CN204147835U - Solid reaction still - Google Patents
Solid reaction still Download PDFInfo
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- CN204147835U CN204147835U CN201420492424.XU CN201420492424U CN204147835U CN 204147835 U CN204147835 U CN 204147835U CN 201420492424 U CN201420492424 U CN 201420492424U CN 204147835 U CN204147835 U CN 204147835U
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Abstract
The utility model provides a kind of solid reaction still, comprises reaction boat and reactor body, and reaction boat is by expecting that boat and splash-back form, material boat two ends arrange pulley, and pulley is wound with electric wire, and electric wire one end is provided with the connector of conduction, the electric wire other end is placed in material boat, and splash-back is placed on material boat; Reactor body comprises still chamber and still door, and still cavity wall both sides arrange electrode rod, and in still chamber, opening surrounding arranges sealing ring, and in still chamber arranged outside igniter, bottom, still chamber arranges blast pipe, and blast pipe arranges air bleeding valve.The beneficial effects of the utility model are: solve the problem that reaction kettle for reaction thing is necessary for liquid, provide a kind of reactor that can be used for solid reaction; This reactor arranges vavuum pump and Pressure gauge; reaction can be carried out under pressure, and this reactor is also provided with intake valve and gas cylinder, after evacuation; open intake valve and be filled with protective gas in reactor, thus avoid the impact that the oxygen in air reacts some.
Description
Technical field
The utility model relates to field of chemical equipment, more specifically to a kind of solid reaction still.
Background technology
The broad understanding of reactor is the rustless steel container having physics or chemical reaction, structural design and the parameter configuration of container is carried out according to different process conditions demands, design condition, process, inspection and manufacture, examination need according to Its Relevant Technology Standards, to realize the mixture response function of the heating of technological requirement, evaporation, cooling and low high speed.Pressure vessel must follow the standard of GB150 (GB150-1998), and non-pressure vessel must follow the standard of NB/T47003.1-2009 (steel welding non-pressure vessel).The designing requirement of pressure requirements thereupon in course of reaction to container is also not quite similar.Production must process, detects and try out in strict accordance with corresponding standard.Stainless steel cauldron is not quite similar according to different production technologies, operating condition etc., and the project organization of reactor and parameter difference, namely the structural style of reactor is different, belongs to nonstandard tankage.
Reactor is combined reaction container, according to reaction condition to reactor structure function and the design configuring annex.From charging-reaction-discharging all can complete pre-set reactions steps with higher automaticity, the temperature in course of reaction, pressure, mechanics are controlled to the important parameter such as (stirring, air blast etc.), reactant/product concentration and carry out strict regulation and control.Its structure is generally made up of kettle, transmission device, agitating device, heater, cooling device, sealing device.Corresponding supporting auxiliary equipment: still, condenser, water knockout drum, collecting tank, filter etc.
Reactor material generally has carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan, Monel) alloy and other composite.Reactor can adopt the stainless steel material manufactures such as SUS304, SUS316L.Agitator has anchor formula, frame, paddle, turbine type, scraper-type, combined type, and rotating mechanism can adopt cycloidal planetary gear speed reducer, stepless reducer or frequency control etc., can meet the special reaction requirement of various material.Sealing device can adopt the hermetically-sealed construction such as mechanical seal, packing seal.Heating, cooling can adopt the structures such as chuck, semicanal, coil pipe, Miller plate, and mode of heating has: steam, electrical heating, conduction oil, to meet the technique needs of the different operating environment such as acidproof, high temperature resistant, wear-resistant, anticorrosive.And can carry out designing, manufacturing according to user's technological requirement.
All with the agitating device for stirring reaction liquid in existing reactor, although agitating device can make reactant liquor mix more fully and react under given conditions, but, if when reactant is solid, this solid is configured to the reactant liquor that can be placed in reactor, the man power and material of the first waste configures corresponding reactant liquor, second this reaction reacts more abundant under solid conditions, and reaction rate is higher, and after this solid is configured to reactant liquor, the reaction rate of this reaction declines, the yield of reaction reduces, thus cause the raising of entreprise cost, if the 3rd this solid is water insoluble, then cannot react in a kettle..
Utility model content
The utility model overcomes deficiency of the prior art, provides a kind of solid reaction still.
The purpose of this utility model is achieved by following technical proposals:
Solid reaction still, comprises reaction boat and reactor body; Described reaction boat forms by for the material boat of placing response thing and the splash-back for preventing reactant in course of reaction from spilling, described material boat two ends are provided with pulley, described pulley is wound with electric wire, described electric wire one end is provided with the connector of conduction, the described electric wire other end is placed in described material boat, and described splash-back is placed on described material boat; Described reactor body comprises still chamber and still door, described still cavity wall both sides are provided with the electrode rod for being connected with described connector, in described still chamber, opening surrounding is provided with sealing ring, in described still chamber, arranged outside has igniter, bottom, described still chamber is provided with the blast pipe for getting rid of air in reactor, and described blast pipe is provided with air bleeding valve.
