CN206184435U - Novel reation kettle of preparation perfluor propionyl fluoride - Google Patents

Novel reation kettle of preparation perfluor propionyl fluoride Download PDF

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Publication number
CN206184435U
CN206184435U CN201621219846.5U CN201621219846U CN206184435U CN 206184435 U CN206184435 U CN 206184435U CN 201621219846 U CN201621219846 U CN 201621219846U CN 206184435 U CN206184435 U CN 206184435U
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CN
China
Prior art keywords
inner bag
propionyl fluoride
agitator
utility
model
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621219846.5U
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Chinese (zh)
Inventor
姚素梅
耿谦
郭海强
李希仑
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Tianjin Changlu Chemical New Materials Co Ltd
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Tianjin Changlu Chemical New Materials Co Ltd
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Priority to CN201621219846.5U priority Critical patent/CN206184435U/en
Application granted granted Critical
Publication of CN206184435U publication Critical patent/CN206184435U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a novel reation kettle of preparation perfluor propionyl fluoride, including the inner bag, the bottom of inner bag is provided with the discharge gate, and inner bag bottom one side position department of being close to the discharge gate is provided with condensate outlet, inner bag bottom is close to condensate outlet one side and is provided with the electrothermal tube, and the left and right sides of inner bag is provided with the ear seat respectively, the bottom of ear seat is provided with anti -skid shock pad, the top position department that the inner bag left and right sides is close to the ear seat is provided with steam inlet, steam inlet's top is provided with the flange, the inside of inner bag is provided with the (mixing) shaft, the bottom of (mixing) shaft is provided with down the agitator, the utility model discloses in be provided with the agitator after, the inside stirring of going on of inner bag will be more abundant, the utility model discloses in be provided with anti -skid shock pad after, when reation kettle at the during operation, can reduce the produced vibration of its during operation, can increase its steadiness to a certain extent simultaneously.

