CN102031205A - Natural plant washing preparation and preparation method thereof - Google Patents

Natural plant washing preparation and preparation method thereof Download PDF

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Publication number
CN102031205A
CN102031205A CN2009100445095A CN200910044509A CN102031205A CN 102031205 A CN102031205 A CN 102031205A CN 2009100445095 A CN2009100445095 A CN 2009100445095A CN 200910044509 A CN200910044509 A CN 200910044509A CN 102031205 A CN102031205 A CN 102031205A
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China
Prior art keywords
seed
extract
chinese soapberry
preparation
cmc
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CN2009100445095A
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CN102031205B (en
Inventor
夏焰明
曹瑾玉
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HUNAN YIYANG ZHONGXIN AGRICULTURAL TECHNOLOGY DEVELOPMENT Co Ltd
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HUNAN YIYANG ZHONGXIN AGRICULTURAL TECHNOLOGY DEVELOPMENT Co Ltd
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Priority to CN200910044509.5A priority Critical patent/CN102031205B/en
Publication of CN102031205A publication Critical patent/CN102031205A/en
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Publication of CN102031205B publication Critical patent/CN102031205B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention discloses a natural plant washing preparation which is prepared from pure natural plants and a preparation method thereof, which solve the problems of poor washing effect and deficiency in handfeel of the washing preparation. The washing preparation is characterized by comprising 20 to 85 weight parts of hibiscus leaf extract and 15 to 80 weight parts of Chinese soapberry fruit peel extract. In the preparation method, the hibiscus leaf extract and the Chinese soapberry fruit peel extract are mixed according to a proportion to prepare the washing preparation. After the hibiscus leaf extract and the Chinese soapberry fruit peel extract are compounded, surface-active substances between the hibiscus leaf extract and the Chinese soapberry fruit peel extract have synergistic effects of different degrees, so the disadvantages of poor using effect, insufficient foams and poor handfeel by using a single plant extract are overcome.

Description

Natural phant detergent compositions and preparation method thereof
Technical field:
The present invention relates to a kind of detergent compositions that is used for human body, specifically a kind of natural phant detergent compositions and preparation method thereof.
Background technology:
At present, the product that the cleaning product on the market especially is used for the washing of partes corporis humani position in people's daily life emerges in an endless stream, and the product of all kinds, various brands is too plenty for the eye to take it all on the market.But mostly be the chemosynthesis product, in many chemosynthesis products, all added many compositions that cause skin, hair quality to change, life-time service all will produce certain influence to skin, hair quality.Also have and partly added the cleaning product of natural components, and pure natural, ecosystem, the cleaning product market of not adding any chemical substance are blank.The juice of useful Leaf of Shrubalthea among the people and the pericarp of Seed of Chinese Soapberry are as the tradition of tableware cleaning, beauty treatment, hair washing, skin care.But the single rose of Sharon is during as articles for washing, and after about 20 minutes, its foam just disappears in the Normal juice of squeezing Leaf of Shrubalthea, makes the feel of washing weaken, and in addition, the viscosity of rose of Sharon Normal juice is lower, and during use, the perceptual image clear water is the same.When washing hair, Normal juice is easy to be difficult for smearing along under the hair spontaneous current, and is so same when using as bath article as the user, therefore, unless a large amount of use, washing effect is bad and lack feel.The fruit of natural phant Seed of Chinese Soapberry tree, by artificial solarization system, removal core, the pericarp that then obtains.Can directly be used for extracting its effective ingredient---saponin(e, make and wash clean articles for use---Seed of Chinese Soapberry soap breast, the manual soap of Seed of Chinese Soapberry etc.This class natural phant is washed clean articles for use, and is quite popular in countries such as Japan, Taiwan, Korea S, the U.S..The juice that same single use Seed of Chinese Soapberry pericarp is endured out is during as the human body articles for washing, and foam is also abundant and stability is bad equally, and has the problem of not enough washing effect that causes of viscosity and feel equally.
Summary of the invention:
The purpose of this invention is to provide a kind of natural phant detergent compositions that adopts the natural plant preparation and preparation method thereof, and solve the bad and shortage feel problem of its washing effect.
The present invention adopts following technical scheme to realize its goal of the invention, a kind of natural phant detergent compositions, and by weight, its composition is 20 parts-85 parts of Leaf of Shrubalthea extracts, 15 parts-80 parts of Seed of Chinese Soapberry peel extracts.
The present invention by weight, its optimum ratio is 80 parts of Leaf of Shrubalthea extracts, 20 parts of Seed of Chinese Soapberry peel extracts.
A kind of preparation method of above-mentioned natural phant detergent compositions is mixed and made into detergent compositions with Leaf of Shrubalthea extract, Seed of Chinese Soapberry peel extract according to proportioning.
The preferred extracting method of Leaf of Shrubalthea extract of the present invention is obtained the Leaf of Shrubalthea extract for adopting physical method to squeeze its Normal juice; The preferred extracting method of Seed of Chinese Soapberry peel extract is obtained the Seed of Chinese Soapberry peel extract for adopting decocting method.
When Seed of Chinese Soapberry peel extract of the present invention adopts decocting method, it comprises the following steps, with Seed of Chinese Soapberry pericarp boiling 2 times, adds 6 times of water gagings for the first time and decocts 2 hours, add for the second time 4 times of water gagings and decocted 1 hour, the filtrate that merges secondary gets the water extract of Seed of Chinese Soapberry pericarp.
The above-mentioned hibiscus Malvaceae plant of mentioning, machaka, leaf is avette, and Xia Qiu is bloomed, and spends single leave armpit, and corolla is purplish red or pink, and Shrubalthea Flower is towards opening to fall dusk.Among the people to fry in shallow oil the washing face with Shrubalthea Flower, can beautify appearance; Can control tinea capitis with leaf juice hair washing, hair comb easily is logical, moistens healthy hair, can discount from right pitch-black and can remove anti-dandruff.Contain a kind of saponin composition in the rose of Sharon leaf, the process of washing by rubbing with the hands forms foam, can be following dirty.The present invention adopts the leaf of the rose of Sharon as raw material.
The above-mentioned Sapindus sapindaceous plant of mentioning, arbor, high 10-15 rice, the seed sphere, black, hard.The florescence 5-6 month, fructescence October.Timber is faint yellow, and matter is crisp, does wooden comb more and uses; Pericarp is mashed and can be made the soap surrogate; Seed can be stir-fried and eaten, and kernel extracts grease can make lubricating oil; Root, fruit are used as medicine, can be clearing heat and detoxicating, and preventing phlegm from forming and stopping coughing.Fruit contains triterpenoid saponins such as sapindoside.The present invention adopts the fruit of natural phant Seed of Chinese Soapberry tree, by artificial solarization system, removal core, and the pericarp that then obtains.
Owing to adopt technique scheme, the present invention has realized goal of the invention preferably, after the water extract of rose of Sharon Normal juice and Seed of Chinese Soapberry pericarp is composite, synergism is in various degree arranged between the surface-active substance between the two, it is not good to have solved a kind of plant extraction liquid result of use of single use, foam is not abundant, the shortcoming that feel is bad.
