CN109251798A - A kind of production method of dark green tea cleaning solution - Google Patents
A kind of production method of dark green tea cleaning solution Download PDFInfo
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- CN109251798A CN109251798A CN201811458131.9A CN201811458131A CN109251798A CN 109251798 A CN109251798 A CN 109251798A CN 201811458131 A CN201811458131 A CN 201811458131A CN 109251798 A CN109251798 A CN 109251798A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
- C11D7/12—Carbonates bicarbonates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/265—Carboxylic acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/329—Carbohydrate or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
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- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Veterinary Medicine (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Molecular Biology (AREA)
- Inorganic Chemistry (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
Abstract
The invention belongs to cleaning solution fields, specifically disclose a kind of dark green tea cleaning solution of long-acting bacteriostatic, raw material including following mass fraction: 50~70 parts of deionized water, 10~30 parts of black tea extract, 5~15 parts of chitosan, 0.5~4 part of sodium carboxymethylcellulose, 1~5 part of pectin, 0.5~4 part of food-grade chelating agent, 0.5~5 part of food-grade wetting agent, 0.5~4 part of food-grade pH adjusting agent.The present invention is nonirritant, has broad-spectrum antibacterial, energy long-acting bacteriostatic and good antimicrobial effect, can serve as dish washing liquid and hand cleanser, for children or the crowd of skin sensitivity.
Description
A kind of dark green tea cleaning solution of long-acting bacteriostatic, the raw material including following mass fraction: 50~70 parts of deionized water, dark green tea
10~30 parts of extract, 5~15 parts of chitosan, 0.5~4 part of sodium carboxymethylcellulose, 1~5 part of pectin, food-grade chelating agent
0.5~4 part, 0.5~5 part of food-grade wetting agent, 0.5~4 part of food-grade pH adjusting agent.One kind that the technical program provides is long-acting
Antibacterial dark green tea cleaning solution use food grade materials, eat by mistake it is non-hazardous, it is non-stimulated to skin, avoid generate skin allergy, be suitble to
Baby and sensitive skin can be used as hand cleanser, dish washing liquid etc..Dark green tea cleaning solution of the invention contains dark green tea extracting solution and chitosan
Two kinds have the active substance of broad-spectrum antibacterial, not only all have the function of long-acting bacteriostatic, including gold to Common fungi and various bacteria
Staphylococcus aureus, Escherichia coli, Candida albicans etc., fungistatic effect are ideal, also to Detection of Porphyromonas, Fusobacterium nucleatum, in
Between the oral cavity pathogens such as general Salmonella and Streptococcus mutans have it is strong effective kill inhibitory effect, while not influencing normal flora
Growth.Sodium carboxymethylcellulose of the invention and pectin collocation can form the thick liquid with stereoscopic three-dimensional network in water
Body, dark green tea extracting solution and chitosan are dispersed in the solution of stereoscopic three-dimensional network, can increase dark green tea extracting solution and shell is poly-
The solubility of sugar, and its antibacterial time can be extended.The present invention is additionally added food-grade chelating agent, can be with complexing heavy metal, energy
The heavy metal being harmful to the human body is effectively removed, the food-grade chelating agent can also promote to promote fungistatic effect；The present invention also adds
Enter wetting agent, skin water can preferably be kept to moisten；The present invention is additionally added the adjustable dark green tea cleaning solution of pH adjusting agent to suitable skin
The acid-base property of skin achievees the effect that not stimulate skin.Preferably, the dark green tea cleaning solution of a kind of long-acting bacteriostatic, including following quality
The raw material of number: 60 parts of deionized water, 20 parts of black tea extract, 10 parts of chitosan, 2 parts of sodium carboxymethylcellulose, pectin 2.5
Part, 1 part of food-grade chelating agent, 3 parts of food-grade wetting agent, 1.5 parts of food-grade pH adjusting agent.This programme optimizes the ratio of each raw material
Example keeps the concentration of bacteriostatic active ingredients more suitable, and the compatibility of each raw material is more preferable in system, and system stability is good, the shelf-life
It is long.Preferably, the chitosan is high deacetylized comprising 30%~50% low deacetylation chitosan and 50%~70%
Chitosan.This programme arrange in pairs or groups different deacetylations chitosan can making it dissolve property it is more preferable, and guarantee bactericidal and bacteriostatic effect
It is good.Preferably, the food-grade chelating agent is at least one of sodium citrate, sodium gluconate, sodium acetate, sodium tartrate.
