CN109430426A - A kind of nutrient solution containing peony seed oil suitable for pregnant woman - Google Patents
A kind of nutrient solution containing peony seed oil suitable for pregnant woman Download PDFInfo
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- CN109430426A CN109430426A CN201811290029.2A CN201811290029A CN109430426A CN 109430426 A CN109430426 A CN 109430426A CN 201811290029 A CN201811290029 A CN 201811290029A CN 109430426 A CN109430426 A CN 109430426A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
- A23D7/005—Edible oil or fat compositions containing an aqueous phase, e.g. margarines characterised by ingredients other than fatty acid triglycerides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
- A23D7/02—Edible oil or fat compositions containing an aqueous phase, e.g. margarines characterised by the production or working-up
- A23D7/04—Working-up
Abstract
The invention belongs to edible oil processing technique fields, and in particular to a kind of nutrient solution containing peony seed oil suitable for pregnant woman.The nutrient solution is, using plant extracts as auxiliary material, by mixing, smashing to pieces at a high speed, emulsify, be ultrasonically treated, homogeneous, to cross colloid mill, second homogenate, sterilizing using peony seed oil, algae oil, fish oil as major ingredient, filling obtained.Nutrient solution of the invention, peony seed oil, fish oil and algae oil three are combined, and provide the nutriments such as the alpha-linolenic acid for meeting dietary standard, DHA, EPA for pregnant woman and fetus；In addition, the form of product is prepared into nutrient solution by the present invention, smelling of fish when directly taking orally fish oil, algae oil is avoided to mouthfeel not pleasant brought by pregnant woman, increases the acceptable degree of pregnant woman.
Description
Technical field
Invention belongs to edible oil processing technique field, and in particular to a kind of nutrition containing peony seed oil suitable for pregnant woman
Liquid.
Background technique
Gestation is a complicated physiology course, for the success of gestation, the physiological status and organism metabolism of pregnant women
Biggish adaptive change has occurred, to meet the growth and development of pregnancy period maternal genital official and fetus, and for postpartum milk secretion into
Support deposit in field headquarters.The superiority and inferiority of maternal weight gain situation is to embryo growth and development until the health after adult will generate vital shadow
It rings, compared with non-pregnant women, pregnant women increased the requirement of energy and various nutrients, especially albumen
The lot of trace nutrient such as matter, essential fatty acid and calcium, iron, folic acid, vitamin A.
Since the rate of development of pregnancy different times embryo is obstructed, the physiological status of pregnant woman, metabolic alterations of body and right
The demand of nutrient is also different.By the physiology course and nutritional need feature of gestation, diet for pregnant woman guide is divided into pregnant early period (before pregnant
3 months~6 months), pregnant early stage (pregnant 1 week~12 weeks) and it is pregnant in (pregnant 13 weeks~27 weeks), latter stage (pregnant 28 weeks~childbirth) three
Point.
Since second trimester, fetus enters the fast-growth puberty, until childbirth.From pregnant 20 weeks, fetal brain cell division
Accelerate to accelerate, is the critical period of fetal brain and retinal development, as brain cell and retina cell's structure and function ingredient
Phosphatide requirement increase, and long-chain polyunsaturated fatty acid, that is, omega-fatty acid on phosphatide is then particularly important.It is modern
Life science confirms that pregnant woman then passes through milk for the alpha-linolenic acid of intake and metabolin DHA and EPA by placenta, puerpera
Send fetus or baby to.Therefore, in the cranial nerve that this period is pregnant, puerpera takes in enough alpha-linolenic acids, fetus or baby
Cell and optic cell are developed, number is more, function is strong.Alpha-linolenic acid can also promote tire, babies function and body hair
It educates, especially to hypogenetic fetus and premature, their physiogeny can be promoted to reach normal level.World health group
Knit (WHO) suggestion: the gestational period, lactating female must take in enough alpha-linolenic acids.If lacking alpha-linolenic acid in pregnant and lying-in women's body,
So baby's there will be brain growths slow, intellectual impairment, body development slowly, have defective vision, the symptoms such as pachylosis.
It is proposed in 2013 editions " Dietary Reference Intakes of Chinese Residents quick checking handbook ", pregnant woman, wet nurse's alpha-linolenic acid
Suitable intake (AI) be the 0.60% of energy, and the daily ingestion of energy of pregnant woman is 2700kcal/d, it is proposed that pregnant and lying-in women day mend
Filling alpha-linolenic acid 1800mg is advisable, and convert needs 4.5g or so for peony seed oil daily.It is provided in quick checking handbook, the reference of DHA is taken the photograph
Entering amount is 200mg/d, and the Dietary reference intakes of EPA are 50mg/d.Peony seed oil solid formulation functional food (pregnant and lying-in women's formula)
The equal strict implement Chinese residents dietary guidelines of content and " Chinese residents diet nutrient reference of middle alpha-linolenic acid, DHA, EPA
Intake ".
