CN109198632A - A kind of preparation method of heat-clearing inflammation relieving additive - Google Patents
A kind of preparation method of heat-clearing inflammation relieving additive Download PDFInfo
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- CN109198632A CN109198632A CN201710549506.1A CN201710549506A CN109198632A CN 109198632 A CN109198632 A CN 109198632A CN 201710549506 A CN201710549506 A CN 201710549506A CN 109198632 A CN109198632 A CN 109198632A
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a kind of preparation method of heat-clearing inflammation relieving additive, the heat-clearing inflammation relieving additive is prepared by pretreatment, ultrasonic extraction, centrifuge separation, concentration, drying and other steps；The heat-clearing inflammation relieving additive raw material component includes (in parts by weight): peppermint, Radix Glycyrrhizae, hawthorn, the root of Chinese clematis, cortex moutan, stringy stonecrop, Radix Rehmanniae；By pretreatment, extraction, centrifuge separation and concentration and etc. be prepared；Heat-clearing inflammation relieving additive of the invention can be used as health-care additive and make an addition in food preparation process, present invention employs ultrasonic extraction and film concentration techniques, the synergistic effect of the two, so that being easy to be retained by the aroma substance of peppermint, cortex moutan, the cloves destroyed etc. in the heat-clearing inflammation relieving additive of preparation, again by with other components optimum organization, obtain a kind of heat-clearing inflammation relieving additive for being with peppermint faint scent and the fragrance of a flower, preparation method technical process is simple and easy, equipment is simple, it is easy to industrialized production, it is easy to promote and utilize.
Description
Technical field
The present invention relates to agent preparation technical field is added, more particularly to a kind of preparation method of heat-clearing inflammation relieving additive.
Background technique
Currently, the common concentration technology of heat-clearing inflammation relieving additive is that Chinese herbal medicine aqueous extract crystalline substance is evaporated concentration, i.e.,
Chinese herbal medicine aqueous extract is heated to boiling, water evaporation is allowed to vaporize, to obtain concentrate, belongs to high temperature concentration, including vacuum
It is concentrated by evaporation and micro-positive pressure is concentrated by evaporation；And high temperature concentration be disadvantageous in that: for effective component be volatile component and
The Chinese herbal medicine aqueous extract of heat-sensitive ingredients, will lead to the loss of effective component using this condensing mode.
Summary of the invention
Present invention aims at propose a kind of heat-clearing inflammation relieving additive to preparation method.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A kind of heat-clearing inflammation relieving additive is prepared by pretreatment, ultrasonic extraction, centrifuge separation, concentration, drying and other steps
It obtains.
Further, pre-treatment step are as follows: the raw material of the additive is cleaned, is mixed, with the water of 2-3 times of parts by weight
80-100 DEG C decocts 1 time, filtering, and filter residue is decocted 1-2 times with 40-70 DEG C of water of 2-3 times of parts by weight again, and filtering obtains mixed liquor；
Further, the material component of heat-clearing inflammation relieving additive includes (in parts by weight): 15-25 parts of peppermint, Radix Glycyrrhizae 10-
16 parts, 12-18 parts of hawthorn, 12-18 parts of the root of Chinese clematis, 6-10 parts of cortex moutan, 6-12 parts of stringy stonecrop, 1-10 parts of Radix Rehmanniae.
Further, the material component of heat-clearing inflammation relieving additive include (in parts by weight): 20 parts of peppermint, 13 parts of Radix Glycyrrhizae,
15 parts of hawthorn, 15 parts of the root of Chinese clematis, 8 parts of cortex moutan, 9 parts of stringy stonecrop, 5 parts of Radix Rehmanniae.
Further, ultrasonic extraction step are as follows: ethyl alcohol is added in mixed liquor, carries out ultrasonic extraction；
Further, step with centrifugal separation are as follows: temperature be 25-35 DEG C, centrifugal rotational speed be 4500-6000r/min condition
Under, the mixed liquor after ultrasonic extraction is subjected to liquid-liquid separation, time 25-45min.Further, concentration step are as follows: will
For the supernatant obtained after centrifugation by ultrafiltration membrane, it is 1.02-1.25's that permeate, which is concentrated into relative density using reverse osmosis membrane,
Concentrate.