Embodiment:
The invention will be further described below in conjunction with embodiment.
A kind of natural phant detergent compositions, by weight, its composition is 20 parts-85 parts of Leaf of Shrubalthea extracts, 15 parts-80 parts of Seed of Chinese Soapberry peel extracts.
The proportioning that present embodiment adopts is 80 parts of Leaf of Shrubalthea extracts, 20 parts of Seed of Chinese Soapberry peel extracts.
A kind of preparation method of above-mentioned natural phant detergent compositions is mixed and made into detergent compositions with Leaf of Shrubalthea extract, Seed of Chinese Soapberry peel extract according to proportioning.
The preferred extracting method of Leaf of Shrubalthea extract of the present invention is obtained the Leaf of Shrubalthea extract for adopting physical method to squeeze its Normal juice; The preferred extracting method of Seed of Chinese Soapberry peel extract is obtained the Seed of Chinese Soapberry peel extract for adopting decocting method.
When Seed of Chinese Soapberry peel extract of the present invention adopts decocting method, it comprises the following steps, with Seed of Chinese Soapberry pericarp boiling 2 times, adds 6 times of water gagings for the first time and decocts 2 hours, add for the second time 4 times of water gagings and decocted 1 hour, the filtrate that merges secondary gets the water extract of Seed of Chinese Soapberry pericarp.
With the water extract of Leaf of Shrubalthea Normal juice and Seed of Chinese Soapberry pericarp composite after, through verification experimental verification, synergism is in various degree arranged between the surface-active substance between the two.It is not good to have solved a kind of plant extraction liquid result of use of single use, and foam is not abundant, the shortcoming that feel is bad.
Test objective: the composite back of the water extract of check Leaf of Shrubalthea extracting solution and Seed of Chinese Soapberry pericarp foam enriches the effect that degree is a tensio-active agent.
Test apparatus and method:
Instrument: KRUSS K122 type surface tension instrument, HAAKE K20 super constant temperature trough.
The mensuration of experimental technique: micelle-forming concentration cmc and surface tension γ cmc is measured automatically by instrument.
The preparation of raw material:
Get fresh Leaf of Shrubalthea, place juice extractor, get its juice after the filtration.
Get the fruit of Seed of Chinese Soapberry tree, by artificial solarization system, removal core, the pericarp that then obtains.
Decoct twice with decocting method, get filtrate after the filtration.
The comparison foundation and the method for calculation of composite effect:
Adopt the micelle-forming concentration cmc of single component 1, cmc 2And surfactivity tension force γ cmc 1, γ cmc 2Weighted mean carry out theoretic composite effect and calculate:
Cmc Reason=X 1Cmc 1+ X 2Cmc 2γ cmc Reason=γ cmc 1X 1+ γ cmc 2X 2
In the formula: X 1, X 2---be respectively the massfraction of the single component rose of Sharon and Seed of Chinese Soapberry;
Cmc Reason, γ cmc Reason---cmc, the γ cmc calculated value of composite back preparation;
It is composite that two kinds of tensio-active agents carry out, and may show compound system performance cmc (cmc because of producing synergistic effect Table) or performance γ cmc (γ cmc Table) can be different from cmc theoretical value or γ cmc theoretical value.Work as cmc TableOr γ cmc TableLess than cmc ReasonOr γ cmc ReasonThe time, show compound system synergy, and work as cmc TableOr γ cmc TableGreater than cmc ReasonOr γ cmc ReasonThe time, show that compound system subtracts effect.
Composite effect:
When table 1 is 25 ℃, the rose of Sharon that records and the cmc of Seed of Chinese Soapberry and γ cmc numerical value.
Table 1: the cmc of tensio-active agent and γ cmc numerical value (testing oneself)
Tensio-active agent Cmc/mg·L -1 ycmc/mN·m -1
The rose of Sharon 38.5 32.7
The Seed of Chinese Soapberry surface-active substance 33.4 36.5
When table 2 is 25 ℃, the data that record after the rose of Sharon and Seed of Chinese Soapberry are composite.
Table 2: the cmc of compound system and γ cmc numerical value
Composite Leaf of Shrubalthea/Seed of Chinese Soapberry fruit Conclusion
Weight ratio 4∶1
cmc Reason/mg·L -1 37.48
γcmc Reason/mN·m -1 33.46
Cmc Table/mg·L -1 23.34 Numerical value is lower, and activity is stronger
ycmc Table/mN·m -1 28.11 Numerical value is lower, and activity is stronger
cmc Table-cmc Reason -14.14 Be lower than theoretical value, synergy
γcmc Table-γcmc Reason -5.35 Be lower than theoretical value, synergy
(cmc Table-cmc Reason)/cmc Reason/% 37.72 It is obvious to improve 37.72% effect
(γcmc Table-γcmc Reason)/γcmc Reason/% 15.98 Improve 15.98%, effect is better
Conclusion: as can be seen from Table 2, cmc The table ratioCmc ReasonLittle by 14.14, the micelle-forming concentration after promptly composite is lower than theoretical value, shows synergistic effect to occur after composite, and the raising ratio is 37.72%, shows that synergy is obvious.γ cmc TableThan γ cmc ReasonLittle by 5.35, the surfactivity tension force after promptly composite is lower than theoretical value, shows equally synergistic effect to occur after composite.The raising ratio is 15.98%, shows that effect is better.In addition, after both were composite, viscosity strengthened, and feel is obviously good than the single use rose of Sharon or Seed of Chinese Soapberry extract.
In suitability for industrialized production, be packing, transportation, easy to use, to mixing the preparation that forms, concentrate according to proportioning, sterilization, detergent compositions is promptly made in can.

Claims (5)

1. a natural phant detergent compositions is characterized in that by weight, and its composition is 20 parts-85 parts of Leaf of Shrubalthea extracts, 15 parts-80 parts of Seed of Chinese Soapberry peel extracts.
2. natural phant detergent compositions according to claim 1 is characterized in that by weight, and optimum ratio is 80 parts of Leaf of Shrubalthea extracts, 20 parts of Seed of Chinese Soapberry peel extracts.
3. the preparation method of natural phant detergent compositions as claimed in claim 1 or 2 is characterized in that Leaf of Shrubalthea extract, Seed of Chinese Soapberry peel extract are mixed and made into detergent compositions according to proportioning.
4. according to the preparation method of the described natural phant detergent compositions of claim 3, it is characterized in that the preferred extracting method of Leaf of Shrubalthea extract is obtained the Leaf of Shrubalthea extract for adopting physical method to squeeze its Normal juice; The preferred extracting method of Seed of Chinese Soapberry peel extract is obtained the Seed of Chinese Soapberry peel extract for adopting decocting method.
5. according to the preparation method of the described natural phant detergent compositions of claim 4, when it is characterized in that the Seed of Chinese Soapberry peel extract adopts decocting method, it comprises the following steps, with Seed of Chinese Soapberry pericarp boiling 2 times, adding for the first time 6 times of water gagings decocted 2 hours, add for the second time 4 times of water gagings and decocted 1 hour, the filtrate that merges secondary gets the water extract of Seed of Chinese Soapberry pericarp.
CN200910044509.5A 2009-10-01 2009-10-01 Natural plant washing preparation and preparation method thereof Expired - Fee Related CN102031205B (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102080028A (en) * 2011-01-05 2011-06-01 中国林业科学研究院林产化学工业研究所 Dryopteris erythrosora/soapberry natural biomass detergent and preparation method thereof
CN104788526A (en) * 2015-03-23 2015-07-22 福建省轻工业研究所 Soapberry saponin solution containing clear and stable compounds and preparation method thereof
CN105524746A (en) * 2016-02-14 2016-04-27 汕头市正能量本草植物研究所 Health-care and sterilizing traditional Chinese medicine cleaning fluid for air conditioner and preparation method of cleaning fluid
CN107022430A (en) * 2017-04-21 2017-08-08 程海权 A kind of natural multiple-effect washes the dishes powder
CN107384607A (en) * 2017-06-02 2017-11-24 南阳师范学院 A kind of natural disinfection liquid detergent and preparation method thereof
CN107418795A (en) * 2017-06-23 2017-12-01 青岛元汇丰企业管理咨询服务有限公司 Student's laundry soap and its production method
CN112430511A (en) * 2019-08-10 2021-03-02 樊龙耀 Traditional Chinese medicine laundry detergent and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
武士威,等: "无患子餐具洗涤剂的研制", 《电力环境保护》 *
沈铭高,等: "木槿叶中表面活性成分的初步研究", 《浙江林业科技》 *

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102080028A (en) * 2011-01-05 2011-06-01 中国林业科学研究院林产化学工业研究所 Dryopteris erythrosora/soapberry natural biomass detergent and preparation method thereof
CN102080028B (en) * 2011-01-05 2013-01-23 中国林业科学研究院林产化学工业研究所 Dryopteris erythrosora/soapberry natural biomass detergent and preparation method thereof
CN104788526A (en) * 2015-03-23 2015-07-22 福建省轻工业研究所 Soapberry saponin solution containing clear and stable compounds and preparation method thereof
CN105524746A (en) * 2016-02-14 2016-04-27 汕头市正能量本草植物研究所 Health-care and sterilizing traditional Chinese medicine cleaning fluid for air conditioner and preparation method of cleaning fluid
CN107022430A (en) * 2017-04-21 2017-08-08 程海权 A kind of natural multiple-effect washes the dishes powder
CN107384607A (en) * 2017-06-02 2017-11-24 南阳师范学院 A kind of natural disinfection liquid detergent and preparation method thereof
CN107418795A (en) * 2017-06-23 2017-12-01 青岛元汇丰企业管理咨询服务有限公司 Student's laundry soap and its production method
CN112430511A (en) * 2019-08-10 2021-03-02 樊龙耀 Traditional Chinese medicine laundry detergent and preparation method thereof

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