CN107384607A - A kind of natural disinfection liquid detergent and preparation method thereof - Google Patents
A kind of natural disinfection liquid detergent and preparation method thereof Download PDFInfo
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- CN107384607A CN107384607A CN201710406367.7A CN201710406367A CN107384607A CN 107384607 A CN107384607 A CN 107384607A CN 201710406367 A CN201710406367 A CN 201710406367A CN 107384607 A CN107384607 A CN 107384607A
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- liquid detergent
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
Abstract
The invention discloses a kind of natural disinfection liquid detergent and preparation method, mainly has fruit of glossy privet crust concentrate, gleditsia sinensis and shrubalthea leaf to pass through supercritical CO2The natural plants saponin of extraction, cedra fruits pericarp essential oil mixed preparing form, and each parts by weight of raw materials array turns into：20 40 parts of fruit of glossy privet crust, 10 20 parts of gleditsia sinensis, 9 15 parts of shrubalthea leaf, 10 20 parts of citrus fruit pericarp.Liquid detergent made by the present invention is all using natural plant composition, convenient material drawing, science extraction, scientific matching, and finished product liquid detergent is free of chemical addition agent, safe and environment-friendly, noresidue, do not stimulate, strong detergency, bactericidal effect it is obvious.
Description
Technical field
The invention belongs to daily chemical products field, and in particular to a kind of natural disinfection liquid detergent and preparation method.
Background technology
Chemical detergent is the mankind's most direct most intimate daily necessities, GB9985-2000《Manual dishwashing detergent》
90%, gross activity thing content >=15% should be not less than by providing the biological degradability of surfactant used in dishwashing detergent agent prescription,
But current liquid detergent mostly and below standard, people widely using chemical detergent wash my hair, chopsticks of washing the dishes, laundry clothes, wash
While bath, chemical toxicant just penetrates into from thousands upon thousands pores, people's health and environment is compromised, due to this pollution
Harm in a short time can not possibly be often ignored it is obvious that therefore.But micro pollution continues into vivo, product
Less into serious consequence can be caused more, cause the various lesions of human body.
Existing liquid detergent is most of all containing the surfactant of chemical synthesis and other chemical compositions, in the process used
In easily opponent skin produce dry, chap etc. injury, security and environment to tableware can also produce certain influence；Also
A part of liquid detergent is only used for cleaning tableware and other items, it is impossible to which the residues of pesticides on the edible article such as vegetable and fruit are entered
Row cleaning, while function is also limited only to remove spot, sterilization, the effect of sterilization are limited, and the scope of application is narrow, function is single.
It is therefore desirable to liquid detergent has safety and environmental protection, clean characteristic gentle, foam is soft and fine, rapid decomposition is oily, it is quick so as to reach
Decontamination, effectively degerming, thorough cleaning, noresidue and there is the purpose of nursing role particularly significant to skin.
The content of the invention
The technical problems to be solved by the invention are to contain chemical composition and surfactant for current detergent, and
Threat is produced to health, while meets the raising that people are required quality of life, there is provided a kind of natural disinfection liquid detergent and
Its preparation method.
In order to realize that the technical scheme that above-mentioned technical purpose uses is：A kind of natural disinfection liquid detergent, by following parts by weight
Number raw material composition：Fruit of glossy privet crust 20-40 parts, gleditsia sinensis 10-20 parts, shrubalthea leaf 9-15 parts, cedra fruits pericarp 10-20 parts.