Further, spray step are as follows: powdered heat-clearing inflammation relieving additive is made through low temperature spray drying in concentrate.
Further, in ultrasonic extraction, the additional amount of ethyl alcohol is 1-2 times of mixing Chinese herbal medicine weight；Ultrasonic extraction
Condition are as follows: time 15-30min, 25-35 DEG C of temperature, power 400-550W, ultrasonic frequency 15-45KHz.
Further, ultrafiltration membrane energy molecular cut off used in concentration is greater than the substance of 1000 dalton, reverse osmosis membrane
The concentration pressure of concentration is 1.4-1.8MPa, and temperature is 28 ± 1 DEG C.
The correlation properties of part material are as follows in the present invention:
Radix Glycyrrhizae: Radix Glycyrrhizae: its is sweet in flavor, flat, slightly cool in nature, enters spleen, stomach, lung channel, and there is invigorating middle warmer and replenishing QI, relieving spasm to stop pain, moistening lung to stop
Cough, purging fire for removing toxin, coordinating the drug actions of a prescription.Abscess of throat is cured mainly, is coughed, weakness of the spleen and the stomach, taste-blindness rate, hepatitis, hysteria, carbuncle
Furuncle poison, drug and food poisoning.
Hawthorn, sour sweet, slightly warm in nature；Containing citric acid, malic acid, ascorbic acid, sugar and protein, carbohydrate.Have
Blood pressure lowering, advantageous invigorating the spleen promoting the circulation of qi, scattered silt resolving sputum help digestion and grind product, promote the effect of gastro-intestinal digestion, can be with health care, beauty, through often eating
With that can soften blood vessel, cardioprotection prevents and treats human body scurvy, whets the appetite.Also have toward acne, beauty, resist old and weak beauty treatment
Effect.
The root of Chinese clematis: it is its acrid flavour, salty, it is warm-natured, return bladder meridian.With dispelling wind and eliminating dampness, effect of removing obstruction in channels to relieve pain.It is mainly used for rheumatism
Numbness pain, extremity numbness, muscle arteries and veins contraction, joint stuffiness, bone are choked with sobs larynx.
Peppermint: being one of Chinese conventional Chinese medicine, is pungent cool property sweating antipyretic medicine, controls influenza, headache, hot eyes, body
The diseases such as heat, throat, gum swelling and pain.External application can control neuralgia, pruitus, fash and eczema etc..The peppermint of light friend's Greenhouse Fruit Picking
It is the fresh vegetable on Spring Festival dining table again.Salubrious palatable, usually with peppermint for tea, clear away heart-fire improving eyesight.Peppermint also incendivity fat, deoils
It is greasy.
Cortex moutan: acrid flavour, hardship, it is cool in nature.Heat-clearing, cool blood and blood, dispersing blood stasis.Heat invading xuefen, macular eruption are controlled, frightened epilepsy is spat, hematochezia,
Hectic fever due to yin labor heat, menostasis, large carbuncle flutter damage.Main fever and chills, apoplexy Chi Zong, convulsion, frightened epilepsy perverse trend, except disease heavily fortified point hemostasis stays house stomach, peace five
It is dirty, treat ulcerative carbuncle.Except when gas have a headache, the hot exhaustion or lesion of the five internal organs of visitor, labor gas head pain in the loins, wind keeps silent, insane disease.Cold air is controlled, all pains are dissipated, controls woman's passages through which vital energy circulates not
Logical, blood drips Low Back Pain.
Stringy stonecrop, it is sweet in flavor, light, it is cool in nature；Return liver, stomach, large intestine channel；With clearing heat and promoting diuresis, removing toxicity for detumescence,
Cooling blood and hemostasis and other effects.
