CN109293244A - A kind of red bottom green statin chun glaze - Google Patents
A kind of red bottom green statin chun glaze Download PDFInfo
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- CN109293244A CN109293244A CN201811557142.2A CN201811557142A CN109293244A CN 109293244 A CN109293244 A CN 109293244A CN 201811557142 A CN201811557142 A CN 201811557142A CN 109293244 A CN109293244 A CN 109293244A
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- glaze
- chun
- red bottom
- bottom green
- green statin
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/04—Frit compositions, i.e. in a powdered or comminuted form containing zinc
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/658—Atmosphere during thermal treatment
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/658—Atmosphere during thermal treatment
- C04B2235/6583—Oxygen containing atmosphere, e.g. with changing oxygen pressures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
Abstract
A kind of red bottom green statin chun glaze, it is prepared by the raw material of following parts by weight: boron frit 25-30, porcelain stone 10-15, spodumene 3-5, zinc oxide 10-20, dolomite 10-15, calcite 15-25, carclazyte 5-10, copper oxide 3-5, tin oxide 1-2.Using formula provided by the invention and preparation method, a kind of chun glaze of moss green speckle that flashes in red background color can be successfully burnt out, the similar liquor-saturated glaze of beauty is red not too much gorgeous, and it is simple and tasteful, there is preferable artistic effect.
Description
Technical field
The invention belongs to pottery production technical fields, and in particular to a kind of red bottom green statin chun glaze and preparation method.
Background technique
Chun glaze is one layer of glaze on pottery product mold surface, is generally fired under high temperature reduction flame using copper, iron as colorant
Form, and because kiln temperature, atmosphere variation due to form the transmutation effect that color desktop, lines are peculiar, artistic conception is infinite.Its feature
Mainly glaze thickness, milkiness, colour generation are complicated and changeable.
Chun glaze can generally be divided into transmutation single colour glaze, transmutation variegation glaze and transmutation fancy glaze, when transmutation single colour glaze such as Song Yuan
Bluish white, sky blue, reddish black, the pea green glaze of phase, the sky blue erythema glaze in transmutation variegation glaze such as Song Yuan period, transmutation fancy glaze such as Tang Junhua
Glaze, with the development of the times with the raising of technique, people no longer meet traditional glaze colours, it is therefore desirable to be badly in need of carrying out new glaze colours
Exploitation.
Summary of the invention
The object of the invention is that providing a kind of red bottom green statin chun glaze to solve the deficiencies in the prior art.
The purpose of the present invention is what is realized with following technical proposals:
A kind of red bottom green statin chun glaze, it is prepared by the raw material of following parts by weight: boron frit 25-30, porcelain stone 10-15, lithium
Pyroxene 3-5, zinc oxide 10-20, dolomite 10-15, calcite 15-25, carclazyte 5-10, copper oxide 3-5, tin oxide 1-2.
Preferably, it is prepared by the raw material of following parts by weight: boron frit 27.5, porcelain stone 12.5, spodumene 4, oxygen
Change zinc 15, dolomite 12.5, calcite 20, carclazyte 7.5, copper oxide 4, tin oxide 1.5.
The boron frit is prepared by the raw material of following parts by weight: borax 30-40, zinc oxide 15-25, quartz
25-30, feldspar 15-25.
The preparation method of red bottom green statin chun glaze as described above, comprising the following steps:
(1) above-mentioned raw materials are mixed, ball milling obtains glaze slip；
(2) glazing on the carcass after biscuiting；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 750-850 DEG C by room temperature in 2-3h；
2. heavy reduction phase: being warming up to 1180-1220 DEG C in 3-4h；
3. light reduction phase: being warming up to 1250-1270 DEG C in 2-2.5h；
4. temperature-fall period: cooled to room temperature.
For the step (2) using leaching glaze method glazing, concentration of glaze slip is 43-46 Baume degrees.
Using formula provided by the invention and preparation method, a kind of moss green of flashing in red background color can be successfully burnt out
The chun glaze of speckle, the similar liquor-saturated glaze of beauty is red not too much gorgeous, simple and tasteful, has preferable artistic effect.
Detailed description of the invention
Fig. 1 is the red bottom green statin chun glaze glaze paint figure that the embodiment of the present invention 2 provides.
Specific embodiment
Embodiment 1
A kind of red bottom green statin chun glaze, it is prepared by the raw material of following parts by weight: boron frit 25-30, porcelain stone 10-15, lithium
Pyroxene 3-5, zinc oxide 10-20, dolomite 10-15, calcite 15-25, carclazyte 5-10, copper oxide 3-5, tin oxide 1-2.
