CN109261112A - Reactive liquid solution experimental provision based on hydraulic rotating injection - Google Patents
Reactive liquid solution experimental provision based on hydraulic rotating injection Download PDFInfo
- Publication number
- CN109261112A CN109261112A CN201811474317.3A CN201811474317A CN109261112A CN 109261112 A CN109261112 A CN 109261112A CN 201811474317 A CN201811474317 A CN 201811474317A CN 109261112 A CN109261112 A CN 109261112A
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- Prior art keywords
- reactor tank
- inlet tube
- cover
- liquid
- rotating
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- 238000002347 injection Methods 0.000 title claims abstract description 23
- 239000007924 injection Substances 0.000 title claims abstract description 23
- 239000006193 liquid solution Substances 0.000 title claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 42
- 239000007921 spray Substances 0.000 claims abstract description 17
- 230000007246 mechanism Effects 0.000 claims abstract description 12
- 238000010438 heat treatment Methods 0.000 claims description 10
- 239000004973 liquid crystal related substance Substances 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 abstract description 30
- 239000000376 reactant Substances 0.000 abstract description 23
- 239000012530 fluid Substances 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 4
- 230000033001 locomotion Effects 0.000 abstract description 4
- 230000004044 response Effects 0.000 abstract description 4
- 238000005096 rolling process Methods 0.000 abstract description 4
- 150000001875 compounds Chemical class 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 2
- 230000009471 action Effects 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 3
- 230000002070 germicidal effect Effects 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000007779 soft material Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000005341 toughened glass Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention provides the reactive liquid solution experimental provision sprayed based on hydraulic rotating, including reactor tank, cover, inlet tube, for the inlet tube from extending into reactor tank after cover outside, the bottom end of the inlet tube is equipped with connection boss, is equipped with rotating-spray mechanism in the connection boss.This reactive liquid solution experimental provision is equipped with the rotating-spray mechanism connecting with inlet tube in reactor tank, and inlet tube is connect with micro pump, make rotating-spray part under fluid pressure effect, to reactor tank rotating-spray liquid reactants, and then carry out the liquid in reactor tank up and down, along compound Multidirectional motions such as counterclockwise and rollings, effectively increase the contact area of two kinds of liquid reactants, full and uniform mixing, react complete, it can also be by adjusting the power of micro pump come flexible modulation liquid injection rates, to effectively adjust reaction rate, convenient for experimenter's observing response process, mechanical automation operation, experimental data is accurate, security performance is high.
Description
Technical field
The present invention relates to a kind of experiment reaction units, and in particular to a kind of reactive liquid solution experiment based on hydraulic rotating injection
Device.
Background technique
Reactive liquid solution belongs to common chemical reaction, generally existing in many industrial circles such as petroleum, chemical industry, metallurgy,
In order to fully understand that liquid liquid chemically reacts, scientific experiment will be generally carried out to observe chemical reaction course or produce newly anti-
Answer object.
Currently, typically being poured into along glass bar to the container equipped with liquid reactants another when carrying out the experiment of liquid liquid
Liquid reactants, such hybrid mode cause the liquid reactants in the liquid reactants and container that pour into that can only partially connect
Touching, reactant cannot be sufficiently mixed, cause to react insufficient, not only influence experimental data, also waste reactant resource.Furthermore
Liquid reactants are added along glass bar, the liquid rate of addition is difficult to control, to be unable to control reaction rate, is unfavorable for reality
Test observation.In addition, especially volatile harmful liquid reactant, hand feed pole has when if the property of reactant is unstable
There may be security risk, security performance is low.
Summary of the invention
In view of the deficienciess of the prior art, the present invention provides a kind of reactive liquid solution experiment dress based on hydraulic rotating injection
It sets, this reactive liquid solution experimental provision is equipped with the rotating-spray mechanism connecting with inlet tube, inlet tube and Miniature water in reactor tank
Pump connection, not only makes rotating-spray mechanism under the action of fluid pressure, to reactor tank rotating-spray liquid reactants, inlet tube
Also it is rotated under the action of hydraulic, and then carries out liquid in reactor tank up and down, along counterclockwise and rolling etc. is compound multidirectional
Movement effectively increases the contact area of two kinds of liquid reactants, and full and uniform mixing reacts complete, can also be micro- by adjusting
The power of type water pump carrys out flexible modulation liquid-liquid injection rate, to effectively adjust reaction rate, observes convenient for experimenter
Reaction process, mechanical automation operation reaction, experimental data is accurate, and security performance is high.
In order to achieve the above object, the technical solution that the present invention takes:
Based on the reactive liquid solution experimental provision of hydraulic rotating injection, including cylindrical reactor tank, the reactor tank
Top is detachably equipped with the cover being cooperatively connected with it, and the cover is equipped with an inlet tube, and the inlet tube is from outside through tank
It is extended into reactor tank after lid, a micro pump is also connected on the inlet tube, it is convex that the bottom end of the inlet tube is equipped with a connection
Platform；A rotating-spray mechanism is equipped in the connection boss, the rotating-spray mechanism includes and connect boss internal engagement company
The fixed rotation support sleeve connect, be arranged in the fixed rotation support sleeve one with connect the connecting tube communicated inside boss, it is described
The top of connecting tube is arranged a firm pullover, and the firm pullover is transverse in the upper end of fixed rotation support sleeve, the connecting tube
Bottom end be set in the liquid storage cylinder communicated with inside it, the liquid storage cylinder prolong its circumferential surface equipped with several with its inside phase
The end of logical injection pipe, the injection pipe is closed, and the injection pipe prolongs its length direction and is full of spray-hole.
Shorten chemical reaction as optimal technical scheme in order to make reactor tank be applied to the reactive liquid solution of heating
Time expands the scope of application of experimental provision, improves the practicability of entire experimental provision, and the bottom end of the cover is additionally provided with one and adds
Hot pin, sets that there are two the temperature control buttons with heating rod electrical connection on the cover surface, then one of them be+heat button, it is another
One is cooling button.
As optimal technical scheme, for the ease of adjusting the power of temperature and micro pump in reactor tank, in order to provide
Preferable reaction condition, further increases reaction rate and reaction effect, is conducive to Germicidal efficacy and experimental study, the cover
Outer surface be equipped with a liquid crystal display, the liquid crystal display can intuitively show the function of the temperature and micro pump in reactor tank
Rate.
Compared with prior art, the invention has the benefit that
1, this reactive liquid solution experimental provision is equipped with the rotating-spray mechanism that connect with inlet tube in reactor tank, inlet tube and
Micro pump connection, not only makes rotating-spray mechanism under the action of fluid pressure, to reactor tank rotating-spray liquid reactants,
Inlet tube also rotates under the action of hydraulic, and then carries out liquid in reactor tank up and down, along counterclockwise and rolling etc. is multiple
Multidirectional motion is closed, the contact area of two kinds of liquid reactants is effectively increased, full and uniform mixing is reacted complete, can also be passed through
The power for adjusting micro pump carrys out flexible modulation liquid injection rates, to effectively adjust reaction rate, sees convenient for experimenter
Reaction process is examined, mechanical automation operation reaction, experimental data is accurate, and security performance is high.
2, heating rod is set, so that reactor tank is applied to the reactive liquid solution of heating, shortens the time of chemical reaction, is expanded
The scope of application of experimental provision improves the practicability of entire experimental provision.
3, liquid crystal display is set, convenient for adjusting the power of temperature and micro pump in reactor tank, in order to provide preferable
Reaction condition, further increase reaction rate and reaction effect, be conducive to Germicidal efficacy and experimental study.
Detailed description of the invention
The present invention is described in further detail in the following with reference to the drawings and specific embodiments.
Fig. 1 is the structural diagram of the present invention；
Fig. 2 is the structural schematic diagram of cover；
Fig. 3 is the structural schematic diagram of rotating-spray mechanism；
Drawing reference numeral: 1, reactor tank, 2, cover, 3, inlet tube, 4, connection boss, 5, rotary support seat, 6, fixed rotation
Support sleeve, 7, connecting tube, 8, firm pullover, 9, liquid storage cylinder, 10, injection pipe, 11, spray-hole, 12, heating rod, 13, temperature control presses
Button, 14, liquid crystal display, 15, rotating handle, 16, POWER LEVEL, 17, start switch, 18, be tamping gasket.
Specific embodiment
A kind of specific embodiment of the present invention, including cylindrical reactor tank 1, the reactor tank 1 are proposed as shown in Figure 1
Top is detachably equipped with the cover 2 being cooperatively connected with it, in order to make this experimental provision suitable for the liquid liquid under the conditions of differential responses
Reaction, while guaranteeing to be completely embedded between cover 2 and reactor tank 1, this implementation offers internal screw thread in 2 bottom end of cover, is reacting
The top of tank 1 offers external screw thread, is connected through a screw thread between reactor tank 1 and cover 2 and realizes that quick distachable closely connects, just
In unscrewing or install cover 2, while being convenient for this experimental provision of taking and placing, it is in the shape of a frame that the present embodiment is also equipped with one on the top of cover 2
Rotating handle 15 due to being strong corrosive reactant, protected to make this experimental provision be suitable for reactant reaction of different nature
Card is convenient for reaction process in observing response tank 1, and reactor tank 1 is arranged in this implementation and cover 2 is by transparent toughened glass material system
At, the cover 2 is equipped with an inlet tube 3, and the inlet tube 3 extends into reactor tank 1 after running through cover 2 outside, in order to
It is uniformly mixed the reactant in reactor tank 1, the inlet tube 3 runs through preferably from 2 center of cover extends into 1 center of reactor tank
At axis, a micro pump is also connected on the inlet tube 3, the micro pump is for can also increase feed liquor while conveying liquid
Fluid pressure in pipe, it is made of soft material that inlet tube 3, which is arranged, in the present embodiment, and optional fire-fighting strap, inlet tube 3 is in liquid
It is rotated, is carried to keep this reaction unit compact-sized in one, conducive to experimenter, the present embodiment under the action of pressure
Micro pump is installed in cover 2, and sets on cover 2 that there are two the POWER LEVELs for adjusting micro pump power
16, the electric wire connecting with micro pump is set in cover 2, which, which extends, connect outside cover 2 with power supply line, the present embodiment
Control power supply line is equipped with also on cover 2 starts switch 17, and in order to make the firm rotation of inlet tube 3, the present embodiment is also in cover 2
Bottom end be equipped with a rotary support seat 5, as shown in Fig. 2, the bottom end of the inlet tube 3 be equipped with one connection boss 4, in order to prevent into
Liquid pipe 3 is arranged inlet tube 3 and is integrally formed with boss 4 is connect with leakage at boss 4, the present embodiment is connect；In the connection boss 4
Equipped with a rotating-spray mechanism, the rotating-spray mechanism includes supporting with the fixed rotation for connecting the connection of 4 internal engagement of boss
Set 6, the present embodiment are respectively provided with screw thread in the outer surface of fixed rotation support sleeve 6, the inner surface of connection boss 4, pass through screw thread
Realize cooperation dismantling connection, be arranged in the fixed rotation support sleeve 6 one with connect the connecting tube 7 communicated inside boss 4, it is described
The top of connecting tube 7 is arranged a firm pullover 8, and in order to flow into all liq in connecting tube 7, the present embodiment is in connecting tube 7
Lower section that is upper and being located at firm pullover 8 is equipped with one and is tamping gasket 18, and the firm pullover 8 is transverse in fixed rotation support sleeve 6
Upper end, then the diameter of the firm pullover 8 is greater than the diameter of fixed rotation support sleeve 6, to guarantee that connecting tube 7 is stabilized in fixation
It rotates in support sleeve 6, the bottom end of the connecting tube 7 is set in the cylindrical liquid storage cylinder 9 communicated with inside it, the storage
Fluid cylinder 9 prolongs its circumferential surface equipped with several injection pipes 10 communicated with inside it, and the end of the injection pipe 10 is closed, and institute
It states injection pipe 10 and prolongs its length direction and be full of spray-hole 11, as shown in Figure 3.
The bottom end of the cover 2 is additionally provided with a heating rod 12, sets that there are two electrical with heating rod 12 on 2 surface of cover
The temperature control button 13 of connection, then one of them be+heat button, another be cooling button, make reactor tank 1 be applied to plus
The reactive liquid solution of heat, shortens the time of chemical reaction, expands the scope of application of experimental provision, improve the practical of entire experimental provision
Property.
The outer surface of the cover 2 is equipped with a liquid crystal display 14, and the liquid crystal display 14 can intuitively show reactor tank 1
The power of interior temperature and micro pump, convenient for adjusting the power of temperature and micro pump in reactor tank 1, in order to provide preferable
Reaction condition, further increase reaction rate and reaction effect, be conducive to Germicidal efficacy and experimental study.
When the present invention uses: rotation can opening lid 2 will be poured into wherein in reactor tank 1 liquid reactants, and cover cover 2, open
Actuating miniature water pump, under the action of micro pump, after another liquid reactants enter inlet tube 3, since fluid pressure is big, feed liquor
Pipe 3 turns in hydraulic drive backspin, and liquid reactants successively pass through connecting tube 7, liquid storage cylinder 9 again, finally enters in injection pipe 10,
Under the action of fixed rotation support sleeve 6, connecting tube 7 drives liquid storage cylinder 9 to turn in hydraulic drive backspin, to make liquid from spray-hole
Middle rotation spray projects, and makes the liquid reactants stress in reactor tank 1, carry out up and down, along counterclockwise and the compound motions such as rolling,
Make the full and uniform mixing of two kinds of reactants, reaction is significant, is easy to the intuitive observing response process of experimenter；It can be real according to reaction
The case where border, starts heating rod 12, or passes through temperature control button by POWER LEVEL 16 come the power of flexible modulation micro pump
13 carry out the temperature in flexible modulation reactor tank 1, effectively control the reaction rate in reactor tank 1.
Certainly, only the preferred embodiments of the disclosure is described in detail in conjunction with attached drawing above, not with this
Limit practical range of the invention, equivalence changes made by all principles under this invention, construction and structure should all be covered by this
In the protection scope of invention.
Claims (3)
1. the reactive liquid solution experimental provision based on hydraulic rotating injection, it is characterised in that: including reactor tank (1), the reactor tank
(1) top is detachably equipped with the cover (2) being cooperatively connected with it, and the cover (2) is equipped with an inlet tube (3), it is described into
Liquid pipe (3) is also connected with a micro pump, institute on the inlet tube (3) from extending into reactor tank (1) after cover (1) outside
The bottom end for stating inlet tube (3) is equipped with connection boss (4)；A rotating-spray mechanism, the rotation are equipped in the connection boss (4)
Turn fixed rotation support sleeve (6) that injection equipment includes with connect the connection of boss (4) internal engagement, the fixed rotation support sleeve
(6) be arranged in one with connect the connecting tube (7) that communicates of boss (4) inside, the top of the connecting tube (7) is arranged a firm pullover
(8), the firm pullover (8) is transverse in the upper end of fixed rotation support sleeve (6), the bottom end of the connecting tube (7) be set in
In the liquid storage cylinder (9) communicated inside it, the liquid storage cylinder (9) prolongs its circumferential surface equipped with several injections communicated with inside it
It manages (10), the end of the injection pipe (10) is closed, and the injection pipe (10) prolongs its length direction and is full of spray-hole (11).
2. the reactive liquid solution experimental provision according to claim 1 based on hydraulic rotating injection, it is characterised in that: the tank
Lid (2) bottom end be additionally provided with a heating rod (12), set on cover (2) surface there are two with heating rod (12) electrical connection
Temperature control button (13).
3. the reactive liquid solution experimental provision according to claim 1 or 2 based on hydraulic rotating injection, it is characterised in that: institute
The outer surface for stating cover (2) is equipped with a liquid crystal display (14), and the liquid crystal display (14) can intuitively show in reactor tank (1)
Temperature and micro pump power.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811474317.3A CN109261112A (en) | 2018-12-04 | 2018-12-04 | Reactive liquid solution experimental provision based on hydraulic rotating injection |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811474317.3A CN109261112A (en) | 2018-12-04 | 2018-12-04 | Reactive liquid solution experimental provision based on hydraulic rotating injection |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109261112A true CN109261112A (en) | 2019-01-25 |
Family
ID=65186835
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811474317.3A Pending CN109261112A (en) | 2018-12-04 | 2018-12-04 | Reactive liquid solution experimental provision based on hydraulic rotating injection |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109261112A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115894183A (en) * | 2022-11-15 | 2023-04-04 | 山东神驰石化有限公司 | Device for recovering methyl tert-butyl ether |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN203610131U (en) * | 2013-11-28 | 2014-05-28 | 广西科技大学 | Uniformly-fed reaction kettle |
| CN205217542U (en) * | 2015-12-02 | 2016-05-11 | 宿州学院 | Washing unit for chemical experiment utensils |
| CN209317669U (en) * | 2018-12-04 | 2019-08-30 | 钦州学院 | Reactive liquid solution experimental provision based on hydraulic rotating injection |
-
2018
- 2018-12-04 CN CN201811474317.3A patent/CN109261112A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN203610131U (en) * | 2013-11-28 | 2014-05-28 | 广西科技大学 | Uniformly-fed reaction kettle |
| CN205217542U (en) * | 2015-12-02 | 2016-05-11 | 宿州学院 | Washing unit for chemical experiment utensils |
| CN209317669U (en) * | 2018-12-04 | 2019-08-30 | 钦州学院 | Reactive liquid solution experimental provision based on hydraulic rotating injection |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115894183A (en) * | 2022-11-15 | 2023-04-04 | 山东神驰石化有限公司 | Device for recovering methyl tert-butyl ether |
| CN115894183B (en) * | 2022-11-15 | 2023-10-20 | 山东神驰石化有限公司 | Device for recycling methyl tertiary butyl ether |
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