Radix Rehmanniae: it is sweet in flavor, it is cool in nature, enter the heart, liver and kidney channel, can cool blood and enriching yin, have heat-clearing enriching yin, cooling blood and hemostasis, life
The effect of saliva quenches the thirst.Modern pharmacological studies have shown that glutinous rehmannia has anti-radiation, liver protection, reduces blood glucose, heart tonifying, hemostasis, diuresis, resists
The effect of fungi.
The beneficial effect of the present invention compared with the prior art includes:
1, present invention employs ultrasonic extraction and film concentration technique, the synergistic effects of the two, so that the heat-clearing of preparation loses
Be easy to be retained by the effective component of peppermint, cortex moutan, the Radix Glycyrrhizae destroyed etc. in fiery additive, then by with other components
Optimum organization, obtains a kind of heat-clearing inflammation relieving additive for being with peppermint faint scent and the fragrance of a flower, and preparation method technical process is simply easy
Row, equipment is simple, easy to industrialized production, easy to promote and utilize.
2, heat-clearing inflammation relieving additive of the invention can be used as health-care additive and be applied in food preparation, wherein that adds is sweet
Grass, peppermint, hawthorn, 4 taste Chinese herbal medicine of Radix Rehmanniae there is clearing away summerheat, inducing diaphoresis to promote the production of body fluid, stomach strengthening and digestion promoting and other effects, by having between drug
Mutual compatibility and the interaction for imitating ingredient, keep its character milder, are especially advantageous for absorption of human body, also, the taste of each ingredient
Road is cleverly fused together, and while realizing heat-clearing inflammation relieving function, food taste is more delicious.
Specific embodiment
Invention is further described in detail With reference to embodiment.It is emphasized that following the description is only
It is merely exemplary, the range and its application being not intended to be limiting of the invention.
The preparation method of heat-clearing inflammation relieving additive of the present invention, the specific steps are as follows:
A kind of preparation method of heat-clearing inflammation relieving additive, comprising the following steps:
S1: pretreatment: raw material is cleaned, and is mixed, and is decocted 1 time with 90 DEG C of water of 2-3 times of parts by weight, with 200-250 purpose
Filter cloth is filtered, and filter residue uses 55 DEG C of water of 3 times of parts by weight to decoct 2 times again, is filtered, is obtained with the filter cloth of 200-250 mesh
Mix medium-height grass liquid；
The material component of the heat-clearing inflammation relieving additive include (in parts by weight): 15-25 parts of peppermint, 10-16 parts of Radix Glycyrrhizae,
12-18 parts of hawthorn, 12-18 parts of the root of Chinese clematis, 6-10 parts of cortex moutan, 6-12 parts of stringy stonecrop, 1-10 parts of Radix Rehmanniae.
S2: ultrasonic extraction: in mixing medium-height grass liquid, the middle ethyl alcohol that 1-2 times of mixing Chinese herbal medicine weight is added is in temperature
25-35 DEG C, power 400-550W, ultrasonic frequency carries out rate ultrasonic extraction 15-30min under conditions of being 15-45KHz；
S3: centrifuge separation: being 25-35 DEG C in temperature by the mixed liquor upper layer supernatant and lower layer's turbid solution after ultrasonic extraction, centrifugation
25-45min is centrifuged under the conditions of being 4500-6000r/min in revolving speed；
S4: concentration: by the supernatant obtained after centrifugation by ultrafiltration membrane, permeate is 1.4- using concentration pressure
1.8MPa, the reverse osmosis membrane that temperature is 28 ± 1 DEG C are concentrated into the concentrate that relative density is 1.02-1.25.
S5: powdered heat-clearing inflammation relieving additive spray drying: is made through low temperature spray drying in concentrate.
