CN106268449A - A kind of liquid mixing reactor - Google Patents
A kind of liquid mixing reactor Download PDFInfo
- Publication number
- CN106268449A CN106268449A CN201610872900.4A CN201610872900A CN106268449A CN 106268449 A CN106268449 A CN 106268449A CN 201610872900 A CN201610872900 A CN 201610872900A CN 106268449 A CN106268449 A CN 106268449A
- Authority
- CN
- China
- Prior art keywords
- kettle
- liquid
- pipeline
- liquid pump
- drawing liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/50—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle
- B01F25/51—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle in which the mixture is circulated through a set of tubes, e.g. with gradual introduction of a component into the circulating flow
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/50—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle
- B01F25/52—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle with a rotary stirrer in the recirculation tube
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/50—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle
- B01F25/53—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle in which the mixture is discharged from and reintroduced into a receptacle through a recirculation tube, into which an additional component is introduced
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/50—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle
- B01F25/54—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle provided with a pump inside the receptacle to recirculate the material within the receptacle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/82—Combinations of dissimilar mixers
- B01F33/822—Combinations of dissimilar mixers with moving and non-moving stirring devices in the same receptacle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a kind of liquid mixing reactor, belong to reactor technical field, solve reactor of the prior art time liquid is stirred, have that stirring is uneven, position at mixing time length, inner wall of kettle cannot be carried out the problems such as stirring.The present invention includes arranging ear mount, observation panel, charging aperture, drain hole on kettle, kettle and adding heat pipe, agitating device is set in kettle, being provided with a drawing liquid pump on kettle, the inlet of drawing liquid pump is connected with autoclave body bottom, and the liquid outlet of drawing liquid pump is connected with the top of kettle；Being provided with a hollow ring on inner wall of kettle, hollow ring is provided with the pipeline fitted with inner wall of kettle, pipeline is provided with multiple liquid outlet, described hollow ring is connected with the liquid outlet of drawing liquid pump.The present invention is for the reaction of liquid.
Description
Technical field
A kind of liquid mixing reactor, for the reaction of liquid, belongs to reactor technical field.
Background technology
The broad understanding of reactor i.e. has the rustless steel container physically or chemically reacted, according to different process conditions demands
Carry out structure design and the parameter configuration of container, design condition, process, check and manufacture, checking and accepting and need according to Its Relevant Technology Standards,
To realize the heating of technological requirement, to evaporate, cool down and the mixture response function of low high speed.Pressure vessel must comply with GB150{ steel
Pressing pressure container } standard, non-pressure vessel must comply with NB/T47003.1-2009{ steel welding non-pressure vessel } standard.With
Course of reaction in pressure requirements require also to be not quite similar to the design of container.Production must add in strict accordance with corresponding standard
Work, detection trail run.Stainless steel cauldron is not quite similar according to different production technologies, operating condition etc., setting of reactor
Meter structure and parameter are different, i.e. the structural style of reactor is different, belongs to nonstandard tankage.
Reactor is combined reaction container, according to reaction condition to reactor structure function and the design of configuration adnexa.From
Charging-reaction-the discharging started all can complete pre-set reactions steps with higher automaticity, to reacting
Temperature in journey, pressure, mechanics control the important parameters such as (stirring, air blast etc.), reactant/product concentration and carry out strict tune
Control.Its structure is typically made up of kettle, actuating device, agitating device, heater, chiller, sealing device.The most supporting
Auxiliary equipment: dephlegmator, condenser, water knockout drum, collecting tank, filter etc..
Reactor material typically has carbon manganese steel, rustless steel, zirconium, Ni-based (Kazakhstan, Monel) alloy and other composite.
Reactor can use the stainless steel material manufactures such as SUS304, SUS316L.Agitator has anchor formula, frame, paddle, turbine type, scraper plate
Formula, combination type, rotating mechanism can use cycloidal planetary gear speed reducer, stepless reducer or frequency control etc., can meet various
The specific response requirement of material.Sealing device can use mechanical seal, packing seal etc. to seal structure.Heating, cooling can use
The structures such as chuck, semicanal, coil pipe, Miller plate, mode of heating has: steam, electrical heating, conduction oil, with meet acidproof, high temperature resistant,
The technique of the different operating environment such as wear-resistant, anticorrosive needs.And can be designed according to user's technological requirement, manufacture.