Comprise the following steps：
Step 1: fruit of glossy privet crust, gleditsia sinensis, shrubalthea leaf and cedra fruits pericarp are cleaned in 20 DEG C of water, dried, it is standby
With；
Step 2: it is in temperature by fruit of glossy privet crust, gleditsia sinensis, shrubalthea leaf and the cedra fruits pericarp after being handled in step 1
Air-dried at 60-70 DEG C, be then crushed to 40-60 mesh respectively, obtain fruit of glossy privet crust powder, spaonin powder, shrubalthea leaf powder and Citrus water
Fruit fruit peel powder, it is standby；
Step 3: by fruit of glossy privet crust powder in step 2 and deionized water using mass ratio as 1-1.5:After 1 ratio is well mixed,
Soaked, boiled and filtered successively, it is 1.5 g-2g/ml that filtrate is concentrated into concentration in vacuum rotary evaporator, obtains female
Loyal sub- crust concentrate, it is standby；
Step 4: the spaonin powder in step 2 and shrubalthea leaf powder are separately added into supercritical CO2In extraction apparatus, using absolute ethyl alcohol as
Extractant, powder and absolute ethyl alcohol mass ratio are 1:2-1:4, it is divided into and extracts to obtain natural plants saponin three times, it is standby；
Step 5: the fruit peel powder in step 2 is placed in into glass container, it is uniform to add absolute ethyl alcohol and stirring, is then in temperature
To be filtered after soaking 5-7d at 20-30 DEG C, filtrate concentrates in vacuum rotary evaporator, obtains cedra fruits pericarp essential oil,
It is standby；
Step 6, take the fruit of glossy privet crust solution in step 3, the citrus in the natural plants saponin and step 5 in step 4
Class Fruit Peel essential oil is added in deionized water, and above component additional proportion is 47-53：927-943：1-1.5：10-20, its
In terms of milliliter, natural plants saponin in gram, stirs for middle fruit of glossy privet crust solution, cedra fruits pericarp essential oil, deionized water
Obtained natural disinfection liquid detergent after uniformly.
Further optimization, the cedra fruits pericarp are the one or more in orange, orange, lemon and shaddock.
Further optimize, soaking temperature is 30-40 DEG C, time 1-2h in the step 3, and the time boiled is 1-2h.
Further optimize, the vacuum of the vacuum rotary evaporator in the step 3 and step 5 is 0.085-
0.1MPa。
Further optimize, supercritical CO in the step 42CO in extraction apparatus2Flow be 30L/h, extraction pressure is 20-
35MPa, temperature are 50-60 DEG C, time 2-4h.
Further optimize, stirred 2-3 times daily in immersion process in the step 5.
Further optimize, the concentration of the sub- crust concentrate of Nuzhen, an ancient nationality in China, ancestors of the Manchus, who founded the Jin Dynasty is 70-80mg/ml in mixed solution in the step 6.
Further optimize, the concentration of natural plants saponin is 1 ~ 1.5 mg/ml in the Natural cleanser essence in the step 6.
Further optimize, the percent concentration of cedra fruits pericarp essential oil is 1%-2% in the step 6.
The beneficial effects of the invention are as follows：
First, there is fruit of glossy privet decocting liquid significant suppression to make to staphylococcus aureus, Escherichia coli and bacillus subtilis etc.
With research shows that 62 mg/g concentrations above fruit of glossy privet decocting liquid energies effectively kill above pathogenic bacteria；
2nd, saponin(e also known as alkali soap body, saponin, it is that aglycon is triterpene or a kind of glucosides of spirostane class compound, there is antibacterial
The valuable bioactivity such as active or antipyretic, calm, anticancer, saponin(e is a kind of natural surfactant, aqueous solution shaking
After can produce persistent soap sample foam, there is good detergency, be a kind of good natural detergent and emulsifying agent；
3rd, cedra fruits pericarp is rich in aromatics essential oil, and main component is alkene, terpene, alcohol, 4 big type organic of ester, these compositions
Its powerful bactericidal and dirt-removing power are assigned, while and can gives the pleasant smell usage experience of user.