Embodiment 1:
S1: pretreatment: raw material is cleaned, and is mixed, and is decocted 1 time with 800 DEG C of water of 2 times of parts by weight, with the filter clothes of 200 mesh into
Row filtering, filter residue use 40 DEG C of water of 2 times of parts by weight to decoct again 1 time, are filtered with the filter cloth of 200 mesh, obtain mixed liquor；
The material component of the heat-clearing inflammation relieving additive includes (in parts by weight): 15 parts of peppermint, 10 parts of Radix Glycyrrhizae, hawthorn 12
Part, 12 parts of the root of Chinese clematis, 6 parts of cortex moutan, 6 parts of stringy stonecrop, 1 part of Radix Rehmanniae.
S2: ultrasonic extraction: in mixed liquor, the middle ethyl alcohol for being added 1 times of mixing Chinese herbal medicine weight is 25 DEG C in temperature, function
Rate is 400W, and ultrasonic frequency carries out rate ultrasonic extraction 15min under conditions of being 15KHz；
S3: centrifuge separation: being 25 in temperature by the mixed liquor upper layer supernatant and lower layer's turbid solution after ultrasonic extraction
DEG C, 25min is centrifuged under the conditions of being 4500r/min in centrifugal rotational speed；
S4: concentration: by the supernatant obtained after centrifugation by ultrafiltration membrane, permeate using concentration pressure be 1.5MPa,
The reverse osmosis membrane that temperature is 28 ± 1 DEG C is concentrated into the concentrate that relative density is 1.02；
S5: powdered heat-clearing inflammation relieving additive spray drying: is made through low temperature spray drying in concentrate.
Embodiment 2:
A kind of preparation method of heat-clearing inflammation relieving additive, comprising the following steps:
S1: pretreatment: raw material is cleaned, and is mixed, and is decocted 1 time with 80-100 DEG C of water of 3 times of parts by weight, with the filter of 230 mesh
Cloth is filtered, and filter residue uses 550 DEG C of water of 3 times of parts by weight to decoct 2 times again, is filtered, is mixed with the filter cloth of 230 mesh
Liquid；
The material component of the heat-clearing inflammation relieving additive includes (in parts by weight): 20 parts of peppermint, 13 parts of Radix Glycyrrhizae, hawthorn 15
Part, 15 parts of the root of Chinese clematis, 8 parts of cortex moutan, 9 parts of stringy stonecrop, 5 parts of Radix Rehmanniae；
S2: ultrasonic extraction: in mixing medium-height grass liquid, the middle ethyl alcohol that 2 times of medicine weight of mixing is added is 30 DEG C in temperature, function
Rate is 500W, and ultrasonic frequency carries out rate ultrasonic extraction 25min under conditions of being 25KHz；
S1: preparation mint flavored health-care additive: by peppermint, the public blueness of duck, Radix Glycyrrhizae, the root of Chinese clematis, hypericum japonicum, cortex moutan, hang down basin
Grass, Radix Rehmanniae, caulis clematidis armandii, 10 taste Chinese herbal medicine of cloves are cleaned, mixing, specifically includes the following steps:
S11: pretreatment: with 80 DEG C of water decoctions 10 taste Chinese herbal medicine 1 time of 2 times of parts by weight, filtering, filter residue uses 2 times of weight again
40 DEG C of water of part decoct 1 time, filtering, obtain mixing medium-height grass liquid；
S12: extraction: ethyl alcohol is added in mixing medium-height grass liquid, carries out ultrasonic extraction；The additional amount of the ethyl alcohol is mixing
1 times of Chinese herbal medicine weight；Ultrasonic extraction condition are as follows: time 15min, 25 DEG C of temperature, power 400W, ultrasonic frequency is
15KHz；
S13: centrifuge separation: being 25 in temperature by the mixed liquor upper layer supernatant and lower layer's turbid solution after ultrasonic extraction
DEG C, 25min is centrifuged under the conditions of being 4500r/min in centrifugal rotational speed；
S14: concentration: by the supernatant obtained after centrifugation by ultrafiltration membrane, the ultrafiltration membrane energy molecular cut off is greater than
The substance of 1000 dalton, using being concentrated, pressure is 1.4MPa to permeate, the reverse osmosis membrane that temperature is 30 ± 1 DEG C is concentrated into phase
The concentrate for being 1.02 to density, is prepared mint flavored health-care additive；
S2: and face: butter is melted, then wheat flour, corn flour, black bean powder are mixed, are put into the wood of the parts by weight
Sugar alcohol, suitable quantity of water mixing, are added melted butter and the resulting mint flavored health-care additive of step S1, and mixing is kneaded into shiny surface
Group covers one layer of preservative film, relaxation 30min；
S3: production biscuit base: will roll into the piece of 5-8mm thickness by dough obtained by step S2, then use Biscuit mold briquetting,
It is stand-by to obtain biscuit base；
S4: baking: taking out preprepared baking tray, and biscuit base is placed on baking tray, so by the brush a little oil on baking tray
Several holes are pricked on biscuit base with toothpick afterwards, and oven temperature is adjusted to 110 DEG C of preheating 4min, is placed into oven in 180 DEG C
20min is toasted, can be prepared by the mint flavored health-caring biscuit that quality is 20g.
