CN109260028B - Make-up fixing spray with isolation and repair effects and preparation method thereof - Google Patents
Make-up fixing spray with isolation and repair effects and preparation method thereof Download PDFInfo
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- CN109260028B CN109260028B CN201811264975.XA CN201811264975A CN109260028B CN 109260028 B CN109260028 B CN 109260028B CN 201811264975 A CN201811264975 A CN 201811264975A CN 109260028 B CN109260028 B CN 109260028B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention discloses a makeup fixing spray with an isolation and repair effect and a preparation method thereof, wherein the makeup fixing spray comprises the following components in parts by weight: 0.2-7 parts of spraying agent, 0.8-11 parts of functional active ingredient, 81-100 parts of solvent, 0.3-11 parts of film forming agent, 0.1-1 part of preservative, 0.01-1.5 parts of pH regulator, 0.05-1 part of chelating agent and 0.1-5 parts of humectant; the makeup fixing spray disclosed by the invention has good functionality, can meet daily makeup fixing requirements, overcomes inconvenience of makeup fixing powder scattering, is simple and convenient to spray, can fix makeup as long as being sprayed, is convenient to carry, and can not lead a makeup bag to be scattered everywhere, and the added functional active ingredients can also play a certain role in isolation, repair and the like; the components such as the spraying agent are added, so that the spraying atomization effect is better, and the makeup feeling is better.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a makeup fixing spray with an isolation and repair effect and a preparation method thereof.
Background
The makeup is to apply cosmetics and tools, and the face, five sense organs and other parts of the human body are rendered, drawn and arranged by adopting steps and skills in accordance with rules, so that the three-dimensional impression is enhanced, the shape and color are adjusted, the defects are covered, and the expression is magical, thereby achieving the purpose of beautifying. The makeup can show unique aesthetic interest of people, express personality and add charm. The successful makeup can arouse the psychological and physiological potential vitality of people, enhance the confidence, refresh the people, also help to eliminate fatigue and delay senility.
The makeup replacement after the makeup removal is an inevitable and anecdotal choice for every women who love makeup. Thus, the makeup setting products such as makeup setting powder, makeup setting liquid and the like which can make makeup more durable have wide and huge markets. The make-up fixing liquid can help the skin which is not easy to make up more durably without making up, can help make up clean and three-dimensional, astringe pores, increase the resistance of the face, keep moisture and balance grease, has an astringing effect, is not easy to remove the make-up and the like. However, the makeup fixing solution has various defects of slow film forming speed, sticky hand of the formed protective film, poor waterproofness and the like, the makeup is easily broken under the action of sweat, tear, rain mist and the like after makeup is finished, and women have higher and higher requirements on self makeup appearance, but a large amount of makeup is inconvenient to carry, and the makeup fixing solution with long lasting effect is needed. The inconvenience of fixing the powder is that the powder makes the dressing bag be powder everywhere; the common effects of the make-up fixing products on the market are single, and the requirements of consumers cannot be met.
Disclosure of Invention
The invention aims to overcome the problems and provide the makeup fixing spray with the isolation and repair functions and the preparation method thereof.
In order to achieve the purpose, the invention adopts the technical scheme that the makeup fixing spray with the isolation and repair function comprises the following components in parts by weight: 0.2-7 parts of spraying agent and 0.8-11 parts of functional active ingredients; the functional components comprise the following components in parts by weight: 0.5-3 parts of elecampane inula root extract, 0.5-3 parts of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butanediol 0.1-1 part of water/propylene glycol/buddleja officinalis flower extract, and 0.1-5 parts of water/glycerin/1, 3-propylene glycol/phenoxyethanol/ethylhexylglycerin/beta-glucan.
The elecampane inula root extract: elecampane Inula root (Inula Helenium) is widely distributed in europe and the world, is a medicinal plant which has been grown for hundreds of years, and becomes a common medicament in the middle-aged century for treating diseases. The elecampane inula root extract of the IBR is extracted from the overground part of the elecampane inula root by a special method, and has the functions of inactivating pollutants and protecting the skin from being damaged by pollutants by chelating and neutralizing the pollutants, and also can repair and reverse the damage of the pollutants (cigarette smoke) to the skin and protect skin cells from being damaged by active oxygen free radicals induced by high-energy visible light (blue light).
Centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol: the compound extract prepared from seven raw materials of asiatic centella, giant knotweed rhizome, baical skullcap root, tea, liquorice, chamomile and rosemary has broad-spectrum bacteriostatic effect and can inhibit the growth of E.coli (escherichia coli), S.aure (staphylococcus aureus), P.aeru (pseudomonas aeruginosa), C.albican (candida albicans) and A.niger (aspergillus niger); simultaneously, the skin allergy symptoms are relieved. The commercial name of this ingredient was Complex anti-allergic agent (CalmYang) supplied by Korea BioSpectrum.
The flos Buddlejae extract is composed of water, propylene glycol, flos Buddlejae extract to obtain compound, and full-effect light protectant, and strong effect is on erythema and oxidation pressure generated by Ultraviolet (UVB), blue light (HEV) and Infrared (IR), and is verified by four-dimensional experiment. The ingredient is provided by Baihabo corporation.
The mushroom glucan is a compound consisting of water/glycerin/1, 3-propylene glycol/phenoxyethanol/ethylhexyl glycerin/beta-glucan, is derived from Agaricus blazei, contains natural beta-glucan, is excellent in hand feeling, and is a multifunctional active ingredient with anti-inflammatory, anti-aging, moisturizing, after-sun repair and whitening effects. It has stronger effects in promoting cell growth, promoting wound healing and enhancing immune system, compared with glucan of yeast and plant origin. In addition, the product can protect skin from pollutants in the air, and has anti-pollution effect. The composition is provided by Guangzhou City jump-to-trade company, Inc.
According to the invention, elecampane inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butanediol, buddleja officinalis flower extract and mushroom glucan are taken as effective active ingredients, and the compounding of the ingredients has good antiallergic, anti-inflammatory and repairing effects.
Preferably, the spray comprises the following components in parts by weight: 0.1-2 parts of acrylic acid (ester)/beheneth-25 methacrylate copolymer and 0.1-5 parts of ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate.
Acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer: provides controlled, directed delivery of the spray emulsion; the novel texture brings surprise to consumers: emollients and beads can be suspended without heavy, even in low viscosity systems. The luxurious formulation of a release spray cream dispenses unique suspension and flow characteristics, excellent ionic resistance, efficient pH activity performance, easy to use, cold dispensable liquids. Acrylic/behenyl polyether-25 methacrylate copolymer, known under the trade name VolarestTM FL is offered by the great Chinese.
Ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetostearyl alcohol/monoglyceride/cetyl palmitate: is a liquid emulsion with a slight odor. The cosmetic contains typical O/W emulsion components including a nonionic emulsifier and a waxy component, and a material body can be sprayed in a nano-scale form and is matched with an acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer for use, so that the spray atomization effect is better, and the cosmetic feel is better. The trade name is nanoemulsion yes, supplied by Shanghai Feng Sheng daily chemical products Co.
Preferably, the makeup fixing spray further comprises the following components in parts by weight: 81-100 parts of solvent, 0.3-11 parts of film forming agent, 0.1-1 part of preservative, 0.01-1.5 parts of pH regulator, 0.05-1 part of chelating agent, 0.1-5 parts of humectant and 1-10 parts of ethanol.
Preferably, the film forming agent comprises the following components in parts by weight: the solvent comprises the following components in parts by weight: 81-100 parts; 350.1-5 parts of polyurethane, 0.1-5 parts of vinyl pyrrolidone/vinyl acetate copolymer and 0.1-1 part of polydimethylsiloxane; the preservative is phenoxyethanol/ethylhexyl glycerin, the pH regulator is triethanolamine, the chelating agent is disodium edetate, and the humectant comprises the following components in parts by weight: 0.01-2 parts of sodium hyaluronate and 0.1-5 parts of glycerol.