At present it was recognized that edible vegetable oil is more advantageous to health, still, if it is eating single vegetable oil
Also undesirable, nutritional ingredient type and content contained in single oil product is limited after all, and the nutritional ingredient of each vegetable oil is not
Identical to the greatest extent, such as often eating peanut oil can effectively zinc supplementation；It is that a kind of stomach can most be born containing the oleic acid of very high percentage in olive oil
Edible oil, it can be such that grease reduces to reduce the generation of cholecystitis and gall stone；Semen setariae oil unsaturated fatty acid is up to 86%,
Human absorptivity is up to 98% or more, and the content of vitamin E is hypertension, high blood also above other common vegetable oils in oil
Rouge, high cholesterol, coronary heart disease and the ideal edible oil of obese patient；Soybean oil can enhance the immunity of body, increase body
Weight ..., therefore, the collocation of various edible oils are edible more preferably, human body especially pregnant woman various fatty acid obtained and DHA,
The nutritional ingredients such as EPA are more balanced.
For pregnant woman of the early stage especially pregnant for pregnant woman with strong pregnancy reaction (morning sickness is reacted), eats and have fishy smell
The nutriment of youngster, though be conducive to pregnant woman herself's health and development of fetus, but for pregnant woman, the smelling of fish pole of fish oil
It is difficult to receive, and is also easy to cause nausea and vomiting reaction after even eating.
CN102907741A discloses a kind of preparation method of peony seed oil oral solution, it is characterised in that: including walking as follows
It is rapid:
(1) peony seed oil is produced
Peony seeds are collected, and underproof peony seeds are eliminated by the screening of vibrating screen, clear up impurity elimination；Then, with peeling off
Machine shells to tree peony son；Peony seeds after shelling pass through squeezing process, solvent extraction process or CO2 supercritical extract again
Peony seed oil is made in technique；
(2) oral solution is prepared
Oral solution is prepared as major ingredient using the peony seed oil produced；
(3) encapsulating
Prepared peony seed oil oral solution is tested, the peony seed oil for examining qualification is quantified with bottle placer
It is filling, and sealed with sealing machine；
(4) it sterilizes
The peony seed oil oral solution good to encapsulating is absolutely sterilized；
(5) it packs, examine, storage.
Above peony seed oil oral solution is peony seed oil to be directly formulated as to oral solution, and do not carry out the phase such as emulsifying to it
The processing answered, and if peony seed oil is directly edible, mouthfeel is difficult for most crowds and is received；In addition provided by peony seed oil
The nutriments such as nutritional ingredient such as alpha-linolenic acid, α-linoleic acid, ω 3, DHA, EPA are difficult to meet special population pregnant woman body institute
Need, accordingly, it is desirable to provide it is a kind of he or she and foetus can be provided for pregnant woman needed for nutritional ingredient, make alpha-linolenic acid,
α-linoleic acid, ω 3, the nutriments such as DHA, EPA meet dietary standard, and can make the healthy oil product of the receiving of pregnant woman's pleasure.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of by these three masters of peony seed oil, fish oil and algae oil
It wants raw material to combine, and prepares the obtained nutrient solution containing peony seed oil suitable for pregnant woman using specific technique, it should
Nutrient solution is comprehensive the advantages of being conducive to peony seed oil, algae oil and fish oil, and the α-for meeting dietary standard is provided for pregnant woman and fetus
Linolenic acid, α-linoleic acid, ω 3, the nutriments such as DHA, EPA, and also its mouthfeel is good, and no smelling of fish is easy to be received by pregnant woman.
The nutrient solution containing peony seed oil suitable for pregnant woman of the invention be solved by following technical solutions with
On technical problem:
A kind of nutrient solution containing peony seed oil suitable for pregnant woman, the nutrient solution mainly using edible oil as major ingredient with
Other nutritional ingredients prepare gained as auxiliary material；
Edible oil is mainly: peony seed oil: 60~100；DHA algal oil: 8~20；Fish oil: 4~15；
Adjunct ingredient:
Extractive of perilla, Flos Sophorae extract, bamboo extractive；
Extractive of perilla accounts for the 0.01-0.03% of edible oil gross weight；
Flos Sophorae extract accounts for the 0.01-0.03% of edible oil gross weight；
Bamboo extractive accounts for the 0.01-0.02% of edible oil gross weight；
Its preparation process is as follows:
(1) 60~100 parts of peony seed oil, 8~20 parts of DHA algal oil, the mixing of 4~15 parts of fish oil are taken, is then added
Extractive of perilla, Flos Sophorae extract, bamboo extractive are uniformly mixed, obtain mixture A；
(2) mixture A is heated to 80-100 DEG C, is smashed to pieces uniformly in high speed bruisher；
(3) addition 0.1~0.8 part of emulsifier, 400~1200 parts of water in uniform material is smashed to pieces in (2),
0.001-0.005 parts of emulsion adjuvant emulsifies 1~2h in mulser；
(4) 0.01-0.04 parts of stabilizer is added in the material in (3) after emulsification, then carries out ultrasonication；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
(6) it sterilizes, it is filling, obtain nutrient solution.