The boron frit is prepared by the raw material of following parts by weight: borax 30-40, zinc oxide 15-25, quartz
25-30, feldspar 15-25；In 1200 DEG C or more high-temperature fusions after raw material is mixed.Using frit, firing temperature can be both reduced,
Glaze quality can also be improved, wherein boron can also contribute to color development.Porcelain stone preferably uses Sanmenxia Gorge porcelain stone, porcelain stone be it is a kind of by
Quartz, sericite, and have the silicate rock mineral comprising feldspar, aluminum oxide etc., there is preferable hydrotropy and milkiness
Property.Lithium in spodumene containing 6% or so can equally reduce firing temperature, contain in dolomite with stronger dissolution assistant effect
The calcium oxide and magnesia of high level, calcite equally can provide a large amount of calcium, they can provide calcium ions and magnesium ions, as hydrotropy
Agent improves glaze quality.Spodumene, dolomite and calcite preferably use Yuzhou native product；Carclazyte is preferably Yuzhou
Ecliptic township carclazyte, aluminum content is high, can enhance and the combination of mold, enhancing suspension reduce sagging.Zinc oxide, copper oxide and
Tin oxide has apparent humidification as chemical assistant, to the stability of colour generation and glaze quality.
Red bottom green statin chun glaze preparation method as described above, it is characterised in that the following steps are included:
(1) above-mentioned raw materials are mixed, ball milling obtains glaze slip；
(2) glazing on the carcass after biscuiting；It is preferred that concentration of glaze slip is 43-46 Baume degrees using leaching glaze method glazing；Using conjunction
Suitable concentration of glaze slip can reduce the defects of contracting glaze, sagging；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 750-850 DEG C by room temperature in 2-3h；
2. heavy reduction phase: being warming up to 1180-1220 DEG C in 3-4h；
3. light reduction phase: being warming up to 1250-1270 DEG C in 2-2.5h；This firing temperature is than general pottery firing temperature
(1300 DEG C or so) are lower, and fire can be improved yield rate at a lower temperature；
4. temperature-fall period: cooled to room temperature.
Under the suitable atmosphere of high temperature, is burnt using bavin burning, coal or gas firing method can successfully burn out red bottom green statin chun glaze,
Middle bavin is burnt, coal firing method fires yield rate 35% or so, and gas firing method is 50% or so.
Embodiment 2
A kind of red bottom green statin chun glaze, it is prepared by the raw material of following parts by weight: boron frit 27.5, porcelain stone 12.5, lithium brightness
Stone 4, zinc oxide 15, dolomite 12.5, calcite 20, carclazyte 7.5, copper oxide 4, tin oxide 1.5.The boron frit is by following
What the raw material of parts by weight was prepared: borax 35, zinc oxide 20, quartzy 27.5, feldspar 20.
Red bottom green statin chun glaze preparation method as described above, comprising the following steps:
(1) above-mentioned raw materials are mixed, ball milling obtains glaze slip；
(2) glazing on the carcass using leaching glaze method after biscuiting；Concentration of glaze slip is 45 Baume degrees；(3) it is burnt using gas firing method
At specifically including following several stages:
1. oxidation stage: rising to 800 DEG C by room temperature in 2.5h；
2. heavy reduction phase: being warming up to 1200 DEG C in 3.5h；
3. light reduction phase: being warming up to 1260 DEG C in 2.5h；
4. temperature-fall period: cooled to room temperature.
Its glaze paint figure after being burnt into is as shown in Figure 1, its yield rate can reach 55%.
Embodiment 3
A kind of red bottom green statin chun glaze, it is prepared by the raw material of following parts by weight: boron frit 29, porcelain stone 10, spodumene 5,
Zinc oxide 18, dolomite 10, calcite 21, carclazyte 7, copper oxide 4, tin oxide 1.8.The boron frit is by following parts by weight
What raw material was prepared: borax 33, zinc oxide 22, quartzy 27.5, feldspar 23.
Red bottom green statin chun glaze preparation method as described above, comprising the following steps:
(1) above-mentioned raw materials are mixed, ball milling obtains glaze slip；
(2) glazing on the carcass using leaching glaze method after biscuiting；Concentration of glaze slip is 45 Baume degrees；(3) it is burnt using gas firing method
At specifically including following several stages:
1. oxidation stage: rising to 800 DEG C by room temperature in 3h；
2. heavy reduction phase: being warming up to 1210 DEG C in 4h；
3. light reduction phase: being warming up to 1260 DEG C in 2h；
4. temperature-fall period: cooled to room temperature.
Embodiment 4
A kind of red bottom green statin chun glaze, it is prepared by the raw material of following parts by weight: boron frit 27, porcelain stone 15, spodumene 4,
Zinc oxide 10, dolomite 14, calcite 25, carclazyte 6, copper oxide 3.5, tin oxide 1.6.The boron frit is by following parts by weight
Raw material be prepared: borax 38, zinc oxide 26, quartzy 26, feldspar 17.
Red bottom green statin chun glaze preparation method as described above, comprising the following steps:
(1) above-mentioned raw materials are mixed, ball milling obtains glaze slip；
(2) glazing on the carcass using leaching glaze method after biscuiting；Concentration of glaze slip is 45 Baume degrees；(3) it is burnt using gas firing method
At specifically including following several stages:
1. oxidation stage: rising to 840 DEG C by room temperature in 2h；
2. heavy reduction phase: being warming up to 1180 DEG C in 3.5h；
3. light reduction phase: being warming up to 1250 DEG C in 2.5h；
4. temperature-fall period: cooled to room temperature.
The formula of 5-14 of the embodiment of the present invention is shown in Table 1, remaining is the same as embodiment 2.
Claims (5)
1. a kind of red bottom green statin chun glaze, it is characterised in that it is prepared by the raw material of following parts by weight: boron frit 25-30,
Porcelain stone 10-15, spodumene 3-5, zinc oxide 10-20, dolomite 10-15, calcite 15-25, carclazyte 5-10, copper oxide 3-5, oxygen
Change tin 1-2.
2. red bottom green statin chun glaze as described in claim 1, it is characterised in that it is prepared by the raw material of following parts by weight:
Boron frit 27.5, porcelain stone 12.5, spodumene 4, zinc oxide 15, dolomite 12.5, calcite 20, carclazyte 7.5, copper oxide 4, oxidation
Tin 1.5.
3. such as the described in any item red bottom green statin chun glazes of claim 1-2, it is characterised in that the boron frit is by following weight
What the raw material of part was prepared: borax 30-40, zinc oxide 15-25, quartz 25-30, feldspar 15-25.
4. the preparation method of red bottom green statin chun glaze as described in any one of claims 1-3, it is characterised in that the following steps are included:
(1) above-mentioned raw materials are mixed, ball milling obtains glaze slip；
(2) glazing on the carcass after biscuiting；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 750-850 DEG C by room temperature in 2-3h；
2. heavy reduction phase: being warming up to 1180-1220 DEG C in 3-4h；
3. light reduction phase: being warming up to 1250-1270 DEG C in 2-2.5h；
4. temperature-fall period: cooled to room temperature.
5. the preparation method of red bottom green statin chun glaze as claimed in claim 4, it is characterised in that the step (2) is using leaching glaze side
Method glazing, concentration of glaze slip are 43-46 Baume degrees.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811557142.2A CN109293244A (en) | 2018-12-19 | 2018-12-19 | A kind of red bottom green statin chun glaze |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811557142.2A CN109293244A (en) | 2018-12-19 | 2018-12-19 | A kind of red bottom green statin chun glaze |
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| CN201811557142.2A Pending CN109293244A (en) | 2018-12-19 | 2018-12-19 | A kind of red bottom green statin chun glaze |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113121114A (en) * | 2020-06-18 | 2021-07-16 | 季友泉 | Longquan kiln snow melting glaze and manufacturing method thereof |
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| CN102249739A (en) * | 2011-05-26 | 2011-11-23 | 山西高陶瓷业有限责任公司 | Preparation method of carbon-golden metallic luster crystalline glaze |
| CN104140245A (en) * | 2014-07-29 | 2014-11-12 | 青岛乾祥环保技术有限公司 | Environment-friendly healthy Junyu glaze porcelain |
| CN107619192A (en) * | 2017-10-17 | 2018-01-23 | 禹州市锦丰源瓷业有限公司 | A kind of new an ancient unit of weight fancy glaze and preparation method thereof |
| CN108409139A (en) * | 2018-05-29 | 2018-08-17 | 禹州市土魂钧瓷有限公司 | A kind of stove chun glaze and preparation method thereof |
| CN108585504A (en) * | 2018-07-30 | 2018-09-28 | 赵红刚 | Coper green glaze and preparation method thereof |
-
2018
- 2018-12-19 CN CN201811557142.2A patent/CN109293244A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102249739A (en) * | 2011-05-26 | 2011-11-23 | 山西高陶瓷业有限责任公司 | Preparation method of carbon-golden metallic luster crystalline glaze |
| CN104140245A (en) * | 2014-07-29 | 2014-11-12 | 青岛乾祥环保技术有限公司 | Environment-friendly healthy Junyu glaze porcelain |
| CN107619192A (en) * | 2017-10-17 | 2018-01-23 | 禹州市锦丰源瓷业有限公司 | A kind of new an ancient unit of weight fancy glaze and preparation method thereof |
| CN108409139A (en) * | 2018-05-29 | 2018-08-17 | 禹州市土魂钧瓷有限公司 | A kind of stove chun glaze and preparation method thereof |
| CN108585504A (en) * | 2018-07-30 | 2018-09-28 | 赵红刚 | Coper green glaze and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113121114A (en) * | 2020-06-18 | 2021-07-16 | 季友泉 | Longquan kiln snow melting glaze and manufacturing method thereof |
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