；The present embodiment is provided
The edible microcapsule powder containing peony seed oil of applicable iii trimester pregnancies, preparation method is as follows:
(1) prepare each raw material by following weight part ratio:
20 parts of peony seed oil, 4 parts of algae oil, 2 parts, VE0.07 kilograms of fish oil are uniformly mixed, obtain miscella；
0.078 kilogram of extractive of perilla, 0.1 kilogram of Flos Sophorae extract, 0.085 bamboo extractive are added in miscella,
Obtain mixture；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin (DE value 15-20): 24.5 kilograms,
Casein sodium: 1.66 kilograms, oligoisomaltose: 13 kilograms；The dosage of distilled water is 156.6 kilograms.
(3) it is added in the mixture in step (1) after emulsifier and integrally shears cream as the wall material in core material, with (2)
Change, homogeneous obtains emulsion；Folic acid is added in emulsion: 0.001-0.004 kilograms, calcium gluconate: 1-3 kilograms, glucose
It is sour ferrous: 0.02-0.1 kilograms, vitamin A: 0.3/ ten thousand, vitamine D3: 0.002/ ten thousand, vitamin B12: 0.15/ ten thousand；
The condition of emulsification pretreatment is: 7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester (linolenic acid), is gathered at single diglycerine fatty acid ester (oleic acid)
Fatty acid glyceride, the proportion of three kinds of emulsifiers are single diglycerine fatty acid ester (linolenic acid): single diglycerine fatty acid ester (oil
Acid): polyglyceryl fatty acid ester=4:3:3, dosage are the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.The condition of spray drying is: inlet air temperature
It is 180 DEG C, leaving air temp is 80 DEG C.
Claims (9)
1. a kind of microcapsule powder containing peony seed oil suitable for pregnant woman, which is characterized in that the microcapsule powder mainly includes edible oil；
Edible oil is made of the raw material of following parts by weight:
Peony seed oil: 10-25 parts；Algae oil: 0.5-2.5 parts；Fish oil: 1-2 parts.
2. a kind of microcapsule powder containing peony seed oil suitable for pregnant woman as described in claim 1, which is characterized in that the micro-capsule
Powder further includes the auxiliary material raw material of following parts by weight: extractive of perilla, Flos Sophorae extract, bamboo extractive；
Extractive of perilla accounts for the 0.2~0.6% of edible oil gross weight；
Flos Sophorae extract accounts for the 0.3-0.5% of edible oil gross weight；
Bamboo extractive accounts for the 0.2-0.5% of edible oil gross weight.
3. a kind of preparation method of the microcapsule powder containing peony seed oil suitable for pregnant woman as described in claim 1, including with
Under step:
(1) prepare each raw material by following weight part ratio:
Peony seed oil, algae oil, fish oil are taken, is uniformly mixed, obtains miscella；
(2) distilled water is added in wall material, is dissolved at 50-70 DEG C；
(3) compound emulsifying agent is added in miscella in (1), then is mixed with the wall material in (2), emulsification pretreatment, homogeneous,
Obtain emulsion；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
4. a kind of microcapsule powder containing peony seed oil suitable for pregnant woman as described in claim 1, it is characterised in that:
(2) wall material employed in specifically: maltodextrin: 10-20 parts, casein sodium: 0.5-2 parts, oligoisomaltose:
5-10 parts；
The DE value 15-20 of maltodextrin；
(3) emulsifier employed in is compound emulsifying agent: single diglycerine fatty acid ester, single diglycerine fatty acid ester, polyglycereol
Aliphatic ester, the weight proportion of three kinds of emulsifiers are single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglycerol fatty acid
Ester=4:3:3；
The condition of emulsification pretreatment is: 6000-7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min；
(4) in, the condition of spray drying is: inlet air temperature is 180 oC, and leaving air temp is 70 ~ 90 oC.