Preferably, in (2), the revolving speed that high speed bruisher is smashed to pieces is 10000~12000r/min, 10~15min of time；
(3) in, emulsifier is sodium carboxymethylcellulose, monoglyceride, casein sodium；Sodium carboxymethylcellulose, monoglyceride,
The weight ratio of casein sodium is 1~3:2~4:1~5；
Emulsion adjuvant are as follows: algal polysaccharides；
(4) it is 300~500W that the time of ultrasonication, which is 5~10min power, in.
(5) in, the condition by high pressure homogenizer homogeneous is: homogenization pressure is 10~25MPa, homogeneous 15min；It is secondary equal
The condition of matter is: homogenization pressure is 10~25MPa, homogeneous 10min.
Preferably, a kind of preparation method of the nutrient solution containing peony seed oil suitable for pregnant woman, includes the following steps:
(1) 60~100 parts of peony seed oil, 8~20 parts of DHA algal oil, the mixing of 4~15 parts of fish oil are taken, is then added
Extractive of perilla, Flos Sophorae extract, bamboo extractive are uniformly mixed, obtain mixture A；
Extractive of perilla accounts for the 0.01-0.03% of peony seed oil, algae oil and fish oil gross weight；
Flos Sophorae extract accounts for the 0.01-0.03% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.01-0.02% of peony seed oil, algae oil and fish oil gross weight；
(2) mixture A is heated to 80-100 DEG C, is smashed to pieces uniformly in high speed bruisher；
(3) addition 0.1~0.8 part of emulsifier, 400~1200 parts of water in uniform material is smashed to pieces in (2),
0.001-0.005 parts of emulsion adjuvant emulsifies 1~2h in mulser；
(4) 0.01-0.04 parts of stabilizer is added in the material in (3) after emulsification, then carries out ultrasonication；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
(6) it sterilizes, it is filling, obtain nutrient solution.
The condition of sterilizing are as follows: sterilize 15min at 121 DEG C.
As an improvement of the present invention, iron, VA, VD, folic acid, VB can be added in the product12These nutrients, with
It is supplied to needed for pregnant woman's body, a kind of specific preparation method of the nutrient solution containing peony seed oil suitable for pregnant woman, including
Following step:
(1) 60~100 parts of peony seed oil, 8~20 parts of DHA algal oil, the mixing of 4~15 parts of fish oil are taken, is then added
Extractive of perilla, Flos Sophorae extract, bamboo extractive are uniformly mixed, obtain mixture A；
Extractive of perilla accounts for the 0.01-0.03% of peony seed oil, algae oil and fish oil gross weight；
Flos Sophorae extract accounts for the 0.01-0.03% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.01-0.02% of peony seed oil, algae oil and fish oil gross weight；
(2) mixture A is heated to 80-100 DEG C, is smashed to pieces uniformly in high speed bruisher；
(3) addition 0.1~0.8 part of emulsifier, 400~1200 parts of water in uniform material is smashed to pieces in (2),
0.001-0.005 parts of emulsion adjuvant emulsifies 1~2h in mulser；
(4) be added in the material in (3) after emulsification 0.01-0.04 part stabilizer, addition iron, VA, VD, folic acid,
VB12, then carry out ultrasonication；The additional amount of iron is 240mg/L；The additional amount of VA is 2mg/L, and the additional amount of VD is 200
μ g/L, the additional amount of folic acid are 8mg/L；VB12Additional amount is 100 μ g/L, then carries out ultrasonication；Ultrasonication when
Between be 5~10min, power be 300~500W；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
(6) it sterilizes, it is filling, obtain nutrient solution.
The present invention uses high-pressure homogeneous method, enhances the emulsifying activity of miscella, exists convenient for subsequent mixing edible oil
Emulsifier effect is emulsified；
The beneficial effects of the present invention are the present invention is handled by microencapsulation, and peony seed oil, oily three are combined, are
Pregnant woman and fetus provide the alpha-linolenic acid, α-linoleic acid, ω 3 for meeting dietary standard, the nutriments such as DHA, EPA；Separately
Outside, the form of product is prepared into nutrient solution by the present invention, is avoided since fish oil and the smelling of fish of algae oil are to brought by pregnant woman
Not pleasant mouthfeel increases acceptable degree.
Specific embodiment
Next With reference to embodiment the present invention will be further explained, more so as to those skilled in the art
Understand the present invention, but the present invention is not limited with this.