4th, the rose of Sharon can hyoscine, be used for the treatment of the diseases such as abscess, skin disease, the extract solution of absolute ethyl alcohol is to golden yellow
Color staphylococcus, shigella dysenteriae, typhoid bacillus and Common Pathogenic dermatophyte have inhibitory action, in addition, shrubalthea leaf it is cool in nature,
It is nontoxic, skin is played a protective role；
5th, means of supercritical extraction is a kind of modern separation technology for using supercritical fluid as solvent, and its extraction effect mainly takes
Certainly in factors such as pressure, temperature, time, solvent flux, the present invention is using fixed CO2The L/h of flow 30 supercritical CO2Extraction
Instrument is extracted three times to spaonin powder and rose of Sharon powder, and compared with conventional method, this method is compared with low temperature（50℃-60℃）Under can
Processing, extraction volatile ingredient effect is good, will not destroy medicinal ingredient and nutritional ingredient in spaonin powder and rose of Sharon powder, oxygen does not occur
Change the advantages of rotten, the effect repeatedly extracted is good, and the CO2 gases used in extraction are recyclable and recycle, and cost is low, can be wide
General application；
Liquid detergent made by the present invention is all using natural plant composition, and convenient material drawing, science extraction scientific matching, finished product is washed clean
Essence is free of chemical addition agent, safe and environment-friendly, noresidue, do not stimulate, strong detergency, bactericidal effect it is obvious.
Embodiment
Embodiment 1：
A kind of natural disinfection liquid detergent, it is made up of following parts by weight raw material：20 parts of fruit of glossy privet crust, 10 parts of gleditsia sinensis, shrubalthea leaf 9
Part, 10 parts of cedra fruits pericarp.
Comprise the following steps：
Step 1: rinsed well again with flowing water after above-mentioned raw materials are soaked in 20 DEG C of water, because raw material concave-convex surface
The pericarp of injustice, especially citrus fruit has residues of pesticides, and easily hides bacterium and impurity, therefore must clean dry
Dried after net, it is standby；
Step 2: by step 1 handle after fruit of glossy privet crust, gleditsia sinensis, shrubalthea leaf and cedra fruits pericarp temperature be 60
Air-dried at DEG C, be then crushed to 40 mesh respectively, obtain fruit of glossy privet crust powder, spaonin powder, shrubalthea leaf powder and cedra fruits fruit peel powder,
It is standby；
Step 3: by fruit of glossy privet crust powder in step 2 and deionized water using mass ratio as 1:After 1 ratio is well mixed, in temperature
Spend to carry out immersion 1h under conditions of 30 DEG C, filtered after then boiling 1h again, by filtrate in the vacuum that vacuum is 0.085MPa
It is 1.5 g/ml that concentration is concentrated into Rotary Evaporators, obtains fruit of glossy privet crust concentrate, standby；
Step 4: the spaonin powder in step 2 and shrubalthea leaf powder are separately added into supercritical CO2In extraction apparatus, using absolute ethyl alcohol as
Extractant, its extraction effect depend primarily on the factors such as pressure, temperature, time, solvent flux, in this powder and absolute ethyl alcohol matter
Amount is than being 1:2, it is broadly divided into and extracts to obtain natural plants saponin three times：
（1）、CO2Flow be 30L/h, extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, and this stage is natural plants
The coarse extraction of saponin；
（2）、CO2Flow be 30L/h, extraction pressure is 27.5MPa, and temperature is 55 DEG C, time 3h, and this stage is by coarse extraction
Natural plant saponin in CO2Flow immobilize, increase pressure, in the case of temperature and time, to spaonin powder and the rose of Sharon
Saponin in leaf powder is further extracted；
（3）、CO2Flow be 30L/h, extraction pressure is 35MPa, and temperature is 60 DEG C, time 4h, this stage CO2Flow
Immobilize, further increase pressure, temperature and time, extraction obtains the final product natural plants saponin of this step；
Step 5: the fruit peel powder in step 2 is placed in into glass container, it is uniform to add absolute ethyl alcohol and stirring, is then in temperature
Filtered after soaking 5d at 20 DEG C, it is daily during immersion to stir 2 times, by filtrate in the vacuum rotating that vacuum is 0.085MPa
Concentrated in evaporimeter, obtain cedra fruits pericarp essential oil, it is standby；
Step 6, take the fruit of glossy privet crust solution in step 3, the citrus in the natural plants saponin and step 5 in step 4
Class Fruit Peel essential oil is added in deionized water, and above component additional proportion is 47：927：1：10, wherein fruit of glossy privet crust is molten
In terms of milliliter, in gram, Nuzhen, an ancient nationality in China, ancestors of the Manchus, who founded the Jin Dynasty is made in natural plants saponin after stirring for liquid, cedra fruits pericarp essential oil, deionized water
The concentration of sub- crust concentrate is 70mg/ml, the concentration of natural plants saponin is 1mg/ml, the hundred of cedra fruits pericarp essential oil
Divide the natural disinfection liquid detergent that specific concentration is 1%.
Embodiment 2：
A kind of natural disinfection liquid detergent, it is made up of following parts by weight raw material：30 parts of fruit of glossy privet crust, 15 parts of gleditsia sinensis, shrubalthea leaf
12 parts, 15 parts of cedra fruits pericarp.
Comprise the following steps：
Step 1: rinsed well again with flowing water after above-mentioned raw materials are soaked in 20 DEG C of water, because raw material concave-convex surface
The pericarp of injustice, especially citrus fruit has residues of pesticides, and easily hides bacterium and impurity, therefore must clean dry
Dried after net, it is standby；
Step 2: by step 1 handle after fruit of glossy privet crust, gleditsia sinensis, shrubalthea leaf and cedra fruits pericarp temperature be 65
Air-dried at DEG C, be then crushed to 50 mesh respectively, obtain fruit of glossy privet crust powder, spaonin powder, shrubalthea leaf powder and cedra fruits fruit peel powder,
It is standby；
Step 3: by fruit of glossy privet crust powder in step 2 and deionized water using mass ratio as 1.25:After 1 ratio is well mixed,
Immersion 1.5h is carried out under conditions of being 35 DEG C in temperature, is filtered after then boiling 1.5h again, in vacuum is 0.09MPa by filtrate
Vacuum rotary evaporator in be concentrated into concentration be 1.75g/ml, obtain fruit of glossy privet crust concentrate, it is standby；
Step 4: the spaonin powder in step 2 and shrubalthea leaf powder are separately added into supercritical CO2In extraction apparatus, using absolute ethyl alcohol as
Extractant, its extraction effect depend primarily on the factors such as pressure, temperature, time, solvent flux, in this powder and absolute ethyl alcohol matter
Amount is than being 1:2, it is broadly divided into and extracts to obtain natural plants saponin three times：
（1）、CO2Flow be 30L/h, extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, and this stage is natural plants
The coarse extraction of saponin；
（2）、CO2Flow be 30L/h, extraction pressure is 27.5MPa, and temperature is 55 DEG C, time 3h, and this stage is by coarse extraction
Natural plant saponin in CO2Flow immobilize, increase pressure, in the case of temperature and time, to spaonin powder and the rose of Sharon
Saponin in leaf powder is further extracted；
（3）、CO2Flow be 30L/h, extraction pressure is 35MPa, and temperature is 60 DEG C, time 4h, this stage CO2Flow
Immobilize, further increase pressure, temperature and time, extraction obtains the final product natural plants saponin of this step；
Step 5: the fruit peel powder in step 2 is placed in into glass container, it is uniform to add absolute ethyl alcohol and stirring, is then in temperature
Filtered after soaking 6d at 25 DEG C, it is daily during immersion to stir 3 times, by filtrate in the vacuum rotating that vacuum is 0.09MPa
Concentrated in evaporimeter, obtain cedra fruits pericarp essential oil, it is standby；
Step 6, take the fruit of glossy privet crust solution in step 3, the citrus in the natural plants saponin and step 5 in step 4
Class Fruit Peel essential oil is added in deionized water, and above component additional proportion is 50：935：1.25：15, wherein outside the fruit of glossy privet
In terms of milliliter, natural plants saponin in gram, is made after stirring for skin solution, cedra fruits pericarp essential oil, deionized water
The concentration of the sub- crust concentrate of Nuzhen, an ancient nationality in China, ancestors of the Manchus, who founded the Jin Dynasty is 75mg/ml, the concentration of natural plants saponin is 1.25 mg/ml, cedra fruits pericarp
The percent concentration of essential oil is 1.5% natural disinfection liquid detergent.
Embodiment 3：
A kind of natural disinfection liquid detergent, it is characterised in that be made up of following parts by weight raw material：40 parts of fruit of glossy privet crust, gleditsia sinensis
20 parts, 15 parts of shrubalthea leaf, 20 parts of cedra fruits pericarp.
Comprise the following steps：
Step 1: rinsed well again with flowing water after above-mentioned raw materials are soaked in 20 DEG C of water, because raw material concave-convex surface
The pericarp of injustice, especially citrus fruit has residues of pesticides, and easily hides bacterium and impurity, therefore must clean dry
Dried after net, it is standby；
Step 2: by step 1 handle after fruit of glossy privet crust, gleditsia sinensis, shrubalthea leaf and cedra fruits pericarp temperature be 70
Air-dried at DEG C, be then crushed to 60 mesh respectively, obtain fruit of glossy privet crust powder, spaonin powder, shrubalthea leaf powder and cedra fruits fruit peel powder,
It is standby；
Step 3: by fruit of glossy privet crust powder in step 2 and deionized water using mass ratio as 1.5:After 1 ratio is well mixed,
Temperature carries out immersion 2h under conditions of being 40 DEG C, is filtered after then boiling 2h again, by filtrate in the vacuum that vacuum is 0.1MPa
It is 2g/ml that concentration is concentrated into Rotary Evaporators, obtains fruit of glossy privet crust concentrate, standby；
Step 4: the spaonin powder in step 2 and shrubalthea leaf powder are separately added into supercritical CO2In extraction apparatus, using absolute ethyl alcohol as
Extractant, its extraction effect depend primarily on the factors such as pressure, temperature, time, solvent flux, in this powder and absolute ethyl alcohol matter
Amount is than being 1:2, it is broadly divided into and extracts to obtain natural plants saponin three times：
（1）、CO2Flow be 30L/h, extraction pressure is 20MPa, and temperature is 50 DEG C, time 2h, and this stage is natural plants
The coarse extraction of saponin；
（2）、CO2Flow be 30L/h, extraction pressure is 27.5MPa, and temperature is 55 DEG C, time 3h, and this stage is by coarse extraction
Natural plant saponin in CO2Flow immobilize, increase pressure, in the case of temperature and time, to spaonin powder and the rose of Sharon
Saponin in leaf powder is further extracted；
（3）、CO2Flow be 30L/h, extraction pressure is 35MPa, and temperature is 60 DEG C, time 4h, this stage CO2Flow
Immobilize, further increase pressure, temperature and time, extraction obtains the final product natural plants saponin of this step；
Step 5: the fruit peel powder in step 2 is placed in into glass container, it is uniform to add absolute ethyl alcohol and stirring, is then in temperature
Filtered after soaking 7d at 30 DEG C, it is daily during immersion to stir 3 times, filtrate is steamed in the vacuum rotating that vacuum is 0.1MPa
Concentrated in hair instrument, obtain cedra fruits pericarp essential oil, it is standby；
Step 6, take the fruit of glossy privet crust solution in step 3, the citrus in the natural plants saponin and step 5 in step 4
Class Fruit Peel essential oil is added in deionized water, and above component additional proportion is 53：943：1.5：20, wherein fruit of glossy privet crust
In terms of milliliter, natural plants saponin in gram, is made after stirring for concentrate, cedra fruits pericarp essential oil, deionized water
The concentration of the sub- crust concentrate of Nuzhen, an ancient nationality in China, ancestors of the Manchus, who founded the Jin Dynasty is 80mg/ml, the concentration of natural plants saponin is 1.5 mg/ml, cedra fruits pericarp
The percent concentration of essential oil is 2% natural disinfection liquid detergent.
Claims (10)
1. a kind of natural disinfection liquid detergent, it is characterised in that be made up of following parts by weight raw material：Fruit of glossy privet crust 20-40 parts,
Gleditsia sinensis 10-20 parts, shrubalthea leaf 9-15 parts, cedra fruits pericarp 10-20 parts.
2. a kind of preparation method of natural disinfection liquid detergent as claimed in claim 1, it is characterised in that comprise the following steps：
Step 1: fruit of glossy privet crust, gleditsia sinensis, shrubalthea leaf and cedra fruits pericarp are cleaned in 20 DEG C of water, dried, it is standby
With；
Step 2: it is in temperature by fruit of glossy privet crust, gleditsia sinensis, shrubalthea leaf and the cedra fruits pericarp after being handled in step 1
Air-dried at 60-70 DEG C, be then crushed to 40-60 mesh respectively, obtain fruit of glossy privet crust powder, spaonin powder, shrubalthea leaf powder and Citrus water
Fruit fruit peel powder, it is standby；
Step 3: by fruit of glossy privet crust powder in step 2 and deionized water using mass ratio as 1-1.5:After 1 ratio is well mixed,
Soaked, boiled and filtered successively, it is 1.5 g-2g/ml that filtrate is concentrated into concentration in vacuum rotary evaporator, obtains female
Loyal sub- crust concentrate, it is standby；
Step 4: the spaonin powder in step 2 and shrubalthea leaf powder are separately added into supercritical CO2In extraction apparatus, using absolute ethyl alcohol as
Extractant, powder and absolute ethyl alcohol mass ratio are 1:2-1:4, it is divided into and extracts to obtain natural plants saponin three times, it is standby;
Step 5: the fruit peel powder in step 2 is placed in into glass container, it is uniform to add absolute ethyl alcohol and stirring, is then in temperature
To be filtered after soaking 5-7d at 20-30 DEG C, filtrate concentrates in vacuum rotary evaporator, obtains cedra fruits pericarp essential oil,
It is standby；
Step 6, take the fruit of glossy privet crust solution in step 3, the citrus in the natural plants saponin and step 5 in step 4
Class Fruit Peel essential oil is added in deionized water, and above component additional proportion is 47-53：927-943：1-1.5：10-20, its
In terms of milliliter, natural plants saponin in gram, stirs for middle fruit of glossy privet crust solution, cedra fruits pericarp essential oil, deionized water
Obtained natural disinfection liquid detergent after uniformly.
A kind of 3. natural disinfection liquid detergent as claimed in claim 1, it is characterised in that the cedra fruits pericarp be orange,
One or more in orange, lemon and shaddock.
4. a kind of preparation method of natural disinfection liquid detergent as claimed in claim 2, it is characterised in that soaked in the step 3
Temperature is 30-40 DEG C, time 1-2h, and the time boiled is 1-2h.
5. a kind of preparation method of natural disinfection liquid detergent as claimed in claim 2, it is characterised in that the step 3 and step
The vacuum of vacuum rotary evaporator in five is 0.085-0.1MPa.
6. a kind of preparation method of natural disinfection liquid detergent as claimed in claim 2, it is characterised in that surpass in the step 4 and face
Boundary CO2CO in extraction apparatus2Flow be 30L/h, extraction pressure is 20-35MPa, and temperature is 50-60 DEG C, time 2-4h.
7. a kind of preparation method of natural disinfection liquid detergent as claimed in claim 2, it is characterised in that soaked in the step 5
During daily stir 2-3 times.
A kind of 8. preparation method of natural disinfection liquid detergent as claimed in claim 2, it is characterised in that the day in the step 6
The final concentration of 70-80mg/ml of the sub- crust concentrate of Nuzhen, an ancient nationality in China, ancestors of the Manchus, who founded the Jin Dynasty in right liquid detergent.
A kind of 9. preparation method of natural disinfection liquid detergent as claimed in claim 2, it is characterised in that the day in the step 6
The concentration of natural plants saponin is 1 ~ 1.5 mg/ml in right liquid detergent.
10. a kind of preparation method of natural disinfection liquid detergent as claimed in claim 2, it is characterised in that in the step 6
The percent concentration of cedra fruits pericarp essential oil is 1%-2% in Natural cleanser essence.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109234040A (en) * | 2018-10-24 | 2019-01-18 | 杨德刚 | Natural plants Saponaria officinalis is mostly used dish washing liquid and the preparation method and application thereof |
| CN115247103A (en) * | 2021-01-28 | 2022-10-28 | 张伟 | Benzene-free heavy stain removal and sterilization soft and bright laundry detergent |
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