5. a kind of preparation method of the microcapsule powder containing peony seed oil suitable for pregnant woman as described in claim 1, including with
Under step:
(1) prepare each raw material by following weight part ratio:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil are taken, is uniformly mixed, obtains miscella；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin: 10-20 parts, casein sodium: 0.5-
2 parts, oligoisomaltose: 5-10 parts；The above number is parts by weight；
The DE value 15-20 of maltodextrin；
(3) it is added in miscella in step (1) integrally as the wall material emulsification pretreatment in core material, with (2) after emulsifier,
Matter obtains emulsion；
The condition of emulsification pretreatment is: 6000-7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester, single diglycerine fatty acid ester, polyglyceryl fatty acid ester, three kinds
The proportion of emulsifier is single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglyceryl fatty acid ester=4:3:3, dosage are
The 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
6. a kind of preparation method of the microcapsule powder containing peony seed oil suitable for pregnant woman as described in claim 1, including with
Under step:
(1) prepare each raw material by following weight part ratio:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil, are uniformly mixed, obtain miscella by VE0.01-0.07 parts；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin: 10-20 parts, casein sodium: 0.5-2
Part, oligoisomaltose: 5-10 parts, folic acid: 0.001-0.004 parts；The DE value 15-20 of maltodextrin；
(3) it is added in miscella in step (1) integrally as the wall material emulsification pretreatment in core material, with (2) after emulsifier,
Matter obtains emulsion；
The condition of emulsification pretreatment is: 6000-7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester, single diglycerine fatty acid ester, polyglyceryl fatty acid ester, three kinds
The proportion of emulsifier is single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglyceryl fatty acid ester=4:3:3, dosage are
The 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
7. a kind of preparation method of the microcapsule powder containing peony seed oil suitable for pregnant woman as described in claim 1, including with
Under step:
(1) prepare each raw material by following weight part ratio:
15-20 parts of peony seed oil, 1-5 parts of algae oil, 1-2 parts of fish oil, are uniformly mixed, obtain miscella by VE0.01-0.07 parts；
Extractive of perilla, Flos Sophorae extract, bamboo extractive are added in miscella, obtains mixture, additional amount is respectively as follows:
Extractive of perilla accounts for the 0.2~0.6% of edible oil gross weight；
Flos Sophorae extract accounts for the 0.3~0.5% of edible oil gross weight；
Bamboo extractive accounts for the 0.2~0.5% of edible oil gross weight；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin: 10-20 parts, casein sodium: 0.5-
2 parts, oligoisomaltose: 5-10 parts,；The DE value 15-20 of maltodextrin；
(3) it is added in mixture in step (1) integrally as the wall material emulsification pretreatment in core material, with (2) after emulsifier,
Matter obtains emulsion；
The condition of emulsification pretreatment is: 6000-7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester, single diglycerine fatty acid ester, polyglyceryl fatty acid ester, three kinds
The proportion of emulsifier is single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglyceryl fatty acid ester=4:3:3, dosage are
The 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
8. a kind of preparation method of the microcapsule powder containing peony seed oil suitable for pregnant woman as described in claim 1, including with
Under step:
(1) prepare each raw material by following weight part ratio:
18 parts of peony seed oil, 4 parts of algae oil, 1.5 parts of fish oil, are uniformly mixed, obtain miscella by VE0.01-0.07 parts；
Extractive of perilla, Flos Sophorae extract, bamboo extractive are added in miscella, obtains mixture, additional amount is respectively as follows:
Extractive of perilla accounts for the 0.3% of edible oil gross weight；
Flos Sophorae extract accounts for the 0.4% of edible oil gross weight；
Bamboo extractive accounts for the 0.3% of edible oil gross weight；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin: 15 parts, casein sodium: 1 part, low
Polyisomaltose: 8 parts；The DE value 18 of maltodextrin；
(3) it is added in mixture in step (1) integrally as the wall material emulsification pretreatment in core material, with (2) after emulsifier,
Matter obtains emulsion；
The condition of emulsification pretreatment is: 6500r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure 20MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester, single diglycerine fatty acid ester, polyglyceryl fatty acid ester, three kinds
The proportion of emulsifier is single diglycerine fatty acid ester: single diglycerine fatty acid ester: polyglyceryl fatty acid ester=4:3:3, dosage are
The 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder.
9. a kind of preparation method of the microcapsule powder containing peony seed oil suitable for pregnant woman as described in claim 1, including with
Under step: (1) prepare each raw material by following weight part ratio:
20 parts of peony seed oil, 4 parts of algae oil, 2 parts, VE0.07 kilograms of fish oil are uniformly mixed, obtain miscella；
0.078 kilogram of extractive of perilla, 0.1 kilogram of Flos Sophorae extract, 0.085 bamboo extractive are added in miscella, obtains mixed
Close object；
(2) distilled water is added in wall material, is dissolved at 60 DEG C；Wall material are as follows: maltodextrin (DE value 15-20): 24.5 kilograms, junket
Protein acid sodium: 1.66 kilograms, oligoisomaltose: 13 kilograms；
(3) it is added in mixture in step (1) integrally as the wall material emulsification pretreatment in core material, with (2) after emulsifier,
Matter obtains emulsion；Folic acid is added in emulsion: 0.001-0.004 kilograms, calcium gluconate: 1-3 kilograms, gluconic acid Asia
Iron: 0.02-0.1 kilograms, vitamin A: 0.3/ ten thousand, vitamine D3: 0.002/ ten thousand, vitamin B12: 0.15/ ten thousand；
The condition of emulsification pretreatment is: 7000r/min high speed shearing emulsification 15 minutes；
The condition of homogeneous is: homogenization pressure is 10~25MPa, homogeneous 10min；
The weight ratio of wall material and core material is 3:2；
Emulsifier is compound emulsifying agent: single diglycerine fatty acid ester (linolenic acid), single diglycerine fatty acid ester (oleic acid), polyglycereol
Aliphatic ester, the proportion of three kinds of emulsifiers are single diglycerine fatty acid ester (linolenic acid): single diglycerine fatty acid ester (oleic acid): poly-
Fatty acid glyceride=4:3:3, dosage are the 0.3% of the sum of wall material and core material weight；
(4) it is spray-dried, then by fluidized bed prilling, obtains finished product microcapsule powder；
The condition of spray drying is: inlet air temperature is 180 oC, and leaving air temp is 80 oC.
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| CN114468298A (en) * | 2022-02-10 | 2022-05-13 | 山东四季园牡丹生物科技有限公司 | Peony seed oil microcapsule and preparation method thereof |
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Denomination of invention: Microcapsulated powder containing peony seed oil suitable for pregnant women and its preparation method Effective date of registration: 20221104 Granted publication date: 20211214 Pledgee: Heze rural commercial bank Limited by Share Ltd. Pledgor: TIANBAO MUDAN BIOTECHNOLOGY Co.,Ltd. Registration number: Y2022980020832 |