CN109234040A - Natural plants Saponaria officinalis is mostly used dish washing liquid and the preparation method and application thereof - Google Patents
Natural plants Saponaria officinalis is mostly used dish washing liquid and the preparation method and application thereof Download PDFInfo
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- CN109234040A CN109234040A CN201811244763.5A CN201811244763A CN109234040A CN 109234040 A CN109234040 A CN 109234040A CN 201811244763 A CN201811244763 A CN 201811244763A CN 109234040 A CN109234040 A CN 109234040A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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Abstract
The present invention relates to a kind of natural plants Saponaria officinalis to be mostly used dish washing liquid and the preparation method and application thereof.Raw material includes 20 parts of Saponaria officinalis extract, 10 parts of soapberry extract, 0.25 part of lemon-grass volatile oil, 0.4 part of grape fruit volatile oil, 0.25 part of seaweed glue, 68 parts of lemon-grass hydrosol, 1 part of citric acid and 0.1 part of Cortex Cinnamomi volatile oil.Natural plant cleanser essence provided by the invention selects the plant extract containing active skull cap components to form, prescription proportion science, any artificial synthesis group point is not added, and natural soap grass and soapberry saponin all rich in, efficient combination complementation produce it is a kind of with it is pure natural, have no toxic side effect, using the health care detergent product of multifunctional safety., can be mild to skin with softening of water in addition, natural plant cleanser essence of the present invention not only has potent cleaning action, the role of substituted chemistry petroleum-type interfacial agent can be played, and easy to use, be with a wide range of applications.
Description
Technical field
The present invention relates to dish washing liquid technical fields, and in particular to a kind of natural plants Saponaria officinalis is mostly used dish washing liquid and its preparation
Method and application.
Background technique
It is well known that dish washing liquid is generally used on cleaning tableware as articles for washing very common in family life
Greasy dirt, main component are surfactant.The ingredients such as surfactant and preservative used in dish washing liquid are commonly at present
The advantages of synthesis of chemicals, such surfactant is that strong detergency, dissolubility are good, and cost is relatively low, but if being used for a long time,
Remaining micro dish washing liquid generates potential threat to human body at branch on tableware, and can generate to the skin of dish washing liquid user
Negative effect, easily makes pachylosis turn yellow, and especially for the more sensitive user of skin, it is double that this kind of dish washing liquid is used for a long time
The symptoms such as hand will appear dry and astringent, decortication, coarse and hand is easily got blister.
In addition, in recent years, with the raising of people's living standard and quality of life, people are to detergent especially dish washing liquid
More stringent requirements are proposed, not only requires dirt-removing power strong, and it is also desirable to have that highly-safe, bactericidal effect is good, non-stimulated
The effect of property.In addition, the dish washing liquid rinse cycle of chemical products synthesis needs a large amount of water that can just be thoroughly rinsed completely, in guarantor
While healthy, need to consume a large amount of water；And the discharge of chemical dish washing liquid on the market at present for underground water and soil all
It will cause very big pollution.Based on this, provide it is a kind of it is novel there is potent cleaning action, and washed to what skin mildly easily rinsed
Clean essence is particularly important.
Summary of the invention
For the defects in the prior art, the present invention is intended to provide a kind of natural plants Saponaria officinalis is mostly used dish washing liquid and its system
Preparation Method and application.Natural plant cleanser essence provided by the invention selects the plant extract containing active skull cap components to form, group
Side's proportion science, does not add any artificial synthesis group point, and natural soap grass and soapberry saponin all rich in,
Efficient combination complementation produce it is a kind of with it is pure natural, have no toxic side effect, using the health care detergent product of multifunctional safety.
In addition, Saponaria officinalis complete stool contains natural plants saponin(e, not only there is potent cleaning action, it can be with softening of water, to skin
Mildly, soapberry has potent cleaning and antifungic action, can play the role of substituted chemistry petroleum-type interfacial agent, and
It is easy to use, it is with a wide range of applications.
For this purpose, the invention provides the following technical scheme:
In a first aspect, the present invention provides a kind of natural plant cleanser essence, raw material components are by weight, comprising: Saponaria officinalis
20~30 parts by weight of extract, 10~20 parts by weight of soapberry extract, 0.2~0.3 parts by weight of lemon-grass volatile oil, grape fruit
0.1~0.5 parts by weight of volatile oil, 0.2~0.3 parts by weight of seaweed glue, 50~70 parts by weight of lemon-grass hydrosol, citric acid 0.5~1
0.1~0.25 parts by weight of parts by weight and Cortex Cinnamomi volatile oil.
