CN209631174U - For being catalyzed the experimental provision of reaction - Google Patents

For being catalyzed the experimental provision of reaction Download PDF

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Publication number
CN209631174U
CN209631174U CN201821848541.XU CN201821848541U CN209631174U CN 209631174 U CN209631174 U CN 209631174U CN 201821848541 U CN201821848541 U CN 201821848541U CN 209631174 U CN209631174 U CN 209631174U
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CN
China
Prior art keywords
cover
reaction
catalyst
shaft
reactor tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821848541.XU
Other languages
Chinese (zh)
Inventor
王伟建
战浩
高文杰
李乾峰
张腾元
田沛霖
卢颖
刘彤
李芳杰
甘秋琴
王学锋
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Qinzhou University
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Qinzhou University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qinzhou University filed Critical Qinzhou University
Priority to CN201821848541.XU priority Critical patent/CN209631174U/en
Application granted granted Critical
Publication of CN209631174U publication Critical patent/CN209631174U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of for being catalyzed the experimental provision of reaction, including reactor tank, cover, a motor cabinet is arranged in the bottom end of the cover, the motor cabinet is equipped with a variable-frequency motor, the revolving speed button being electrically connected there are two being set on the cover with variable-frequency motor, the output shaft of the variable-frequency motor is connect with the shaft being vertically arranged in reactor tank, and the shaft is equipped with several catalyst and sprays skeleton.Rotary feeding mechanism is arranged in this experimental provision in reactor tank, catalyst is sprayed into liquid reactants in rotation, increase effectively the contact area of catalyst and reactant, catalyst uniformly comes into full contact with reactant, shorten the reaction time, reaction is sufficiently and reactivity is high, is conducive to Germicidal efficacy and experimental study.