The stability of the preferred several foods grade chelating agent of this programme is good, edible, and the dissolubility in system is good.Preferably, described
Food-grade moisturizer include 50% D-sorbite and 50% beta glucan.The not only day of food-grade moisturizer described in this prioritization scheme
So non-stimulated, moistening effect is good, can be used as metal-chelator removal part metals ion, moreover it is possible to promote antibacterial effect.It is preferred that
Ground, the food-grade pH adjusting agent are at least one of lactic acid, acetic acid, sodium carbonate or sodium bicarbonate.This programme is preferred
The type of food-grade pH adjusting agent, preferred pH adjusting agent are edible, and facilitate the acid-base property for adjusting cleaning solution.This hair
The production method of the bright dark green tea cleaning solution for additionally providing a kind of above-mentioned long-acting bacteriostatic, includes the following steps: (1), goes described
Ionized water is added in stirring container, stirs at low speed 50~200rpm/min at a temperature of 20~30 DEG C, is slowly added to while stirring
Sodium carboxymethylcellulose and pectin, then 600~800rpm/min of high-speed stirred is uniformly dispersed.(2), Partial Food grade pH is added
PH is adjusted to 5.0~6.0 by regulator, and the black tea extract and the chitosan is then added into stirring container, high speed
It is dispersed with stirring uniformly.(3), food-grade chelating agent is sequentially added, then food-grade wetting agent is slowly taken out true when stirring at low speed
PH is adjusted to 6.5~7.0 by sky, the food-grade pH adjusting agent that remainder is added, be gradually increased vacuum degree to -0.9MPa with
Under, it then maintains vacuum degree to carry out high-speed stirred to being uniformly dispersed, stops stirring and vacuumize, obtain long-acting suppression of the invention
The dark green tea cleaning solution of bacterium.In production method of the invention, sodium carboxymethylcellulose and pectin are first added in ionized water, using elder generation
The mode for stirring at low speed again high-speed stirred makes sodium carboxymethylcellulose and pectin and water form uniform 3 D stereo mesh space
Structure.Then addition dark green tea extracting solution and chitosan high-speed stirred under slightly acidic condition is added to be allowed to be dispersed in stereoscopic three-dimensional
In the solution of network, the solubility of dark green tea extracting solution and chitosan can be increased, and its restraining and sterilizing bacteria time can be extended.Most
Food-grade chelating agent, food-grade wetting agent are added afterwards, and adjusts pH close to neutrality, stirring can remove bubble under vacuum conditions,
And dispersion is more evenly.In conclusion a kind of dark green tea cleaning solution of long-acting bacteriostatic of the present invention and preparation method thereof has the beneficial effect that
Production method and simple production process, are easy to industrialization；Dark green tea cleaning solution obtained is non-stimulated to skin close to neutrality；It uses
Raw material is food-grade, is not concerned about child and eats by mistake；Good antimicrobial effect, broad-spectrum antibacterial and long-acting bacteriostatic；Can with complexing heavy metal from
Son；Moistening effect is good.Product of the present invention can be used for the bacteriostatic hand sanitizer and antibacterial dish washing liquid of child and sensitive skin.
Specific embodiment
Specific embodiment in order to make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with reality
Example is applied, the present invention will be described in further detail.It should be appreciated that specific embodiment described herein is only used to explain this
Invention, is not intended to limit the present invention.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creation
Property labour under the premise of every other embodiment obtained, shall fall within the protection scope of the present invention.Unless stated otherwise, of the invention
The reagent that uses, method and apparatus is the art conventional reagents, method and apparatus.
A kind of dark green tea cleaning solution of the long-acting bacteriostatic of 1 the present embodiment of embodiment, the raw material including following mass fraction: go from
60 parts of sub- water, 20 parts of black tea extract, 4 parts of low deacetylation chitosan, 6 parts of chitosan with high deacetylation degree, carboxymethyl cellulose
2 parts of sodium, 2.5 parts of pectin, 1 part of sodium gluconate, 1.5 parts of D-sorbite, 1.5 parts of beta glucan, 1 part of lactic acid, sodium carbonate 0.5
Part.A kind of production method of the dark green tea cleaning solution of long-acting bacteriostatic of the present embodiment includes the following steps: (1), by the deionization
Water is added in stirring container, stirs at low speed 50~200rpm/min at a temperature of 20~30 DEG C, is slowly added to carboxylic first while stirring
Base sodium cellulosate and pectin, then 600~800rpm/min of high-speed stirred is uniformly dispersed.(2), lactic acid is added to be adjusted to pH
5.0~6.0, the black tea extract and the chitosan is then added into stirring container, high-speed stirred is uniformly dispersed.(3),
Sodium gluconate, D-sorbite are sequentially added, then beta glucan is slowly vacuumized when stirring at low speed, sodium carbonate is added will
PH is adjusted to 6.5~7.0, and vacuum degree is gradually increased to -0.9MPa hereinafter, vacuum degree is then maintained to carry out high-speed stirred to dispersion
Uniformly, stop stirring and vacuumize, obtain the dark green tea cleaning solution of long-acting bacteriostatic of the invention.
A kind of dark green tea cleaning solution of the long-acting bacteriostatic of 2 the present embodiment of embodiment, the raw material including following mass fraction: go from
70 parts of sub- water, 10 parts of black tea extract, 7.5 parts of low deacetylation chitosan, 7.5 parts of chitosan with high deacetylation degree, carboxymethyl is fine
Plain 0.5 part of the sodium of dimension, 2 parts of pectin, 0.5 part of sodium acetate, 0.5 part of D-sorbite, 0.5 part of beta glucan, 0.5 part of acetic acid, bicarbonate
0.5 part of sodium.A kind of production method of the dark green tea cleaning solution of long-acting bacteriostatic of the present embodiment, includes the following steps: (1), will be described
Deionized water is added in stirring container, stirs at low speed 50~200rpm/min at a temperature of 20~30 DEG C, slowly adds while stirring
Enter sodium carboxymethylcellulose and pectin, then 600~800rpm/min of high-speed stirred is uniformly dispersed.(2), acetic acid is added by pH tune
Section is 5.0~6.0, the black tea extract and the chitosan is then added into stirring container, high-speed stirred is uniformly dispersed.
(3), sodium acetate, D-sorbite are sequentially added, then beta glucan is slowly vacuumized when stirring at low speed, sodium bicarbonate is added
PH is adjusted to 6.5~7.0, vacuum degree is gradually increased to -0.9MPa and extremely divides hereinafter, vacuum degree is then maintained to carry out high-speed stirred
It dissipates uniformly, stop stirring and vacuumizes, obtain the dark green tea cleaning solution of long-acting bacteriostatic of the invention.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (9)
1. a kind of dark green tea cleaning solution of long-acting bacteriostatic, which is characterized in that the raw material including following mass fraction: deionized water 50~
70 parts, 10~30 parts of black tea extract, 5~15 parts of chitosan, 0.5~4 part of sodium carboxymethylcellulose, 1~5 part of pectin, food
0.5~4 part of chelating agent, 0.5~5 part of food-grade wetting agent, 0.5~4 part of food-grade pH adjusting agent of grade.
2. a kind of dark green tea cleaning solution of long-acting bacteriostatic according to claim 1, which is characterized in that including following mass fraction
Raw material: 60 parts of deionized water, 20 parts of black tea extract, 10 parts of chitosan, 2 parts of sodium carboxymethylcellulose, 2.5 parts of pectin, food
1 part of grade chelating agent, 3 parts of food-grade wetting agent, 1.5 parts of food-grade pH adjusting agent.
3. a kind of dark green tea cleaning solution of long-acting bacteriostatic according to claim 1 or 2, which is characterized in that the chitosan
Include 30%~50% low deacetylation chitosan and 50%~70% chitosan with high deacetylation degree.
4. a kind of dark green tea cleaning solution of long-acting bacteriostatic according to claim 1 or 2, which is characterized in that the food-grade
Chelating agent is at least one of sodium citrate, sodium gluconate, sodium acetate.
5. a kind of dark green tea cleaning solution of long-acting bacteriostatic according to claim 1 or 2, which is characterized in that the food-grade
Moisturizer includes 50% D-sorbite and 50% beta glucan.
6. a kind of dark green tea cleaning solution of long-acting bacteriostatic according to claim 1 or 2, which is characterized in that food-grade pH is adjusted
Agent includes at least one of acid regulator lactic acid, acetic acid and alkaline conditioner sodium carbonate, sodium bicarbonate, the long-acting suppression
The dark green tea cleaning solution final pH of bacterium is adjusted to 6.5~7.0.
7. a kind of production method of the dark green tea cleaning solution of long-acting bacteriostatic as described in claim 1, which is characterized in that including as follows
Step: (1) it, by the deionized water is added in stirring container, stirs at low speed 50~200rpm/ at a temperature of 20~30 DEG C
Min is slowly added to sodium carboxymethylcellulose and pectin while stirring, and then 600~800rpm/min of high-speed stirred is uniformly dispersed.
8. Partial Food grade pH adjusting agent (2), which is added, is adjusted to 5.0~6.0 for pH, the black tea extract and institute is then added
Chitosan is stated into stirring container, high-speed stirred is uniformly dispersed.
9. (3), sequentially adding food-grade chelating agent, then food-grade wetting agent is slowly vacuumized when stirring at low speed, and is added surplus
PH is adjusted to 6.5~7.0 by the food-grade pH adjusting agent of remaining part point, and vacuum degree is gradually increased to -0.9MPa hereinafter, then maintaining
Vacuum degree carries out high-speed stirred to being uniformly dispersed, and stops stirring and vacuumizes, the dark green tea for obtaining long-acting bacteriostatic of the invention is clear
Clean liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811458131.9A CN109251798A (en) | 2018-11-30 | 2018-11-30 | A kind of production method of dark green tea cleaning solution |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811458131.9A CN109251798A (en) | 2018-11-30 | 2018-11-30 | A kind of production method of dark green tea cleaning solution |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109251798A true CN109251798A (en) | 2019-01-22 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811458131.9A Withdrawn CN109251798A (en) | 2018-11-30 | 2018-11-30 | A kind of production method of dark green tea cleaning solution |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107854369A (en) * | 2017-12-21 | 2018-03-30 | 湖南华莱生物科技有限公司 | A kind of black tea cleaning solution of long-acting bacteriostatic and preparation method thereof |
-
2018
- 2018-11-30 CN CN201811458131.9A patent/CN109251798A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107854369A (en) * | 2017-12-21 | 2018-03-30 | 湖南华莱生物科技有限公司 | A kind of black tea cleaning solution of long-acting bacteriostatic and preparation method thereof |
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Application publication date: 20190122 |