Specifically, Saponaria officinalis is called Saponaria officinalis, belongs to a kind of perennial herb soapsort persistent root herbs.At me
The cities such as state Dalian, Qingdao wild plant；Its root can be used as medicine, and have the function of eliminating the phlegm, control tracheitis, diuresis.Soapberry
Have the function of antibacterial, anti-dandruff, anticreep, whitening despeckle, skin care；" soapberry can pre- anti-dandruff ", containing abundant natural
Saponin(e is natural washing product raw material.Lemon-grass is the general designation of about 55 kinds of fragment plants of grass family Cymbopogon, as
One of common vanilla is a kind of high and thin plant, most common in South Asia region (especially Philippine)；Because there is lemon
Fragrance, therefore the lemon grass (Cymbopogon citratus) that is otherwise known as；It is with excellent treatment rheumatism, migraine, anti-infective, improvement digestive function, deodorization, drive
Worm, the greasy unclean skin of conditioning, assigns freshness, restores balance of body and spirit (especially sick rank just more anti-infective, Cress
Section) and other effects, it is the volatile oil that purposes is most wide in aromatotherapy and medical method, it can also be used to work as aromatic in interior.It is answered
This product is used, natural flavor can be banned, it is good and cheap.Grape fruit, it is cool in nature, it is sweet in flavor acid, there is the benefits of heat-clearing, quench the thirst, grape
Shaddock volatile oil is obtained by being squeezed as pericarp, and smell is pure and fresh, fragrant and sweet, there is the fruit flavor of citrus；Grapefruit essential oil energy nurse tissue
Cell increases physical strength, is bronchitis of releiving, diuresis, the disease for improving fat, oedema and lymph glandular system, anti-infective；Grape fruit
Essential oil can also resist melancholy that can make one to refresh when especially the symptoms such as melancholy or drowsy occurs in winter, be seasonal
The regulator of psychataxia.This product, which is added, can replace essence, and naturally pure and fresh fragrance increases pleasant feeling when using.Lemon
Acid is a kind of important organic acid also known as citric acid, the natural product from plant fermentation, adjustable product pH value, increase tune
Reason sense；Citric acid is edible acids, can eubolism in reinforcement, dosage appropriate is harmless；Add in certain food
Enter in good taste after citric acid, and can promote appetite；Builder is made using citric acid, the performance of cleaning product, Ke Yixun can be improved
Fast precipitate metal ion prevents pollutant to be re-attached on the object after cleaning.Seaweed glue has excellent stability, glue
Solidifying property, conformality, film shaped property, and there is unique healthcare function, also frequently as the primary raw material of skin protection cosmetics, increase
The water-retaining property for adding skin increases the moistening effect of skin, thus promotes skin more aobvious beautiful and be not likely to produce allergic reaction；Add
Skin can be improved by entering this product, prevent dry skin.Cortex Cinnamomi volatile oil, have powerful antifungal efficacy, as naturally
Preservative, antibacterial agent, it is all effective in cure to flu or respiratory tract infection；To pacify effect excellent to drained and weak, dejected；
Its warm speciality pacified, chemical preservative can be banned by being added to this product, be accomplished really natural no added.
Preferably, raw material components are by weight, comprising: 20 parts by weight of Saponaria officinalis extract, 10 weight of soapberry extract
Measure part, 0.25 parts by weight of lemon-grass volatile oil, 0.4 parts by weight of grape fruit volatile oil, 0.25 parts by weight of seaweed glue, lemon-grass hydrosol
0.1 parts by weight of 68 parts by weight, 1 parts by weight of citric acid and Cortex Cinnamomi volatile oil.
Preferably, raw material components further include: 5~10 parts by weight of tea tree extract, 3~6 parts by weight of Herb Gynostemmae Pentaphylli extract, peppery
Wooden 2~5 parts by weight of leaf extract and 1~2 parts by weight of cashew nut oil.
Preferably, be made of following raw material components: 20 parts by weight of Saponaria officinalis extract, 10 parts by weight of soapberry extract,
0.25 parts by weight of lemon-grass volatile oil, 0.4 parts by weight of grape fruit volatile oil, 0.25 parts by weight of seaweed glue, 68 weight of lemon-grass hydrosol
Measure part, 1 parts by weight of citric acid, 0.1 parts by weight of Cortex Cinnamomi volatile oil, 6 parts by weight of tea tree, 5 parts by weight of gynostemma pentaphylla, 2 weight of leaf of Moringa
Part and 1 parts by weight of cashew nut oil.
Preferably, Saponaria officinalis extract includes Saponaria officinalis saponin(e, and soapberry extract includes sapindoside.
It should be noted that each raw material component of preparation natural plant cleanser essence of the present invention is to be used as to match according to parts by weight
Than, production when can according to corresponding ratio increase or reduce, as large-scale production can by kilogram or as unit of ton, on a small scale
Production can also in grams, and quality can increase or reduce, but the quality proportioning constant rate between each composition.