Polydimethylsiloxane: the product is also called dimeticone, has good lubricating property, can form a layer of uniform protective film with water resistance after being coated on skin, does not have any sticky or greasy feeling, and has good glossiness. The performance of resisting ultraviolet radiation is good: it is not oxidized and deteriorated under ultraviolet rays to cause skin irritation. The antistatic performance is good: tests show that the skin static electricity after being wiped by the skin care cream containing polysiloxane is completely eliminated, and the skin care cream has obvious dustproof effect. The air permeability is good: even the formation of a silicone film on the skin does not affect sweat discharge. It has the functions of slowly releasing and fixing fragrance, so that it has long fragrance-retaining period, high stability, chemical inertia and good compatibility with other components of cosmetics, especially active component. Has no toxicity, odor or taste, no irritation or allergy to skin, high safety, and certain therapeutic effect on dermatoses such as eczema neurodermatitis and occupational dermatitis with dyshidrosis.
VP/VA copolymer: can be used as binder, film forming agent and hair styling agent in cosmetics.
Disodium EDTA: can be used as chelating agent for stabilizing in cosmetic, and mineral chelating agent for synergistic preservation. And has a certain synergistic effect on an anticorrosion system and an antioxidant system.
Ethanol: is the only solvent allowed to be used in cosmetics other than water, and is the safest solvent for the skin. Ethanol is often found in the lotion, and the product added with ethanol for creating cool skin feeling is only suitable for specific skin, and the general skin is easy to dry and rough after long-term use and has the risk of premature keratinization. However, most of the regular cosmetics contain a small amount of ethanol and are often used as a solvent.
Phenoxyethanol/ethylhexyl glycerin (PE 9010): innovative novel compound preservative and global approval. Has broad-spectrum balanced inhibiting effect on bacteria, yeast and mold. Non-formaldehyde slow release type, mild action and no influence of hydrolysis, temperature and pH. The ideal anticorrosion system for the transparent condensation is suitable for products containing natural raw materials, and the safety is supported by a large amount of toxicological data. The pH is suitable for use in formulations with a pH of up to 12 and a temperature tolerance of up to 120 ℃ for contact with mucous membranes.
Preferably, the elecampane inula root extract: centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol: water/propylene glycol/buddleja officinalis extract: the mass ratio of water/glycerol/1, 3-propylene glycol/phenoxyethanol/ethylhexylglycerol/beta-glucan is 1:0.3:1: 1.5. The content ratios of the functional components are different, the sweat resistance, the durability and the makeup feeling are not greatly different from those of the embodiment 1, the anti-inflammation performance is reduced, and the ratios of the components influence the anti-inflammation effect, when the elecampane inula root extract: centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol: water/propylene glycol/buddleja officinalis extract: when the ratio of water to glycerin to 1, 3-propylene glycol to phenoxyethanol to ethylhexylglycerin to beta-glucan is 1:0.3:1:1.5, the effects of sweat resistance, durability, make-up feel and anti-inflammation are optimal;
preferably, the mass ratio of the acrylic acid (ester)/beheneth-25 methacrylate copolymer to ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate is 0.3: 2. The ratio was varied, and the anti-sweat, anti-persistence and anti-inflammatory properties were comparable to those of example 1, but the cosmetic feel was affected, and when the mass ratio of acrylic acid (ester)/beheneth-25 methacrylate copolymer to ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate was 0.3:2, the anti-sweat, persistence, cosmetic feel and anti-inflammatory properties were all optimized.
Preferably, the makeup fixing spray comprises the following components in parts by weight: 0.3 part of acrylic acid (ester)/beheneth-25 methacrylate copolymer, 2 parts of ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetostearyl alcohol/monoglyceride/cetyl palmitate, 1 part of elecampane inula root extract, 1 part of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomilla flower extract/rosemary leaf extract/butylene glycol, 1 part of water/propylene glycol/buddleja officinalis flower extract, 1.5 parts of water/glycerin/1, 3-propylene glycol/phenoxyethanol/ethylhexylglycerin/beta-glucan, and 86.15 parts of water. The inventor of the present application has found through a great deal of experiments that the sweat resistance, the durability, the cosmetic feeling and the anti-inflammatory performance of each component are optimal under the specific content.
Preferably, the feed also comprises the following components in parts by weight: 0.05 part of triethanolamine, 2 parts of polyurethane-351.5, 2 parts of ethanol, 1 part of vinyl pyrrolidone/vinyl acetate copolymer, 0.1 part of sodium hyaluronate, 0.1 part of disodium oxalate, 0.5 part of polydimethylsiloxane, 0.5 part of phenoxyethanol/ethylhexyl glycerin, 2 parts of glycerol and 86.15 parts of water.
The invention also provides a preparation method of the makeup fixing spray, which comprises the following steps:
1) adding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer into 90 wt% of water at 80 ℃ according to the weight parts, and stirring;
2) adding triethanolamine into the step 1) according to the parts by weight, stirring and neutralizing;
3) adding sodium hyaluronate, disodium oxalate, polydimethylsiloxane and glycerol into the step 2), and uniformly stirring;
4) mixing the rest water with ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetostearyl alcohol/monoglyceride/cetyl palmitate, cooling to 45 ℃ in step 3), adding the mixed solution of ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate and water into step 3), and uniformly stirring.
5) Adding polyurethane-35, ethanol, vinyl pyrrolidone/vinyl acetate copolymer, phenoxyethanol/ethylhexyl glycerol, elecampane inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol, buddleja officinalis flower extract and mushroom glucan into the mixture obtained in the step 4), stirring and uniformly mixing, discharging and filling.
The invention has the beneficial effects that: the makeup fixing spray disclosed by the invention has good functionality, can meet daily makeup fixing requirements, and meanwhile, the buddleja officinalis extract, mushroom glucan and the like are added, so that the makeup fixing spray has the functions of ultraviolet isolation, inflammation resistance and the like. The cosmetic bag is convenient to carry, and the cosmetic bag is not scattered everywhere. At present, the makeup fixing spray only has a single makeup fixing effect, and the added effective active ingredients can also play a certain role in isolation, repair and the like. The invention adds VolarestTM FL and other components, so that the spray atomization effect is better, and the makeup feeling is better. The invention adds active substances with the functions of ultraviolet isolation, anti-inflammation and the like, thereby further reducing the external damage to the skin.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
The raw materials used in the following examples are all commercially available general-purpose products unless otherwise specified.
Ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetostearyl alcohol/monoglyceride/cetyl palmitate in the present invention are the mixtures of ceteareth-20, ceteareth-12 and glycerol and of cetearyl isononanoate, cetearyl alcohol, monoglyceride, cetyl palmitate and glycerol, phenoxyethanol/ethylhexyl glycerol are the mixtures of phenoxyethanol and ethylhexyl glycerol, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomilla flower extract/rosemary leaf extract/butylene glycol, A mixture of Polygonum cuspidatum root extract, Scutellaria baicalensis root extract, Camellia sinensis extract, Glycyrrhiza glabra root extract, Matricaria chamomilla flower extract, Rosmarinus officinalis leaf extract, and butylene glycol.
Example 1
As an embodiment of the makeup fixing spray with the isolation and repair effect, the makeup fixing spray comprises the following components in parts by weight: acrylic acid (ester)/beheneth-25 methacrylate copolymer 0.3 parts, triethanolamine 0.05 parts, polyurethane-351.5 parts, ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate 2 parts, ethanol 2 parts, vinylpyrrolidone/vinyl acetate copolymer 1 parts, sodium hyaluronate 0.1 parts, edetate disodium 0.1 parts, polydimethylsiloxane 0.5 parts, phenoxyethanol/ethylhexyl glycerin 0.5 parts, glycerol 2 parts, elecampane root extract 1 parts, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 0.3 parts, 1 part of butterflybush flower extract, 1.5 parts of mushroom glucan and 86.15 parts of water.
The preparation method of the makeup remover spray of the embodiment comprises the following steps:
1) adding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer into 90 wt% of water at 80 ℃ according to the weight parts, and stirring;
2) adding triethanolamine into the step 1) according to the parts by weight, stirring and neutralizing;
3) adding sodium hyaluronate, disodium oxalate, polydimethylsiloxane and glycerol into the step 2), and uniformly stirring;
4) mixing the rest water with ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetostearyl alcohol/monoglyceride/cetyl palmitate, cooling to 45 ℃ in the step 3), adding the mixed solution of ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate and water into the step 3), and uniformly stirring;
5) adding polyurethane-35, ethanol, vinyl pyrrolidone/vinyl acetate copolymer, phenoxyethanol/ethylhexyl glycerol, elecampane inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol, buddleja officinalis flower extract and mushroom glucan into the mixture obtained in the step 4), stirring and uniformly mixing, discharging and filling.
