CN208066340U - Pipeline flow-type microwave reactor - Google Patents
Pipeline flow-type microwave reactor Download PDFInfo
- Publication number
- CN208066340U CN208066340U CN201820220370.XU CN201820220370U CN208066340U CN 208066340 U CN208066340 U CN 208066340U CN 201820220370 U CN201820220370 U CN 201820220370U CN 208066340 U CN208066340 U CN 208066340U
- Authority
- CN
- China
- Prior art keywords
- microwave
- reactor
- type
- casing body
- pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model is related to microwave catalysis synthesis technical fields, it is a kind of pipeline flow-type microwave reactor, including casing body, microwave chamber, microwave generating apparatus, camera, external peristaltic pump and microcontroller, it is fixed with casing body in microwave cavity outside, and there is installation cavity between microwave chamber and casing body, it is installed with microcontroller, microwave generating apparatus, built-in machines agitating device in installation cavity, the fire door that can be closed and open microwave chamber is installed on casing body.The beneficial effects of the utility model are：The utility model is reasonable for structure, continuous continual microwave catalysis mode can must be carried out in environmental condition, the physical processes products such as unbroken solvent extraction for constantly producing organic and inorganic, drug and biochemical reaction and food, product of natural gas and mineral can be being reacted, reach desired effect.
Description
Technical field
The utility model is related to microwave catalysis synthesis technical fields, are a kind of pipeline flow-type microwave reactors.
Background technology
Microwave catalysis synthetic technology is catalyzed organic chemical reaction, improves the common technology of reaction yield.Microwave technology is adopted
With interior mode of heating, heating speed is fast, while it has been reported that low molecular activation energy can drop in its non-thermal effect having, promotion is anti-
It should occur.Ultrasonic technology converts electrical current into high-frequency mechanical vibration by ultrasonic transducer, utilizes cavitation and mechanism
Accelerate solute dissolving, the huge concentration of energy is caused when cavitation bubble collapse, to improve sample dissolving, extraction efficiency and instead
Product yield.Existing microwave catalysis synthetic technology is difficult to realize in the microwave catalysis synthetic reaction carried out in the lab, continuously
Charging, successive reaction, the demand of continuous production product and real-time high-precision thermometric, the reactant such as are sufficiently stirred work(at temperature control
Energy.
Utility model content
The utility model provides a kind of pipeline flow-type microwave reactor, overcomes the deficiency of the above-mentioned prior art,
It can effectively solve the problems, such as that existing microwave chemical instrument catalysis yield is not achieved expected and catalytic process and can not accurately control.
The purpose of this utility model is achieved through the following technical solutions：
A kind of pipeline flow-type microwave reactor, including casing body, microwave chamber, microwave generating apparatus, temperature pass
Sensor and microcontroller are fixed with casing body in microwave cavity outside, and have installation between microwave chamber and casing body
Chamber is installed with microcontroller, microwave generating apparatus, interior agitating device motor in installation cavity, pacifies on casing body
Equipped with the fire door that can be closed and open microwave chamber, two through-holes pass through water above and below casing body and microwave chamber-side have
Pipe is connected with external peristaltic pump, and a through-hole connects water inlet pipe, another through-hole connects outlet pipe.In microwave cavity room be equipped with
The temperature sensor of monolithic mechatronics is equipped with the liquid crystal display with monolithic mechatronics on casing body.
Further, movable reactor is equipped in the microwave cavity room, temperature sensor is set to movable reactor
In the temperature sensor interface of side, water inlet and the pagoda connector that water outlet is respectively movable reactor side, wherein on
Portion's pagoda connector is movable reactor water outlet, and lower part pagoda connector is movable reactor water inlet, and pagoda connector passes through
The through-hole of microwave cavity side passes through outside external shell extending equipment.
Further, the movable reactor is divided into two kinds, stirring reactor and coil pipe type reactor, water inlet
It is identical as water outlet connection type.
Further, the flow-type stirring reactor stirring-type is by upper cover, agitating shaft, upper cover dashpot, built-in fiber crops
Flower agitating paddle, reaction chamber, temperature sensor sealed base, hold-down bolt and pagoda connector composition, built-in fried dough twist agitating paddle and stream
Dynamic formula reactor top agitating shaft is connected, and agitating shaft is connected to the motor by being open in microwave cavity room.