Second aspect, the present invention provide a kind of preparation method of natural plant cleanser essence, comprising the following steps: S1: will be fertile
Saponaria officinalis and soapberry are cleaned up with warm water, crush after drying at 40~50 DEG C later, supercritical CO is respectively adopted2Extract number
It is secondary, obtain Saponaria officinalis extract and soapberry extract；S2: crushing after lemon-grass is dried, and is refined using steam extraction method
Lemon-grass hydrosol and volatile oil are obtained, later separates hydrosol and volatile oil, it is spare；S3: preset ratio is pressed by each raw material component
It is displayed after emulsification, after lather collapse, obtains natural plant cleanser essence.
Preferably, in S1, using supercritical CO2It extracts 3 times, specifically includes step: S101: using dehydrated alcohol as solvent,
CO2Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, and time 2h obtains Saponaria officinalis saponin(e and sapindoside
Crude product；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, temperature is 55 DEG C, time 3h, further
Extract the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, temperature 60
DEG C, time 4h obtains Saponaria officinalis extract and soapberry extract；It is highly preferred that the mass ratio of powder and dehydrated alcohol
For 1:(2~4), warm water refers to 20~25 DEG C of water, and the raw material after drying is crushed to 80~100 mesh.
In super critical extraction process, in S102, by the natural plant saponin of coarse extraction in CO2Flow immobilize, increase
In the case where big pressure, temperature and time, the saponin in soap grass meal and spaonin powder is further extracted；In S103,
On the basis of S102, CO is kept2Flow immobilize, further increase pressure, temperature and time, extraction obtains institute of the present invention
The final product natural plants Saponaria officinalis extract and soapberry extract saponin(e needed.
Preferably, in S2, the lemon-grass after drying is crushed to 80~100 mesh, deionized water is added later and carries out water steaming
Air lift takes, and the ratio of lemongrass grass meal and deionized water is 1:(2~4)；In S3, emulsion process is in high shear emulsifying pot
It carries out, and emulsification times are 20min.
Preferably, it will be crushed after the drying of tea tree, gynostemma pentaphylla and leaf of Moringa respectively, impregnated with saline solution, decoct mention later
It takes, filters and collect filtrate, respectively obtain tea tree extract, Herb Gynostemmae Pentaphylli extract and moringa oleifera leaf extractive；Wherein, saline solution
In, the mass percentage concentration of sodium chloride is 10~15%, and soaking time is 20~50min, is decocted specifically: first boil 5 by intense fire
~8min, rear mild fire heat 60~100min.
The third aspect, natural plant cleanser essence provided by the invention is in the product and/or product with sterilization, cleaning efficacy
Use in additive.
The above technical solution of the present invention has the following advantages over the prior art:
(1) applicant has found by numerous studies: natural plant cleanser essence selection provided by the invention contains natural activity
The plant extract of ingredient forms, and prescription proportion science does not add any artificial synthesis group point, and natural soap grass and soapberry are all
Saponin rich in, efficient combination complementation produce it is a kind of have it is pure natural, have no toxic side effect, using safe more function
The health care detergent product of energy property.In addition, Saponaria officinalis complete stool contains natural plants saponin(e, not only there is potent cleaning action,
Can be with softening of water, mild to skin, soapberry has potent cleaning and antifungic action, can play substituted chemistry petroleum
The role of class interfacial agent, and it is easy to use, it is with a wide range of applications.
(2) preparation method provided by the invention, can be while retaining each bulk pharmaceutical chemicals active constituent to greatest extent, can
The effective component in each raw medicinal material is sufficiently released, so that the natural plant cleanser essence being finally prepared be made to have
Excellent effect.
(3) saponin rich in natural plant cleanser essence provided by the invention, as by Saponaria officinalis and nothing
Suffer from the pure natural product of nonionic surface active agent of sub- extracted form natural plant, it can be effectively instead of generally making in current dish washing liquid
The surfactant of petrochemical industry class chemical industry synthesis, there is sizable market value；If Saponaria officinalis can be planted on a large scale, it is not necessarily to
Use agriculture chemical, so that it may generate big content of starting materials, for realization " blue mountains and green waters, be exactly Kingsoft Yin Shan " target have it is constructive
Paces.
Additional aspect and advantage of the invention will be set forth in part in the description, and will partially become from the following description
Obviously, or practice through the invention is recognized.
Specific embodiment
The embodiment of technical solution of the present invention will be described in detail below.Following embodiment is only used for clearer
Illustrate technical solution of the present invention, therefore be only used as example, and not intended to limit the protection scope of the present invention.
Experimental method in following embodiments is unless otherwise specified conventional method.Examination as used in the following examples
Material is tested, is to be commercially available from conventional reagent shop unless otherwise specified.Quantitative test in following embodiment, is all provided with
Three repeated experiments are set, data are the average value or mean+SD of three repeated experiments.
