CN202683216U - Industrial large reaction kettle device for preparing graphene - Google Patents
Industrial large reaction kettle device for preparing graphene Download PDFInfo
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- CN202683216U CN202683216U CN201220294865XU CN201220294865U CN202683216U CN 202683216 U CN202683216 U CN 202683216U CN 201220294865X U CN201220294865X U CN 201220294865XU CN 201220294865 U CN201220294865 U CN 201220294865U CN 202683216 U CN202683216 U CN 202683216U
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- reaction bulb
- reaction
- industrial preparation
- reaction kettle
- reactor device
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Abstract
The utility model relates to an industrial large reaction kettle device for preparing graphene. The industrial large reaction kettle device comprises a shaft seal device, a transmission device, a protection support frame (2), a gas collection bottle (8), a frequency control stirrer (6) and a temperature tube. A reaction bottle (1) is arranged on the protection support frame (2), the reaction bottle (1) is externally connected with a thermostatic bath (3), feeding ports (4) and a tail gas discharging port (5) are arranged in the upper part of the reaction bottle (1), and a discharging port (13) is arranged in the lower part of the reaction bottle (1). The industrial large reaction kettle device is capable of automatically controlling the reaction temperature, the stirring rotating speed and the constant temperature state in a total process of preparing the graphene oxide. A plurality of feeding holes can avoid pollution among different raw materials. The industrial large reaction kettle device has the advantages of wide constant temperature range, large volume and compact structure, and is a container suitable for large-dosage physical and chemical reactions.
Description
Affiliated technical field
The utility model relates to a kind of container for physics or chemical reaction, especially a kind of industrial reactor device for the graphene oxide preparation.
Background technology
At present, the reactor material generally is carbon manganese steel, stainless steel, zirconium, nickel-base alloy and other composite, the agitator rotating mechanism is cycloidal planetary gear speed reducer, electrodeless variable-speed reductor etc., and the volume of reactor is less also, and the constant temperature scope is minimum can only be for above freezing.
Summary of the invention
The prior art material corrosion is poor in order to solve, the difficult control of mixing speed, reactor volume
The problem such as less than normal, the utility model provides a kind of large-size reactor device of industrial preparation Graphene, and it can use under the deep-etching condition, and overall process is controlled automatically, adapts to the requirement of producing in enormous quantities.
For reaching above purpose, the technical scheme that its technical problem that solves the utility model adopts is: a kind of large-size reactor device of industrial preparation Graphene, comprise gland seal device, transmission device, the ballistic support framework, the gas collection bottle, on the described ballistic support framework reaction bulb is housed, the external thermostat of reaction bulb, reaction bulb top is provided with charge door, exhaust port, the bottom is provided with feed opening, described reaction bulb is double-decker, the centre is provided with interlayer, be provided with the frequency control agitator in the reaction bulb, temperature tube, described frequency control agitator is provided with the digital display rotational speed device, temperature tube is provided with the temperature digital-display watch-dog, is connected by condenser pipe between exhaust port and gas collection bottle.
Be connected by pipeline between thermostat described in the utility model and the reaction bulb interlayer, the whole internal circulation system that forms is provided with thermostatic medium in the interlayer, and the constant temperature controlled range is between subzero tens degree are spent to more than 100; Reaction bulb adopts resistant material to make, volume 5L～50L, and the reaction bulb profile is geometry; The reaction bulb material is Pyrex, and profile is cylindrical or spherical; 20 ℃～100 ℃ of thermostatic medium constant temperature Fan Wei –; Charging valve is housed, 2～3 of charge door operated by rotary motion, but reinforcing body or liquid on the charge door; The frequency control agitator comprises a shaft, an AC induction motor and a digital display rotational speed device, mixing speed 60-1000rpm.
The utility model fitted shaft seal apparatus, transmission device are realized the technological requirement that graphene oxide prepares.
Adopt above technical scheme, the beneficial effects of the utility model are: the large-size reactor device of the industrial preparation Graphene that provides, can automatically control reaction temperature, speed of agitator, temperature constant state that graphene oxide prepares in the overall process, a plurality of charge doors being set can avoiding pollution between the different material, also is the container of a kind of suitable heavy dose of physics, chemical reaction simultaneously.
Description of drawings
Below in conjunction with accompanying drawing the utility model is further described.
Fig. 1 is the utility model structural representation.
The specific embodiment
According to shown in Figure 1, the large-size reactor device of a kind of industrial preparation Graphene of the utility model, comprise gland seal device, transmission device, ballistic support framework 2, gas collection bottle 8, on the described ballistic support framework 2 reaction bulb 1 is housed, the external thermostat 3 of reaction bulb 1 interlayer, thermostat 3 passes into Cooling and Heat Source by pipeline and plays the circulating reflux effect in the interlayer for Cooling and Heat Source being freezed or heating, the temperature in the control reaction bulb 1.Temperature range is-20 degrees centigrade to 100 degrees centigrade.
Described in the utility model Reaction bulb 1 top is provided with charge door 4, exhaust port 5, charge door 4 mainly is for the passage that adds reaction raw materials toward reaction bulb 1, can by reinforced speed and the quantity of charging valve control, can also add toward the mouth of pipe solid material of liquid or molecule.As: graphite powder, sulfuric acid, potassium permanganate, hydrogen peroxide etc.Charge door 4 generally is provided with 2-3, can avoid the pollution between the different material.Exhaust port 5 is to begin the various gases that produce to terminal procedure for discharging from reaction, comprises toxic and harmful, and tail gas enters that gas collection bottle 8 is interior to be absorbed by water after through condenser pipe 9 reflux condensation modes.Be furnished with a shaft and an AC induction motor and a digital display rotational speed device 10 on the frequency control agitator 6, rotate by the driven by motor shaft.Be mainly used in reaction bulb 1 internal reaction raw material is stirred, make between each raw material contact full and uniform, reaction thoroughly.Also play simultaneously the function of heat radiation.By digital display rotational speed device 10 knobs can the Artificial Control shaft the rotating speed speed, show simultaneously the Digital size of rotating speed, intuitively easy.Use in service steadily reliably, the stirring dynamics is strong, no-spark, but continuity work.Mixing speed: 60-1000rpm.
Described reaction bulb 1 is double-decker, the centre is provided with interlayer, be provided with frequency control agitator 6, temperature tube 7 in the reaction bulb 1, described frequency control agitator 6 is provided with digital display rotational speed device 10, temperature tube 7 is provided with temperature digital-display watch-dog 11, and temperature tube stretches in the reaction bulb and immerses reaction media inside.In time monitor the temperature of reactant liquor inside, and by the accurate displays temperature numerical value of intelligent digital.8 in exhaust port 5 and gas collection bottle are connected by condenser pipe 9.
Be connected by pipeline between thermostat 3 described in the utility model and reaction bulb 1 interlayer, the whole internal circulation system that forms is provided with thermostatic medium 12 in reaction bulb 1 interlayer, and the constant temperature controlled range is between subzero tens degree are spent to more than 100; Described reaction bulb 1 adopts resistant material to make, and volume is 5L～50L, and reaction bulb 1 profile is geometry; Described reaction bulb 1 material is Pyrex, and profile is cylindrical or spherical; On the charge door 4 charging valve is housed, charge door 4 is set to 2～3, but reinforcing body or liquid.
The utility model ballistic support framework 2 is with the horn ring of stopping, and is convenient mobile.Ballistic support framework 2 supports reaction bulb 1, and reaction bulb 1 is used for dress collection reaction raw materials, is the place that whole course of reaction is carried out.Its material generally adopts Pyrex, has good physics, chemical property.The appearance and size variation, volume capacity can expand several decaliters to from several liters, reactionless dead angle.At its outside vial that also has the identical material of one deck, form an interlayer with internal layer, can pass through Cooling and Heat Source (water, ethanol, freezing liquid, heat conduction wet goods) circulation, make reaction bulb 1 realize heated at constant temperature or cooling reaction.
The utility model reaction bulb 1 bottom is provided with feed opening 13, mainly is after finishing for whole production process, to emit the passage that generates raw material, can discharge smoothly dope and trace solid.
Claims (6)
1. the large-size reactor device of an industrial preparation Graphene, comprise gland seal device, transmission device, ballistic support framework (2), gas collection bottle (8), it is characterized in that: reaction bulb (1) is housed on the described ballistic support framework (2), the external thermostat of reaction bulb (1) (3), reaction bulb (1) top is provided with charge door (4), exhaust port (5), the bottom is provided with feed opening (13), described reaction bulb (1) is double-decker, the centre is provided with interlayer, be provided with frequency control agitator (6) in the reaction bulb (1), temperature tube (7), described frequency control agitator (6) is provided with digital display rotational speed device (10), temperature tube (7) is provided with temperature digital-display watch-dog (11), is connected by condenser pipe (9) between exhaust port (5) and gas collection bottle (8).
2. the large-size reactor device of a kind of industrial preparation Graphene according to claim 1, it is characterized in that: be connected by pipeline between thermostat (3) and reaction bulb (1) interlayer, the whole internal circulation system that forms, be provided with thermostatic medium (12) in reaction bulb (1) interlayer, the constant temperature controlled range is between subzero tens degree are spent to more than 100.
3. the large-size reactor device of a kind of industrial preparation Graphene according to claim 1 is characterized in that: described reaction bulb (1) adopts resistant material to make, and volume is 5L～50L.
4. according to claim 1 or the large-size reactor device of 3 described a kind of industrial preparation Graphenes, it is characterized in that: described reaction bulb (1) material is Pyrex, and profile is cylindrical or spherical.
5. the large-size reactor device of a kind of industrial preparation Graphene according to claim 1, it is characterized in that: charge door is equipped with charging valve on (4), and charge door (4) is set to 2～3, but reinforcing body or liquid.
6. the large-size reactor device of a kind of industrial preparation Graphene according to claim 1, it is characterized in that: frequency control agitator (6) comprises shaft, AC induction motor and digital display rotational speed device, mixing speed 60-1000rpm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201220294865XU CN202683216U (en) | 2012-06-21 | 2012-06-21 | Industrial large reaction kettle device for preparing graphene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201220294865XU CN202683216U (en) | 2012-06-21 | 2012-06-21 | Industrial large reaction kettle device for preparing graphene |
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| Publication Number | Publication Date |
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| CN202683216U true CN202683216U (en) | 2013-01-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201220294865XU Expired - Lifetime CN202683216U (en) | 2012-06-21 | 2012-06-21 | Industrial large reaction kettle device for preparing graphene |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102744028A (en) * | 2012-06-21 | 2012-10-24 | 泰州巨纳新能源有限公司 | Industrial large-scale reaction vessel for preparing graphene |
| CN104722261A (en) * | 2015-04-15 | 2015-06-24 | 南通晨光石墨设备有限公司 | Agitating mechanism for graphite reaction kettle |
| CN106943979A (en) * | 2017-05-11 | 2017-07-14 | 河南欣博矿山装备技术有限公司 | A kind of synthesizer of esterified hydramine |
| CN108408722A (en) * | 2018-06-05 | 2018-08-17 | 李训祺 | A kind of graphene oxide preparation method |
| CN108455589A (en) * | 2018-06-05 | 2018-08-28 | 李训祺 | A kind of graphene oxide prepares reaction kettle |
| CN108483436A (en) * | 2018-06-12 | 2018-09-04 | 杨柳 | A kind of technical grade graphene oxide process units |
| CN110385095A (en) * | 2019-07-15 | 2019-10-29 | 刘彦杰 | A kind of confined reaction device of the good seal performance for graphene production |
-
2012
- 2012-06-21 CN CN201220294865XU patent/CN202683216U/en not_active Expired - Lifetime
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102744028A (en) * | 2012-06-21 | 2012-10-24 | 泰州巨纳新能源有限公司 | Industrial large-scale reaction vessel for preparing graphene |
| CN104722261A (en) * | 2015-04-15 | 2015-06-24 | 南通晨光石墨设备有限公司 | Agitating mechanism for graphite reaction kettle |
| CN104722261B (en) * | 2015-04-15 | 2016-04-27 | 南通晨光石墨设备有限公司 | A kind of graphite reactor rabbling mechanism |
| CN106943979A (en) * | 2017-05-11 | 2017-07-14 | 河南欣博矿山装备技术有限公司 | A kind of synthesizer of esterified hydramine |
| CN108408722A (en) * | 2018-06-05 | 2018-08-17 | 李训祺 | A kind of graphene oxide preparation method |
| CN108455589A (en) * | 2018-06-05 | 2018-08-28 | 李训祺 | A kind of graphene oxide prepares reaction kettle |
| CN108483436A (en) * | 2018-06-12 | 2018-09-04 | 杨柳 | A kind of technical grade graphene oxide process units |
| CN110385095A (en) * | 2019-07-15 | 2019-10-29 | 刘彦杰 | A kind of confined reaction device of the good seal performance for graphene production |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20130123 |