CN109188730A - A kind of broadband terahertz wave modulator, preparation method and modulating system - Google Patents

A kind of broadband terahertz wave modulator, preparation method and modulating system Download PDF

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Publication number
CN109188730A
CN109188730A CN201811178507.0A CN201811178507A CN109188730A CN 109188730 A CN109188730 A CN 109188730A CN 201811178507 A CN201811178507 A CN 201811178507A CN 109188730 A CN109188730 A CN 109188730A
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China
Prior art keywords
modulator
hot spot
thz wave
laser
preparation
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CN201811178507.0A
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Chinese (zh)
Inventor
胡放荣
王红
江明珠
张文涛
银珊
熊显名
陈元枝
陈涛
韩家广
王月娥
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Guilin University of Electronic Technology
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Guilin University of Electronic Technology
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Priority to CN201811178507.0A priority Critical patent/CN109188730A/en
Publication of CN109188730A publication Critical patent/CN109188730A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G02OPTICS
    • G02FOPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
    • G02F1/00Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
    • G02F1/01Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour 
    • G02F1/0126Opto-optical modulation, i.e. control of one light beam by another light beam, not otherwise provided for in this subclass

Abstract

The present invention proposes that a kind of broadband Terahertz modulating system, including first laser transmitter, second laser transmitter, THz wave transmitter and modulator, first laser transmitter issue first laser beam and be irradiated to the one side of modulator and form the first hot spot;Second laser transmitter issues second laser beam and is irradiated to the another side of modulator and forms the second hot spot;THz wave transmitter issues THz wave and is incident on the wherein one side of modulator and forms third hot spot;Third hot spot and first hot spot or the second hot spot are least partially overlapped.The present invention irradiates two surfaces of print with two beam laser respectively, and photo-thermal effect changes phase-change material vanadium dioxide from insulation state to metallic state, to realize the big depth modulation to THz wave intensity in transmission.Wideband, big depth and fast modulation can be achieved in the present invention under lower optical power, and the Terahertz modulator of this method production has important application value in the Terahertz communication of the following quickly full photocontrol.

Description

A kind of broadband terahertz wave modulator, preparation method and modulating system
Technical field
The present invention relates to Terahertz Technology field, in particular to a kind of broadband terahertz wave modulator, preparation method and tune System processed.
Background technique
Terahertz (Terahertz:THz) wave typically refers to electromagnetic wave of the frequency within the scope of 0.1THz-10THz.Due to THz wave have penetrability is strong, photon energy is low, bandwidth and substance finger print spectrum etc. characteristics, make it in airport security, biology The fields such as medicine, broadband connections have huge application potential.THz wave intensity modulated is must not in Terahertz Technology application Link can be lacked, and current THz wave intensity modulating method is unfavorable for the popularization and application of Terahertz Technology.
THz wave intensity modulating method is generally divided into automatically controlled modulation, light-operated modulation, temperature control modulation, magnetic modulation and mechanical tune System etc..Automatically controlled modulator approach and ic process compatibility are big, easy of integration, but technics comparing is cumbersome.Temperature control modulator approach Response speed is slow, and is influenced by working environment bigger.The modulating speed of machinery modulation method and magnetic modulator approach also compares Slowly, device size is big, and not easy to operate.
The modulating speed of light-operated modulator approach is fast, easy to operate, becomes a kind of ideal scheme of fast modulation THz wave. Currently, the Terahertz modulator based on light modulation mostly uses greatly graphene and vanadium oxide material, since the light modulation of graphene is deep Spend it is low, be not able to satisfy it is many to modulation the higher application field of depth requirements.Vanadium oxide in 68 degrees centigrades because have very Good insulator-metal phase transition characteristic, becomes a kind of ideal material of light-operated Terahertz modulator.But currently based on oxidation There are the following problems for the terahertz light control modulator of vanadium:
(1) general modulation depth is generally no more than 80%.
(2) although also there is a small amount of more than 80%, the very high pumping light power of needs (greater than 2W), and high pump light Power is easy to bring thermal damage to device.
(3) this kind of device surface all has a metal structure and pattern, and due to THz wave be to metal it is impervious, Very big insertion loss can be introduced in this way.
Summary of the invention
In view of the foregoing deficiencies of prior art, the purpose of the present invention is to provide a kind of modulation of broadband THz wave Device, preparation method and modulating system.
In order to achieve the above objects and other related objects, the present invention provides a kind of preparation side of broadband terahertz wave modulator Method, the preparation method include: respectively in one layer of vanadium dioxide film layer of substrate two sides spin coating.
Optionally, the vanadium dioxide film layer is formed by the spin coating vanadium dioxide solution in substrate.
Optionally, the substrate is High Resistivity Si, the High Resistivity Si with a thickness of 300 μm -700 μm, resistance value is greater than 3000 Europe Centimetres of nurse.
Optionally, the vanadium dioxide film layer with a thickness of 50nm-2000nm.
Optionally, the vanadium dioxide film layer is to anneal 5-30 minutes to be formed in substrate under 80-300 degrees Celsius.
In order to achieve the above objects and other related objects, the present invention also provides a kind of broadband terahertz wave modulators, by institute The method stated is prepared.
In order to achieve the above objects and other related objects, the present invention also provides a kind of broadband THz wave modulating systems, should System includes first laser transmitter, second laser transmitter, THz wave transmitter and the modulator,
The first laser transmitter issues first laser beam and is irradiated to the one side of the modulator and forms the first hot spot;
The second laser transmitter issues second laser beam and is irradiated to the another side of the modulator and forms the second light Spot;
The THz wave transmitter issues THz wave and is incident on the wherein one side of the modulator and forms third light Spot;
The third hot spot and first hot spot or the second hot spot are least partially overlapped.
Optionally, the first laser beam and second laser beam are respectively with oblique two tables for being mapped to modulator of 10-75 degree Face;The wave-length coverage of the first laser beam and second laser speed is 350nm-950nm.
Optionally, the region of the third hot spot is located in first spot area or the second spot area.
Optionally, the center of first hot spot, the second hot spot center be overlapped respectively with the center of the third hot spot. As described above, a kind of broadband terahertz wave modulator, preparation method and modulating system of the invention, have the advantages that
(1) preparation process is simple, at low cost.The conventional device for carrying out THz wave modulation based on vanadium oxide phase transformation is most Vanadium oxide, complex process, preparation cost height are prepared using magnetron sputtering technique.The present invention prepares vanadium oxide using spin coating proceeding, Preparation process is simple, at low cost.
(2) modulation depth is big.It is compared with conventional light modulating method (light modulating method for being based particularly on vanadium oxide), The Terahertz modulator that the present invention makes is modulated due to using two-sided vanadium oxide and double light path, can be in lower optical power It is lower to obtain big modulation depth.
(3) modulating speed is fast.Due to using light modulating method, the present invention can achieve a picosecond amount the theoretic response time Grade, therefore can be used for the field high to modulation rate request such as THz wave communication.
Detailed description of the invention
In order to which the present invention is further explained, described content, with reference to the accompanying drawing makees a specific embodiment of the invention Further details of explanation.It should be appreciated that these attached drawings are only used as typical case, and it is not to be taken as to the scope of the present invention It limits.
Fig. 1 light path schematic diagram of the invention that THz wave modulation in broadband is carried out using modulator;
Fig. 2 is print to THz wave intensity modulated effect diagram (optical maser wavelength 650nm);
Wherein, 1, the THz wave before modulation, 2, first laser beam, 3, vanadium dioxide film, 4, vanadium dioxide film, 5, Substrate, 6, modulated THz wave, 7, second laser beam.
Specific embodiment
Illustrate embodiments of the present invention below by way of specific specific example, those skilled in the art can be by this specification Other advantages and efficacy of the present invention can be easily understood for disclosed content.The present invention can also pass through in addition different specific realities The mode of applying is embodied or practiced, the various details in this specification can also based on different viewpoints and application, without departing from Various modifications or alterations are carried out under spirit of the invention.It should be noted that in the absence of conflict, following embodiment and implementation Feature in example can be combined with each other.
It should be noted that illustrating the basic structure that only the invention is illustrated in a schematic way provided in following embodiment Think, only shown in schema then with related component in the present invention rather than component count, shape and size when according to actual implementation Draw, when actual implementation kenel, quantity and the ratio of each component can arbitrarily change for one kind, and its assembly layout kenel It is likely more complexity.
Embodiment one
The present invention provides a kind of preparation method of broadband terahertz wave modulator, which includes: using sol evenning machine It is specific that spin coating one layer of phase-change material vanadium dioxide film, preparation process are distinguished in the front and back sides of the high resistant silicon base of twin polishing The following steps are included:
1, select it is a piece of with a thickness of 300 μm -700 μm, resistance value be greater than 3000 ohm of cm sizes be the two-sided of 1cm*1cm High resistant silicon wafer is polished as substrate.
2, twin polishing high resistant silicon wafer is put into supersonic wave cleaning machine to clean be 5-10 minutes.
3, cleaned high resistant silicon wafer is put into drying box and is heated 15-20 minutes, dry print.
4, the high resistant silicon wafer of drying is placed on sol evenning machine, opens vacuum pump and print is sucked, and in the upper drop two of surface drop Vanadium oxide solution is rotated 2 minutes, the vanadium dioxide for forming one layer of 50nm-2000nm or so is thin with 1000-4000 revs/min of revolving speed Film layer 3.
5, the print of vanadium dioxide film is put into anneal station single side spin coating, with 80-300 degrees Celsius of annealing 5-30 points Clock.
6, the print after annealing is placed again into sol evenning machine, opens vacuum pump and be sucked, is existed with the method as step 4 The vanadium dioxide film layer of high resistant silicon wafer another side spin coating same thickness.
7, the good high resistant silicon wafer of spin coating is annealed again with the same method of step 5, annealing time is constant.
In an embodiment, substrate with a thickness of 500 μm.
In an embodiment, vanadium dioxide film layer with a thickness of 100nm, the revolving speed of sol evenning machine is 1000 revs/min, annealing Temperature be 150 degrees Celsius, time of annealing is 10min.
Embodiment two
The present invention also provides a kind of broadband terahertz wave modulator, the method described in embodiment one is prepared.
Embodiment three
In order to achieve the above objects and other related objects, the present invention also provides a kind of broadband THz wave modulating systems, should System includes first laser transmitter, second laser transmitter, THz wave transmitter and modulator above-mentioned,
The first laser transmitter issues first laser beam and is irradiated to the one side of the modulator and forms the first hot spot;
The second laser transmitter issues second laser beam and is irradiated to the another side of the modulator and forms the second light Spot;
The THz wave transmitter issues THz wave and is incident on the wherein one side of the modulator and forms third light Spot;
The third hot spot and first hot spot or the second hot spot are least partially overlapped.
Wherein, modulator is vertically put into THz wave transmission optical path as shown in Figure 1.
In an embodiment, the first laser beam and second laser beam are respectively with the oblique modulator that is mapped to of 10-75 degree Two surfaces;The wave-length coverage of the first laser beam and second laser speed is 350nm-950nm.
In an embodiment, the region of the third hot spot is located in first spot area or the second spot area. The face of first laser beam irradiation and the face of THz wave incidence belong to the same face, then the region of third hot spot is located at first light In spot region;Or second laser beam irradiation face and the face of THz wave incidence belong to the same face, then the region of third hot spot In in second spot area.It can guarantee that THz wave various pieces can be by the modulation of pump light in this way.
In an embodiment, the center of first hot spot, the second hot spot center respectively and in the third hot spot The heart is overlapped.
In an embodiment, the wavelength of the first laser beam and second laser speed is 650nm, first laser transmitting The peak power output of device and second laser transmitter is 120mW, and first laser transmitter and second laser transmitter are with 45 degree It is oblique to be mapped to print (i.e. modulator) former and later two surfaces.
The photo-thermal effect of laser causes vanadium dioxide film that the phase transformation of insulator-metal occurs, to realize to transmission too The modulation of hertz intensity of wave.The Output optical power for adjusting the included adjustable pump laser of attenuator of pump laser, can To change the phase transformation effect that insulator-metal occurs for vanadium dioxide film, finally changeable light modulation Terahertz wave modulation is deep Degree.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe The personage for knowing this technology all without departing from the spirit and scope of the present invention, carries out modifications and changes to above-described embodiment.Cause This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as At all equivalent modifications or change, should be covered by the claims of the present invention.

