CN206199255U - A kind of D Phenylglycine methyl esters hydrochloride synthesis consersion unit - Google Patents
A kind of D Phenylglycine methyl esters hydrochloride synthesis consersion unit Download PDFInfo
- Publication number
- CN206199255U CN206199255U CN201621100979.0U CN201621100979U CN206199255U CN 206199255 U CN206199255 U CN 206199255U CN 201621100979 U CN201621100979 U CN 201621100979U CN 206199255 U CN206199255 U CN 206199255U
- Authority
- CN
- China
- Prior art keywords
- kettle
- probe tube
- consersion unit
- methyl ester
- hydrochloride synthesis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a kind of D Phenylglycine methyl esters hydrochloride synthesis consersion unit, belong to D Phenylglycine methyl ester hydrochloride synthesis consersion unit technical fields, the sampling for solving reactive material in the prior art in reactor is particularly difficult, as equipment is excessive, during reaction initial reaction, reactant grade in the bottom of equipment, so as to cause sampling it is difficult the problems such as.The utility model includes setting ear mount, observation panel, charging aperture, drain hole and heating tube on kettle, kettle, agitating device is set in kettle, multiple probe tubes are provided with the outer wall of kettle,, outwards in 15 45 ° of inclinations, the sampling outlet of each probe tube is higher than a upper probe tube and the junction of kettle for probe tube.The utility model is used for the synthesis of D Phenylglycine methyl ester hydrochlorides.
Description
Technical field
A kind of D-PG methyl ester hydrochloride synthesis consersion unit, for the conjunction of D-PG methyl ester hydrochloride
Into belonging to D-PG methyl ester hydrochloride synthesis consersion unit technical field.
Background technology
The broad understanding of reactor has the rustless steel container for physically or chemically reacting, according to different process conditions demands
The structure design and parameter configuration of container are carried out, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards,
To realize the mixture response function of heating, evaporation, cooling and the low high speed of technological requirement.Pressure vessel must comply with GB150 { steel
Pressing pressure container } standard, non-pressure vessel must comply with the standard of NB/T47003.1-2009 { steel welding non-pressure vessel }.With
Course of reaction in pressure requirements the design requirement of container is also not quite similar.Production must add in strict accordance with corresponding standard
Work, detection and trial operation.Stainless steel cauldron is not quite similar according to different production technologies, operating condition etc., and reactor sets
Meter structure and parameter are different, i.e. the structural style of reactor is different, belongs to nonstandard tankage.
Reactor is combined reaction container, the design according to reaction condition to reactor structure function and configuration annex.From
Charging-reaction-the discharging of beginning can complete pre-set reactions steps with automaticity higher, to reacting
The important parameters such as temperature, pressure, mechanics control (stirring, air blast etc.), reactant/product concentration in journey carry out strict tune
Control.Its structure is typically made up of kettle, transmission device, agitating device, heater, cooling device, sealing device.It is corresponding supporting
Auxiliary equipment：Still, condenser, water knockout drum, collecting tank, filter etc..
Reactor material typically has carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan, Monel) alloy and other composites.
Reactor can be using the manufacture of the stainless steel materials such as SUS304, SUS316L.Agitator has anchor formula, frame, paddle, turbine type, scraper plate
Formula, combined type, rotating mechanism be able to can be met various using cycloidal planetary gear speed reducer, stepless reducer or frequency control etc.
The special reaction requirement of material.Sealing device can be using sealing structures such as mechanical seal, packing seals.Heating, cooling can be used
The structures such as chuck, semicanal, coil pipe, Miller plate, mode of heating has：Steam, electrical heating, conduction oil, with meet acidproof, high temperature resistant,
The technique of the different operating environment such as wear-resistant, anticorrosive needs.And can be designed according to user's technological requirement, manufactured.
In the prior art, the sampling for the reactive material in reactor is particularly difficult, and such as equipment is excessive, and reaction is preliminary anti-
At once, reactant grade is in the bottom of equipment, so as to cause the difficulty of sampling.
The content of the invention
The utility model is set there is provided a kind of D-PG methyl ester hydrochloride synthesis for above-mentioned weak point with reaction
Standby, the sampling for solving reactive material in the prior art in reactor is particularly difficult, and such as equipment is excessive, during reaction initial reaction,
Reactant grade in the bottom of equipment, so as to cause sampling it is difficult the problems such as.
To achieve these goals, the technical solution adopted in the utility model is：
A kind of D-PG methyl ester hydrochloride synthesis consersion unit, including ear mount, observation are set on kettle, kettle
Agitating device is set in mouth, charging aperture, drain hole and heating tube, kettle, it is characterised in that：Multiple is provided with the outer wall of kettle
Probe tube, probe tube is outwards in 15-45 ° of inclination, the connection of the sampling outlet higher than a upper probe tube and kettle of each probe tube
Place.
Further, the ear mount is arranged with gravity sensor.
