CN109289753A - The reactive liquid solution experiment instrument of rotary jet type - Google Patents
The reactive liquid solution experiment instrument of rotary jet type Download PDFInfo
- Publication number
- CN109289753A CN109289753A CN201811472961.7A CN201811472961A CN109289753A CN 109289753 A CN109289753 A CN 109289753A CN 201811472961 A CN201811472961 A CN 201811472961A CN 109289753 A CN109289753 A CN 109289753A
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- China
- Prior art keywords
- rotating
- reactor tank
- inlet tube
- cover
- rotation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 238000002474 experimental method Methods 0.000 title claims abstract description 16
- 239000006193 liquid solution Substances 0.000 title claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 59
- 239000007921 spray Substances 0.000 claims abstract description 32
- 230000007246 mechanism Effects 0.000 claims abstract description 25
- 238000002347 injection Methods 0.000 claims abstract description 13
- 239000007924 injection Substances 0.000 claims abstract description 13
- 238000003860 storage Methods 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 11
- 239000004973 liquid crystal related substance Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 abstract description 34
- 239000000376 reactant Substances 0.000 abstract description 26
- 230000009471 action Effects 0.000 abstract description 9
- 239000012530 fluid Substances 0.000 abstract description 5
- 230000004044 response Effects 0.000 abstract description 5
- 230000033001 locomotion Effects 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 4
- 238000005096 rolling process Methods 0.000 abstract description 4
- 150000001875 compounds Chemical class 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000002070 germicidal effect Effects 0.000 description 3
- 238000001816 cooling Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005304 joining Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000007779 soft material Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 239000005341 toughened glass Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/28—Moving reactors, e.g. rotary drums
Abstract
The reactive liquid solution experiment instrument of present invention offer rotary jet type, including reactor tank, cover, inlet tube, for the inlet tube from extending into reactor tank after cover outside, the bottom end of the inlet tube is equipped with connection boss, and the connection boss is sequentially connected connecting mechanism for rotating and rotating-spray mechanism.This reactive liquid solution experiment instrument not only makes rotating-spray mechanism under the action of fluid pressure, to reactor tank rotating-spray liquid reactants, inlet tube also rotates under the action of hydraulic, and then carry out the liquid in reactor tank up and down, along compound Multidirectional motions such as counterclockwise and rollings, effectively increase the contact area of two kinds of liquid reactants, full and uniform mixing, react complete, it can also be by adjusting the power of micro pump come flexible modulation liquid injection rates, to effectively adjust reaction rate, convenient for experimenter's observing response process, mechanical automation operation reaction, experimental data is accurate, security performance is high.
Description
Technical field
The present invention relates to a kind of experiment reaction units, and in particular to a kind of reactive liquid solution experiment instrument of rotary jet type.
Background technique
Reactive liquid solution belongs to common chemical reaction, generally existing in many industrial circles such as petroleum, chemical industry, metallurgy,
In order to fully understand that liquid liquid chemically reacts, scientific experiment will be generally carried out to observe chemical reaction course or produce newly anti-
Answer object.
Currently, typically being poured into along glass bar to the container equipped with liquid reactants another when carrying out the experiment of liquid liquid
Liquid reactants, such hybrid mode cause the liquid reactants in the liquid reactants and container that pour into that can only partially connect
Touching, reactant cannot be sufficiently mixed, cause to react insufficient, not only influence experimental data, also waste reactant resource.Furthermore
Liquid reactants are added along glass bar, the liquid rate of addition is difficult to control, to be unable to control reaction rate, is unfavorable for reality
Test observation.In addition, especially volatile harmful liquid reactant, hand feed pole has when if the property of reactant is unstable
There may be security risk, security performance is low.