Description

A kind of new reactor for preparing perfluoro-propionyl fluoride
Technical field
The utility model belongs to reactor technical field, and in particular to a kind of new reactor for preparing perfluoro-propionyl fluoride.
Background technology
The broad understanding of reactor has the container for physically or chemically reacting, and is matched somebody with somebody by the structure design to container and parameter Put, realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed, reactor be widely used in oil, chemical industry, Rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrifying, hydrogenate, hydrocarbonylation, polymerization, the pressure of the technical process such as condensation Force container, the broad understanding of reactor has the rustless steel container for physically or chemically reacting, according to different process conditions demands The structure design and parameter configuration of container are carried out, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards, To realize the mixture response function of heating, evaporation, cooling and the low high speed of technological requirement.Pressure vessel must comply with GB150 { steel Pressing pressure container } standard, non-pressure vessel must comply with the standard of NB/T47003.1-2009 { steel welding non-pressure vessel }.With Course of reaction in pressure requirements the design requirement of container is also not quite similar.Production must add in strict accordance with corresponding standard Work, detection and trial operation.Stainless steel cauldron is not quite similar according to different production technologies, operating condition etc., and reactor sets Meter structure and parameter are different, i.e. the structural style of reactor is different, belongs to nonstandard tankage.
But existing reactor is still present some irrational factors during use, when reactor is used, Its ear mount is merely able to play a part of support, it is possible that the situation slided, and the design of agitator causes stirring not It is very uniform.
Utility model content
The purpose of this utility model is to provide a kind of new reactor for preparing perfluoro-propionyl fluoride, to solve above-mentioned background The ear mount unitary function of proposition and the uneven problem of the agitating function of agitator in technology.
To achieve the above object, the utility model provides following technical scheme:It is a kind of new to prepare the anti-of perfluoro-propionyl fluoride The bottom of kettle, including inner bag, the inner bag is answered to be provided with discharging opening, and inner bag bottom is set at a side position of discharging opening There is condensation-water drain, the inner bag bottom is provided with electrothermal tube near condensation-water drain side, and the left and right sides of inner bag is distinguished Ear mount is provided with, the bottom of the ear mount is provided with antiskid, shock-absorbing pad, and the inner bag left and right sides is near the top position of ear mount Place is provided with steam inlet, is provided with flange above the steam inlet, and the inner bag is internally provided with agitating shaft, described The bottom of agitating shaft is provided with lower agitator, and agitator is provided with above the lower agitator, is set above the inner bag Be equipped with charging aperture, and inner bag top is provided with hand hole on the right side of charging aperture, be provided with the top of the hand hole can photoscope, Motor cabinet is provided with above the agitating shaft, servomotor, the servomotor and electricity are provided with above the motor cabinet Heat pipe is electrically connected with external power source.
Preferably, the charging aperture is provided with O-ring seal with the junction of inner bag.
Preferably, the upper agitator passes through threaded engagement connection with agitating shaft.
Preferably, the antiskid, shock-absorbing pad is provided with two altogether, and two antiskid, shock-absorbing pads are separately mounted to two ear mounts Bottom.
Preferably, the steam inlet is provided with two altogether, and two steam inlets are separately mounted to the left and right two of inner bag Side.
Compared with prior art, the beneficial effects of the utility model are:
(1) it is provided with after O-ring seal in the utility model, can to a certain extent prevents internal gas from leaking outside.
(2) it is provided with after agitator in the utility model, the stirring carried out inside inner bag will be more abundant.
(3) be provided with the utility model after antiskid, shock-absorbing pad, when reactor operationally, when can reduce its work Produced vibration, while its steadiness can be increased to a certain extent.
(4) it is provided with the utility model after two steam inlets, when adding steam, will be more quick.
(5) being provided with the utility model can be after photoscope, when reactor works, can be by that can have an X-rayed sem observation Internal working condition, if what surprisingly occurs, can timely withdraw.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model;
In figure:1- charging apertures, 2- inner bags, 3- ear mounts, the upper agitators of 4-, 5- agitating shafts, 6- electrothermal tubes, 7- discharging openings, 8- Condensation-water drain, 9- antiskid, shock-absorbings pad, 10- steam inlets, 11- flanges, 12- hand holes, 13- can photoscope, 14- servomotors, Agitator under 15- motor cabinets, 16-.
Specific embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the utility model embodiment is carried out Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of the utility model, rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made The every other embodiment for being obtained, belongs to the scope of the utility model protection.
Fig. 1 is referred to, the utility model provides a kind of technical scheme:A kind of new reactor for preparing perfluoro-propionyl fluoride, Including inner bag 2, the bottom of inner bag 2 is provided with discharging opening 7, and the bottom of inner bag 2 be provided with a side position of discharging opening 7 it is cold Solidifying water out 8, the bottom of inner bag 2 is provided with electrothermal tube 6 near the side of condensation-water drain 8, and the left and right sides of inner bag 2 is respectively provided with The bottom for having ear mount 3, ear mount 3 is provided with antiskid, shock-absorbing pad 9, and the left and right sides of inner bag 2 is provided with the top position of ear mount 3 Steam inlet 10, the top of steam inlet 10 is provided with flange 11, and inner bag 2 is internally provided with agitating shaft 5, the bottom of agitating shaft 5 Portion is provided with lower agitator 16, and the top of lower agitator 16 is provided with agitator 4, and the top of inner bag 2 is provided with charging aperture 1, And the top of inner bag 2 is provided with hand hole 12 near the right side of charging aperture 1, the top of hand hole 12 is provided with can photoscope 13, agitating shaft 5 Top be provided with motor cabinet 15, the top of motor cabinet 15 is provided with servomotor 14, servomotor 14 and electrothermal tube 6 with outward Portion's power supply is electrically connected with.
Charging aperture 1 is provided with O-ring seal with the junction of inner bag 2, is provided with after O-ring seal, can be in certain journey Prevent internal gas from leaking outside on degree.
Upper agitator 4, by threaded engagement connection, is provided with after agitator 4 with agitating shaft 5, is entered inside inner bag 2 Capable stirring will be more abundant.
Antiskid, shock-absorbing pad 9 is provided with two altogether, and two antiskid, shock-absorbing pads 9 are separately mounted to two bottoms of ear mount 3, if Be equipped with after antiskid, shock-absorbing pad 9, when reactor operationally, vibration produced during its work can be reduced, while certain journey Can increase its steadiness on degree.
Steam inlet 10 is provided with two altogether, and two steam inlets 10 are separately mounted to the left and right sides of inner bag 2, set After having two steam inlets 10, when adding steam, will be more quick.
Operation principle of the present utility model and use flow:After the utility model is installed, the sealing of reactor is checked Property and its installation fix, afterwards i.e. can be used, when using, first passing through ear mount 3 is well placed reactor, then plugs in Line, starts servomotor 14, and now servomotor 14 starts running, there is provided power can drive stirring to agitating shaft 5 Device 4 and lower agitator 16 are rotated together, and then being added from charging aperture 1 will prepare the material of perfluoro-propionyl fluoride, and then material leads to The rotation for crossing agitator 4 and lower agitator 16 is stirred to it, and then electrothermal tube 6 starts to start, and the table wall to inner bag 2 is added Heat, starts simultaneously at the addition steam from steam inlet 10, and the condensed water that steam is formed is discharged from condensation-water drain 8, is reacted Afterwards, the perfluoro-propionyl fluoride for preparing can discharge from discharging opening 7.
While there has been shown and described that embodiment of the present utility model, for the ordinary skill in the art, It is appreciated that these embodiments can be carried out various changes in the case where principle of the present utility model and spirit is not departed from, repaiies Change, replace and modification, scope of the present utility model is defined by the appended claims and the equivalents thereof.