But existing reactor equipment has the following disadvantages, when liquid is stirred, exist stirring uneven, stir
Mix the position at time length, inner wall of kettle and cannot be carried out the problems such as stirring.
Summary of the invention
The present invention is directed to above-mentioned weak point and provide a kind of liquid mixing reactor, solve reaction of the prior art
When liquid is stirred by still, there is the position at stirring uneven, mixing time length, inner wall of kettle and cannot be carried out stirring etc. and ask
Topic.
To achieve these goals, the technical solution used in the present invention is:
A kind of liquid mixing reactor, including arranging ear mount, observation panel, charging aperture, drain hole on kettle, kettle and adding
Heat pipe, arranges agitating device in kettle, it is characterised in that: it is provided with a drawing liquid pump on kettle, the inlet of drawing liquid pump and kettle
Bottom is connected, and the liquid outlet of drawing liquid pump is connected with the top of kettle；A hollow ring, open circles it is provided with on inner wall of kettle
It is provided with the pipeline fitted with inner wall of kettle on ring, pipeline is provided with multiple liquid outlet, described hollow ring and drawing liquid pump
Liquid outlet be connected.
Further, described pipeline is perpendicular with the bottom of kettle, and the inwall of kettle is provided with many pipelines.
Further, described agitating device includes shaft, the stirring vane being arranged on shaft, and stirring vane is screw thread
Dress is arranged on shaft.
Further, the inlet of described drawing liquid pump is connected with kettle with liquid discharging tube by liquid suction pipe with liquid outlet, drawing liquid
Pipe is less than liquid discharging tube and takes out less than liquid suction pipe and the junction of drawing liquid pump, liquid discharging tube with the junction of kettle with the junction of kettle
The junction of liquid pump.
Further, it is connected between described pipeline and pipeline.
Compared with prior art, it is an advantage of the current invention that:
One, by drawing liquid pump, liquid is extracted out from bottom, then flowed out from the inwall of kettle by pipeline, having agitating device
In the case of cooperation, can be quickly uniform by liquid agitation, mixing time is short, it is simple to inner wall of kettle edge is sufficiently stirred for；
Two, stirring vane is that screw thread dress is arranged on shaft, can reduce resistance during stirring；
Three, liquid suction pipe and the junction of kettle are less than liquid suction pipe and the connection of the junction of drawing liquid pump, liquid discharging tube and kettle
Place is less than the junction of liquid discharging tube with drawing liquid pump, it is simple to when not carrying out drawing liquid mixing, the liquid in liquid suction pipe and liquid discharging tube can return
Flow in kettle.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention.
Detailed description of the invention
The present invention is further illustrated with embodiment below in conjunction with the accompanying drawings.
Embodiment 1
A kind of liquid mixing reactor, including arranging ear mount 2, observation panel 3, charging aperture 4, blowing on kettle 1, kettle 1
Mouthfuls 5 and add heat pipe 6, agitating device 7 is set in kettle 1, kettle 1 is provided with a drawing liquid pump 8, the inlet 9 of drawing liquid pump 8 and still
Being connected bottom body 1, the liquid outlet 10 of drawing liquid pump 8 is connected with the top of kettle 1；It is provided with an open circles on kettle 1 inwall
Ring 11, hollow ring 11 is provided with the pipeline 12 fitted with kettle 1 inwall, and pipeline 12 is provided with multiple liquid outlet 13,
Described hollow ring 11 is connected with the liquid outlet 13 of drawing liquid pump 8.By drawing liquid pump from autoclave body bottom drawing liquid, then from hollow ring
Enter pipeline, enter out liquid by the liquid outlet on pipeline and mix, hollow ring is both provided with aperture.By drawing liquid pump by liquid
Body is extracted out from bottom, then is flowed out from the inwall of kettle by pipeline, in the case of having agitating device to coordinate, and can be quickly by liquid
Stirring, mixing time is short, it is simple to inner wall of kettle edge is sufficiently stirred for.
Embodiment 2
A kind of liquid mixing reactor, including arranging ear mount 2, observation panel 3, charging aperture 4, blowing on kettle 1, kettle 1
Mouthfuls 5 and add heat pipe 6, agitating device 7 is set in kettle 1, kettle 1 is provided with a drawing liquid pump 8, the inlet 9 of drawing liquid pump 8 and still
Being connected bottom body 1, the liquid outlet 10 of drawing liquid pump 8 is connected with the top of kettle 1；It is provided with an open circles on kettle 1 inwall
Ring 11, hollow ring 11 is provided with the pipeline 12 fitted with kettle 1 inwall, and pipeline 12 is provided with multiple liquid outlet 13,
Described hollow ring 11 is connected with the liquid outlet 13 of drawing liquid pump 8.By drawing liquid pump from autoclave body bottom drawing liquid, then from hollow ring
Enter pipeline, enter out liquid by the liquid outlet on pipeline and mix, hollow ring is both provided with aperture.By drawing liquid pump by liquid
Body is extracted out from bottom, then is flowed out from the inwall of kettle by pipeline, in the case of having agitating device to coordinate, and can be quickly by liquid
Stirring, mixing time is short, it is simple to inner wall of kettle edge is sufficiently stirred for.Described pipeline 12 hangs down mutually with the bottom of kettle 1
Directly, the inwall of kettle 1 is provided with many pipelines 12.
Embodiment 3
A kind of liquid mixing reactor, including arranging ear mount 2, observation panel 3, charging aperture 4, blowing on kettle 1, kettle 1
Mouthfuls 5 and add heat pipe 6, agitating device 7 is set in kettle 1, kettle 1 is provided with a drawing liquid pump 8, the inlet 9 of drawing liquid pump 8 and still
Being connected bottom body 1, the liquid outlet 10 of drawing liquid pump 8 is connected with the top of kettle 1；It is provided with an open circles on kettle 1 inwall
Ring 11, hollow ring 11 is provided with the pipeline 12 fitted with kettle 1 inwall, and pipeline 12 is provided with multiple liquid outlet 13,
Described hollow ring 11 is connected with the liquid outlet 13 of drawing liquid pump 8.By drawing liquid pump from autoclave body bottom drawing liquid, then from hollow ring
Enter pipeline, enter out liquid by the liquid outlet on pipeline and mix, hollow ring is both provided with aperture.By drawing liquid pump by liquid
Body is extracted out from bottom, then is flowed out from the inwall of kettle by pipeline, in the case of having agitating device to coordinate, and can be quickly by liquid
Stirring, mixing time is short, it is simple to inner wall of kettle edge is sufficiently stirred for.Described pipeline 12 hangs down mutually with the bottom of kettle 1
Directly, the inwall of kettle 1 is provided with many pipelines 12.Described agitating device 7 includes shaft 14, is arranged on shaft 14
Stirring vane 15, stirring vane 15 fills in screw thread and is arranged on shaft 14.
Embodiment 4
A kind of liquid mixing reactor, including arranging ear mount 2, observation panel 3, charging aperture 4, blowing on kettle 1, kettle 1
Mouthfuls 5 and add heat pipe 6, agitating device 7 is set in kettle 1, kettle 1 is provided with a drawing liquid pump 8, the inlet 9 of drawing liquid pump 8 and still
Being connected bottom body 1, the liquid outlet 10 of drawing liquid pump 8 is connected with the top of kettle 1；It is provided with an open circles on kettle 1 inwall
Ring 11, hollow ring 11 is provided with the pipeline 12 fitted with kettle 1 inwall, and pipeline 12 is provided with multiple liquid outlet 13,
Described hollow ring 11 is connected with the liquid outlet 13 of drawing liquid pump 8.By drawing liquid pump from autoclave body bottom drawing liquid, then from hollow ring
Enter pipeline, enter out liquid by the liquid outlet on pipeline and mix, hollow ring is both provided with aperture.By drawing liquid pump by liquid
Body is extracted out from bottom, then is flowed out from the inwall of kettle by pipeline, in the case of having agitating device to coordinate, and can be quickly by liquid
Stirring, mixing time is short, it is simple to inner wall of kettle edge is sufficiently stirred for.Described pipeline 12 hangs down mutually with the bottom of kettle 1
Directly, the inwall of kettle 1 is provided with many pipelines 12.Described agitating device 7 includes shaft 14, is arranged on shaft 14
Stirring vane 15, stirring vane 15 fills in screw thread and is arranged on shaft 14.The inlet 9 of described drawing liquid pump 8 and liquid outlet 10
Being connected with kettle 1 with liquid discharging tube 17 by liquid suction pipe 16, liquid suction pipe 16 is less than liquid suction pipe 16 and drawing liquid with the junction of kettle 1
The junction of pump 8, the junction of liquid discharging tube 17 and kettle 1 is less than the junction of liquid discharging tube 17 with drawing liquid pump 8.Described pipeline 12 with
It is connected between pipeline 12.
Claims (5)
1. a liquid mixing reactor, including arranging ear mount (2), observation panel (3), charging aperture on kettle (1), kettle (1)
(4), drain hole (5) and add heat pipe (6), agitating device (7) is set in kettle (1), it is characterised in that: kettle is provided with on (1)
One drawing liquid pump (8), the inlet (9) of drawing liquid pump (8) is connected with kettle (1) bottom, the liquid outlet (10) of drawing liquid pump (8) and still
The top of body (1) is connected；Being provided with a hollow ring (11) on kettle (1) inwall, hollow ring is provided with and still on (11)
The pipeline (12) that body (1) inwall fits, pipeline (12) is provided with multiple liquid outlet (13), described hollow ring (11) with take out
The liquid outlet (13) of liquid pump (8) is connected.
A kind of liquid mixing reactor the most according to claim 1, it is characterised in that: described pipeline (12) and kettle
(1) bottom is perpendicular, and the inwall of kettle (1) is provided with many pipelines (12).
A kind of liquid mixing reactor the most according to claim 1, it is characterised in that: described agitating device (7) includes
Shaft (14), the stirring vane (15) being arranged on shaft (14), stirring vane (15) fills in screw thread and is arranged on shaft
(14) on.
A kind of liquid mixing reactor the most according to claim 1, it is characterised in that: the feed liquor of described drawing liquid pump (8)
Mouth (9) is connected with kettle (1) with liquid discharging tube (17) by liquid suction pipe (16) with liquid outlet (10), liquid suction pipe (16) and kettle
(1) junction is less than the junction of liquid suction pipe (16) with drawing liquid pump (8), and liquid discharging tube (17) is less than with the junction of kettle (1)
Liquid discharging tube (17) and the junction of drawing liquid pump (8).
A kind of liquid mixing reactor the most according to claim 2, it is characterised in that: described pipeline (12) and pipeline
(12) it is connected between.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610872900.4A CN106268449A (en) | 2016-09-30 | 2016-09-30 | A kind of liquid mixing reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610872900.4A CN106268449A (en) | 2016-09-30 | 2016-09-30 | A kind of liquid mixing reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106268449A true CN106268449A (en) | 2017-01-04 |
Family
ID=57716702
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610872900.4A Pending CN106268449A (en) | 2016-09-30 | 2016-09-30 | A kind of liquid mixing reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106268449A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109939635A (en) * | 2019-04-11 | 2019-06-28 | 淄博询知方技术开发有限公司 | A kind of highly effective reaction kettle facilitating sampling |
| CN113908731A (en) * | 2021-10-29 | 2022-01-11 | 江苏优普生物化学科技股份有限公司 | Equipment and method for manufacturing bis (trifluoromethyl) sulfonyl imide lithium with low water content |
-
2016
- 2016-09-30 CN CN201610872900.4A patent/CN106268449A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109939635A (en) * | 2019-04-11 | 2019-06-28 | 淄博询知方技术开发有限公司 | A kind of highly effective reaction kettle facilitating sampling |
| CN113908731A (en) * | 2021-10-29 | 2022-01-11 | 江苏优普生物化学科技股份有限公司 | Equipment and method for manufacturing bis (trifluoromethyl) sulfonyl imide lithium with low water content |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170104 |