Peony seed oil: Yao and Shun tree peony Biotechnology Co., Ltd；
Algae oil: Qingdao Hai Zhiyuan Life Science Co., Ltd；
Fish oil: Qingdao Hai Zhiyuan Life Science Co., Ltd；
Algal polysaccharides: Xi'an Lv Quan Science and Technology Ltd.；
Extractive of perilla: Xi'an Si Nuote Bioisystech Co., Ltd；
Flos Sophorae extract: Xi'an Si Nuote Bioisystech Co., Ltd；
Bamboo extractive: Xi'an Jin Heng Chemical Co., Ltd.；
Sodium carboxymethylcellulose: Zibo Hailan Chemical Co., Ltd.；
Monoglyceride: Wuhan Lang Shangjia Biotechnology Co., Ltd；
Casein sodium: Henan Qian Feng food additives Co., Ltd
Colloid mill: Shanghai Yi Ken mechanical equipment Co., Ltd；
Homogenizer: Wuxi Yi Kai Autotek S. r. l.；
Mulser: this Machinery Manufacturing Co., Ltd. of tin-free steel；
Colloid mill: Shanghai Yi Ken mechanical equipment Co., Ltd；
Embodiment 1
Production is suitable for the edible nutrient solution containing peony seed oil of second trimester pregnant woman (pregnant 4-7 months), specific preparation side
Method is as follows:
(1) take 80 parts of peony seed oil, 15 parts of DHA algal oil, 12 parts fish oil mixing, then be added extractive of perilla,
Flos Sophorae extract, bamboo extractive are uniformly mixed, obtain mixture A；
Extractive of perilla accounts for the 0.02% of peony seed oil, algae oil and fish oil gross weight；
Flos Sophorae extract accounts for the 0.02% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.015% of peony seed oil, algae oil and fish oil gross weight；
(2) mixture A is heated to 90 DEG C or so, is smashed to pieces uniformly in high speed bruisher；The revolving speed that high speed bruisher is smashed to pieces
It is 12000r/min, time 10min；
(3) addition 0.2 part of emulsifier, 800 parts of water, 0.003 part of emulsification in uniform material is smashed to pieces in (2) to help
Agent emulsifies 1.5h in mulser；
Emulsifier is sodium carboxymethylcellulose, monoglyceride, casein sodium；Sodium carboxymethylcellulose, monoglyceride, casein
The weight ratio of sour sodium is 2:3:4；
Emulsion adjuvant are as follows: algal polysaccharides；
(4) 0.02 part of stabilizer is added in the material in (3) after emulsification, iron, VA, VD, folic acid, VB is added12, so
After carry out ultrasonication；The additional amount of iron is 240mg/L；The additional amount of VA is 2mg/L, and the additional amount of VD is 200 μ g/L,
The additional amount of folic acid is 8mg/L；VB12Additional amount is 100 μ g/L；Then ultrasonication is carried out；The time of ultrasonication is
8min, power 400W；
Stabilizer is Karaya Gum, propylene glycol alginate, polyglycerolpolyrici.oleate and sodium tripolyphosphate；
Karaya Gum, propylene glycol alginate, polyglycerolpolyrici.oleate and sodium tripolyphosphate weight fraction ratio be 2:
1:1:3；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
Condition by high pressure homogenizer homogeneous is: homogenization pressure 20MPa, homogeneous 15min；The condition of second homogenate
It is: homogenization pressure 20MPa, homogeneous 10min；The time for crossing colloid mill is 5min；
Sterilize 15min at (6) 121 DEG C, filling, obtains nutrient solution.
Embodiment 2
Production is suitable for the edible nutrient solution containing peony seed oil of second trimester pregnant woman (pregnant 4-7 months), specific preparation side
Method is as follows:
(1) 90 parts of peony seed oil, 15 parts of DHA algal oil, the mixing of 9 parts of fish oil are taken, extractive of perilla, Chinese scholartree is then added
Flower extract, bamboo extractive are uniformly mixed, obtain mixture A；
Extractive of perilla accounts for the 0.02% of peony seed oil, algae oil and fish oil gross weight；
Flos Sophorae extract accounts for the 0.015% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.02% of peony seed oil, algae oil and fish oil gross weight；
(2) mixture A is heated to 80 DEG C, is smashed to pieces uniformly in high speed bruisher；The revolving speed that high speed bruisher is smashed to pieces is
12000 turns, time 12min；
(3) addition 0.3 part of emulsifier, 900 parts of water, 0.003 part of emulsification in uniform material is smashed to pieces in (2) to help
Agent emulsifies 1.2h in mulser；
Emulsifier is sodium carboxymethylcellulose, monoglyceride, casein sodium；Sodium carboxymethylcellulose, monoglyceride, casein
The weight ratio of sour sodium is 1:2:3；
Emulsion adjuvant are as follows: algal polysaccharides；
(4) 0.03 part of stabilizer is added in the material in (3) after emulsification, iron, VA, VD, folic acid, VB is added12, so
After carry out ultrasonication；The additional amount of iron is 240mg/L；The additional amount of VA is 2mg/L, and the additional amount of VD is 200 μ g/L, leaf
The additional amount of acid is 8mg/L；VB12Additional amount is 100 μ g/L；Then ultrasonication is carried out；The time of ultrasonication is
7min, power 400W；
Stabilizer is Karaya Gum, propylene glycol alginate, polyglycerolpolyrici.oleate and sodium tripolyphosphate；
Karaya Gum, propylene glycol alginate, polyglycerolpolyrici.oleate and sodium tripolyphosphate weight fraction ratio be 2:
1:1:3；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
Condition by high pressure homogenizer homogeneous is: homogenization pressure 15MPa, homogeneous 15min；The condition of second homogenate
It is: homogenization pressure 20MPa, homogeneous 10min；The time for crossing colloid mill is 5min；
Sterilize 15min at (6) 121 DEG C, filling, obtains nutrient solution.