Claims (10)

1. a kind of preparation method of broadband terahertz wave modulator, which is characterized in that the preparation method includes:
Respectively in one layer of vanadium dioxide film layer of substrate two sides spin coating.
2. a kind of preparation method of broadband terahertz wave modulator according to claim 1, which is characterized in that the dioxy It changes vanadium film layer, is formed by the spin coating vanadium dioxide solution in substrate.
3. a kind of preparation method of broadband terahertz wave modulator according to claim 1, which is characterized in that the substrate For High Resistivity Si, the High Resistivity Si with a thickness of 300 μm -700 μm, resistance value is greater than 3000 ohm centimetres.
4. a kind of preparation method of broadband terahertz wave modulator according to claim 2, which is characterized in that the dioxy Change vanadium film layer with a thickness of 50nm-2000nm.
5. a kind of preparation method of broadband terahertz wave modulator according to claim 3, which is characterized in that the dioxy Changing vanadium film layer is to anneal 5-30 minutes to be formed in substrate under 80-300 degrees Celsius.
6. a kind of broadband terahertz wave modulator, which is characterized in that the preparation of the method as described in Claims 1 to 5 any one It forms.
7. a kind of broadband THz wave modulating system, which is characterized in that the system includes first laser transmitter, second laser hair Emitter, THz wave transmitter and the modulator as described in claims 6,
The first laser transmitter issues first laser beam and is irradiated to the one side of the modulator and forms the first hot spot;
The second laser transmitter issues second laser beam and is irradiated to the another side of the modulator and forms the second hot spot;
The THz wave transmitter issues THz wave and is incident on the wherein one side of the modulator and forms third hot spot;
The third hot spot and first hot spot or the second hot spot are least partially overlapped.
8. a kind of broadband THz wave modulating system according to claim 7, which is characterized in that the first laser beam with Second laser beam is respectively with oblique two surfaces for being mapped to modulator of 10-75 degree;The first laser beam and the second laser The wave-length coverage of speed is 350nm-950nm.
9. a kind of broadband THz wave modulating system according to claim 8, which is characterized in that the area of the third hot spot Domain is located in first spot area or the second spot area.
10. a kind of broadband THz wave modulating system according to claim 9, which is characterized in that first hot spot Center, the second hot spot center be overlapped respectively with the center of the third hot spot.
CN201811178507.0A 2018-10-10 2018-10-10 A kind of broadband terahertz wave modulator, preparation method and modulating system Pending CN109188730A (en)

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