The present invention provides a kind of natural plant cleanser essence, and raw material components are by weight, comprising: and Saponaria officinalis extract 20~
30 parts by weight, 10~20 parts by weight of soapberry extract, 0.2~0.3 parts by weight of lemon-grass volatile oil, grape fruit volatile oil 0.1
~0.5 parts by weight, 0.2~0.3 parts by weight of seaweed glue, 50~70 parts by weight of lemon-grass hydrosol, 0.5~1 parts by weight of citric acid and
0.1~0.25 parts by weight of Cortex Cinnamomi volatile oil；And it is also preferable to include 5~10 parts by weight of tea tree extract, gynostemma pentaphylla to mention for raw material components
Take 1~2 parts by weight of 3~6 parts by weight of object, 2~5 parts by weight of moringa oleifera leaf extractive and cashew nut oil.
In addition, being directed to above-mentioned raw materials component, the present invention specially devises the preparation method of natural plant cleanser essence, including with
Lower step:
S1: Saponaria officinalis and soapberry are cleaned up with 20~25 DEG C of water, are crushed after drying at 40~50 DEG C later
To 80~100 mesh, supercritical CO is respectively adopted2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract.Wherein, it adopts
Use supercritical CO2Extract 3 times, specifically include step: S101: using dehydrated alcohol as solvent, the quality of powder and dehydrated alcohol it
Than for 1:(2~4), CO2Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, and time 2h obtains Saponaria officinalis soap
The crude product of glycosides and sapindoside；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, and temperature is 55 DEG C,
Time is 3h, further extracts the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure extremely
35MPa, temperature are 60 DEG C, and time 4h obtains Saponaria officinalis extract and soapberry extract.
S2: being crushed to 80~100 mesh after lemon-grass is dried, in lemongrass grass meal and deionized water 1:(2~4) ratio add
Enter deionized water, refine to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later separates hydrosol and volatile oil,
It is spare.
S3: each raw material component is placed in high shear emulsifying pot after emulsification 20min by preset ratio and is displayed, to foam
After disappearance, natural plant cleanser essence is obtained.
In further embodiment of the invention, it will be crushed after the drying of tea tree, gynostemma pentaphylla and leaf of Moringa respectively, use quality
The saline solution that percentage concentration is 10~15% impregnates 20~50min, first boils 5~8min, rear mild fire heating 60 by intense fire later
~100min filters and collects filtrate, respectively obtains tea tree extract, Herb Gynostemmae Pentaphylli extract and moringa oleifera leaf extractive.
It is illustrated With reference to embodiment:
Embodiment one
The present embodiment provides a kind of natural plant cleanser essences, are made of following raw material components: 20 weight of Saponaria officinalis extract
Part, 10 parts by weight of soapberry extract, 0.25 parts by weight of lemon-grass volatile oil, 0.4 parts by weight of grape fruit volatile oil, seaweed glue
0.25 parts by weight, 0.1 parts by weight of 68 parts by weight of lemon-grass hydrosol, 1 parts by weight of citric acid and Cortex Cinnamomi volatile oil.
According to above-mentioned raw materials component, natural plant cleanser essence is prepared:
S1: Saponaria officinalis and soapberry are cleaned up with 20 DEG C of water, are crushed to 80~100 after drying at 50 DEG C later
Supercritical CO is respectively adopted in mesh2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract.Wherein, using supercritical CO2
Extract 3 times, specifically include step: S101: using dehydrated alcohol as solvent, the mass ratio of powder and dehydrated alcohol is 1:3, CO2
Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, obtains Saponaria officinalis saponin(e and sapindoside
Crude product；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, temperature is 55 DEG C, and time 3h is further mentioned
Take the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, and temperature is 60 DEG C,
Time is 4h, obtains Saponaria officinalis extract and soapberry extract.
S2: being crushed to 80~100 mesh after lemon-grass is dried, goes in the addition of the ratio of lemongrass grass meal and deionized water 1:3
Ionized water refines to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later separates hydrosol and volatile oil, standby
With.
S3: each raw material component is placed in high shear emulsifying pot after emulsification 20min by preset ratio and is displayed, to foam
After disappearance, natural plant cleanser essence is obtained.
Embodiment two
The present embodiment provides a kind of natural plant cleanser essences, are made of following raw material components: 30 weight of Saponaria officinalis extract
Part, 10 parts by weight of soapberry extract, 0.3 parts by weight of lemon-grass volatile oil, 0.1 parts by weight of grape fruit volatile oil, seaweed glue 0.3
Parts by weight, 0.1 parts by weight of 50 parts by weight of lemon-grass hydrosol, 1 parts by weight of citric acid and Cortex Cinnamomi volatile oil.
According to above-mentioned raw materials component, natural plant cleanser essence is prepared:
S1: Saponaria officinalis and soapberry are cleaned up with 25 DEG C of water, are crushed to 80~100 after drying at 40 DEG C later
Supercritical CO is respectively adopted in mesh2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract.Wherein, using supercritical CO2
Extract 3 times, specifically include step: S101: using dehydrated alcohol as solvent, the mass ratio of powder and dehydrated alcohol is 1:2, CO2
Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, obtains Saponaria officinalis saponin(e and sapindoside
Crude product；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, temperature is 55 DEG C, and time 3h is further mentioned
Take the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, and temperature is 60 DEG C,
Time is 4h, obtains Saponaria officinalis extract and soapberry extract.
