CN109894057A - A kind of thermostatic type liquid chemical reaction unit - Google Patents
A kind of thermostatic type liquid chemical reaction unit Download PDFInfo
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- CN109894057A CN109894057A CN201711302405.0A CN201711302405A CN109894057A CN 109894057 A CN109894057 A CN 109894057A CN 201711302405 A CN201711302405 A CN 201711302405A CN 109894057 A CN109894057 A CN 109894057A
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- kettle
- interior
- interior kettle
- chemical reaction
- mixer
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Abstract
The present invention relates to a kind of thermostatic type liquid chemical reaction units, including interior kettle, it is characterized in that, interior kettle top end is fixedly connected with motor, controller is installed above motor, the output shaft of motor is connected with shaft, and shaft is extend into interior kettle, it is fixedly connected with stirring rod in shaft, heater strip is housed inside stirring rod；Radio temperature sensor and supersonic generator are installed in interior kettle；Interior kettle top end offers feeding-passage, and feeding-passage is equipped with metering switch, and feeding-passage top is connected with mixer, is equipped with mixing case lid above mixer, mixer surface is equipped with PLC controller and display dial；The other side at interior kettle top end is equipped with pressure gauge and relief valve；Interior kettle lower part is equipped with outer kettle, is equipped with condenser in outer kettle；Interior bottom portion is equipped with tapping channel；Interior kettle upper face is equipped with observation panel.The reaction kettle has the function of preparatory mixing, accurate charging, controllable, abundant, the reaction process observable of reaction stirring of reaction temperature etc., has very strong practicability.
Description
Technical field
The present invention relates to reaction kettles, especially related with a kind of structure of thermostatic type liquid chemical reaction unit.
Background technique
Chemical reaction kettle is a kind of container physically or chemically reacted, by the structure design and parameter configuration to container,
Realize the mixed function for heating, evaporation, cooling and the low high speed that technique requires.
Currently, traditional chemical reaction kettle has the following problems:
Reaction temperature is difficult to control；In whipping process, there is stirring unevenly or solute is difficult to the case where dissolving, influence
The concentration of reaction；Reaction process is unable to real-time monitoring, and the extent of reaction can not be controlled.For this purpose, we have proposed one kind accurately to add
Material, chemical reaction kettle device control reaction temperature, stirred evenly.
Summary of the invention
The present invention provides a kind of thermostatic type liquid chemical reaction unit, to solve above-mentioned the deficiencies in the prior art, makes to react
Kettle has many advantages, such as that preparatory mixing, accurate charging, reaction temperature is controllable, reaction stirring is abundant, reaction process observable.
In order to achieve the object of the present invention, the following technology of proposed adoption:
A kind of thermostatic type liquid chemical reaction unit, including interior kettle, which is characterized in that the interior kettle top end is fixedly connected with
Motor, the output shaft of the motor are fixedly connected with shaft, and shaft is extend into interior kettle, and stirring is fixedly connected in the shaft
Stick, stirring rod inside are equipped with heater strip, and the power supply for carrying out start-up and shut-down control to heater strip is provided at the top of the motor and is controlled
Device；The interior kettle inner wall is equipped with radio temperature sensor and supersonic generator；The side at the interior kettle top end offer into
Expect channel, be provided with metering switch on the feeding-passage, the feeding-passage top is connected with mixer, on the mixer
Side is equipped with mixing case lid, and the mixer surface is equipped with PLC controller and display dial；Pacify the other side at the interior kettle top end
Equipped with pressure gauge and relief valve；The interior kettle lower part is equipped with outer kettle, is equipped with condenser in outer kettle；The interior bottom portion installation
There is tapping channel；The radio temperature sensor, supersonic generator, metering switch, pressure gauge, relief valve, condenser, power supply
Controller is connected with PLC controller respectively；The interior kettle upper face is equipped with observation panel.
Further, agitating device is installed inside the mixer.
Further, the radio temperature sensor is fixed on the inner wall of interior kettle, receives and convert its temperature by PLC controller
Spend signal.
Further, the supersonic generator is side wall supersonic generator.
Further, by screw connection, condenser is cooled down by way of air cooling for the condenser and outer kettle.
Further, the relief valve is that electromagnetic relief valve, the pressure gauge and relief valve are connect with interior kettle by connector.
The beneficial effects of the present invention are: a kind of thermostatic type liquid chemical reaction unit is opened by installing mixing device and metering additional
It closes, realizes preparatory mixing, precisely charging；By installing radio temperature sensor, heater strip, condenser additional, reaction kettle is realized
The real-time control and adjusting of temperature；By installing supersonic generator additional, stirs the solution in reaction kettle more evenly, improve and stir
Mix efficiency；By installing pressure measurement device, the monitoring and adjusting of reactor pressure situation are realized；The device has very strong
Practicability.
Detailed description of the invention
Fig. 1 shows structural schematic diagram of the invention.
Specific embodiment
As shown in Figure 1, a kind of thermostatic type liquid chemical reaction unit, including interior kettle 1, which is characterized in that the interior kettle 1 pushes up
End is fixedly connected with motor 2, and the output shaft of the motor 2 is fixedly connected with shaft 3, and shaft 3 is extend into interior kettle 1, and described turn
It is fixedly connected with stirring rod 4 on axis 3, heater strip 5 is housed inside stirring rod 4, is provided at the top of the motor 2 for heater strip
5 carry out the power-supply controller of electric 20 of start-up and shut-down control；1 inner wall of interior kettle is equipped with radio temperature sensor 6 and supersonic generator
7；The side on 1 top of interior kettle offers feeding-passage 8, and metering switch 9, the charging are provided on the feeding-passage 8
8 top of channel is connected with mixer 10, is equipped with mixing case lid 11 above the mixer 10,10 surface of mixer is equipped with
PLC controller 12 and display dial 13；The other side on 1 top of interior kettle is equipped with pressure gauge 14 and relief valve 15；In described
1 lower part of kettle is equipped with outer kettle 16, is equipped with condenser 17 in outer kettle 16；1 bottom of interior kettle is equipped with tapping channel 18；It is described
Radio temperature sensor 6, supersonic generator 7, metering switch 9, pressure gauge 14, relief valve 15, condenser 17, power-supply controller of electric
20 are connected with PLC controller 12 respectively；1 upper face of interior kettle is equipped with observation panel 19.
Preferably, being equipped with agitating device inside the mixer 10.
Preferably, the radio temperature sensor 6 is fixed on the inner wall of interior kettle 1, is received and turned by PLC controller 12
Change its temperature signal.
Preferably, the supersonic generator 7 is side wall supersonic generator.
Preferably, the condenser 17 passes through screw connection with outer kettle 16, condenser 17 is by way of air cooling
Cooling.
Preferably, the relief valve 15 is electromagnetic relief valve, the pressure gauge 14 and relief valve 15 pass through with interior kettle to be connect
Part connection.
Before reaction kettle work, first material is mixed in a certain ratio in mixer 10, closes mixing case lid 11, is opened mixed
Hopper power supply, the agitating device starting inside mixer, carries out material mixing.Material after mixing, in PLC controller 12
Set inlet amount, reaction temperature, vibration of ultrasonic wave frequency and pressure limit.After each parameter setting, start motor switch, this
When, 2 drive shaft 3 of motor, shaft 3 drives stirring rod 4 to start to stir, meanwhile, metering switch 9 is opened, mixture passes through charging
Channel 8 enters interior kettle 1, and the heater strip switch opened on power-supply controller of electric 20 is brought rapidly up reactant in kettle；When inlet amount reaches
When to setting value, metering switch 9 is closed, to close feeding-passage 8；During the reaction, radio temperature sensor 6 passes through
PLC controller 12 converts numerical value for the temperature signal detected and is presented to display dial 13, and operator pays attention to observing temperature
Numerical value when the temperature needed for temperature reaches reaction, need to close the heater strip switch on power-supply controller of electric 20, when temperature is excessively high,
While closing heater strip switch, the condenser switch of PLC controller 12 need to be opened, is carried out using the cold wind that condenser 17 manufactures
Cooling.PLC need to be utilized if there is material agglomerate in reactant by the response situation in 19 observing response kettle of observation panel simultaneously
The frequency of supersonic generator 7 is turned up in controller 12, and shatter agglomerate guarantees the consistent of material concentration.In reaction process, if pressure
The numerical value that power table 14 is shown is more than setting range, and PLC controller 12 will start relief valve 15 and carry out air pressure adjustment.Reaction is completed
Afterwards, supersonic generator 7 can cavity open, anti-deposition processes are carried out to reactant remaining in autoclave body, facilitate reaction kettle
Cleaning.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (6)
1. a kind of thermostatic type liquid chemical reaction unit, including interior kettle (1), which is characterized in that interior kettle (1) top is fixed to be connected
It is connected to motor (2), the output shaft of the motor (2) is fixedly connected with shaft (3), and shaft (3) is extend into interior kettle (1), described
It is fixedly connected in shaft (3) stirring rod (4), heater strip (5) is housed inside stirring rod (4), be provided at the top of the motor (2)
For heater strip (5) to be carried out with the power-supply controller of electric (20) of start-up and shut-down control；Interior kettle (1) inner wall is equipped with wireless temperature sensing
Device (6) and supersonic generator (7)；The side on interior kettle (1) top offers feeding-passage (8), the feeding-passage (8)
On be provided with metering switch (9), feeding-passage (8) top is connected with mixer (10), is set above the mixer (10)
Have mixing case lid (11), mixer (10) surface is equipped with PLC controller (12) and display dial (13)；The interior kettle
(1) other side on top is equipped with pressure gauge (14) and relief valve (15)；Interior kettle (1) lower part is equipped with outer kettle (16), outside
Condenser (17) are installed in kettle (16)；Interior kettle (1) bottom is equipped with tapping channel (18)；The radio temperature sensor
(6), supersonic generator (7), metering switch (9), pressure gauge (14), relief valve (15), condenser (17), power-supply controller of electric
(20) it is connected respectively with PLC controller (12)；
Interior kettle (1) upper face is equipped with observation panel (19).
2. chemical reaction kettle according to claim 1, it is characterised in that: be equipped with stirring dress inside the mixer (10)
It sets.
3. chemical reaction kettle according to claim 1, it is characterised in that: in the radio temperature sensor (6) is fixed on
On the inner wall of kettle (1), its temperature signal is received and converted by PLC controller (12).
4. chemical reaction kettle according to claim 1, it is characterised in that: the supersonic generator (7) is side wall ultrasound
Wave producer.
5. chemical reaction kettle according to claim 1, it is characterised in that: the condenser (17) and outer kettle (16) pass through spiral shell
Silk connection, condenser (17) are cooled down by way of air cooling.
6. chemical reaction kettle according to claim 1, it is characterised in that: the relief valve (15) is electromagnetic relief valve, should
Pressure gauge (14) and relief valve (15) are connect with interior kettle by connector.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711302405.0A CN109894057A (en) | 2017-12-10 | 2017-12-10 | A kind of thermostatic type liquid chemical reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711302405.0A CN109894057A (en) | 2017-12-10 | 2017-12-10 | A kind of thermostatic type liquid chemical reaction unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109894057A true CN109894057A (en) | 2019-06-18 |
Family
ID=66941414
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711302405.0A Pending CN109894057A (en) | 2017-12-10 | 2017-12-10 | A kind of thermostatic type liquid chemical reaction unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109894057A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111282537A (en) * | 2020-03-26 | 2020-06-16 | 河南东澳化工有限公司 | Preparation facilities of resistant strong solvent alkyd |
| CN112553268A (en) * | 2020-11-10 | 2021-03-26 | 南宁汉和生物科技股份有限公司 | Method and device for synthesizing trehalose by using ultrasonic-assisted enzyme |
| CN113855606A (en) * | 2021-09-17 | 2021-12-31 | 西藏山南德诺农林产业开发有限责任公司 | Ginger shampoo and preparation method thereof |
-
2017
- 2017-12-10 CN CN201711302405.0A patent/CN109894057A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111282537A (en) * | 2020-03-26 | 2020-06-16 | 河南东澳化工有限公司 | Preparation facilities of resistant strong solvent alkyd |
| CN112553268A (en) * | 2020-11-10 | 2021-03-26 | 南宁汉和生物科技股份有限公司 | Method and device for synthesizing trehalose by using ultrasonic-assisted enzyme |
| CN112553268B (en) * | 2020-11-10 | 2023-10-03 | 南宁汉和生物科技股份有限公司 | Method and device for synthesizing trehalose by ultrasound-assisted enzyme |
| CN113855606A (en) * | 2021-09-17 | 2021-12-31 | 西藏山南德诺农林产业开发有限责任公司 | Ginger shampoo and preparation method thereof |
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| Date | Code | Title | Description |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190618 |
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| WD01 | Invention patent application deemed withdrawn after publication |