On the left of described reactor, be provided with bleeding point, described bleeding point is connected by the first pipeline with vavuum pump, and described first pipeline is provided with vacuum pumping valve.
On the right side of described reactor, be provided with air inlet, described air inlet is connected with gas cylinder by the second pipeline, and described second pipeline is provided with intake valve.
Be provided with dust plug in described first pipeline and described second pipeline, described dust plug skin is coated with gauze.
The pressure sensor for monitoring reacting kettle inner pressure is provided with in described reactor.
Described igniter is provided with the ammeter for detecting reactant whether successful ignition.
Described still chamber arranged outside has the cooling water switch for cooling described still chamber.
The beneficial effects of the utility model are: compared with existing reactor, and the utility model solves the problem that must be liquid of reaction kettle for reaction thing, provide a kind of reactor that can be used for solid reaction; Vavuum pump and Pressure gauge is provided with in the utility model; reaction can be carried out under pressure; and this reactor is also provided with intake valve and gas cylinder; can be after evacuation; open intake valve and be filled with protective gas in reactor, thus avoid the impact that the oxygen in air reacts some.
Accompanying drawing explanation
Fig. 1 is the structural representation reacting boat in the utility model;
Fig. 2 is the structural representation of the utility model reactor.
In figure: 1, expect boat, 2, pulley, 3, electric wire, 4, connector, 5, splash-back, 6, still chamber, 7, sealing ring, 8, pressure sensor, 9, igniter, 10, vavuum pump, 11, vacuum pumping valve, 12, gas cylinder, 13, intake valve, 14, exhaust-valve, 15, electrode rod.
Detailed description of the invention
Below by specific embodiment, the technical solution of the utility model is further described.
Embodiment 1
Solid reaction still, comprises reaction boat and reactor body, and reaction boat is by expecting that boat 1 and splash-back 5 form, material boat 1 two ends are provided with pulley 2, and pulley 2 is wound with electric wire 3, electric wire 3 one end is provided with the connector 4 of conduction, electric wire 3 other end is placed in material boat 1, and splash-back 5 is placed on material boat 1; Reactor body comprises still chamber 6 and still door, inwall both sides, still chamber 6 are provided with the electrode rod 15 be connected with connector 4, in still chamber 6, opening surrounding is provided with sealing ring 7, in still chamber 6, arranged outside has igniter 9, bottom, still chamber 6 is provided with exhaust outlet, exhaust ports is provided with air bleeding valve 14, is provided with bleeding point on the left of reactor, bleeding point is connected by the first pipeline with vavuum pump 10, and the first pipeline is provided with vacuum pumping valve 11.
Embodiment 2
Solid reaction still, comprises reaction boat and reactor body, and reaction boat is by expecting that boat 1 and splash-back 5 form, material boat 1 two ends are provided with pulley 2, and pulley 2 is wound with electric wire 3, electric wire 3 one end is provided with the connector 4 of conduction, electric wire 3 other end is placed in material boat 1, and splash-back 5 is placed on material boat 1; Reactor body comprises still chamber 6 and still door, inwall both sides, still chamber 6 are provided with the electrode rod 15 be connected with connector 4, in still chamber 6, opening surrounding is provided with sealing ring 7, in still chamber 6, arranged outside has igniter 9, bottom, still chamber 6 is provided with exhaust outlet, exhaust ports is provided with air bleeding valve 14, bleeding point is provided with on the left of reactor, bleeding point is connected by the first pipeline with vavuum pump 10, first pipeline is provided with vacuum pumping valve 11, be provided with air inlet on the right side of reactor, air inlet is connected with gas cylinder 12 by the second pipeline, the second pipeline is provided with intake valve 13.