Embodiment 3
Production is suitable for the edible nutrient solution containing peony seed oil of second trimester pregnant woman (pregnant 4-7 months), specific preparation side
Method is as follows:
(1) take 100 parts of peony seed oil, 15 parts of DHA algal oil, 12 parts fish oil mixing, then be added extractive of perilla,
Flos Sophorae extract, bamboo extractive are uniformly mixed, obtain mixture A；
Extractive of perilla accounts for the 0.01% of peony seed oil, algae oil and fish oil gross weight；
Flos Sophorae extract accounts for the 0.03% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.02% of peony seed oil, algae oil and fish oil gross weight；
(2) mixture A is heated to 80 DEG C, is smashed to pieces uniformly in high speed bruisher；The revolving speed that high speed bruisher is smashed to pieces is
12000 turns, time 12min；
(3) addition 0.3 part of emulsifier, 600 parts of water, 0.003 part of emulsification in uniform material is smashed to pieces in (2) to help
Agent emulsifies 2h or so in mulser；
Emulsifier is sodium carboxymethylcellulose, monoglyceride, casein sodium；Sodium carboxymethylcellulose, monoglyceride, casein
The weight ratio of sour sodium is 2:3:4；
Emulsion adjuvant are as follows: algal polysaccharides；
(4) 0.02 part of stabilizer is added in the material in (3) after emulsification, iron, VA, VD, folic acid, VB is added12, so
After carry out ultrasonication；The additional amount of iron is 240mg/L；The additional amount of VA is 2mg/L, and the additional amount of VD is 200 μ g/L,
The additional amount of folic acid is 8mg/L；VB12Additional amount is 100 μ g/L；Then ultrasonication is carried out；The time of ultrasonication is
8min, power 400W；
Stabilizer is Karaya Gum, propylene glycol alginate, polyglycerolpolyrici.oleate and sodium tripolyphosphate；
Karaya Gum, propylene glycol alginate, polyglycerolpolyrici.oleate and sodium tripolyphosphate weight fraction ratio be 2:
1:1:3；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
Condition by high pressure homogenizer homogeneous is: homogenization pressure 25MPa, homogeneous 15min；The condition of second homogenate
It is: homogenization pressure 15MPa, homogeneous 10min；The time for crossing colloid mill is 5min；
Sterilize 15min at (6) 121 DEG C, filling, obtains nutrient solution.
Comparative example 1
It is with the difference of embodiment 1, specific steps in (1) are as follows:
80 parts of peony seed oil, 15 parts of DHA algal oil, the mixing of 12 parts of fish oil are taken, extractive of perilla is then added, mixes
Uniformly, mixture A is obtained；
Extractive of perilla accounts for the 0.055% of peony seed oil, algae oil and fish oil gross weight；
Remaining step is identical with embodiment 1；
Comparative example 2
It is with the difference of embodiment 1, specific steps in (1) are as follows:
80 parts of peony seed oil, 15 parts of DHA algal oil, the mixing of 12 parts of fish oil are taken, Flos Sophorae extract is then added, mixes
Uniformly, mixture A is obtained；
Flos Sophorae extract accounts for the 0.055% of peony seed oil, algae oil and fish oil gross weight；
Remaining step is identical with embodiment 1；
Comparative example 3
It is with the difference of embodiment 1, specific steps in (1) are as follows:
80 parts of peony seed oil, 15 parts of DHA algal oil, the mixing of 12 parts of fish oil are taken, Flos Sophorae extract is then added, mixes
Uniformly, mixture A is obtained；
Flos Sophorae extract accounts for the 0.055% of peony seed oil, algae oil and fish oil gross weight；
Remaining step is identical with embodiment 1；
Comparative example 4
(1) take 80 parts of peony seed oil, 15 parts of DHA algal oil, 12 parts fish oil mixing, then be added extractive of perilla,
Flos Sophorae extract is uniformly mixed, obtains mixture A；
Extractive of perilla accounts for the 0.03% of peony seed oil, algae oil and fish oil gross weight；
Flos Sophorae extract accounts for the 0.025% of peony seed oil, algae oil and fish oil gross weight；
Remaining step is identical with embodiment 1；
Comparative example 5
(1) take 80 parts of peony seed oil, 15 parts of DHA algal oil, 12 parts fish oil mixing, then be added extractive of perilla,
Bamboo extractive is uniformly mixed, obtains mixture A；
Extractive of perilla accounts for the 0.02% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.025% of peony seed oil, algae oil and fish oil gross weight；
Remaining step is identical with embodiment 1；
Comparative example 6
(1) take 80 parts of peony seed oil, 15 parts of DHA algal oil, 12 parts fish oil mixing, then be added Flos Sophorae extract,
Bamboo extractive is uniformly mixed, obtains mixture A；
Flos Sophorae extract accounts for the 0.03% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.025% of peony seed oil, algae oil and fish oil gross weight；
Remaining step is identical with embodiment 1；
Comparative example 7
(1) it takes 80 parts of peony seed oil, 15 parts of DHA algal oil, 12 parts of fish oil to be uniformly mixed, obtains mixture A；It is not added
Any extract, remaining step are identical with embodiment 1；
About the product in embodiment 1-3 and comparative example 1-7, the present inventor has made following test experience:
Peroxide value is measured according to GB/T5538-2005, specific as follows:
It is detected by below raw material of the high performance liquid chromatography to product and (has chosen three kinds of main band bad smells
Substance), data are as follows:
The fishy smell detection of product in 1 embodiment 1-3 of table and comparative example 1-7 and peroxide value detect
It is the content of main fishy smell substance in embodiment 1-3 and comparative example 1-7 in above table, the production in embodiment 1-3
Its fishy smell content of material of product is suitable；Fishy smell substance in comparative example 1-7 will be higher by much compared to embodiment 1-3, and be compared
It is many that the peroxide value of product in example 1-7 is also apparently higher than embodiment 1-3；
In comparative example 1-3, only with a Plant Extracts, two kinds of plant extracts are relatively added in fishy smell substance therein
The comparative example 4-6 of object wants high, this illustrates that compound plant extracts is added, and for inhibiting the generation of fishy smell substance, has significant
Effect, and its peroxide value is also low compared with comparative example 4-6.