Embodiment two:
A kind of mint flavored health-caring biscuit, material component include (in parts by weight): 500 parts of wheat flour, corn flour 400
Part, 300 parts of black bean powder, 250 parts of butter, 30 parts of xylitol, 20 parts of peppermint, duck public green 7 parts, 8 parts of Radix Glycyrrhizae, 8 parts of the root of Chinese clematis, Tian Ji
Yellow 6 parts, 8 parts of cortex moutan, 6 parts of stringy stonecrop, 2 parts of Radix Rehmanniae, 2 parts of caulis clematidis armandii, 2 parts of cloves, appropriate amount of water.
The present invention also provides the preparation methods of Chinese herbal medicine concentrate, the specific steps are as follows:
S1: preparation mint flavored health-care additive: by peppermint, the public blueness of duck, Radix Glycyrrhizae, the root of Chinese clematis, hypericum japonicum, cortex moutan, hang down basin
Grass, Radix Rehmanniae, caulis clematidis armandii, 10 taste Chinese herbal medicine of cloves are cleaned, mixing, specifically includes the following steps:
S11: pretreatment: with 90 DEG C of water decoctions 10 taste Chinese herbal medicine 1 time of 2 times of parts by weight, filtering, filter residue uses 2 times of weight again
55 DEG C of water of part decoct 2 times, filtering, obtain mixing medium-height grass liquid；
S12: extraction: ethyl alcohol is added in mixing medium-height grass liquid, carries out ultrasonic extraction；The additional amount of the ethyl alcohol is mixing
2 times of Chinese herbal medicine weight；Ultrasonic extraction condition are as follows: time 20min, 30 DEG C of temperature, power 500W, ultrasonic frequency is
30KHz；
S13: centrifuge separation: being 30 in temperature by the mixed liquor upper layer supernatant and lower layer's turbid solution after ultrasonic extraction
DEG C, 35min is centrifuged under the conditions of being 5000r/min in centrifugal rotational speed；
S14: concentration: by the supernatant obtained after centrifugation by ultrafiltration membrane, the ultrafiltration membrane energy molecular cut off is greater than
The substance of 1000 dalton, using being concentrated, pressure is 1.6MPa to permeate, the reverse osmosis membrane that temperature is 30 ± 1 DEG C is concentrated into phase
The concentrate for being 1.15 to density, is prepared mint flavored health-care additive；
S2: and face: butter is melted, then wheat flour, corn flour, black bean powder are mixed, are put into the wood of the parts by weight
Sugar alcohol, suitable quantity of water mixing, are added melted butter and the resulting mint flavored health-care additive of step S1, and mixing is kneaded into shiny surface
Group covers one layer of preservative film, relaxation 35min；
S3: production biscuit base: the piece of 6mm thickness will be rolled by dough obtained by step S2, then use Biscuit mold briquetting, obtain
It is stand-by to biscuit base；
S4: baking: taking out preprepared baking tray, and biscuit base is placed on baking tray, so by the brush a little oil on baking tray
Several holes are pricked on biscuit base with toothpick afterwards, and oven temperature is adjusted to 130 DEG C of preheating 5min, is placed into oven in 220 DEG C
25min is toasted, can be prepared by the mint flavored health-caring biscuit that quality is 25g.
Embodiment three
A kind of mint flavored health-caring biscuit, material component include (in parts by weight): 600 parts of wheat flour, corn flour 450
Part, 400 parts of black bean powder, 300 parts of butter, 40 parts of xylitol, 25 parts of peppermint, duck be 10 parts public green, 10 parts of Radix Glycyrrhizae, 10 parts of the root of Chinese clematis,
8 parts of hypericum japonicum, 10 parts of cortex moutan, 8 parts of stringy stonecrop, 3 parts of Radix Rehmanniae, 3 parts of caulis clematidis armandii, 3 parts of cloves, appropriate amount of water.
The present invention also provides the preparation methods of Chinese herbal medicine concentrate, the specific steps are as follows:
S1: preparation mint flavored health-care additive: by peppermint, the public blueness of duck, Radix Glycyrrhizae, the root of Chinese clematis, hypericum japonicum, cortex moutan, hang down basin
Grass, Radix Rehmanniae, caulis clematidis armandii, 10 taste Chinese herbal medicine of cloves are cleaned, mixing, specifically includes the following steps:
S11: pretreatment: with 100 DEG C of water decoctions 10 taste Chinese herbal medicine 1 time of 3 times of parts by weight, filtering, filter residue uses 3 times of weight again
70 DEG C of water of part decoct 2 times, filtering, obtain mixing medium-height grass liquid；
S12: extraction: ethyl alcohol is added in mixing medium-height grass liquid, carries out ultrasonic extraction；The additional amount of the ethyl alcohol is mixing
2 times of Chinese herbal medicine weight；Ultrasonic extraction condition are as follows: time 30min, 35 DEG C of temperature, power 550W, ultrasonic frequency is
45KHz；
S13: centrifuge separation: being 35 in temperature by the mixed liquor upper layer supernatant and lower layer's turbid solution after ultrasonic extraction
DEG C, 45min is centrifuged under the conditions of being 6000r/min in centrifugal rotational speed；
S14: concentration: by the supernatant obtained after centrifugation by ultrafiltration membrane, the ultrafiltration membrane energy molecular cut off is greater than
The substance of 1000 dalton, using being concentrated, pressure is 1.8MPa to permeate, the reverse osmosis membrane that temperature is 30 ± 1 DEG C is concentrated into phase
The concentrate for being 1.25 to density, is prepared mint flavored health-care additive；
S2: and face: butter is melted, then wheat flour, corn flour, black bean powder are mixed, are put into the wood of the parts by weight
Sugar alcohol, suitable quantity of water mixing, are added melted butter and the resulting mint flavored health-care additive of step S1, and mixing is kneaded into shiny surface
Group covers one layer of preservative film, relaxation 45min；
S3: production biscuit base: the piece of 8mm thickness will be rolled by dough obtained by step S2, then use Biscuit mold briquetting, obtain
It is stand-by to biscuit base；
S4: baking: taking out preprepared baking tray, and biscuit base is placed on baking tray, so by the brush a little oil on baking tray
Several holes are pricked on biscuit base with toothpick afterwards, and oven temperature is adjusted to 140 DEG C of preheating 7min, is placed into oven in 250 DEG C
35min is toasted, can be prepared by the mint flavored health-caring biscuit that quality is 35g.
The above content is combine it is specific/further detailed description of the invention for preferred embodiment, cannot
Assert that specific implementation of the invention is only limited to these instructions.General technical staff of the technical field of the invention is come
It says, without departing from the inventive concept of the premise, some replacements or modifications can also be made to the embodiment that these have been described,
And these substitutions or variant all shall be regarded as belonging to protection scope of the present invention.