S2: being crushed to 80~100 mesh after lemon-grass is dried, goes in the addition of the ratio of lemongrass grass meal and deionized water 1:4
Ionized water refines to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later separates hydrosol and volatile oil, standby
With.
S3: each raw material component is placed in high shear emulsifying pot after emulsification 20min by preset ratio and is displayed, to foam
After disappearance, natural plant cleanser essence is obtained.
Embodiment three
The present embodiment provides a kind of natural plant cleanser essences, are made of following raw material components: 20 weight of Saponaria officinalis extract
Part, 10 parts by weight of soapberry extract, 0.25 parts by weight of lemon-grass volatile oil, 0.4 parts by weight of grape fruit volatile oil, seaweed glue
0.25 parts by weight, 68 parts by weight of lemon-grass hydrosol, 1 parts by weight of citric acid, 0.1 parts by weight of Cortex Cinnamomi volatile oil, 6 parts by weight of tea tree,
1 parts by weight of 5 parts by weight of gynostemma pentaphylla, 2 parts by weight of leaf of Moringa and cashew nut oil.Wherein, tea tree, gynostemma pentaphylla and leaf of Moringa are dried respectively
After crush, impregnate 20min with the saline solution that mass percentage concentration is 15%, first boil 8min by intense fire later, rear mild fire heating
60min filters and collects filtrate, respectively obtains tea tree extract, Herb Gynostemmae Pentaphylli extract and moringa oleifera leaf extractive.
According to above-mentioned raw materials component, natural plant cleanser essence is prepared:
S1: Saponaria officinalis and soapberry are cleaned up with 20 DEG C of water, are crushed to 80~100 after drying at 50 DEG C later
Supercritical CO is respectively adopted in mesh2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract.Wherein, using supercritical CO2
Extract 3 times, specifically include step: S101: using dehydrated alcohol as solvent, the mass ratio of powder and dehydrated alcohol is 1:3, CO2
Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, obtains Saponaria officinalis saponin(e and sapindoside
Crude product；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, temperature is 55 DEG C, and time 3h is further mentioned
Take the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, and temperature is 60 DEG C,
Time is 4h, obtains Saponaria officinalis extract and soapberry extract.
S2: being crushed to 80~100 mesh after lemon-grass is dried, goes in the addition of the ratio of lemongrass grass meal and deionized water 1:3
Ionized water refines to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later separates hydrosol and volatile oil, standby
With.
S3: each raw material component is placed in high shear emulsifying pot after emulsification 20min by preset ratio and is displayed, to foam
After disappearance, natural plant cleanser essence is obtained.
Example IV
The present embodiment provides a kind of natural plant cleanser essences, are made of following raw material components: 30 weight of Saponaria officinalis extract
Part, 10 parts by weight of soapberry extract, 0.3 parts by weight of lemon-grass volatile oil, 0.1 parts by weight of grape fruit volatile oil, seaweed glue 0.3
Parts by weight, 50 parts by weight of lemon-grass hydrosol, 1 parts by weight of citric acid, 0.1 parts by weight of Cortex Cinnamomi volatile oil, 10 weight of tea tree extract
Part, 1 parts by weight of 3 parts by weight of natural plant cleanser essence, 5 parts by weight of moringa oleifera leaf extractive and cashew nut oil.Wherein, respectively by tea tree,
It is crushed after gynostemma pentaphylla and leaf of Moringa drying, impregnates 50min with the saline solution that mass percentage concentration is 10%, first intense fire boils later
5min is boiled, rear mild fire heats 100min, filters and collect filtrate, respectively obtain tea tree extract, Herb Gynostemmae Pentaphylli extract and Moringa
Leaf extract.
According to above-mentioned raw materials component, natural plant cleanser essence is prepared:
S1: Saponaria officinalis and soapberry are cleaned up with 25 DEG C of water, are crushed to 80~100 after drying at 40 DEG C later
Supercritical CO is respectively adopted in mesh2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract.Wherein, using supercritical CO2
Extract 3 times, specifically include step: S101: using dehydrated alcohol as solvent, the mass ratio of powder and dehydrated alcohol is 1:2, CO2
Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, obtains Saponaria officinalis saponin(e and sapindoside
Crude product；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, temperature is 55 DEG C, and time 3h is further mentioned
Take the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, and temperature is 60 DEG C,
Time is 4h, obtains Saponaria officinalis extract and soapberry extract.
S2: being crushed to 80~100 mesh after lemon-grass is dried, goes in the addition of the ratio of lemongrass grass meal and deionized water 1:4
Ionized water refines to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later separates hydrosol and volatile oil, standby
With.
S3: each raw material component is placed in high shear emulsifying pot after emulsification 20min by preset ratio and is displayed, to foam
After disappearance, natural plant cleanser essence is obtained.
In addition, following comparative example is arranged in order to further highlight the advantage of technical solution of the present invention.It should be noted that
Following comparative examples change relative parameters setting on the basis of example 1 and form.
Comparative example one
This comparative example provides a kind of natural plant cleanser essence, is made of following raw material components: 20 weight of Saponaria officinalis extract
Part, 10 parts by weight of soapberry extract, 0.4 parts by weight of grape fruit volatile oil, 0.25 parts by weight of seaweed glue, lemon-grass hydrosol
0.1 parts by weight of 68.25 parts by weight, 1 parts by weight of citric acid and Cortex Cinnamomi volatile oil.
According to above-mentioned raw materials component, natural plant cleanser essence is prepared:
S1: Saponaria officinalis and soapberry are cleaned up with 20 DEG C of water, are crushed to 80~100 after drying at 50 DEG C later
Supercritical CO is respectively adopted in mesh2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract.Wherein, using supercritical CO2
Extract 3 times, specifically include step: S101: using dehydrated alcohol as solvent, the mass ratio of powder and dehydrated alcohol is 1:3, CO2
Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, obtains Saponaria officinalis saponin(e and sapindoside
Crude product；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, temperature is 55 DEG C, and time 3h is further mentioned
Take the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, and temperature is 60 DEG C,
Time is 4h, obtains Saponaria officinalis extract and soapberry extract.
S2: being crushed to 80~100 mesh after lemon-grass is dried, goes in the addition of the ratio of lemongrass grass meal and deionized water 1:3
Ionized water refines to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later separates hydrosol and volatile oil, standby
With.
S3: each raw material component is placed in high shear emulsifying pot after emulsification 20min by preset ratio and is displayed, to foam
After disappearance, natural plant cleanser essence is obtained.
Comparative example two
This comparative example provides a kind of natural plant cleanser essence, is made of following raw material components: 20 weight of Saponaria officinalis extract
Part, 10 parts by weight of soapberry extract, 0.25 parts by weight of lemon-grass volatile oil, 0.4 parts by weight of grape fruit volatile oil, seaweed glue
0.25 parts by weight, 68 parts by weight of lemon-grass hydrosol, 1 parts by weight of citric acid, 0.1 parts by weight of Cortex Cinnamomi volatile oil, 6 parts by weight of tea tree and
5 parts by weight of gynostemma pentaphylla.Wherein, it will be crushed after tea tree and gynostemma pentaphylla drying respectively, the salt for being 15% with mass percentage concentration is water-soluble
Liquid impregnates 20min, first boils 8min by intense fire later, and rear mild fire heats 60min, filters and collect filtrate, respectively obtain tea tree and mention
Take object and Herb Gynostemmae Pentaphylli extract.
According to above-mentioned raw materials component, natural plant cleanser essence is prepared:
S1: Saponaria officinalis and soapberry are cleaned up with 20 DEG C of water, are crushed to 80~100 after drying at 50 DEG C later
Supercritical CO is respectively adopted in mesh2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract.Wherein, using supercritical CO2
Extract 3 times, specifically include step: S101: using dehydrated alcohol as solvent, the mass ratio of powder and dehydrated alcohol is 1:3, CO2
Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, obtains Saponaria officinalis saponin(e and sapindoside
Crude product；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, temperature is 55 DEG C, and time 3h is further mentioned
Take the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, and temperature is 60 DEG C,
Time is 4h, obtains Saponaria officinalis extract and soapberry extract.
S2: being crushed to 80~100 mesh after lemon-grass is dried, goes in the addition of the ratio of lemongrass grass meal and deionized water 1:3
Ionized water refines to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later separates hydrosol and volatile oil, standby
With.
S3: each raw material component is placed in high shear emulsifying pot after emulsification 20min by preset ratio and is displayed, to foam
After disappearance, natural plant cleanser essence is obtained.
Comparative example three
This comparative example provides a kind of natural plant cleanser essence, is made of following raw material components: 20 weight of Saponaria officinalis extract
Part, 10 parts by weight of soapberry extract, 0.25 parts by weight of lemon-grass volatile oil, 0.4 parts by weight of grape fruit volatile oil, seaweed glue
0.25 parts by weight, 68 parts by weight of lemon-grass hydrosol, 1 parts by weight of citric acid, 0.1 parts by weight of Cortex Cinnamomi volatile oil, 6 parts by weight of tea tree,
1 parts by weight of 2 parts by weight of leaf of Moringa and cashew nut oil.Wherein, it will be crushed after tea tree and leaf of Moringa drying respectively, use mass percentage concentration
20min is impregnated for 15% saline solution, first boils 8min by intense fire later, rear mild fire heats 60min, filters and collect filtrate,
Respectively obtain tea tree extract and moringa oleifera leaf extractive.