Any plant extracts is not added in comparative example 7, fishy smell content of material is apparently higher than other comparative examples and implementation
Example, this illustrates that its fishy smell substance is denseer, and peroxide value is higher, this illustrates that plant extracts of the present invention is anti-oxidant
Effect is also more apparent；
Extractive of perilla, Flos Sophorae extract, bamboo extractive in the present invention all have oxidation resistant effect, and purple perilla mentions
Take object and Flos Sophorae extract for deodorization effect than more significant；The principle of the two deodorization is: fish oil, which has, to be stored in the process easily
Oxidation, the fishy smell ingredient such as carbide that omega-3 unsaturated fatty acid autoxidation generates, such as 2,4- decadienal, 2,4, the 7- last of the ten Heavenly stems
Three olefine aldehydrs etc., during fish oil storage, the effect or lipid autoxidation of microorganism or enzyme will also result in the corruption of fish oil, and
And also contain trimethylamine oxide in fish oil, which can degrade under the collective effect of microorganism and enzyme generates trimethylamine and diformazan
Amine, pure trimethylamine only have ammonia taste, in many fresh fishes and are not present, but in the fish oil of storage but content compared with
Height, the pure trimethylamine effect either fish oil lipid autoxidation by microorganism or enzyme during storage, with δ -2 ammonia
Base valeric acid, hexahydropyridine etc., which coexist, produces the olfactory of stronger fishy smell.
Therefore, present invention adds plant extracts, extractive of perilla, Flos Sophorae extract and bamboo extractive, three's
Inoxidizability is relatively strong, considerably beyond antioxidants such as VC, prevents fish oil from aoxidizing during storage and generates fishy smell ingredient, than
The carbide generated such as omega-3 unsaturated fatty acid autoxidation；One obvious action of extractive of perilla and bamboo extractive
It is that there is antibacterial effect, bamboo extractive can inhibit fish oil to generate microorganism during storage, prevent three in fish oil
Methylamine is coexisted with δ -2 aminovaleric acid, hexahydropyridine etc. and generates the strong smelling of fish by microbial action；To reach inhibition
The purpose of the smelling of fish, meanwhile, extractive of perilla, Flos Sophorae extract itself contain aroma substance, can cover or cover fishlike smell
Youngster, therefore the addition of these three plant extracts have good effect for the removal of fishlike smell；
In addition the extractive of perilla that the present invention is added, highly-safe, purple perilla is a kind of two kinds of medicine food of raw material,
Body has the function of miscarriage prevention, and extract is also safe from harm for pregnant woman；Flos Sophorae extract, highly-safe, inoxidizability is strong,
And it acts synergistically with extractive of perilla, can remove the smelling of fish in microcapsule powder.Although being equally plant extracts, peppermint is mentioned
Take object that can also play the role of a degree of deodorization, but mint extract is not suitable for pregnant woman, with Robust speaker feature
Effect, therefore not any plant extracts is adapted to pregnant woman.It is primarily to examine safely when selecting plant extracts
The factor of worry, followed by remove the effect of fishy smell；Materials safety of the present invention is all higher, and its dosage is very
It is few, undesirable effect will not be generated to the body of pregnant woman.