Example 2
As an embodiment of the makeup fixing spray with the isolation and repair effect, the makeup fixing spray comprises the following components in parts by weight: acrylic acid (ester)/beheneth-25 methacrylate copolymer 0.5 parts, triethanolamine 0.08 parts, polyurethane-353 parts, ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate 1 parts, ethanol 3 parts, vinylpyrrolidone/vinyl acetate copolymer 0.5 parts, sodium hyaluronate 0.1 parts, edetate disodium 0.05 parts, polydimethylsiloxane 0.2 parts, phenoxyethanol/ethylhexyl glycerin 0.5 parts, glycerol 4 parts, elecampane root extract 1.5 parts, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 0.5 parts, 1 part of butterflybush flower extract, 2 parts of mushroom glucan and 82.07 parts of water. The preparation method of the makeup remover spray of this example is the same as that of example 1.
Example 3
As an embodiment of the makeup fixing spray with the isolation and repair effect, the makeup fixing spray comprises the following components in parts by weight: acrylic acid (ester)/beheneth-25 methacrylate copolymer 0.2 parts, triethanolamine 0.01 parts, polyurethane-351 parts, ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate 1 parts, ethanol 2 parts, vinylpyrrolidone/vinyl acetate copolymer 0.8 parts, sodium hyaluronate 0.02 parts, disodium oxalate 0.1 parts, polydimethylsiloxane 0.5 parts, phenoxyethanol/ethylhexyl glycerin 0.5 parts, glycerol 1 part, elecampane root extract 0.8 parts, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 0.8 parts, 1.5 parts of butterflybush flower extract, 1 part of mushroom glucan and 88.77 parts of water. The preparation method of the makeup remover spray of this example is the same as that of example 1. The preparation method of the makeup remover spray of this example is the same as that of example 1.
Example 4
As an embodiment of the makeup fixing spray with the isolation and repair effect, the makeup fixing spray comprises the following components in parts by weight: acrylic acid (ester)/beheneth-25 methacrylate copolymer 0.6 parts, triethanolamine 0.1 parts, polyurethane-352 parts, ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglycerides/cetyl palmitate 1.5 parts, ethanol 4 parts, vinylpyrrolidone/vinyl acetate copolymer 1.5 parts, sodium hyaluronate 0.05 parts, edetate disodium 0.05 parts, polydimethylsiloxane 0.2 parts, phenoxyethanol/ethylhexyl glycerin 0.5 parts, glycerol 3 parts, elecampane root extract 1 part, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 0.5 part, 1 part of butterflybush flower extract, 3 parts of mushroom glucan and 81 parts of water. The preparation method of the makeup remover spray of this example is the same as that of example 1. The preparation method of the makeup remover spray of this example is the same as that of example 1.
Example 5
As an embodiment of the makeup fixing spray with the isolation and repair effect, the makeup fixing spray comprises the following components in parts by weight: acrylic acid (ester)/beheneth-25 methacrylate copolymer 0.1 part, triethanolamine 0.01 part, polyurethane-350.1 part, ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate 0.1 part, ethanol 1 part, vinylpyrrolidone/vinyl acetate copolymer 0.1 part, sodium hyaluronate 1.5 part, edetate disodium 1 part, polydimethylsiloxane 0.1 part, phenoxyethanol/ethylhexyl glycerin 0.1 part, glycerol 0.1 part, elecampane root extract 3 parts, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 0.1 part, 0.1 part of butterflybush flower extract, 0.1 part of mushroom glucan and 80 parts of water. The preparation method of the makeup remover spray of this example is the same as that of example 1. The preparation method of the makeup remover spray of this example is the same as that of example 1.
Example 6
As an embodiment of the makeup fixing spray with the isolation and repair effect, the makeup fixing spray comprises the following components in parts by weight: acrylic acid (ester)/beheneth-25 methacrylate copolymer 2 parts, triethanolamine 1.5 parts, polyurethane-355 parts, ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate 5 parts, ethanol 10 parts, vinylpyrrolidone/vinyl acetate copolymer 5 parts, sodium hyaluronate 2 parts, disodium oxalate 0.5 part, polydimethylsiloxane 1 part, phenoxyethanol/ethylhexyl glycerin 1 part, glycerol 5 parts, elecampane root extract 1 part, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 1 part, and mixtures thereof, 2 parts of butterflybush flower extract, 5 parts of mushroom glucan and 90 parts of water. The preparation method of the makeup remover spray of this example is the same as that of example 1. The preparation method of the makeup remover spray of this example is the same as that of example 1.
Example 7
The difference between this example and example 1 is that the contents of the above-mentioned contents by weight of inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol, water/propylene glycol/buddleja officinalis flower extract, water/glycerin/1, 3-propylene glycol/phenoxyethanol/ethylhexylglycerin/beta-glucan are different, and the contents by weight of inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol are 0.8 parts, 1.5 parts, and, And 1 part of mushroom glucan.
Example 8
The difference between this example and example 1 is that the contents of the above-mentioned inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol, water/propylene glycol/buddleja officinalis flower extract, water/glycerin/1, 3-propylene glycol/phenoxyethanol/ethylhexylglycerin/beta-glucan are different, and the contents of inula root extract 1.5 parts, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 0.5 parts, buddleja officinalis flower extract 1 part, polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 0.5 parts, etc, 0.8 part of mushroom glucan.
Example 9
The difference between this example and example 1 is that the contents of the above-mentioned contents by weight of inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol, water/propylene glycol/buddleja officinalis flower extract, water/glycerin/1, 3-propylene glycol/phenoxyethanol/ethylhexylglycerin/beta-glucan are different, and the contents by weight of inula root extract 1.8 parts, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol 0.3 part of buddleja officinalis flower extract 0.9 part, and the contents by weight of the above-mentioned contents are different, And 1.8 parts of mushroom glucan.
Example 10
The difference between this example and example 1 is that the acrylic acid (ester)/beheneth-25 methacrylate copolymer and ceteareth-20/ceteareth-12/glycerin/isononanoic acid cetyl ester/cetostearyl alcohol/monoglyceride/cetyl palmitate content are different, the acrylic acid (ester)/beheneth-25 methacrylate copolymer of this example is 0.5 part, and the acrylic acid (ester)/beheneth-25 methacrylate copolymer is 1.8 parts.
Example 11
The difference between this example and example 1 is that the acrylic acid (ester)/beheneth-25 methacrylate copolymer and ceteareth-20/ceteareth-12/glycerin/isononanoic acid cetyl ester/cetostearyl alcohol/monoglyceride/cetyl palmitate content are different, and the acrylic acid (ester)/beheneth-25 methacrylate copolymer of this example is 1 part, and the acrylic acid (ester)/beheneth-25 methacrylate copolymer is 1.3 parts.
Example 12
The difference between this example and example 1 is that the acrylic acid (ester)/beheneth-25 methacrylate copolymer and ceteareth-20/ceteareth-12/glycerin/isononanoic acid cetyl ester/cetostearyl alcohol/monoglyceride/cetyl palmitate content by weight parts are different, and the acrylic acid (ester)/beheneth-25 methacrylate copolymer of this example is 1.3 parts, and acrylic acid (ester)/beheneth-25 methacrylate copolymer is 1 part.
Comparative example 1
This comparative example differs from example 1 only in that it does not contain an inula root extract.
Comparative example 2
The present comparative example differs from example 1 only in that centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol component is not included.
Comparative example 3
This comparative example differs from example 1 only in that it does not contain water/propylene glycol/buddleja officinalis extract.
Comparative example 4
This comparative example differs from example 1 only in that no mushroom glucan is included.
Comparative example 5
This comparative example differs from example 1 only in that it does not contain an elecampane extract, a buddleja officinalis extract.
Comparative example 6
This comparative example differs from example 1 only in that the ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate components are not included.
Comparative example 7
This comparative example differs from example 1 only in that it does not contain an acrylic/beheneth-25 methacrylate copolymer.
Example 13 stability test
The makeup remover sprays prepared in examples 1 to 12 were left at different temperatures for one month, and their stability was observed. The results are shown in table 1:
TABLE 1 examples 1-12 stability testing
| -18℃ | 5℃ | 25℃ | 48℃ | 5℃ | |
| Example 1 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 2 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 3 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 4 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 5 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 6 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 7 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 8 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 9 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 10 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 11 | Is normal | Is normal | Is normal | Is normal | Is normal |
| Example 12 | Is normal | Is normal | Is normal | Is normal | Is normal |
As can be seen from Table 1, the make-up fixing spray prepared by the present invention has good stability at-18 deg.C, 5 deg.C, 25 deg.C, 48 deg.C and 5 deg.C.
Example 14
Effect test of make-up spray
The experimental method comprises the following steps: randomly selecting 120 human volunteers with the age of 20-40. The makeup fixing spray of the examples and the comparative examples was used after makeup was performed daily in the morning for a total of 1 month without makeup. Carrying out questionnaire survey on volunteers, and comparing evaluation item feelings before and after use; table 2 shows the average scores of the fixed makeup sprays obtained in examples 1 to 12 and comparative examples 1 to 7.
TABLE 2 evaluation of Effect tests of examples 1 to 12 and comparative examples 1 to 7
| Sweat resistance | Durability | Make-up feel | Anti-inflammatory | |
| Example 1 | 9.6 | 9.7 | 9.5 | 9.8 |
| Example 2 | 9.4 | 9.5 | 9.2 | 9.3 |
| Example 3 | 9.5 | 9.3 | 9.1 | 9.2 |
| Example 4 | 9.4 | 9.5 | 9.1 | 9.2 |
| Example 5 | 9.2 | 9.4 | 9.0 | 9.1 |
| Example 6 | 9.4 | 9.2 | 9.0 | 9.2 |
| Example 7 | 9.5 | 9.3 | 9.4 | 9.0 |
| Example 8 | 9.4 | 9.5 | 9.3 | 9.2 |
| Example 9 | 9.3 | 9.4 | 9.5 | 9.0 |
| Example 10 | 9.4 | 9.4 | 9.0 | 9.7 |
| Example 11 | 9.5 | 9.4 | 8.9 | 9.5 |
| Example 12 | 9.3 | 9.5 | 8.7 | 9.4 |
| Comparative example 1 | 9.4 | 9.3 | 9.5 | 8.0 |
| Comparative example 2 | 9.5 | 9.4 | 9.3 | 8.2 |
| Comparative example 3 | 9.4 | 9.3 | 9.5 | 8.1 |
| Comparative example 4 | 9.6 | 9.5 | 9.3 | 8.2 |
| Comparative example 5 | 9.5 | 9.6 | 9.5 | 7.8 |
| Comparative example 6 | 9.4 | 9.4 | 8.0 | 9.4 |
| Comparative example 7 | 9.3 | 9.5 | 8.1 | 9.5 |
As can be seen from table 2, the makeup fixing spray of the present invention has good effects on sweat resistance, durability, makeup feel, and anti-inflammation, wherein, when the total content of elecampane inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomilla flower extract/rosemary leaf extract/butylene glycol, butterflybush flower extract, and mushroom glucan is consistent in examples 1 and 7 to 8, and in comparative examples 1 to 5, the content ratio of each component is different, and the sweat resistance, durability, and makeup feel are not greatly different from example 1, and the anti-inflammation property is reduced, indicating that the ratio of each component affects the anti-inflammation effect, when the total content of elecampane inula root extract: centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol: extract of butterflybush flower: when the ratio of mushroom glucan to glucan is 1:0.3:1:1.5, the effects of sweat resistance, durability, make-up feel and inflammation resistance of the mushroom glucan are optimal; compared with example 1, comparative examples 1 to 5 lack one or two components, and the anti-inflammation property is correspondingly reduced according to the results, which shows that the inula root extract, the centella asiatica extract/the polygonum cuspidatum root extract/the scutellaria baicalensis root extract/the tea leaf extract/the glycyrrhiza glabra root extract/the chamomile flower extract/the rosemary leaf extract/the butanediol, the butterflybush flower extract and the mushroom glucan have synergistic effect of anti-inflammation function when used simultaneously; by comparing examples 1, 10 to 12, and 6 to 7, examples 10 to 12 were identical to examples 1 in terms of total content of acrylic acid (ester)/beheneth-25 methacrylate copolymer and ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl cetonol monoglyceride/cetyl palmitate, but the ratio was different, and it was found that the antiperspirant, the persistence and the anti-inflammatory properties were not much different from those of example 1, and the cosmetic feel was slightly inferior to that of example 1, indicating that when the mass ratio of acrylic acid (ester)/beheneth-25 methacrylate copolymer to ceteareth-20/ceteareth-12/glycerin/cetearyl isononate/cetyl alcohol/monoglyceride/cetyl palmitate was 0.3:2 When used, it has excellent sweat resistance, durability, makeup feeling and anti-inflammatory property. Compared with example 1, examples 6 to 7 lack the acrylic acid (ester)/beheneth-25 methacrylate copolymer and ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl/monoglyceride/cetyl palmitate, respectively, and the cosmetic feel is different from example 1, which shows that the cosmetic feel is optimal when the acrylic acid (ester)/beheneth-25 methacrylate copolymer and ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl/monoglyceride/cetyl palmitate are used simultaneously.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like made within the spirit and principle of the present invention should be included in the scope of the present invention.
Claims (3)
1. The makeup fixing spray with the isolation and repair effect is characterized by comprising the following components in parts by weight: 0.2-7 parts of spraying agent and 0.8-11 parts of functional active ingredients; the functional active ingredients comprise the following components in parts by weight: 0.5-3 parts of elecampane inula root extract, 0.5-3 parts of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butanediol 0.1-1 part, 0.1-2 parts of butterflybush flower extract and 0.1-5 parts of mushroom glucan;
the spray comprises the following components in parts by weight: 0.1-2 parts of acrylic acid (ester)/beheneth-25 methacrylate copolymer, and 0.1-5 parts of ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate;
the elecampane inula root extract: centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol: extract of butterflybush flower: the mass ratio of the mushroom glucan is 1:0.3:1: 1.5; the mass ratio of the acrylic acid (ester)/beheneth-25 methacrylate copolymer to ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate is 0.3: 2.
2. The makeup fixing spray according to claim 1, which is characterized by comprising the following components in parts by weight: 0.3 part of acrylic acid (ester)/beheneth-25 methacrylate copolymer, 2 parts of ceteareth-20/ceteareth-12/glycerin/cetearyl isononanoate/cetostearyl alcohol/monoglyceride/cetyl palmitate, 1 part of elecampane inula root extract, 1 part of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomilla flower extract/rosemary leaf extract/butylene glycol 0.3 part, 1 part of butterflybush flower extract, 1.5 parts of mushroom dextran, 0.05 part of triethanolamine, 0.32 part of polyurethane-351.5 part of ethanol 2 part, 1 part of vinylpyrrolidone/vinyl acetate copolymer, 0.1 part of sodium hyaluronate, 0.1 part of disodium edetate, 0.5 part of polydimethylsiloxane, 0.1 part of sodium hyaluronate, 0.5 part of phenoxyethanol/ethylhexyl glycerin, 2 parts of glycerol and 86.15 parts of water.
3. A method of preparing a make-up mist according to claim 2, comprising the steps of:
1) adding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer into 90 wt% of water at 80 ℃ according to the weight parts, and stirring;
2) adding triethanolamine into the step 1) according to the parts by weight, stirring and neutralizing;
3) adding sodium hyaluronate, disodium oxalate, polydimethylsiloxane and glycerol into the step 2), and uniformly stirring;
4) mixing the rest water with ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetostearyl alcohol/monoglyceride/cetyl palmitate, cooling to 45 ℃ in the step 3), adding the mixed solution of ceteareth-20/ceteareth-12/glycerol/cetearyl isononanoate/cetearyl alcohol/monoglyceride/cetyl palmitate and water into the step 3), and uniformly stirring;
5) adding polyurethane-35, ethanol, vinyl pyrrolidone/vinyl acetate copolymer, phenoxyethanol/ethylhexyl glycerol, elecampane inula root extract, centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol, buddleja officinalis flower extract and mushroom glucan into the mixture obtained in the step 4), stirring and uniformly mixing, discharging and filling.
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| CN112315885A (en) * | 2020-12-03 | 2021-02-05 | 中山市美源化妆品有限公司 | Makeup fixing spray and manufacturing method thereof |
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