Further, the flow-type coil pipe type reactor is by hose, water inlet pipe, outlet pipe, temperature sensor interface, branch
Frame forms.
Further, the waveguide cut-off pipe is located in microwave cavity room.
Further, the peristaltic pump is made of driver and pump head, and liquid is answered to access peristaltic pump by water pipe before anti-, and
It is connected with the water inlet pagoda connector of movable reactor by water pipe, the water outlet that liquid passes through movable reactor after reaction
Pagoda connector exports.
Further, microwave generating apparatus is magnetron in the microwave cavity room；Or/and it is set respectively on casing body
There are mini-printer, mechanical agitation switch, magnetic agitation switch, power switch and door open button；Or/and control panel is number
Word button, or/and, fan is installed in installation cavity.
The utility model is reasonable for structure, easy to use, in the case where not changing reaction condition, can with flow-type carry out
Microwave catalysis synthetic reaction, by peristaltic pump by reaction raw materials import and export and agitating paddle in movable reactor to original
Material is stirred, and realizes the function that production microwave catalysis synthetic reaction product is largely made in laboratory.The utility model
Technical solution, which can be catalyzed, completes substitution, addition, esterification, alkylation, acylation, hydrolysis, condensation, polymerization, cyclization and oxidation etc. perhaps
The physical processes such as the solvent extraction of the organic of polymorphic type, drug and biochemical reaction and video, product of natural gas and mineral, it is real
Show the purpose that flow-type reacts under stable environment in laboratory, reaches desired effect.
Description of the drawings
Fig. 1 is the structural schematic diagram that the utility model does not install movable reactor additional.
Fig. 2 is the structural schematic diagram of the utility model embodiment 1.
Fig. 3 is the structural schematic diagram of the utility model embodiment 2.
Coding is respectively in figure：1. casing, 2. microwave chambers, 3. agitating shafts, 4. upper covers, 5. stirring reactor chambers
Body, 6. fire doors, 7. pagoda connectors, 8. reaction chambers, 9. temperature sensors, 10. mechanical agitations switch, 11. power switches, 12. open
Door button, 13. magnetic agitations switch, 14. magnetic agitation indicator lights, 15. mini-printers, 16. function keys, 17. numbers are pressed
Key, 18. liquid crystal displays, 19. waveguide cut-off pipes, 20. stirring motors, 21. water outlets, 22. water inlets, 23. outlet pipes, 24.
Water inlet pipe, liquid before 25. reactions, 26. peristaltic pumps, liquid after 27. reactions, 28. coiled water outlets, the water inlet of 29. coileds
Mouthful, 30. pipe-coiling racks.
Specific implementation mode
As shown in Figure 1 to Figure 3, which includes casing body 1, microwave chamber 2, microwave hair
Generating apparatus 19, temperature sensor 9 and microcontroller are fixed with casing body 1 in the outside of microwave chamber 2, and microwave chamber 2 with
There is installation cavity between casing body 1, microcontroller, microwave generating apparatus 19, built-in stirring dress are installed in installation cavity
Motor is set, the fire door 6 that can be closed and open microwave chamber is installed on casing body 1, in casing body 1 and microwave cavity
2 side of room has up and down that two through-holes are connected by water pipe with external peristaltic pump, connects and intakes as water inlet 22 in through-hole
Pipe 24, another through-hole connect outlet pipe 23 as water outlet 21.The temperature with monolithic mechatronics is equipped in microwave chamber 2
Sensor 9 is equipped with the liquid crystal display 18 with monolithic mechatronics on casing body 1.
The utility model can carry out conventional microwave catalysis in the case where not starting peristaltic pump and being reacted without flow-type
Synthetic reaction is equivalent to a microwave catalysis synthesis abstraction instrument.It, can in the case where starting peristaltic pump and carrying out flow-type reaction
To realize under two kinds of different conditions of stirring-type and coiled, it is anti-to carry out to the flow-type of constant reaction conditions microwave catalysis synthesis
It answers.
The utility model is imported and exported reaction raw materials by peristaltic pump in the case where installing stirring reactor state, and
Agitating paddle carries out mechanically and magnetically power to raw material in movable reactor and stirs, and is in the reactor sufficiently mixed liquid before reaction
And realize for liquid charging stock before the reaction that is not sufficiently stirred during the reaction be sufficiently mixed stirring, can be constantly by raw material
Do not stop being added in reactor under the premise of reacting from equipment is external, while reaction product is drawn into reactor, realizes experiment
Indoor uninterrupted a large amount of functions of making production microwave catalysis synthetic reaction product.