Further, the agitating device includes agitating shaft, " mouth " the type stirring structure being arranged on agitating shaft, and sets
Undaform stirring structure on agitating shaft and " mouth " type stirring structure.
Further, it is provided with hollow kettle set outside the kettle, kettle puts and is provided with coolant inlet and coolant goes out
Mouthful.
Further, the kettle is provided with a groove for concaving, and probe tube is arranged in groove.
Compared with prior art, the technical solution adopted in the utility model is：
The first, probe tube is set on kettle, can according to residing for reactant kettle height, open corresponding probe tube,
Can quickly be sampled；
2nd, the setting of gravity sensor, can accurate metered reagent weight, there is provided the purity of thing is synthesized；
3rd, by " mouth " type stirring structure and undaform stirring structure, the reactant in kettle that can make is stirred agitating device
That mixes is more uniform；
4th, kettle set be disposed to be easy to reactant that can be quickly by cooling the need in kettle to be cooled down；
5th, groove be disposed to probe tube is set within it, prevent probe tube influence install.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Specific embodiment
The invention will be further described with reference to the accompanying drawings and examples.
Embodiment 1
A kind of D-PG methyl ester hydrochloride synthesis consersion unit, including ear mount 2 is set on kettle 1, kettle 1, is seen
Examine and agitating device 7 is set in mouth 3, charging aperture 4, drain hole 5 and heating tube 6, kettle 1, be provided with multiple on the outer wall of kettle 1 and take
Sample pipe 8, outwards in 15-45 ° of inclination, the sampling outlet of each probe tube 8 is higher than a upper probe tube 8 and the company of kettle 1 for probe tube 8
Meet place.Probe tube is set on kettle, can according to residing for reactant kettle height, open corresponding probe tube, can be quick
It is sampled.
Embodiment 2
A kind of D-PG methyl ester hydrochloride synthesis consersion unit, including ear mount 2 is set on kettle 1, kettle 1, is seen
Examine and agitating device 7 is set in mouth 3, charging aperture 4, drain hole 5 and heating tube 6, kettle 1, be provided with multiple on the outer wall of kettle 1 and take
Sample pipe 8, outwards in 15-45 ° of inclination, the sampling outlet of each probe tube 8 is higher than a upper probe tube 8 and the company of kettle 1 for probe tube 8
Meet place.Probe tube is set on kettle, can according to residing for reactant kettle height, open corresponding probe tube, can be quick
It is sampled.The ear mount 2 is arranged with gravity sensor 9.The setting of gravity sensor, can accurate metered reagent weight
Amount, there is provided the purity of thing is synthesized.
Embodiment 3
A kind of D-PG methyl ester hydrochloride synthesis consersion unit, including ear mount 2 is set on kettle 1, kettle 1, is seen
Examine and agitating device 7 is set in mouth 3, charging aperture 4, drain hole 5 and heating tube 6, kettle 1, be provided with multiple on the outer wall of kettle 1 and take
Sample pipe 8, outwards in 15-45 ° of inclination, the sampling outlet of each probe tube 8 is higher than a upper probe tube 8 and the company of kettle 1 for probe tube 8
Meet place.Probe tube is set on kettle, can according to residing for reactant kettle height, open corresponding probe tube, can be quick
It is sampled.The ear mount 2 is arranged with gravity sensor 9.The setting of gravity sensor, can accurate metered reagent weight
Amount, there is provided the purity of thing is synthesized.The agitating device 7 includes that agitating shaft 11, " mouth " type being arranged on agitating shaft 11 are stirred
Structure 10 is mixed, and is arranged on the undaform stirring structure 12 on agitating shaft 11 and " mouth " type stirring structure 10.Agitating device by
" mouth " type stirring structure and undaform stirring structure, the reactant in kettle that can make, what is be stirred is more uniform.
Embodiment 4
A kind of D-PG methyl ester hydrochloride synthesis consersion unit, including ear mount 2 is set on kettle 1, kettle 1, is seen
Examine and agitating device 7 is set in mouth 3, charging aperture 4, drain hole 5 and heating tube 6, kettle 1, be provided with multiple on the outer wall of kettle 1 and take
Sample pipe 8, outwards in 15-45 ° of inclination, the sampling outlet of each probe tube 8 is higher than a upper probe tube 8 and the company of kettle 1 for probe tube 8
Meet place.Probe tube is set on kettle, can according to residing for reactant kettle height, open corresponding probe tube, can be quick
It is sampled.The ear mount 2 is arranged with gravity sensor 9.The setting of gravity sensor, can accurate metered reagent weight
Amount, there is provided the purity of thing is synthesized.The agitating device 7 includes that agitating shaft 11, " mouth " type being arranged on agitating shaft 11 are stirred
Structure 10 is mixed, and is arranged on the undaform stirring structure 12 on agitating shaft 11 and " mouth " type stirring structure 10.Agitating device by
" mouth " type stirring structure and undaform stirring structure, the reactant in kettle that can make, what is be stirred is more uniform.The kettle
Hollow kettle set 13 is provided with outside 1, coolant inlet 14 and cooling liquid outlet 15 are provided with kettle set 13.
Kettle described in the utility model 1 is provided with a groove 16 for concaving, and probe tube 8 is arranged in groove 16.Groove
Do not wrapped up by kettle set 13.
Claims (5)
1. a kind of D-PG methyl ester hydrochloride synthesis consersion unit, including kettle (1), kettle set ear mount on (1)
(2) agitating device (7), its feature are set in, observation panel (3), charging aperture (4), drain hole (5) and heating tube (6), kettle (1)
It is：Multiple probe tubes (8) are provided with the outer wall of kettle (1), probe tube (8) is outwards in 15-45 ° of inclination, each probe tube
(8) sampling outlet is higher than a upper probe tube (8) and the junction of kettle (1).
2. a kind of D-PG methyl ester hydrochloride synthesis consersion unit according to claim 1, it is characterised in that：Institute
State ear mount (2) and be arranged with gravity sensor (9).
3. a kind of D-PG methyl ester hydrochloride synthesis consersion unit according to claim 1, it is characterised in that：Institute
Stating agitating device (7) includes agitating shaft (11), " mouth " type stirring structure (10) being arranged on agitating shaft (11), and is arranged on
Undaform stirring structure (12) on agitating shaft (11) and " mouth " type stirring structure (10).
4. a kind of D-PG methyl ester hydrochloride synthesis consersion unit according to claim 1, it is characterised in that：Institute
State and be provided with hollow kettle set (13) outside kettle (1), coolant inlet (14) and cooling liquid outlet are provided with kettle set (13)
(15)。
5. a kind of D-PG methyl ester hydrochloride synthesis consersion unit according to claim 1, it is characterised in that：Institute
State kettle (1) and be provided with a groove for concaving (16), probe tube (8) is arranged in groove (16).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621100979.0U CN206199255U (en) | 2016-09-30 | 2016-09-30 | A kind of D Phenylglycine methyl esters hydrochloride synthesis consersion unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621100979.0U CN206199255U (en) | 2016-09-30 | 2016-09-30 | A kind of D Phenylglycine methyl esters hydrochloride synthesis consersion unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206199255U true CN206199255U (en) | 2017-05-31 |
Family
ID=58762029
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621100979.0U Expired - Fee Related CN206199255U (en) | 2016-09-30 | 2016-09-30 | A kind of D Phenylglycine methyl esters hydrochloride synthesis consersion unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206199255U (en) |
-
2016
- 2016-09-30 CN CN201621100979.0U patent/CN206199255U/en not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107551955A (en) | A kind of chemical industry reaction agitating device of separation of solid and liquid charging | |
| CN202683216U (en) | Industrial large reaction kettle device for preparing graphene | |
| CN204051668U (en) | A kind of efficient coating reaction still | |
| CN102744028A (en) | Industrial large-scale reaction vessel for preparing graphene | |
| CN201664609U (en) | Mixing reaction pot | |
| CN206435189U (en) | A kind of stirred reactor | |
| CN206199255U (en) | A kind of D Phenylglycine methyl esters hydrochloride synthesis consersion unit | |
| CN207187757U (en) | A kind of experimental rig for being used to prepare ternary precursor | |
| CN106268449A (en) | A kind of liquid mixing reactor | |
| CN102872778A (en) | Stirring equipment for production of raw material medicament | |
| CN206199214U (en) | A kind of measuring tank in isotretinoin production technology | |
| CN206199096U (en) | A kind of liquid mixing reactor | |
| CN106268592A (en) | A kind of D Phenylglycine methyl ester hydrochlorate synthesis consersion unit | |
| CN205435742U (en) | High -efficient simplification worker reation kettle | |
| CN102908966B (en) | Environment-friendly liquid circulation reactor | |
| CN211051383U (en) | Sulfuric acid process titanium dioxide alkali dissolving tank | |
| CN206199252U (en) | A kind of reactor for being easy to discharging powder | |
| CN208554164U (en) | It is a kind of for producing the jacket reactor of unsaturated polyester resin | |
| CN204074070U (en) | Vacuum rapid dispersion reactor | |
| CN209155845U (en) | A kind of chemical reaction kettle | |
| CN204147835U (en) | Solid reaction still | |
| CN204174118U (en) | A kind of specific equipment of industrial producing urea ammonium nitrate solution | |
| CN206366379U (en) | It is a kind of to detect the stirring-type reaction kettle of kettle material actual temperature | |
| CN207463217U (en) | A kind of sulfonating reaction kettle for being used to produce sildenafil intermediate | |
| CN206139194U (en) | External recycling production device of non -ion surfactant |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170531 Termination date: 20190930 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |