CN207520996U - A kind of thermostatic type liquid chemical reaction unit - Google Patents
A kind of thermostatic type liquid chemical reaction unit Download PDFInfo
- Publication number
- CN207520996U CN207520996U CN201721476869.9U CN201721476869U CN207520996U CN 207520996 U CN207520996 U CN 207520996U CN 201721476869 U CN201721476869 U CN 201721476869U CN 207520996 U CN207520996 U CN 207520996U
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- CN
- China
- Prior art keywords
- kettle
- interior kettle
- interior
- chemical reaction
- type liquid
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The utility model is related to a kind of thermostatic type liquid chemical reaction units, including interior kettle, it is characterized in that, interior kettle top end is fixedly connected with motor, controller is installed above motor, the output shaft of motor is connected with shaft, and shaft is extend into interior kettle, stirring rod is fixedly connected in shaft, heater strip is housed inside stirring rod；Radio temperature sensor and supersonic generator are installed in interior kettle；Interior kettle top end offers feeding-passage, and feeding-passage is equipped with metering switch, and feeding-passage top is connected with mixer, is equipped with batch mixing case lid above mixer, mixer surface is equipped with PLC controller and display dial；The opposite side at interior kettle top end is equipped with pressure gauge and relief valve；Interior kettle lower part is equipped with outer kettle, and condenser is equipped in outer kettle；Interior bottom portion is equipped with tapping channel；Interior kettle upper face is equipped with observation panel.The reaction kettle has the function of advance batch mixing, accurate charging, controllable, abundant, the reaction process observable of reaction stirring of reaction temperature etc., has very strong practicability.
Description
Technical field
The utility model is related to reaction kettles, especially related with a kind of structure of thermostatic type liquid chemical reaction unit.
Background technology
Chemical reaction kettle is a kind of container physically or chemically reacted, by the structure design and parameter configuration to container,
Realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.
At present, traditional chemical reaction kettle has the following problems：
Reaction temperature is difficult control；In whipping process, there is a situation where that stirring uneven or solute is difficult to dissolve, and influences
The concentration of reaction；Reaction process cannot monitor in real time, and the extent of reaction can not be controlled.Can accurately it add for this purpose, we have proposed one kind
Material, controlling reaction temperature, the chemical reaction kettle device stirred evenly.
Utility model content
The utility model provides a kind of thermostatic type liquid chemical reaction unit, to solve above-mentioned the deficiencies in the prior art, makes
Reaction kettle has many advantages, such as that advance batch mixing, accurate charging, reaction temperature is controllable, reaction stirring is abundant, reaction process observable.
In order to realize the purpose of this utility model, intend using following technology：
A kind of thermostatic type liquid chemical reaction unit, including interior kettle, which is characterized in that the interior kettle top end is fixedly connected with
Motor, the output shaft of the motor are fixedly connected with shaft, and shaft is extend into interior kettle, and stirring is fixedly connected in the shaft
Stick, equipped with heater strip, the motor top is provided with to be controlled for carrying out the power supply of start-up and shut-down control to heater strip for stirring rod inside
Device；The interior kettle inner wall is equipped with radio temperature sensor and supersonic generator；The side at the interior kettle top end offer into
Expect channel, be provided with metering switch on the feeding-passage, the feeding-passage top is connected with mixer, on the mixer
Side is equipped with batch mixing case lid, and the mixer surface is equipped with PLC controller and display dial；The opposite side peace at the interior kettle top end
Equipped with pressure gauge and relief valve；The interior kettle lower part is equipped with outer kettle, and condenser is equipped in outer kettle；The interior bottom portion installation
There is tapping channel；The radio temperature sensor, supersonic generator, metering switch, pressure gauge, relief valve, condenser, power supply
Controller is connected respectively with PLC controller；The interior kettle upper face is equipped with observation panel.
Further, agitating device is installed inside the mixer.
Further, the radio temperature sensor is fixed on the inner wall of interior kettle, receives and convert its temperature by PLC controller
Spend signal.
Further, the supersonic generator is side wall supersonic generator.
Further, with outer kettle by screw connection, condenser is cooled down the condenser by way of air cooling.
Further, the relief valve is electromagnetic relief valve, and the pressure gauge and relief valve are connect with interior kettle by connector.
The beneficial effects of the utility model are：A kind of thermostatic type liquid chemical reaction unit is by installing mixing device and meter additional
Amount switch realizes advance batch mixing, precisely charging；By installing radio temperature sensor, heater strip, condenser additional, realize anti-
It answers the real-time control of kettle temperature degree and adjusts；By installing supersonic generator additional, the solution in reaction kettle is made to stir evenly, is improved
Stirring efficiency；By installing pressure measurement device, the monitoring and adjusting of reactor pressure situation are realized；The device has very
Strong practicability.
Description of the drawings
Fig. 1 shows the structure diagram of the utility model.
Specific embodiment
As shown in Figure 1, a kind of thermostatic type liquid chemical reaction unit, including interior kettle 1, which is characterized in that the interior kettle 1 pushes up
End is fixedly connected with motor 2, and the output shaft of the motor 2 is fixedly connected with shaft 3, and shaft 3 is extend into interior kettle 1, described turn
Stirring rod 4 is fixedly connected on axis 3,4 inside of stirring rod is provided with equipped with heater strip 5,2 top of motor for heater strip
5 carry out the power-supply controller of electric 20 of start-up and shut-down control；1 inner wall of interior kettle is equipped with radio temperature sensor 6 and supersonic generator
7；The side on 1 top of interior kettle offers feeding-passage 8, and metering switch 9, the charging are provided on the feeding-passage 8
8 top of channel is connected with mixer 10, and 10 top of mixer is equipped with batch mixing case lid 11, and 10 surface of mixer is equipped with
PLC controller 12 and display dial 13；The opposite side on 1 top of interior kettle is equipped with pressure gauge 14 and relief valve 15；In described
1 lower part of kettle is equipped with outer kettle 16, and condenser 17 is equipped in outer kettle 16；1 bottom of interior kettle is equipped with tapping channel 18；It is described
Radio temperature sensor 6, supersonic generator 7, metering switch 9, pressure gauge 14, relief valve 15, condenser 17, power-supply controller of electric
20 are connected respectively with PLC controller 12；1 upper face of interior kettle is equipped with observation panel 19.
Preferably, agitating device is installed inside the mixer 10.
Preferably, the radio temperature sensor 6 is fixed on the inner wall of interior kettle 1, is received and turned by PLC controller 12
Change its temperature signal.
Preferably, the supersonic generator 7 is side wall supersonic generator.
Preferably, the condenser 17 and outer kettle 16, by screw connection, condenser 17 is by way of air cooling
Cooling.
Preferably, the relief valve 15 is electromagnetic relief valve, the pressure gauge 14 and relief valve 15 pass through with interior kettle to be connect
Part connects.
Before reaction kettle work, first material is mixed in a certain ratio in mixer 10, closes batch mixing case lid 11, is opened mixed
Hopper power supply, the agitating device inside mixer start, and carry out material mixing.Material after mixing, in PLC controller 12
Set inlet amount, reaction temperature, vibration of ultrasonic wave frequency and pressure limit.After each parameter setting, start motor switch, this
When, 2 drive shaft 3 of motor, shaft 3 drives stirring rod 4 to start to stir, meanwhile, metering switch 9 is opened, mixture passes through charging
Channel 8 enters interior kettle 1, and opening the switch of the heater strip on power-supply controller of electric 20 is brought rapidly up reactant in kettle；When inlet amount reaches
During to setting value, metering switch 9 is closed, so as to close feeding-passage 8；During the reaction, radio temperature sensor 6 passes through
The temperature signal detected is converted into numerical value and is presented to display dial 13 by PLC controller 12, and operating personnel pay attention to observing temperature
Numerical value when the temperature needed for temperature reaches reaction, need to close the heater strip switch on power-supply controller of electric 20, when temperature is excessively high,
While closing heater strip switch, the condenser switch of PLC controller 12 need to be opened, is carried out using the cold wind that condenser 17 manufactures
Cooling.Simultaneously by the response situation in 19 observing response kettle of observation panel, if there is material agglomerate in reactant, PLC need to be utilized
The frequency of supersonic generator 7 is turned up in controller 12, and shatter agglomerate ensures the consistent of material concentration.In reaction process, if pressure
The numerical value that power table 14 is shown is more than setting range, and PLC controller 12 carries out air pressure adjustment by relief valve 15 is started.Reaction is completed
Afterwards, supersonic generator 7 can cavity open, anti-deposition processes are carried out to reactant remaining in autoclave body, contribute to reaction kettle
Cleaning.
The preferable specific embodiment of the above, only the utility model, but the scope of protection of the utility model is not
This is confined to, in the technical scope that any one skilled in the art discloses in the utility model, according to this practicality
Novel technical solution and its utility model design are subject to equivalent substitution or change, should all cover the protection model in the utility model
Within enclosing.
Claims (6)
1. a kind of thermostatic type liquid chemical reaction unit, including interior kettle（1）, which is characterized in that the interior kettle（1）Top, which is fixed, to be connected
It is connected to motor（2）, the motor（2）Output shaft be fixedly connected with shaft（3）, shaft（3）It extend into interior kettle（1）It is interior, it is described
Shaft（3）On be fixedly connected with stirring rod（4）, stirring rod（4）Inside is equipped with heater strip（5）, the motor（2）Top is provided with
For to heater strip（5）Carry out the power-supply controller of electric of start-up and shut-down control（20）；The interior kettle（1）Inner wall is equipped with wireless temperature sensing
Device（6）And supersonic generator（7）；The interior kettle（1）The side on top offers feeding-passage（8）, the feeding-passage（8）
On be provided with metering switch（9）, the feeding-passage（8）Top is connected with mixer（10）, the mixer（10）Top is set
There is batch mixing case lid（11）, the mixer（10）Surface is equipped with PLC controller（12）And display dial（13）；The interior kettle
（1）The opposite side on top is equipped with pressure gauge（14）And relief valve（15）；The interior kettle（1）Lower part is equipped with outer kettle（16）, outside
Kettle（16）Condenser is inside installed（17）；The interior kettle（1）Bottom is equipped with tapping channel（18）；The radio temperature sensor
（6）, supersonic generator（7）, metering switch（9）, pressure gauge（14）, relief valve（15）, condenser（17）, power-supply controller of electric
（20）Respectively with PLC controller（12）It is connected；The interior kettle（1）Upper face is equipped with observation panel（19）.
2. a kind of thermostatic type liquid chemical reaction unit according to claim 1, it is characterised in that：The mixer（10）
Inside is equipped with agitating device.
3. a kind of thermostatic type liquid chemical reaction unit according to claim 1, it is characterised in that：The wireless temperature passes
Sensor（6）It is fixed on interior kettle（1）Inner wall on, by PLC controller（12）Receive and convert its temperature signal.
4. a kind of thermostatic type liquid chemical reaction unit according to claim 1, it is characterised in that：The ultrasonic wave occurs
Device（7）For side wall supersonic generator.
5. a kind of thermostatic type liquid chemical reaction unit according to claim 1, it is characterised in that：The condenser（17）
With outer kettle（16）Pass through screw connection, condenser（17）Cooled down by way of air cooling.
6. a kind of thermostatic type liquid chemical reaction unit according to claim 1, it is characterised in that：The relief valve（15）
For electromagnetic relief valve, the pressure gauge（14）And relief valve（15）It is connect with interior kettle by connector.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721476869.9U CN207520996U (en) | 2017-11-08 | 2017-11-08 | A kind of thermostatic type liquid chemical reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721476869.9U CN207520996U (en) | 2017-11-08 | 2017-11-08 | A kind of thermostatic type liquid chemical reaction unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207520996U true CN207520996U (en) | 2018-06-22 |
Family
ID=62581771
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721476869.9U Expired - Fee Related CN207520996U (en) | 2017-11-08 | 2017-11-08 | A kind of thermostatic type liquid chemical reaction unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207520996U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108993362A (en) * | 2018-09-03 | 2018-12-14 | 湖北中澳纳米材料技术有限公司 | A kind of device and method preparing high-purity nm molybdic acid potassium solution |
| CN109276899A (en) * | 2018-10-18 | 2019-01-29 | 葛映东 | A kind of chemical material solvent recovery cleaning device and its working method |
-
2017
- 2017-11-08 CN CN201721476869.9U patent/CN207520996U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108993362A (en) * | 2018-09-03 | 2018-12-14 | 湖北中澳纳米材料技术有限公司 | A kind of device and method preparing high-purity nm molybdic acid potassium solution |
| CN109276899A (en) * | 2018-10-18 | 2019-01-29 | 葛映东 | A kind of chemical material solvent recovery cleaning device and its working method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180622 Termination date: 20191108 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |