CN204147842U - Solid reaction still body - Google Patents

Solid reaction still body Download PDF

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Publication number
CN204147842U
CN204147842U CN201420492986.4U CN201420492986U CN204147842U CN 204147842 U CN204147842 U CN 204147842U CN 201420492986 U CN201420492986 U CN 201420492986U CN 204147842 U CN204147842 U CN 204147842U
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CN
China
Prior art keywords
still
solid reaction
reactor
pipeline
chamber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420492986.4U
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Chinese (zh)
Inventor
刘建
刘伟
李力
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TIANJIN DEVELOPMENT ZONES XINDA CHEMICAL TECHNOLOGY DEVELOPMENT Co Ltd
Original Assignee
TIANJIN DEVELOPMENT ZONES XINDA CHEMICAL TECHNOLOGY DEVELOPMENT Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by TIANJIN DEVELOPMENT ZONES XINDA CHEMICAL TECHNOLOGY DEVELOPMENT Co Ltd filed Critical TIANJIN DEVELOPMENT ZONES XINDA CHEMICAL TECHNOLOGY DEVELOPMENT Co Ltd
Priority to CN201420492986.4U priority Critical patent/CN204147842U/en
Application granted granted Critical
Publication of CN204147842U publication Critical patent/CN204147842U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model provides a kind of solid reaction still body, comprise still chamber and still door, still cavity wall both sides are provided with electrode rod, in still chamber, opening surrounding is provided with sealing ring, in still chamber, arranged outside has igniter, bottom, still chamber is provided with the blast pipe for getting rid of air in reactor, and blast pipe is provided with air bleeding valve.The beneficial effects of the utility model are: compared with existing reactor body, and the utility model solves the problem that must be liquid of reaction kettle for reaction thing, provide a kind of reactor body that can be used for solid reaction; Vavuum pump and Pressure gauge is provided with in the utility model; reaction can be carried out under pressure; and this reactor body is also provided with intake valve and gas cylinder; can be after evacuation; open intake valve and be filled with protective gas in reactor body, thus avoid the impact that the oxygen in air reacts some.

Description

Solid reaction still body
Technical field
The utility model relates to field of chemical equipment, more specifically to a kind of solid reaction still body.
Background technology
The broad understanding of reactor is the rustless steel container having physics or chemical reaction, structural design and the parameter configuration of container is carried out according to different process conditions demands, design condition, process, inspection and manufacture, examination need according to Its Relevant Technology Standards, to realize the mixture response function of the heating of technological requirement, evaporation, cooling and low high speed.Pressure vessel must follow the standard of GB150 (GB150-1998), and non-pressure vessel must follow the standard of NB/T47003.1-2009 (steel welding non-pressure vessel).The designing requirement of pressure requirements thereupon in course of reaction to container is also not quite similar.Production must process, detects and try out in strict accordance with corresponding standard.Stainless steel cauldron is not quite similar according to different production technologies, operating condition etc., and the project organization of reactor and parameter difference, namely the structural style of reactor is different, belongs to nonstandard tankage.
Reactor is combined reaction container, according to reaction condition to reactor structure function and the design configuring annex.From charging-reaction-discharging all can complete pre-set reactions steps with higher automaticity, the temperature in course of reaction, pressure, mechanics are controlled to the important parameter such as (stirring, air blast etc.), reactant/product concentration and carry out strict regulation and control.Its structure is generally made up of kettle, transmission device, agitating device, heater, cooling device, sealing device.Corresponding supporting auxiliary equipment: still, condenser, water knockout drum, collecting tank, filter etc.
Reactor material generally has carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan, Monel) alloy and other composite.Reactor can adopt the stainless steel material manufactures such as SUS304, SUS316L.Agitator has anchor formula, frame, paddle, turbine type, scraper-type, combined type, and rotating mechanism can adopt cycloidal planetary gear speed reducer, stepless reducer or frequency control etc., can meet the special reaction requirement of various material.Sealing device can adopt the hermetically-sealed construction such as mechanical seal, packing seal.Heating, cooling can adopt the structures such as chuck, semicanal, coil pipe, Miller plate, and mode of heating has: steam, electrical heating, conduction oil, to meet the technique needs of the different operating environment such as acidproof, high temperature resistant, wear-resistant, anticorrosive.And can carry out designing, manufacturing according to user's technological requirement.
All with the agitating device for stirring reaction liquid in existing reactor, although agitating device can make reactant liquor mix more fully and react under given conditions, but, if when reactant is solid, this solid is configured to the reactant liquor that can be placed in reactor, the man power and material of the first waste configures corresponding reactant liquor, second this reaction reacts more abundant under solid conditions, and reaction rate is higher, and after this solid is configured to reactant liquor, the reaction rate of this reaction declines, the yield of reaction reduces, thus cause the raising of entreprise cost, if the 3rd this solid is water insoluble, then cannot react in a kettle..
Utility model content
The utility model overcomes deficiency of the prior art, provides a kind of solid reaction still body.
The purpose of this utility model is achieved by following technical proposals:
Solid reaction still body, comprise still chamber and still door, described still cavity wall both sides are provided with electrode rod, in described still chamber, opening surrounding is provided with sealing ring, in described still chamber, arranged outside has igniter, bottom, described still chamber is provided with the blast pipe for getting rid of air in reactor, and described blast pipe is provided with air bleeding valve.
On the left of described reactor, be provided with bleeding point, described bleeding point is connected by the first pipeline with vavuum pump, and described first pipeline is provided with vacuum pumping valve.
On the right side of described reactor, be provided with air inlet, described air inlet is connected with gas cylinder by the second pipeline, and described second pipeline is provided with intake valve.
Be provided with dust plug in described first pipeline and described second pipeline, described dust plug skin is coated with gauze.
The pressure sensor for monitoring reacting kettle inner pressure is provided with in described reactor.
Described igniter is provided with the ammeter for detecting reactant whether successful ignition.
Described still chamber arranged outside has the cooling water switch for cooling described still chamber.
The beneficial effects of the utility model are: compared with existing reactor body, and the utility model solves the problem that must be liquid of reaction kettle for reaction thing, provide a kind of reactor body that can be used for solid reaction; Vavuum pump and Pressure gauge is provided with in the utility model; reaction can be carried out under pressure; and this reactor body is also provided with intake valve and gas cylinder; can be after evacuation; open intake valve and be filled with protective gas in reactor body, thus avoid the impact that the oxygen in air reacts some.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1, still chamber, 2, sealing ring, 3, pressure sensor, 4, igniter, 5, vavuum pump, 6, vacuum pumping valve, 7, gas cylinder, 8, intake valve, 9, air bleeding valve, 10, electrode rod.
Detailed description of the invention
Below by specific embodiment, the technical solution of the utility model is further described.
Embodiment 1
Solid reaction still body, comprise still chamber 1 and still door, inwall both sides, still chamber 1 are provided with electrode rod 10, in still chamber 1, opening surrounding is provided with sealing ring 2, and in still chamber 1, arranged outside has igniter 4, and bottom, still chamber 1 is provided with exhaust outlet, exhaust ports is provided with air bleeding valve 9, be provided with bleeding point on the left of reactor, bleeding point is connected by the first pipeline with vavuum pump 5, and the first pipeline is provided with vacuum pumping valve 6.
Embodiment 2
Solid reaction still body, comprise still chamber 1 and still door, inwall both sides, still chamber 1 are provided with electrode rod 10, in still chamber 1, opening surrounding is provided with sealing ring 2, in still chamber 1, arranged outside has igniter 4, bottom, still chamber 1 is provided with exhaust outlet, exhaust ports is provided with air bleeding valve 9, bleeding point is provided with on the left of reactor, bleeding point is connected by the first pipeline with vavuum pump 5, the first pipeline is provided with vacuum pumping valve 6, is provided with air inlet on the right side of reactor, air inlet is connected with gas cylinder 7 by the second pipeline, the second pipeline is provided with intake valve 8.
Embodiment 3
Solid reaction still body, comprise still chamber 1 and still door, inwall both sides, still chamber 1 are provided with electrode rod 10, in still chamber 1, opening surrounding is provided with sealing ring 2, in still chamber 1, arranged outside has igniter 4, bottom, still chamber 1 is provided with exhaust outlet, exhaust ports is provided with air bleeding valve 9, bleeding point is provided with on the left of reactor, bleeding point is connected by the first pipeline with vavuum pump 5, first pipeline is provided with vacuum pumping valve 6, air inlet is provided with on the right side of reactor, air inlet is connected with gas cylinder 7 by the second pipeline, second pipeline is provided with intake valve 8, the dust plug of outer layer covers gauze is provided with in the first pipeline and the second pipeline, the pressure sensor 3 for monitoring reacting kettle inner pressure is provided with in reactor, still chamber arranged outside has the cooling water switch for cooling reactor chamber.
Igniter 4 is provided with the ammeter for detecting reactant whether successful ignition.
Solid reaction still in the present embodiment solves the problem being liquid of reaction kettle for reaction thing, provides a kind of reactor that can be used for solid reaction.
Solid reaction still in the present embodiment is provided with vavuum pump and Pressure gauge, and reaction can be carried out under pressure.
Solid reaction still in the present embodiment is also provided with intake valve and gas cylinder, after evacuation, can open intake valve and be filled with protective gas in reactor, thus avoids the impact that the oxygen in air reacts some.
Above three embodiments of the present utility model have been described in detail, but described content being only preferred embodiment of the present utility model, can not being considered to for limiting practical range of the present utility model.All equalizations done according to the utility model application range change and improve, and all should still belong within patent covering scope of the present utility model.

Claims (7)

1. solid reaction still body, it is characterized in that: comprise still chamber and still door, described still cavity wall both sides are provided with electrode rod, in described still chamber, opening surrounding is provided with sealing ring, in described still chamber, arranged outside has igniter, bottom, described still chamber is provided with the blast pipe for getting rid of air in reactor, and described blast pipe is provided with air bleeding valve.
2. solid reaction still body according to claim 1, it is characterized in that: on the left of described reactor, be provided with bleeding point, described bleeding point is connected by the first pipeline with vavuum pump, and described first pipeline is provided with vacuum pumping valve.
3. solid reaction still body according to claim 2, is characterized in that: on the right side of described reactor, be provided with air inlet, and described air inlet is connected with gas cylinder by the second pipeline, and described second pipeline is provided with intake valve.
4. solid reaction still body according to claim 3, is characterized in that: be provided with dust plug in described first pipeline and described second pipeline, described dust plug skin is coated with gauze.
5., according to the arbitrary described solid reaction still body of Claims 1-4, it is characterized in that: in described reactor, be provided with the pressure sensor for monitoring reacting kettle inner pressure.
6. according to the arbitrary described solid reaction still body of Claims 1-4, it is characterized in that: described igniter is provided with the ammeter for detecting reactant whether successful ignition.
7., according to the arbitrary described solid reaction still body of Claims 1-4, it is characterized in that: described still chamber arranged outside has the cooling water switch for cooling described still chamber.
CN201420492986.4U 2014-08-29 2014-08-29 Solid reaction still body Expired - Fee Related CN204147842U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420492986.4U CN204147842U (en) 2014-08-29 2014-08-29 Solid reaction still body

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420492986.4U CN204147842U (en) 2014-08-29 2014-08-29 Solid reaction still body

Publications (1)

Publication Number Publication Date
CN204147842U true CN204147842U (en) 2015-02-11

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CN201420492986.4U Expired - Fee Related CN204147842U (en) 2014-08-29 2014-08-29 Solid reaction still body

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106932007A (en) * 2017-04-21 2017-07-07 海正化工南通股份有限公司 A kind of reactor gas displacement checking system

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106932007A (en) * 2017-04-21 2017-07-07 海正化工南通股份有限公司 A kind of reactor gas displacement checking system

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150211

Termination date: 20160829