About emulsifier, more important role is also played in the present invention, and the present inventor in an experiment, just starts to select
What is selected is single emulsifier, it is found that its performance is good not as good as compound emulsifier effect.The experiment that the present inventor is specifically done is such as
Under:
Comparative example 8
(3) in, emulsifier is sodium carboxymethylcellulose；Remaining step is identical with embodiment 1；
Comparative example 9
(3) in, emulsifier is monoglyceride；Remaining step is identical with embodiment 1；
Comparative example 10
(3) in, emulsifier is casein sodium；Remaining step is identical with embodiment 1；
Comparative example 11
(3) in, emulsifier is sodium carboxymethylcellulose and monoglyceride；
Comparative example 12
(3) in, emulsifier is monoglyceride and casein sodium；
Comparative example 13
(3) in, emulsifier is sodium carboxymethylcellulose and casein sodium；
To embodiment 1-3 and comparative example viscosity: being measured using viscosity of the rotational viscometer to emulsion；
The nutrient solution in about 8mL embodiment 1 is taken, is stood, is recorded the time of layering, the nutrient solution in embodiment 1 is put
30 days, 60 days are set, its viscosity is investigated and changes over time；
Viscosity: it is measured using viscosity of the rotational viscometer to emulsion；
Product viscosity in 2 embodiment 1-3 of table detects table
| 0d | 30d | 60d | |
| Embodiment 1 | 24.3 | 25.1 | 25.8 |
| Embodiment 2 | 24.6 | 25.3 | 25.9 |
| Embodiment 3 | 24.1 | 24.7 | 25.4 |
| Comparative example 8 | 51.2 | 55.3 | 57.9 |
| Comparative example 9 | 51.7 | 54.4 | 58.3 |
| Comparative example 10 | 51.3 | 54.2 | 59.1 |
| Comparative example 11 | 42.2 | 45.9 | 48.3 |
| Comparative example 12 | 43.6 | 47.5 | 49.8 |
| Comparative example 13 | 42.5 | 48.8 | 50.2 |
As can be seen from the above table, for the product in embodiment 1-3 compared to the product in comparative example 8-13, viscosity is lower,
After 30 days, 60 days storage phases, viscosity variation is less, almost unchanged；Viscosity in comparative example 8-13, viscosity
It changes greatly, and its k value is also above embodiment 1-3.Analyze reason, it may be possible to use compound emulsifier, formed
Emulsification membrane fluidity it is larger, in this way oil mutually be just easy to spread by the gap of emulsifying film into water phase, then by be added
Emulsion adjuvant algal polysaccharides help the emulsifier sodium carboxymethylcellulose with water-wet side, monoglyceride, casein sodium and emulsification
Agent algal polysaccharides constitute thicker hydrophilic interface layer, overcome the deficiency of single layer emulsifying film, enhance emulsifying effectiveness.
The measurement of particle number
By the microscopic count inspection in the grain inspection technique in particulate matter inspection technique, in each every milli of time point sequentially determining
It rises particle diameter and is greater than 10 microns but less than 25 microns, the particle number greater than 25 microns.
10-25 microns of particle number (a/mL) changes over time table in 3 product of table
| 0d | 10d | 15d | 20d | 25d | 30d | 40d | |
| Embodiment 1 | 142 | 139 | 141 | 150 | 147 | 155 | 160 |
| Embodiment 2 | 147 | 140 | 135 | 143 | 151 | 154 | 149 |
| Embodiment 3 | 138 | 141 | 135 | 141 | 156 | 150 | 142 |
| Comparative example 8 | 158 | 152 | 146 | 139 | 131 | 128 | 127 |
| Comparative example 9 | 163 | 154 | 147 | 139 | 132 | 130 | 128 |
| Comparative example 10 | 172 | 166 | 170 | 160 | 153 | 144 | 145 |
| Comparative example 11 | 169 | 164 | 159 | 162 | 153 | 158 | 147 |
| Comparative example 12 | 154 | 145 | 148 | 143 | 140 | 142 | 136 |
| Comparative example 13 | 166 | 165 | 155 | 161 | 158 | 153 | 149 |
Particle number (a/mL) in 4 product of table greater than 25 microns changes over time table
The result shows that in embodiment 1-3, particle diameter is greater than 10 microns and 25 microns with the extension that the time places
Particle number variation less, illustrates that the quantity of the particle dispersion in every milliliter is in relatively steady state, the dispersion performance of product
It is good.In comparative example 8-13,10-25 microns and the particle number greater than 25 microns are all reduced, illustrate may some particle it is heavy
It forms sediment, the slight lamination of product more or less appearance.Judge in terms of stability, the product in embodiment 1-3 its
Stability is better than comparative example 8-13.
Claims (9)
1. a kind of nutrient solution containing peony seed oil suitable for pregnant woman, which is characterized in that the nutrient solution is mainly with edible oil
Gained is prepared as auxiliary material as major ingredient and other nutritional ingredients；
Edible oil is mainly: peony seed oil: 60~100；DHA algal oil: 8~20；Fish oil: 4~15；
Adjunct ingredient:
Extractive of perilla, Flos Sophorae extract, bamboo extractive；
Extractive of perilla accounts for the 0.01-0.03% of edible oil gross weight；
Flos Sophorae extract accounts for the 0.01-0.03% of edible oil gross weight；
Bamboo extractive accounts for the 0.01-0.02% of edible oil gross weight；
Its preparation process is as follows:
(1) 60~100 parts of peony seed oil, 8~20 parts of DHA algal oil, the mixing of 4~15 parts of fish oil are taken, purple perilla is then added
Extract, Flos Sophorae extract, bamboo extractive are uniformly mixed, obtain mixture A；
(2) mixture A is heated to 80-100 DEG C, is smashed to pieces uniformly in high speed bruisher；
(3) addition 0.1~0.8 part of emulsifier, 400~1200 parts of water, 0.001- in uniform material are smashed to pieces in (2)
0.005 part of emulsion adjuvant emulsifies 1~2h in mulser；
(4) 0.01-0.04 parts of stabilizer is added in the material in (3) after emulsification, then carries out ultrasonication；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
(6) it sterilizes, it is filling, obtain nutrient solution.