Embodiment 3
Solid reaction still, comprises reaction boat and reactor body, and reaction boat is by expecting that boat 1 and splash-back 5 form, material boat 1 two ends are provided with pulley 2, and pulley 2 is wound with electric wire 3, electric wire 3 one end is provided with the connector 4 of conduction, electric wire 3 other end is placed in material boat 1, and splash-back 5 is placed on material boat 1, reactor body comprises still chamber 6 and still door, inwall both sides, still chamber 6 are provided with the electrode rod 15 be connected with connector 4, in still chamber 6, opening surrounding is provided with sealing ring 7, in still chamber 6, arranged outside has igniter 9, bottom, still chamber 6 is provided with exhaust outlet, exhaust ports is provided with air bleeding valve 14, bleeding point is provided with on the left of reactor, bleeding point is connected by the first pipeline with vavuum pump 10, first pipeline is provided with vacuum pumping valve 11, air inlet is provided with on the right side of reactor, air inlet is connected with gas cylinder 12 by the second pipeline, second pipeline is provided with intake valve 13, the dust plug of outer layer covers gauze is provided with in the first pipeline and the second pipeline, the pressure sensor 8 for monitoring reacting kettle inner pressure is provided with in reactor, still chamber arranged outside has the cooling water switch for cooling reactor chamber.
Igniter 9 is provided with the ammeter for detecting reactant whether successful ignition.
Solid reaction still in the present embodiment solves the problem being liquid of reaction kettle for reaction thing, provides a kind of reactor that can be used for solid reaction.
Solid reaction still in the present embodiment is provided with vavuum pump and Pressure gauge, and reaction can be carried out under pressure.
Solid reaction still in the present embodiment is also provided with intake valve and gas cylinder, after evacuation, can open intake valve and be filled with protective gas in reactor, thus avoids the impact that the oxygen in air reacts some.
Above three embodiments of the present utility model have been described in detail, but described content being only preferred embodiment of the present utility model, can not being considered to for limiting practical range of the present utility model.All equalizations done according to the utility model application range change and improve, and all should still belong within patent covering scope of the present utility model.
Claims (7)
1. solid reaction still, it is characterized in that: comprise reaction boat and reactor body, described reaction boat forms by for the material boat of placing response thing and the splash-back for preventing reactant in course of reaction from spilling, described material boat two ends are provided with pulley, described pulley is wound with electric wire, described electric wire one end is provided with the connector of conduction, and the described electric wire other end is placed in described material boat, and described splash-back is placed on described material boat; Described reactor body comprises still chamber and still door, described still cavity wall both sides are provided with the electrode rod for being connected with described connector, in described still chamber, opening surrounding is provided with sealing ring, in described still chamber, arranged outside has igniter, bottom, described still chamber is provided with the blast pipe for getting rid of air in reactor, and described blast pipe is provided with air bleeding valve.
2. solid reaction still according to claim 1, it is characterized in that: on the left of described reactor, be provided with bleeding point, described bleeding point is connected by the first pipeline with vavuum pump, and described first pipeline is provided with vacuum pumping valve.
3. solid reaction still according to claim 2, is characterized in that: on the right side of described reactor, be provided with air inlet, and described air inlet is connected with gas cylinder by the second pipeline, and described second pipeline is provided with intake valve.
4. solid reaction still according to claim 3, is characterized in that: be provided with dust plug in described first pipeline and described second pipeline, described dust plug skin is coated with gauze.
5., according to the arbitrary described solid reaction still of Claims 1-4, it is characterized in that: in described reactor, be provided with the pressure sensor for monitoring reacting kettle inner pressure.
6. according to the arbitrary described solid reaction still of Claims 1-4, it is characterized in that: described igniter is provided with the ammeter for detecting reactant whether successful ignition.
7., according to the arbitrary described solid reaction still of Claims 1-4, it is characterized in that: described still chamber arranged outside has the cooling water switch for cooling described still chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420492424.XU CN204147835U (en) | 2014-08-29 | 2014-08-29 | Solid reaction still |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420492424.XU CN204147835U (en) | 2014-08-29 | 2014-08-29 | Solid reaction still |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204147835U true CN204147835U (en) | 2015-02-11 |
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ID=52505988
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420492424.XU Expired - Fee Related CN204147835U (en) | 2014-08-29 | 2014-08-29 | Solid reaction still |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204147835U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105214565A (en) * | 2015-10-28 | 2016-01-06 | 太仓东能环保设备有限公司 | A kind of vacuum still tail gas unit |
| CN109266822A (en) * | 2018-11-19 | 2019-01-25 | 中国科学院地球化学研究所 | Rapid quenching minitype high voltage kettle |
-
2014
- 2014-08-29 CN CN201420492424.XU patent/CN204147835U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105214565A (en) * | 2015-10-28 | 2016-01-06 | 太仓东能环保设备有限公司 | A kind of vacuum still tail gas unit |
| CN109266822A (en) * | 2018-11-19 | 2019-01-25 | 中国科学院地球化学研究所 | Rapid quenching minitype high voltage kettle |
| CN109266822B (en) * | 2018-11-19 | 2023-11-24 | 中国科学院地球化学研究所 | Small-sized autoclave for rapid quenching |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150211 Termination date: 20160829 |