Summary of the invention
In view of the deficienciess of the prior art, the present invention provides a kind of reactive liquid solution experiment instrument of rotary jet type, this liquid
Liquid reaction experiment instrument is equipped with the connecting mechanism for rotating that connect with inlet tube and rotating-spray mechanism in reactor tank, and inlet tube and
Micro pump connection, not only makes rotating-spray mechanism under the action of fluid pressure, to reactor tank rotating-spray liquid reactants,
Inlet tube also rotates under the action of hydraulic, and then carries out liquid in reactor tank up and down, along counterclockwise and rolling etc. is multiple
Multidirectional motion is closed, the contact area of two kinds of liquid reactants is effectively increased, full and uniform mixing is reacted complete, can also be passed through
The power for adjusting micro pump carrys out flexible modulation liquid injection rates, to effectively adjust reaction rate, sees convenient for experimenter
Reaction process is examined, mechanical automation operation reaction, experimental data is accurate, and security performance is high.
In order to achieve the above object, the technical solution that the present invention takes:
The reactive liquid solution experiment instrument of rotary jet type, including cylindrical reactor tank, the top of the reactor tank is removable
The cover for being equipped with and being cooperatively connected with it is unloaded, the cover is equipped with an inlet tube, and the inlet tube extends after running through cover outside
Enter in reactor tank, a micro pump is also connected on the inlet tube, the bottom end of the inlet tube is equipped with a connection boss；The company
It connects and is equipped with a connecting mechanism for rotating in boss, the connecting mechanism for rotating includes fixing rotation with connect the connection of boss internal engagement
Turn connector sleeve, be arranged in the fixed rotation connector sleeve one with connect the rotation liquid storage chamber communicated inside boss, the rotation is stored up
The upper end of sap cavity is arranged a fixation big envelope being fixed, and the fixed big envelope is transverse in the top of fixed rotation connector sleeve, institute
The side for stating rotation liquid storage chamber is equipped with the rotating-spray mechanism being cooperatively connected with it, and the rotating-spray mechanism includes storing up with rotation
The fixed rotation support sleeve that sap cavity is laterally cooperatively connected, fixed rotate in support sleeve are arranged a rotating-spray chamber, the rotation
The upper end for turning spray chamber is arranged a support big envelope being fixed, and the support big envelope is transverse in the top of fixed rotation support sleeve
It holds, is equipped with several injection pipes along its circumferential direction on the rotating-spray chamber.
Shorten chemical reaction as optimal technical scheme in order to make reactor tank be applied to the reactive liquid solution of heating
Time expands the scope of application of experimental provision, improves the practicability of entire experimental provision, and the bottom end of the cover is additionally provided with one and adds
Hot pin, sets that there are two the temperature control buttons with heating rod electrical connection on the cover surface, then one of them be+heat button, it is another
One is cooling button.
As optimal technical scheme, for the ease of adjusting the power of temperature and micro pump in reactor tank, in order to provide
Preferable reaction condition, further increases reaction rate and reaction effect, is conducive to Germicidal efficacy and experimental study, the cover
Outer surface be equipped with a liquid crystal display, the liquid crystal display can intuitively show the function of the temperature and micro pump in reactor tank
Rate.
Compared with prior art, the invention has the benefit that
1, this reactive liquid solution experiment instrument is equipped with the connecting mechanism for rotating connecting with inlet tube and rotating-spray in reactor tank
Mechanism, and inlet tube is connect with micro pump, not only makes rotating-spray mechanism under the action of fluid pressure, is rotated to reactor tank
Liquid reactants are sprayed, inlet tube also rotates under the action of hydraulic, and then carries out the liquid in reactor tank up and down, along the inverse time
The compound Multidirectional motion such as needle and rolling effectively increases the contact area of two kinds of liquid reactants, full and uniform mixing, reaction
It is complete, it can also be by the power of adjusting micro pump come flexible modulation liquid injection rates, to effectively adjust reaction rate, just
In experimenter's observing response process, mechanical automation operation reaction, experimental data is accurate, and security performance is high.
2, heating rod is set, so that reactor tank is applied to the reactive liquid solution of heating, shortens the time of chemical reaction, is expanded
The scope of application of experimental provision improves the practicability of entire experimental provision.
3, liquid crystal display is set, convenient for adjusting the power of temperature and micro pump in reactor tank, in order to provide preferable
Reaction condition, further increase reaction rate and reaction effect, be conducive to Germicidal efficacy and experimental study.
Detailed description of the invention
The present invention is described in further detail in the following with reference to the drawings and specific embodiments.
Fig. 1 is the structural diagram of the present invention；
Fig. 2 is the structural schematic diagram of cover；
Fig. 3 is the structural schematic diagram of connecting mechanism for rotating and rotating-spray mechanism；
Drawing reference numeral: 1, reactor tank, 2, cover, 3, inlet tube, 4, connection boss, 5, connecting mechanism for rotating, 5-1, fixation
Rotate connector sleeve, 5-2, rotation liquid storage chamber, 5-3, fixed big envelope, 5-4, closing gasket, 6, rotating-spray mechanism, 6-1, fixed rotation
Turn support sleeve, 6-2, rotating-spray chamber, 6-3, support big envelope, 6-4, injection pipe, 6-5, anti-overflow gasket, 7, heating rod, 8, temperature
Control button, 9, liquid crystal display, 10, rotating handle, 11, power reconcile key, 12, start switch, 13, rotary support seat.
Specific embodiment
A kind of specific embodiment of the present invention, including cylindrical reactor tank 1, the reactor tank 1 are proposed as shown in Figure 1
Top is detachably equipped with the cover 2 being cooperatively connected with it, in order to make this experimental provision suitable for the liquid liquid under the conditions of differential responses
Reaction, while guaranteeing to be completely embedded between cover 2 and reactor tank 1, this implementation offers internal screw thread in 2 bottom end of cover, is reacting
The top of tank 1 offers external screw thread, is connected through a screw thread between reactor tank 1 and cover 2 and realizes that quick distachable closely connects, just
In unscrewing or install cover 2, while being convenient for this experiment instrument of taking and placing, it is in the shape of a frame that the present embodiment is also equipped with one on the top of cover 2
Rotating handle 10, due to being strong corrosive reactant, guarantees to make this experimental provision be suitable for reactant reaction of different nature
Convenient for reaction process in observing response tank 1, this implementation setting reactor tank 1 and cover 2 are made of transparent toughened glass material
, the cover 2 is equipped with an inlet tube 3, and the inlet tube 3 after cover 2 from extending into reactor tank 1 outside, in order to make
Reactant in reactor tank 1 is uniformly mixed, and the inlet tube 3 runs through preferably from 2 center of cover extends into 1 central axis of reactor tank
Locate, a micro pump is also connected on the inlet tube 3, the micro pump is for can also increase inlet tube while conveying liquid
Interior fluid pressure, it is made of soft material that inlet tube 3, which is arranged, in the present embodiment, and optional fire-fighting strap, inlet tube 3 is in liquid pressure
It is rotated, is carried to keep this reaction unit compact-sized in one, conducive to experimenter, the present embodiment will under the action of power
Micro pump is installed in cover 2, and is set on cover 2 there are two the POWER LEVEL 11 for adjusting micro pump power,
The electric wire connecting with micro pump is set in cover 2, which, which extends, connect outside cover 2 with power supply line, and the present embodiment is also
Control power supply line is equipped on cover 2 starts switch 12, and in order to make the firm rotation of inlet tube 3, the present embodiment is also in cover 2
Bottom end be equipped with a rotary support seat 13, as shown in Fig. 2, the bottom end of the inlet tube 3 be equipped with one connection boss 4, in order to prevent into
Liquid pipe 3 is arranged inlet tube 3 and is integrally formed with boss 4 is connect with leakage at boss 4, the present embodiment is connect；In the connection boss 4
Equipped with a connecting mechanism for rotating 5, the connecting mechanism for rotating 5 includes connecting with the fixed rotation for connecting the connection of 5 internal engagement of boss
Be arranged in female connector 5-1, the fixed rotation connector sleeve 5-1 one with connect the rotation liquid storage chamber 5-2 communicated inside boss 4, it is described
The upper end of rotation liquid storage chamber 5-2 is arranged fixation big envelope 5-3, the fixed big envelope 5-3 that one is fixed and is transverse in fixed rotation
The top of connector sleeve 5-1, the then diameter for being greater than the fixed rotation connector sleeve 5-1 by the way that the diameter of fixed big envelope 5-3 is arranged are real
Now rotation liquid storage chamber 5-2 is fixed in connection boss 4, and the liquid reactions in inlet tube 3 are flowed out from joining place in order to prevent, this reality
Example is applied on rotation liquid storage chamber 5-2 and the lower section for being located at fixed big envelope 5-3 is equipped with a closing gasket 5-4；The rotation liquid storage chamber
The side of 5-2 is equipped with the rotating-spray mechanism 6 being cooperatively connected with it, and the present embodiment setting rotation liquid storage chamber 5-2 is in inverted T-shape,
The upper end of the rotation liquid storage chamber 5-2 is sheathed in connection boss 4, and rotation is arranged in the lower end side of the rotation liquid storage chamber 5-2
Injection equipment 6, the rotating-spray mechanism 6 include the fixed rotation support sleeve 6- being laterally cooperatively connected with rotation liquid storage chamber 5-2
1, between the fixed rotation connector sleeve 5-1 of the present embodiment setting and connection boss 4, fix rotation support sleeve 6-1 and rotation liquid storage chamber
It is to realize to be cooperatively connected by screw thread between 5-2, is arranged a rotating-spray chamber 6-2, institute in the fixed rotation support sleeve 6-1
The upper end for stating rotating-spray chamber 6-2 is arranged support big envelope 6-3, the support big envelope 6-3 that one is fixed and is transverse in fixed rotation
Turn the top of support sleeve 6-1, then and by the diameter of setting support big envelope 6-3 be greater than the diameter of fixed rotation support sleeve 6-1,
Realize that rotating-spray chamber 6-2 is fixed in fixed rotation support sleeve 6-1, in order to guarantee to rotate the liquid reactions in liquid storage chamber 5-2
Object all enters in rotating-spray chamber 6-2, and the present embodiment is set in the upper of rotating-spray chamber 6-2 and below support big envelope 6-3
Have and is equipped with several injection pipe 6-4, the present embodiment along its circumferential direction on anti-overflow gasket a 6-5, the rotating-spray chamber 6-2
Two injection pipe 6-4 are only set, and offer spray-hole in the end of every injection pipe 6-4, as shown in Figure 3.
The bottom end of the cover 2 is additionally provided with a heating rod 7, is set on 2 surface of cover there are two electrically connecting with heating rod 7
The temperature control button 8 connect, then one of them be+heat button, another be cooling button, make reactor tank 1 be applied to heating
Reactive liquid solution shortens the time of chemical reaction, expands the scope of application of experimental provision, improves the practicability of entire experimental provision.
The outer surface of the cover 2 is equipped with a liquid crystal display 9, and the liquid crystal display 9 can intuitively be shown in reactor tank 1
Temperature and micro pump power, convenient for adjust reactor tank 1 in temperature and micro pump power, in order to provide preferable
Reaction condition further increases reaction rate and reaction effect, is conducive to Germicidal efficacy and experimental study.
When the present invention uses: rotation can opening lid 2 will be poured into wherein in reactor tank 1 liquid reactants, and cover cover 2, open
Actuating miniature water pump, under the action of micro pump, after another liquid reactants enter inlet tube 3, since fluid pressure is big, feed liquor
Pipe 3 turns in hydraulic drive backspin, and liquid reactants flow through rotation liquid storage chamber 5-2, rotates liquid storage chamber 5-2 under the action of hydraulic
It is rotated, liquid reactants are rotated into rotating-spray chamber 6-2, and liquid reactants are rotated into rotating-spray chamber 6-2
Enter injection pipe 6-4, injection pipe 6-4 is with rotating-spray chamber 6-2 synchronous rotary, and then the multi-direction injection liquid into reactor tank 1
Reactant, makes the liquid reactants stress in reactor tank 1, carry out up and down, along counterclockwise and the compound motions such as rolling, realize two
The full and uniform mixing of kind reactant, reaction is significant, is easy to the intuitive observing response process of experimenter；It can be actual according to reaction
Situation starts heating rod 7, or by POWER LEVEL 11 come the power of flexible modulation micro pump, by temperature control button 8 come clever
The temperature living adjusted in reactor tank 1 effectively controls the reaction rate in reactor tank 1.
Certainly, only the preferred embodiments of the disclosure is described in detail in conjunction with attached drawing above, not with this
Limit practical range of the invention, equivalence changes made by all principles under this invention, construction and structure should all be covered by this
In the protection scope of invention.
Claims (3)
1. the reactive liquid solution experiment instrument of rotary jet type, it is characterised in that: including reactor tank (1), the top of the reactor tank (1)
Detachable to be equipped with the cover (2) being cooperatively connected with it, the cover (2) is equipped with an inlet tube (3), the inlet tube (3) from
It is extended into after cover (2) in reactor tank (1) outside, is also connected with a micro pump, the inlet tube on the inlet tube (3)
(3) bottom end is equipped with connection boss (4)；A connecting mechanism for rotating (5) are equipped in the connection boss (4), the rotation connects
Connection mechanism (5) includes and fixed rotation connector sleeve (5-1) that connect the connection of boss (4) internal engagement, the fixed rotation connection
Be arranged in set (5-1) one with connect the rotation liquid storage chamber (5-2) that communicates of boss (4) inside, it is described to rotate the upper of liquid storage chamber (5-2)
End cap sets a fixation big envelope (5-3) being fixed, and the fixed big envelope (5-3) is transverse in fixed rotation connector sleeve (5-1)
Top；The side of rotation liquid storage chamber (5-2) is equipped with the rotating-spray mechanism (6) being cooperatively connected with it, the rotating-spray
Mechanism (6) includes fixed rotation support sleeve (6-1) being laterally cooperatively connected with rotation liquid storage chamber (5-2), the fixed rotation branch
It is arranged a rotating-spray chamber (6-2) in support set (6-1), the upper end of the rotating-spray chamber (6-2) is arranged a branch being fixed
It supports big envelope (6-3), support big envelope (6-3) is transverse in the top of fixed rotation support sleeve (6-1), the rotating-spray chamber
Several injection pipes (6-4) are equipped with along its circumferential direction on (6-2).
2. the reactive liquid solution experiment instrument of rotary jet type according to claim 1, it is characterised in that: the cover (2)
Bottom end is additionally provided with a heating rod (7), set on cover (2) surface there are two with heating rod (7) electrical connection temperature control button
(8)。
3. the reactive liquid solution experiment instrument of rotary jet type according to claim 1 or 2, it is characterised in that: the cover (2)
Outer surface be equipped with a liquid crystal display (9), the liquid crystal display (9) can intuitively show temperature in reactor tank (1) and micro-
The power of type water pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811472961.7A CN109289753A (en) | 2018-12-04 | 2018-12-04 | The reactive liquid solution experiment instrument of rotary jet type |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811472961.7A CN109289753A (en) | 2018-12-04 | 2018-12-04 | The reactive liquid solution experiment instrument of rotary jet type |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109289753A true CN109289753A (en) | 2019-02-01 |
Family
ID=65141562
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811472961.7A Pending CN109289753A (en) | 2018-12-04 | 2018-12-04 | The reactive liquid solution experiment instrument of rotary jet type |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109289753A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN203610131U (en) * | 2013-11-28 | 2014-05-28 | 广西科技大学 | Uniformly-fed reaction kettle |
| CN205217542U (en) * | 2015-12-02 | 2016-05-11 | 宿州学院 | Washing unit for chemical experiment utensils |
| CN209317689U (en) * | 2018-12-04 | 2019-08-30 | 钦州学院 | The reactive liquid solution experiment instrument of rotary jet type |
-
2018
- 2018-12-04 CN CN201811472961.7A patent/CN109289753A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN203610131U (en) * | 2013-11-28 | 2014-05-28 | 广西科技大学 | Uniformly-fed reaction kettle |
| CN205217542U (en) * | 2015-12-02 | 2016-05-11 | 宿州学院 | Washing unit for chemical experiment utensils |
| CN209317689U (en) * | 2018-12-04 | 2019-08-30 | 钦州学院 | The reactive liquid solution experiment instrument of rotary jet type |
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