2. a kind of nutrient solution containing peony seed oil suitable for pregnant woman as described in claim 1, which is characterized in that (2) in,
The revolving speed that high speed bruisher is smashed to pieces is 10000~12000r/min, 10~15min of time.
3. a kind of nutrient solution containing peony seed oil suitable for pregnant woman as described in claim 1, which is characterized in that (3) in,
Emulsifier is sodium carboxymethylcellulose, monoglyceride, casein sodium；Sodium carboxymethylcellulose, monoglyceride, casein sodium weight
Amount is than being 1~3:2~4:1~5.
4. a kind of nutrient solution containing peony seed oil suitable for pregnant woman as described in claim 1, which is characterized in that (3) in,
Emulsion adjuvant are as follows: algal polysaccharides.
5. a kind of nutrient solution containing peony seed oil suitable for pregnant woman as described in claim 1, which is characterized in that (4) in,
The time of ultrasonication is 5~10min, and power is 300~500W.
6. a kind of nutrient solution containing peony seed oil suitable for pregnant woman as described in claim 1, which is characterized in that (5) in,
Condition by high pressure homogenizer homogeneous is: homogenization pressure is 10~25MPa, homogeneous 15min；The condition of second homogenate is:
Matter pressure is 10~25MPa, homogeneous 10min.
7. a kind of nutrient solution containing peony seed oil suitable for pregnant woman as described in claim 1, preparation process are as follows:
(1) 60~100 parts of peony seed oil, 8~20 parts of DHA algal oil, the mixing of 4~15 parts of fish oil are taken, purple perilla is then added
Extract, Flos Sophorae extract, bamboo extractive are uniformly mixed, obtain mixture A；
Extractive of perilla accounts for the 0.01-0.03% of peony seed oil, algae oil and fish oil gross weight；
Flos Sophorae extract accounts for the 0.01-0.03% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.01-0.02% of peony seed oil, algae oil and fish oil gross weight；
(2) mixture A is heated to 80-100 DEG C, is smashed to pieces uniformly in high speed bruisher；
(3) addition 0.1~0.8 part of emulsifier, 400~1200 parts of water, 0.001- in uniform material are smashed to pieces in (2)
0.005 part of emulsion adjuvant emulsifies 1~2h in mulser；
(4) 0.01-0.04 parts of stabilizer is added in the material in (3) after emulsification, then carries out ultrasonication；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
(6) it sterilizes, it is filling, obtain nutrient solution.
8. a kind of nutrient solution containing peony seed oil suitable for pregnant woman, which is characterized in that the condition of sterilizing are as follows: go out at 121 DEG C
Bacterium 15min.
9. a kind of nutrient solution containing peony seed oil suitable for pregnant woman as described in claim 1, preparation method are as follows:
(1) 60~100 parts of peony seed oil, 8~20 parts of DHA algal oil, the mixing of 4~15 parts of fish oil are taken, purple perilla is then added
Extract, Flos Sophorae extract, bamboo extractive are uniformly mixed, obtain mixture A；
Extractive of perilla accounts for the 0.01-0.03% of peony seed oil, algae oil and fish oil gross weight；
Flos Sophorae extract accounts for the 0.01-0.03% of peony seed oil, algae oil and fish oil gross weight；
Bamboo extractive accounts for the 0.01-0.02% of peony seed oil, algae oil and fish oil gross weight；
(2) mixture A is heated to 80-100 DEG C, is smashed to pieces uniformly in high speed bruisher；
(3) addition 0.1~0.8 part of emulsifier, 400~1200 parts of water, 0.001- in uniform material are smashed to pieces in (2)
0.005 part of emulsion adjuvant emulsifies 1~2h in mulser；
(4) 0.01-0.04 parts of stabilizer is added in the material in (3) after emulsification, iron, VA, VD, folic acid, VB is added12, so
After carry out ultrasonication；The additional amount of iron is 240mg/L；The additional amount of VA is 2mg/L, and the additional amount of VD is 200 μ g/L, leaf
The additional amount of acid is 8mg/L；VB12Additional amount is 100 μ g/L；Then ultrasonication is carried out；The time of ultrasonication be 5~
10min, power are 300~500W；
(5) second homogenate is then carried out thereafter after colloid mill by high pressure homogenizer homogeneous again；
(6) it sterilizes, it is filling, obtain nutrient solution.
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| CN112167366A (en) * | 2020-10-29 | 2021-01-05 | 张国浩 | Nutritional sunflower seed oil |
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| CN111011545A (en) * | 2019-12-25 | 2020-04-17 | 菏泽瑞璞牡丹产业科技发展有限公司 | High-grade flavor oil containing peony seed oil and preparation method thereof |
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