Claims (5)

1. a kind of new reactor for preparing perfluoro-propionyl fluoride, including inner bag (2), it is characterised in that:The bottom of the inner bag (2) Discharging opening (7) is provided with, and inner bag (2) bottom is provided with condensation-water drain (8), institute at a side position of discharging opening (7) State inner bag (2) bottom and condensation-water drain (8) side is provided with electrothermal tube (6), and the left and right sides of inner bag (2) is respectively provided with The bottom for having ear mount (3), the ear mount (3) is provided with antiskid, shock-absorbing pad (9), and inner bag (2) left and right sides is near ear mount (3) Top position at be provided with steam inlet (10), be provided with flange (11), the inner bag above the steam inlet (10) (2) be internally provided with agitating shaft (5), the bottom of the agitating shaft (5) is provided with lower agitator (16), the lower agitator (16) agitator (4) is provided with above, charging aperture (1) is provided with above the inner bag (2), and inner bag (2) top is leaned on Hand hole (12) is provided with the right side of nearly charging aperture (1), being provided with the top of the hand hole (12) can photoscope (13), the stirring Motor cabinet (15) is provided with above axle (5), servomotor (14), the servo electricity are provided with above the motor cabinet (15) Machine (14) and electrothermal tube (6) are electrically connected with external power source.
2. a kind of new reactor for preparing perfluoro-propionyl fluoride according to claim 1, it is characterised in that:The charging aperture (1) junction with inner bag (2) is provided with O-ring seal.
3. a kind of new reactor for preparing perfluoro-propionyl fluoride according to claim 1, it is characterised in that:The upper stirring Device (4) is with agitating shaft (5) by threaded engagement connection.
4. a kind of new reactor for preparing perfluoro-propionyl fluoride according to claim 1, it is characterised in that:It is described anti-skidding to subtract Shake pad (9) is provided with two altogether, and two antiskid, shock-absorbing pads (9) are separately mounted to two bottoms of ear mount (3).
5. a kind of new reactor for preparing perfluoro-propionyl fluoride according to claim 1, it is characterised in that:The steam enters Mouthful (10) are provided with two altogether, and two steam inlets (10) are separately mounted to the left and right sides of inner bag (2).
CN201621219846.5U 2016-11-11 2016-11-11 Novel reation kettle of preparation perfluor propionyl fluoride Expired - Fee Related CN206184435U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621219846.5U CN206184435U (en) 2016-11-11 2016-11-11 Novel reation kettle of preparation perfluor propionyl fluoride

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621219846.5U CN206184435U (en) 2016-11-11 2016-11-11 Novel reation kettle of preparation perfluor propionyl fluoride

Publications (1)

Publication Number Publication Date
CN206184435U true CN206184435U (en) 2017-05-24

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Country Status (1)

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CN (1) CN206184435U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107185471A (en) * 2017-05-31 2017-09-22 张家港市科华化工装备制造有限公司 High intensity reactor
CN107824149A (en) * 2017-12-11 2018-03-23 合肥右传媒科技有限公司 One kind is used for sulfonic acid chloride fluorination reaction kettle

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107185471A (en) * 2017-05-31 2017-09-22 张家港市科华化工装备制造有限公司 High intensity reactor
CN107824149A (en) * 2017-12-11 2018-03-23 合肥右传媒科技有限公司 One kind is used for sulfonic acid chloride fluorination reaction kettle

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170524

Termination date: 20191111