Description

For being catalyzed the experimental provision of reaction
Technical field
The utility model relates to a kind of experimental provisions, and in particular to a kind of for being catalyzed the experimental provision of reaction.
Background technique
Reactive liquid solution belongs to common chemical reaction, generally existing in many industrial circles such as petroleum, chemical industry, metallurgy, And the condition of some reactive liquid solutions is more complicated, needs to carry out under some special environmental conditions, such as urging for catalyst is added Change reaction, in order to fully understand the catalysis reaction of reactive liquid solution, scientific chemical experiment will be generally carried out, to observe chemical reaction Process produces new reactant.
Currently, the experimental provision of liquid liquid catalysis reaction, structure is all unreasonable, directly pours into solid powder to reaction vessel and urges Agent, though being stirred in experimentation using glass stick, solid powder th-1 catalyst still can only be contacted with partially liq reactant, thus The contact area of reactant and catalyst is small, causes reactant reaction insufficient, and long and reaction effect is unknown the time required to reaction Aobvious, reactivity is low, waste reactant resource, experimental data there are deviation, be unfavorable for experimental study.
Utility model content
In view of the deficienciess of the prior art, the utility model provide it is a kind of for be catalyzed reaction experimental provision, this reality Rotary feeding mechanism is arranged in experiment device in reactor tank, and catalyst is sprayed into liquid reactants in rotation, increases effectively The contact area of catalyst and reactant, catalyst uniformly come into full contact with reactant, shorten the reaction time, and reaction is sufficiently and anti- Should rate it is high, be conducive to Germicidal efficacy and experimental study.
In order to achieve the above object, the technical solution that the utility model is taken:
For being catalyzed the experimental provision of reaction, including reactor tank, the reactor tank be removably equipped with and its mating connection Cover, the cover is equipped with a L-shape rotation handle, and a motor cabinet, the motor cabinet is arranged in the bottom end of the cover It is equipped with a variable-frequency motor, sets that there are two the revolving speed buttons with variable-frequency motor electrical connection on the cover, then one of them is Revolving speed accelerate button, another be revolving speed retard button, the output shaft of the variable-frequency motor and be vertically arranged in reactor tank Shaft connection, the shaft are equipped with several catalyst and spray skeleton, and catalyst sprinkling skeleton is cylindrical and from upper It is sequentially arranged in shaft down or catalyst sprinkling skeleton is in fusiform and the circumferential bottom end for being set to shaft, each catalyst Sprinkling skeleton is that inner hollow, its surface open up full spray hole, each catalyst sprinkling skeleton it is detachable into two.
It is anti-to shorten catalysis in order to make reactor tank be applied to the liquid liquid catalysis reaction of heating as optimal technical scheme The time answered expands the scope of application of experimental provision, improves the practicability of entire experimental provision, is additionally provided with one on the motor cabinet Heating rod, sets that there are two the temperature control buttons with heating rod electrical connection on the cover, then one of them be+heat button, it is another A is cooling button.
As optimal technical scheme, for the ease of adjusting the revolving speed of temperature and shaft in reactor tank, in order to provide preferable Reaction condition, further increase reaction rate and reaction effect, be conducive to Germicidal efficacy and experimental study, the cover it is outer Surface is equipped with a liquid crystal display, and the liquid crystal display can intuitively show the revolving speed of the temperature and shaft in reactor tank.
Compared with prior art, the utility model has the advantages that
1, rotary feeding mechanism is arranged in this experimental provision in reactor tank, and catalyst is sprayed into liquid reactants in rotation In, the contact area of catalyst and reactant is increased effectively, catalyst uniformly comes into full contact with reactant, when shortening reaction Between, reaction is sufficiently and reactivity is high, is conducive to Germicidal efficacy and experimental study.
2, heating rod is set, so that reactor tank is applied to the liquid liquid catalysis reaction of heating, shortens the time of catalysis reaction, The scope of application for expanding experimental provision, improves the practicability of entire experimental provision.
3, liquid crystal display is set, convenient for adjusting the revolving speed of temperature and shaft in reactor tank, in order to provide preferably anti- Condition is answered, reaction rate and reaction effect are further increased, is conducive to Germicidal efficacy and experimental study.
Detailed description of the invention
The utility model is described in further detail in the following with reference to the drawings and specific embodiments.
Fig. 1 is a kind of structural schematic diagram of the utility model;
Fig. 2 is another structural schematic diagram of the utility model;
Fig. 3 is the structural schematic diagram that shaft and catalyst spray skeleton;
Fig. 4 is the structural schematic diagram that catalyst sprays skeleton;
Drawing reference numeral: 1, reactor tank, 2, cover, 3, rotation handle, 4, motor cabinet, 5, variable-frequency motor, 6, revolving speed button, 7, Shaft, 8, catalyst sprinkling skeleton, 9, heating rod, 10, temperature control button, 11, liquid crystal display, 12, starting electric button, 13, Spray hole.
Specific embodiment
For being catalyzed the experimental provision of reaction, including cylindrical reactor tank 1, for the ease of the process of observing response, Reactor tank 1 is set to can be applied to the reaction of corrosive liquids simultaneously, the present embodiment setting reactor tank 1 is made of transparent toughened glass , the reactor tank 1 is removably equipped with the cover 2 with its mating connection, and the cover 2 is equipped with a L-shape rotation handle Handle 3, the present embodiment is the bottom end of cover 2 opens up internal screw thread, the top of reactor tank 1 opens up external screw thread, the reactor tank 1 and cover It is detachably connected between 2 by screw thread realization, opening between cover 2 and reactor tank 1 can be realized by rotation rotation handle 3 It closes, a motor cabinet 4 is arranged in the bottom end of the cover 2, and the motor cabinet 4 is equipped with a variable-frequency motor 5, considers that carrying out liquid liquid urges Change reaction, for the dampness of variable-frequency motor 5 with induced damage resistive, waterproof and dampproof protection is arranged in the present embodiment on variable-frequency motor 5 in order to prevent It covers, is set on 2 surface of cover there are two the revolving speed button 6 being electrically connected with variable-frequency motor 5, then one of them adds for revolving speed Fast button, another be revolving speed retard button, the present embodiment be additionally provided on cover 2 starting electric button 12, the variable-frequency electric The output shaft of machine 5 is connect with the shaft 7 being vertically arranged in reactor tank 1, and the shaft 7 is sprayed equipped with several catalyst Skeleton 8, the catalyst sprinkling skeleton 8 is cylindrical and is sequentially arranged in shaft 7 from top to bottom, as shown in Figure 1, or described Catalyst sprays skeleton 8 in fusiform and the circumferential bottom end for being set to shaft 7, as shown in Fig. 2, each catalyst sprinkling skeleton 8 is Inner hollow, its surface open up full spray hole 13, each catalyst sprinkling skeleton 8 it is detachable into two, for the ease of each Catalyst sprinkling skeleton 8 is dismantled and is assembled, and the present embodiment is by cylindric or fusiform catalyst sprinkling skeleton 8 to partly splitting into two Section, a section end is equipped with external screw thread, another section end is equipped with internal screw thread, realizes that each catalyst ejector skeleton 9 is fast by screw thread Speed is detachably connected, as shown in Figures 3 and 4.
A heating rod 9 is additionally provided on the motor cabinet 4, set on the cover 2 there are two with heating rod 9 be electrically connected Temperature control button 10, then one of them be+heat button, another be cooling button, in order to make reactor tank 2 be applied to heat Liquid liquid be catalyzed reaction, shorten catalysis reaction time, expand the scope of application of experimental provision, improve the reality of entire experimental provision The property used.
The outer surface of the cover 2 is equipped with a liquid crystal display 11, and the liquid crystal display 11 can intuitively show reactor tank 1 The revolving speed of interior temperature and shaft 7, convenient for adjusting the revolving speed of temperature and shaft 7 in reactor tank 1, in order to provide preferable reaction Condition further increases reaction rate and reaction effect, is conducive to Germicidal efficacy and experimental study.
When the utility model is used: unscrewing catalyst sprinkling skeleton 8, placement is divided equally according to the reaction dosage of catalyst In in each catalyst sprinkling skeleton 8, two liquid reactants are placed in reactor tank 1, cover 2 is tightened, connect experimental provision Power supply line, started by press electric button 12 can start entire experimental provision, the temperature and variable-frequency motor 5 in reactor tank 1 Revolving speed can intuitively show that experimenter can pass through pressing revolving speed button 6 and temperature according to actually reporting situations on liquid crystal display Button 10 is controlled to adjust temperature and revolving speed, and then makes experimenter that can test process by transparent 1 clear view of reactor tank.
This experimental provision is mainly used in liquid catalyst reaction, also can be applied to during liquid reacts with powder solid, Charging is sprayed in rotation, makes being sufficiently mixed for powder solid reactant and liquid reactants.
Certainly, only the utility model preferred embodiment is described in detail in conjunction with attached drawing above, not The scope of the utility model is limited with this, it is all according to equivalence changes made by the principles of the present invention, construction and structure, It should all be covered by the protection scope of the utility model.

Claims (3)

1. the experimental provision for being catalyzed reaction, it is characterised in that: including reactor tank (1), the reactor tank (1) is removably set Have and is equipped with a L-shape rotation handle (3), the bottom of the cover (2) with the cover of its mating connection (2), the cover (2) End setting one motor cabinet (4), the motor cabinet (4) are equipped with a variable-frequency motor (5), set on the cover (2) there are two with change The revolving speed button (6) of frequency motor (5) electrical connection, the output shaft of the variable-frequency motor (5) and is vertically arranged in reactor tank (1) Shaft (7) connection, the shaft (7) is equipped with several catalyst sprinkling skeleton (8), and the catalyst sprays skeleton (8) It is cylindrical and be sequentially arranged on shaft (7) from top to bottom or catalyst sprinkling skeleton (8) is in fusiform and circumferential direction is set to The bottom end of shaft, each catalyst sprinkling skeleton (8) are that inner hollow, its surface open up full spray hole (13), each catalysis Agent spray skeleton (8) it is detachable into two.
2. according to claim 1 for being catalyzed the experimental provision of reaction, it is characterised in that: on the motor cabinet (4) also Equipped with a heating rod (9), set on the cover (2) there are two with heating rod (9) electrical connection temperature control button (10).
3. according to claim 2 for being catalyzed the experimental provision of reaction, it is characterised in that: the appearance of the cover (2) Face is equipped with a liquid crystal display (11), and the liquid crystal display (11) can intuitively show temperature and shaft (7) in reactor tank (1) Revolving speed.
CN201821848541.XU 2018-11-09 2018-11-09 For being catalyzed the experimental provision of reaction Expired - Fee Related CN209631174U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821848541.XU CN209631174U (en) 2018-11-09 2018-11-09 For being catalyzed the experimental provision of reaction

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821848541.XU CN209631174U (en) 2018-11-09 2018-11-09 For being catalyzed the experimental provision of reaction

Publications (1)

Publication Number Publication Date
CN209631174U true CN209631174U (en) 2019-11-15

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821848541.XU Expired - Fee Related CN209631174U (en) 2018-11-09 2018-11-09 For being catalyzed the experimental provision of reaction

Country Status (1)

Country Link
CN (1) CN209631174U (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111229141A (en) * 2020-02-04 2020-06-05 佛山市金净创环保技术有限公司 Device for accurately controlling catalytic reaction and using method thereof
CN114197129A (en) * 2021-12-02 2022-03-18 德州华源生态科技有限公司 Method and device for producing loose and soft vortex yarns
CN114197129B (en) * 2021-12-02 2024-04-16 德州华源生态科技有限公司 Method and device for producing loose soft vortex yarn

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111229141A (en) * 2020-02-04 2020-06-05 佛山市金净创环保技术有限公司 Device for accurately controlling catalytic reaction and using method thereof
CN114197129A (en) * 2021-12-02 2022-03-18 德州华源生态科技有限公司 Method and device for producing loose and soft vortex yarns
CN114197129B (en) * 2021-12-02 2024-04-16 德州华源生态科技有限公司 Method and device for producing loose soft vortex yarn

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20191115

Termination date: 20201109