Claims (10)
1. a kind of preparation method of heat-clearing inflammation relieving additive, which is characterized in that the heat-clearing inflammation relieving additive is by pre-processing, surpassing
Sound wave extraction, centrifuge separation, concentration, drying and other steps are prepared.
2. the preparation method of heat-clearing inflammation relieving additive as described in claim 1, which is characterized in that the pre-treatment step are as follows: will
The raw material of the additive is cleaned, mixing, is decocted 1 time with 80-100 DEG C of water of 2-3 times of parts by weight, filtering, filter residue is again with 2-3 times
40-70 DEG C of water of parts by weight decocts 1-2 times, and filtering obtains mixed liquor.
3. the preparation method of heat-clearing inflammation relieving additive as claimed in claim 2, which is characterized in that the heat-clearing inflammation relieving additive
Material component includes (in parts by weight): 15-25 parts of peppermint, 10-16 parts of Radix Glycyrrhizae, 12-18 parts of hawthorn, 12-18 parts of the root of Chinese clematis, male
6-10 parts of the root bark of tree peony, 6-12 parts of stringy stonecrop, 1-10 parts of Radix Rehmanniae.
4. the preparation method of heat-clearing inflammation relieving additive as claimed in claim 3, which is characterized in that the heat-clearing inflammation relieving additive
Material component includes (in parts by weight): 20 parts of peppermint, 13 parts of Radix Glycyrrhizae, 15 parts of hawthorn, 15 parts of the root of Chinese clematis, 8 parts of cortex moutan, hang down basin
9 parts, 5 parts of Radix Rehmanniae of grass.
5. the preparation method of heat-clearing inflammation relieving additive as described in claim 1, which is characterized in that the ultrasonic extraction step
Are as follows: ethyl alcohol is added in mixed liquor, carries out ultrasonic extraction.
6. the preparation method of heat-clearing inflammation relieving additive as described in claim 1, which is characterized in that the step with centrifugal separation are as follows:
It is 25-35 DEG C in temperature, under the conditions of centrifugal rotational speed is 4500-6000r/min, the mixed liquor after ultrasonic extraction is subjected to liquid-
Liquid separation, time 25-45min.
7. the preparation method of heat-clearing inflammation relieving additive as described in claim 1, which is characterized in that the concentration step are as follows: will be from
For the supernatant obtained after the heart by ultrafiltration membrane, it is the dense of 1.02-1.25 that permeate, which is concentrated into relative density using reverse osmosis membrane,
Contracting liquid.
8. the preparation method of heat-clearing inflammation relieving additive as described in claim 1, which is characterized in that the spray step are as follows: will be dense
Powdered heat-clearing inflammation relieving additive is made through low temperature spray drying in contracting liquid.
9. the preparation method of heat-clearing inflammation relieving additive as claimed in claim 5, which is characterized in that in the ultrasonic extraction, second
The additional amount of alcohol is 1-2 times of mixing Chinese herbal medicine weight；Ultrasonic extraction condition are as follows: time 15-30min, 25-35 DEG C of temperature,
Power 400-550W, ultrasonic frequency 15-45KHz.
10. the preparation method of heat-clearing inflammation relieving additive as claimed in claim 7, which is characterized in that surpass used in the concentration
Filter membrane energy molecular cut off is greater than the substance of 1000 dalton, and the concentration pressure of reverse osmosis membrane concentration is 1.4-1.8MPa, temperature
It is 28 ± 1 DEG C.
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|---|---|---|---|---|
| CN110537730A (en) * | 2019-09-20 | 2019-12-06 | 安徽坤大生物工程技术有限公司 | mint taste puffed bead for cigarettes and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110537730A (en) * | 2019-09-20 | 2019-12-06 | 安徽坤大生物工程技术有限公司 | mint taste puffed bead for cigarettes and preparation method thereof |
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