According to above-mentioned raw materials component, natural plant cleanser essence is prepared:
S1: Saponaria officinalis and soapberry are cleaned up with 20 DEG C of water, are crushed to 80~100 after drying at 50 DEG C later
Supercritical CO is respectively adopted in mesh2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract.Wherein, using supercritical CO2
Extract 3 times, specifically include step: S101: using dehydrated alcohol as solvent, the mass ratio of powder and dehydrated alcohol is 1:3, CO2
Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, obtains Saponaria officinalis saponin(e and sapindoside
Crude product；S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, temperature is 55 DEG C, and time 3h is further mentioned
Take the saponin in Saponaria officinalis and soapberry；S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, and temperature is 60 DEG C,
Time is 4h, obtains Saponaria officinalis extract and soapberry extract.
S2: being crushed to 80~100 mesh after lemon-grass is dried, goes in the addition of the ratio of lemongrass grass meal and deionized water 1:3
Ionized water refines to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later separates hydrosol and volatile oil, standby
With.
S3: each raw material component is placed in high shear emulsifying pot after emulsification 20min by preset ratio and is displayed, to foam
After disappearance, natural plant cleanser essence is obtained.
In addition, the effect of in order to preferably evaluate each embodiment natural plant cleanser essence, carry out following experiment:
One, detergency test
With reference to GB9985-2000 " detergent for washing dishware with hand " in Appendix B detergency measuring method.The measurement present invention
The detergency of the pure plant dish washing liquid of each embodiment and comparative example preparation.Wherein, the judgement of detergency are as follows: if tested dishwashing detergent
Agent goes oil cut rate to go oil cut rate then and be qualified not less than standard dish washing detergent, is otherwise unqualified.
Each embodiment and comparative example dish washing liquid detergency correlation data of table 1
Two, bacteriostasis property measures
The natural plant cleanser essence that each embodiment and comparative example is obtained, the natural plants of preparation 0.2mg/mL are washed clean respectively
Smart solution detects its biocidal property to staphylococcus aureus, Escherichia coli, Candida albicans and Pseudomonas aeruginosa respectively later
Can, specific test method: being added dropwise 5 μ L natural plant cleanser essence solution on small filter paper, and bacterium is cultivated for 24 hours at 37 DEG C, fungi
In 28 DEG C of culture 48h, sterile water does negative control, observes the size of its inhibition zone, judges its bacteriostasis, specific data such as table
Shown in 2.
Inhibition zone size/mm of each embodiment and comparative example dish washing liquid of table 2
| Staphylococcus aureus | Escherichia coli | Candida albicans | Pseudomonas aeruginosa | Sterile water | |
| Embodiment one | 12.25 | 12.35 | 6.29 | 7.65 | 6.00 |
| Embodiment two | 12.19 | 12.06 | 6.22 | 7.99 | 6.00 |
| Embodiment three | 13.66 | 13.89 | 7.18 | 8.98 | 6.00 |
| Example IV | 13.24 | 13.56 | 7.01 | 8.34 | 6.00 |
| Comparative example one | 9.47 | 10.41 | 6.09 | 7.35 | 6.00 |
| Comparative example two | 8.16 | 9.38 | 6.11 | 7.68 | 6.00 |
| Comparative example three | 9.05 | 9.97 | 6.03 | 8.05 | 6.00 |
Certainly, the case where being enumerated in addition to embodiment one to example IV, the type and weight percent of other raw material components,
Condition and parameter in preparation process etc. are also possible.
Natural plant cleanser essence provided by the invention selects the plant extract containing active skull cap components to form, prescription proportion
Science is not added any artificial synthesis group and is divided, and natural soap grass and soapberry saponin all rich in, and effective group
Close complementation produce it is a kind of with it is pure natural, have no toxic side effect, using the health care detergent product of multifunctional safety.In addition,
Saponaria officinalis complete stool contains natural plants saponin(e, not only has potent cleaning action, can be mild to skin with softening of water,
Soapberry has potent cleaning and antifungic action, can play the role of substituted chemistry petroleum-type interfacial agent, and use
It is convenient, it is with a wide range of applications.
In the description of this specification, it is to be understood that reference term " one embodiment ", " is shown " some embodiments "
The description of example ", " specific example " or " some examples " etc. mean specific features described in conjunction with this embodiment or example, structure,
Material or feature are included at least one embodiment or example of the invention.In the present specification, above-mentioned term is shown
The statement of meaning property is necessarily directed to identical embodiment or example.Moreover, specific features, structure, material or the spy of description
Point may be combined in any suitable manner in any one or more of the embodiments or examples.In addition, without conflicting with each other,
Those skilled in the art can be by different embodiments or examples described in this specification and different embodiments or examples
Feature is combined.
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example
Property, it is not considered as limiting the invention, those skilled in the art within the scope of the invention can be to above-mentioned
Embodiment is changed, modifies, replacement and variant.
Claims (10)
1. a kind of natural plant cleanser essence, which is characterized in that raw material components are by weight, comprising:
20~30 parts by weight of Saponaria officinalis extract, 10~20 parts by weight of soapberry extract, 0.2~0.3 weight of lemon-grass volatile oil
Measure part, 0.1~0.5 parts by weight of grape fruit volatile oil, 0.2~0.3 parts by weight of seaweed glue, 50~70 parts by weight of lemon-grass hydrosol,
0.1~0.25 parts by weight of 0.5~1 parts by weight of citric acid and Cortex Cinnamomi volatile oil.
2. natural plant cleanser essence according to claim 1 characterized by comprising
20 parts by weight of Saponaria officinalis extract, 10 parts by weight of soapberry extract, 0.25 parts by weight of lemon-grass volatile oil, grape fruit are waved
0.4 parts by weight of hair oil, 0.25 parts by weight of seaweed glue, 68 parts by weight of lemon-grass hydrosol, 1 parts by weight of citric acid and Cortex Cinnamomi volatile oil
0.1 parts by weight.
3. natural plant cleanser essence according to claim 1, which is characterized in that further include:
5~10 parts by weight of tea tree extract, 3~6 parts by weight of Herb Gynostemmae Pentaphylli extract, 2~5 parts by weight of moringa oleifera leaf extractive and cashew nut
Oily 1~2 parts by weight.
4. natural plant cleanser essence according to claim 1, which is characterized in that be made of following raw material components:
20 parts by weight of Saponaria officinalis extract, 10 parts by weight of soapberry extract, 0.25 parts by weight of lemon-grass volatile oil, grape fruit are waved
0.4 parts by weight of hair oil, 0.25 parts by weight of seaweed glue, 68 parts by weight of lemon-grass hydrosol, 1 parts by weight of citric acid, Cortex Cinnamomi volatile oil 0.1
Parts by weight, 6 parts by weight of tea tree, 1 parts by weight of 5 parts by weight of gynostemma pentaphylla, 2 parts by weight of leaf of Moringa and cashew nut oil.
5. natural plant cleanser essence according to any one of claims 1 to 4, it is characterised in that:
The Saponaria officinalis extract includes Saponaria officinalis saponin(e, and the soapberry extract includes sapindoside.
6. the preparation method of any one of Claims 1 to 5 natural plant cleanser essence, which comprises the following steps:
S1: Saponaria officinalis and soapberry are cleaned up with warm water, are crushed after drying at 40~50 DEG C later, and super face is respectively adopted
Boundary CO2It extracts for several times, obtains Saponaria officinalis extract and soapberry extract；
S2: crushing after lemon-grass is dried, and refines to obtain lemon-grass hydrosol and volatile oil using steam extraction method, later will be pure
Dew is separated with volatile oil, spare；
S3: displaying after emulsifying each raw material component by preset ratio, after lather collapse, obtains the natural plant cleanser essence.
7. the preparation method of natural plant cleanser essence according to claim 6, it is characterised in that:
In the S1, using supercritical CO2It extracts 3 times, specifically includes step:
S101: using dehydrated alcohol as solvent, CO2Flow is 30L/h, and extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h,
Obtain the crude product of Saponaria officinalis saponin(e and sapindoside；
S102: CO is kept2Flow is 30L/h, increases pressure to 27.5MPa, and temperature is 55 DEG C, time 3h, further extracts fertilizer
Saponin in Saponaria officinalis and soapberry；
S103: CO is kept2Flow is 30L/h, increases pressure to 35MPa, and temperature is 60 DEG C, time 4h, obtains Saponaria officinalis extraction
Object and soapberry extract；
Preferably,
The mass ratio of powder and dehydrated alcohol is 1:(2~4), warm water refers to 20~25 DEG C of water, and by the raw material after drying
It is crushed to 80~100 mesh.
8. the preparation method of natural plant cleanser essence according to claim 6, it is characterised in that:
In the S2, the lemon-grass after drying is crushed to 80~100 mesh, deionized water is added later and carries out steam extraction,
And the ratio of lemongrass grass meal and deionized water is 1:(2~4)；
In the S3, the emulsion process carries out in high shear emulsifying pot, and emulsification times are 20min.
9. the preparation method of natural plant cleanser essence according to claim 6, it is characterised in that:
It will be crushed after the drying of tea tree, gynostemma pentaphylla and leaf of Moringa respectively, impregnated with saline solution, decoct extract later, filter and receive
Collect filtrate, respectively obtains tea tree extract, Herb Gynostemmae Pentaphylli extract and moringa oleifera leaf extractive；
Wherein, in the saline solution, the mass percentage concentration of sodium chloride is 10~15%, and soaking time is 20~50min, is decocted
It boils specifically: first boil 5~8min by intense fire, rear mild fire heats 60~100min.
10. any one of Claims 1 to 5 natural plant cleanser essence is in the product and/or product with sterilization, cleaning efficacy
Use in additive.
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