The utility model may be implemented former for liquid before the reaction that is sufficiently stirred in the case where installing coil pipe type reactor state
Material carries out microwave catalysis reaction by ordering in launching, ensures that all liq sample obtains similarly reacting duration and same reaction item
Part.
The utility model can be catalyzed before reaction as the anti-of four kinds of forms such as liquid, solid-liquid mixture, suspension, emulsion
Preceding liquid is answered, during the reaction can be with two kinds of independent choice mechanical agitation, magnetic agitation agitating modes, it can be to different experiments item
Reactant realization under part is sufficiently stirred and reacts, the function of keeping each batch reactant reaction condition, duration constant.
The technical solution of the utility model can be catalyzed complete substitution, addition, esterification, alkylation, acylation, hydrolysis, condensation,
The organic of many types, drug and biochemical reaction and the video such as polymerization, cyclization and oxidation, product of natural gas and mineral it is molten
The physical processes such as agent extraction, have reached desired effect.
Embodiment 1：As shown in Figure 1, 2, stirring reactor cavity 5, temperature sensor are provided in the microwave cavity 2
9 are located at the side of reactor cavity 5, and magnetic stirring apparatus magnet rotor is located at the inside of reactor cavity 5, and the two of reactor cavity 5
A pagoda connector 7 is located in water outlet 21 and water inlet 22, and waveguide cut-off pipe 19 is located in microwave cavity 2.
Further, the water outlet 21 passes through water inlet pipe by liquid 27 after the importing reaction of outlet pipe 23, water inlet 22
24 are connected with peristaltic pump 26, and 26 front end of peristaltic pump passes through liquid 25 before 24 sucting reaction of water inlet pipe.
Embodiment 2：As shown in figure 3, difference from Example 1 is：It is anti-it to be provided with coiled in the microwave cavity 2
Device, reactor is answered to be located on pipe-coiling rack 30.
Further, the water outlet 28 of the coil pipe type reactor is connect with water outlet 21, and coiled is into 29 and water inlet
22 connections.
As shown in Figure 1, microwave generating apparatus is waveguide cut-off pipe 19 in the microwave cavity room；Or/and on casing body
It is respectively equipped with mini-printer 15, mechanical agitation switch 10, magnetic agitation switch 13, power switch 11 and door open button 12；Or/
With, control panel is digital keys 17, or/and, fan is installed in installation cavity.
Operation principle：After opening power supply, microcontroller controls magnetron microwave by transformer, to being reacted in reactor
Object is irradiated catalysis, and peristaltic pump is controlled by independent power supply and switch, can be connected with movable reactor in microwave cavity,
It is independent liquid compression before new reaction is entered in reactor reacts, and will liquid extraction device after reaction.
Claims (8)
1. a kind of pipeline flow-type microwave reactor, including casing body, microwave chamber, microwave generating apparatus, temperature sensing
Device and microcontroller are fixed with casing body in microwave cavity outside, and have installation cavity between microwave chamber and casing body,
It is installed with microcontroller, microwave generating apparatus, built-in machines agitating device in installation cavity, is equipped on casing body
Can be closed and open the fire door of microwave chamber, casing body and microwave chamber-side have up and down two through-holes by water pipe with
External peristaltic pump is connected, and is used as water inlet pipe, another through-hole to connect outlet pipe in a through-hole, is equipped with and list in microwave cavity room
The temperature sensor of piece mechatronics is equipped with the liquid crystal display with monolithic mechatronics on casing body.
2. pipeline flow-type microwave reactor according to claim 1, which is characterized in that be equipped with flow-type in microwave cavity room
Reactor, temperature sensor are set in the temperature sensor interface of movable reactor side, and water inlet is distinguished with water outlet
For the pagoda connector of movable reactor side, middle and upper part pagoda connector is movable reactor water outlet, and lower part pagoda connects
Head is movable reactor water inlet, and pagoda connector is passed through by the through-hole of microwave cavity side outside external shell extending equipment
Portion.
3. pipeline flow-type microwave reactor according to claim 1 or 2, which is characterized in that movable reactor is divided into
Two kinds, stirring reactor and coil pipe type reactor, water inlet are identical as water outlet connection type.
4. pipeline flow-type microwave reactor according to claim 1 or 2, which is characterized in that flow-type stirring-type reacts
Device stirring-type is by upper cover, agitating shaft, upper cover dashpot, built-in fried dough twist agitating paddle, reaction chamber, temperature sensor sealed base, pressure
Tight bolt and pagoda connector composition, built-in fried dough twist agitating paddle are connected with movable reactor top agitating shaft, and agitating shaft passes through micro-
Wave chamber inner opening is connected to the motor.
5. pipeline flow-type microwave reactor according to claim 1 or 2, which is characterized in that flow-type coiled reacts
Device is made of hose, water inlet pipe, outlet pipe, temperature sensor interface, holder.
6. pipeline flow-type microwave reactor according to claim 1, which is characterized in that waveguide cut-off pipe is located at microwave cavity
It is indoor.
7. pipeline flow-type microwave reactor according to claim 1, which is characterized in that peristaltic pump is by driver and pump head
Composition answers liquid to access peristaltic pump by water pipe, and passes through the water inlet pagoda connector phase of water pipe and movable reactor before anti-
Even, liquid is exported by the water outlet pagoda connector of movable reactor after reaction.
8. pipeline flow-type microwave reactor according to claim 1, which is characterized in that microwave fills in microwave cavity room
It is set to magnetron；Or/and mini-printer, mechanical agitation switch, magnetic agitation switch, electricity are respectively equipped on casing body
Source switch and door open button；Or/and control panel is digital keys, or/and, fan is installed in installation cavity.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820220370.XU CN208066340U (en) | 2018-02-08 | 2018-02-08 | Pipeline flow-type microwave reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820220370.XU CN208066340U (en) | 2018-02-08 | 2018-02-08 | Pipeline flow-type microwave reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208066340U true CN208066340U (en) | 2018-11-09 |
Family
ID=64037499
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820220370.XU Active CN208066340U (en) | 2018-02-08 | 2018-02-08 | Pipeline flow-type microwave reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208066340U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112439375A (en) * | 2020-11-06 | 2021-03-05 | 天津全和诚科技有限责任公司 | Coil pipe type microwave reactor |
-
2018
- 2018-02-08 CN CN201820220370.XU patent/CN208066340U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112439375A (en) * | 2020-11-06 | 2021-03-05 | 天津全和诚科技有限责任公司 | Coil pipe type microwave reactor |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105597651B (en) | A kind of nitromethane flow reactor | |
| CN206566912U (en) | A kind of high hydroscopic resin agitating device | |
| CN208066340U (en) | Pipeline flow-type microwave reactor | |
| CN105561904A (en) | Microwave synthesizer | |
| CN205308206U (en) | Energy -efficient agitator tank | |
| CN206549640U (en) | High efficiency reaction unit | |
| CN207694795U (en) | A kind of chemical industry stirred autoclave | |
| CN203577798U (en) | Reaction kettle with improved kettle body | |
| CN206064415U (en) | A kind of laboratory highly effective reaction kettle | |
| CN205683998U (en) | A kind of ultrasonic atomization micro-wave digestion synergism reactor | |
| CN202212138U (en) | Constant temperature magnetic stirring device | |
| CN206688695U (en) | A kind of industrial chemicals reaction unit | |
| CN215506793U (en) | High-flux induction heating type rotary reaction kettle | |
| CN209287315U (en) | The device of continuous production methyl tetrahydro phthalic anhydride | |
| CN202447063U (en) | High-efficiency reaction kettle | |
| CN208066338U (en) | The combination of dual-frequency ultrasonic wave microwave ultraviolet catalyzes and synthesizes instrument | |
| CN206823768U (en) | A kind of multifunctional reaction still | |
| CN219051210U (en) | Daily chemical product mixing stirring equipment | |
| CN204973905U (en) | Reactor | |
| CN209397203U (en) | A kind of agitating device of microbial fermentation | |
| CN214106891U (en) | Lithium dioxalate borate processing reaction accelerating device | |
| CN219849582U (en) | Novel organic synthesis reactor for laboratory | |
| CN203501733U (en) | Electro-thermal constant-temperature air blowing drying box with magnetic stirring function | |
| CN107537431A (en) | The reaction kettle device that a kind of Novel heating for Chemical Manufacture stirs | |
| CN219942846U (en) | Preparation facilities of trimethylsilyl diazomethane |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |