CN109183417A - Miao ethnic group's needlework and preparation method thereof - Google Patents
Miao ethnic group's needlework and preparation method thereof Download PDFInfo
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- CN109183417A CN109183417A CN201810966995.5A CN201810966995A CN109183417A CN 109183417 A CN109183417 A CN 109183417A CN 201810966995 A CN201810966995 A CN 201810966995A CN 109183417 A CN109183417 A CN 109183417A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
- D06M15/277—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof containing fluorine
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/11—Compounds containing epoxy groups or precursors thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/203—Unsaturated carboxylic acids; Anhydrides, halides or salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/59—Polyamides; Polyimides
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/12—Hydrophobic properties
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Automatic Embroidering For Embroidered Or Tufted Products (AREA)
- Decoration Of Textiles (AREA)
Abstract
Miao ethnic group's needlework and preparation method thereof, belongs to textile technology field.A kind of preparation method of Miao ethnic group embroidery includes by embroider line and drawing figuratum base fabric by water-proofing treatment, with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained, embroidery first product is handled by sizing and arrangement, obtains needlework after cleaning.Miao ethnic group's needlework that this preparation method prepares can waterproof, while it is very smooth at embroidery, it is bright and new beautiful.A kind of Miao ethnic group's needlework, is made by above-mentioned preparation method, smooth beautiful at embroidery, and water pools drop on needlework, and needlework wearability is good, and richness is high.
Description
Technical field
The present invention relates to textile technology fields, and in particular to Miao ethnic group's needlework and preparation method thereof.
Background technique
Embroidery is a kind of ancient art, with the design and production addition of needle and bundle of lines people on any existing fabric
A kind of art.The embroidery of China is of long standing and well established, occupies important position in world's product culture treasure-house, in Chinese tratitional technology
Quite have an impact in fine arts industry, be the crystallization of wisdom of Chinese name race, in embroidery industry, during Suzhou embroidery, Hunan embroidery, Sichuan embroidery and Guangdong embroidery be
State's the four famous embroideries are enjoyed great prestige both at home and abroad.
Miao ethnic group's embroidery has the function of passing on history culture, be mainly manifested on the pattern of embroidery.Almost each is embroidered
Pattern line kind has an origin or legend, all deep containing national culture, is all the expression of national sentiment, is Miao ethnic group's history and life
Displaying living.The patterns such as butterfly, dragon, flying bird, fish, dot, duckweed are all the contents that " the Ancient Song of Miao ethnics " is circulated and sung, and color is fresh
Gorgeous, composition is bright and clear, simple generous.
Existing needlework is easy to fade, not waterproof, and needlework location is formed than less easily, and fold is more, crosses one
The phenomenon that will appear three-dimensional sense no longer after the section time.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation method of Miao ethnic group's needlework, this preparation method is added anti-in step
Water step and arrangement step.
Another object of the present invention is to provide a kind of Miao ethnic group's needlework, this Miao ethnic group's needlework being capable of effectively waterproof and anti-
Fold.
The present invention solves its technical problem and adopts the following technical solutions to realize.
The present invention proposes a kind of Miao ethnic group's needlework preparation method comprising: by embroider line and figuratum base fabric is drawn by anti-
Water process obtains embroidery first product with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, by embroidery first product warp
Sizing and arrangement processing are crossed, obtains needlework after cleaning；
In parts by weight, the waterproofing agent that water-proofing treatment uses includes that 30~40 parts of mass concentrations contain for 6%~10%
Fluorinated monomer lotion and 5~10 parts of methacrylic acids；
In parts by weight, the finishing agent for arranging use gathers including 50~70 parts of aqueous silicon elastic emulsions, 15~30 parts
Amide and 5~10 parts of crosslinking agents.
The present invention also proposes a kind of Miao ethnic group's needlework, is prepared by above-mentioned preparation method.
The beneficial effect of the embodiment of the present invention is:
Waterproofing step and whole is added in needlework preparation method in a kind of preparation method of Miao ethnic group's needlework provided by the invention
Step is managed, enables the needlework waterproof prepared, while very smooth at embroidery, it is bright and new beautiful.Using waterproofing agent to thorn
Embroidery carries out water-proofing treatment, so that needlework is had hydrophobicity, fades after preventing needlework to be wetted in eclipse.Using finishing agent
Make needlework will not fold, wearability and richness raising with sizing dual mode.
A kind of Miao ethnic group's needlework provided by the invention, bright and new beautiful at embroidery, water pools drop, needlework on needlework
Wearability is good, and richness is high.
Specific embodiment
It in order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below will be in the embodiment of the present invention
Technical solution be clearly and completely described.The person that is not specified actual conditions in embodiment, according to normal conditions or manufacturer builds
The condition of view carries out.Reagents or instruments used without specified manufacturer is the conventional production that can be obtained by commercially available purchase
Product.
Miao ethnic group's needlework of the embodiment of the present invention and preparation method thereof is specifically described below.
The embodiment of the present invention provides a kind of Miao ethnic group's needlework preparation method comprising: by embroider line and draw figuratum base fabric
Embroidery first product is obtained, will be embroidered with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment by water-proofing treatment
First product obtains needlework after cleaning by sizing and arrangement processing.
Specifically, a kind of Miao ethnic group's needlework preparation method mainly comprises the steps that
1, water-proofing treatment
Prepare waterproofing agent: in parts by weight, waterproofing agent includes that 30~40 parts of mass concentrations are 6%~10% fluorine-containing third
Olefin(e) acid ester lotion and 5~10 parts of methacrylic acids；
Waterproofing agent further includes 10~20 parts of epoxychloropropane and 0.1~1 part of surfactant；
Preferably, it is 6%~10% fluorinated acrylate emulsion, 5~8 parts of first that waterproofing agent, which includes 32~38 parts of mass concentrations,
Base acrylic acid, 12~18 parts of epoxychloropropane and 0.1~0.5 part of surfactant, it is highly preferred that waterproofing agent includes 35~38 parts
Mass concentration is 6%~10% fluorinated acrylate emulsion, 6~8 parts of methacrylic acids, 12~15 parts of epoxychloropropane and 0.2
~0.5 part of surfactant；
There is fluorinated acrylate emulsion excellent high surface and hydrophobic to increase oiliness energy, be good waterproof material；
Methacrylic acid can be dissolved in hot water, while be good adhesive and organic solvent；
Epoxychloropropane is good adhesive；
Surfactant selects tricarboxylic ester or neopelex, and surfactant one end is clear water group, separately
One end is hydrophobic grouping；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 50~70 DEG C.
2, soften and embroider
Prepare softening agent: in parts by weight, softening agent includes 10~18 parts of amino-modified silicone oils, 5~10 parts of poly- second
Enol and 40~60 parts of ethyl alcohol；
Amino-modified silicone oil handles fabric, keeps fabric fluffy, plentiful, soft；
Polyvinyl alcohol and ethyl alcohol are good organic solvents；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product 1~2h of thermal finalization at 100~120 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, finishing agent gathers including 50~70 parts of aqueous silicon elastic emulsions, 15~30 parts
Amide and 5~10 parts of crosslinking agents；
Finishing agent further includes 2~5 parts of silicone oil and 5~8 parts of ethyl acetate；
Preferably, finishing agent includes 55~70 parts of aqueous silicon elastic emulsions, 15~25 parts of polyamide, 5~8 parts of crosslinking agents, 2
~4 parts of silicone oil and 5~7 parts of ethyl acetate, it is highly preferred that finishing agent includes 55~60 parts of aqueous silicon elastic emulsions, 15~20 parts
Polyamide, 5~6 parts of crosslinking agents, 3~4 parts of silicone oil and 5~6 parts of ethyl acetate；
Aqueous silicon elastic emulsion and high-molecular polyamide are adhered to by being capable of forming silicon elasticity glue film after cross-linking agents
Inside face liber surface and blister cavities, so that needlework be made to obtain excellent bending resistance and wrinkle recovery performance, performance
Persistence is good；
Crosslinking agent selects blocked isocyanate class crosslinking agent；
Silicone oil is able to ascend the fluffy degree of fabric, improves wrinkle recovery, improves tearing brute force, reduces ultimate strength decline,
Adjust out the feel of soft and smooth exquisiteness；
Ethyl acetate is good organic solvent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 1~3 time with cleaning agent, is then cleaned 3~5 times with deionized water again.
The embodiment of the present invention also provides a kind of Miao ethnic group's needlework, is prepared according to the preparation method of above-mentioned silver jeweleries.
Feature and performance of the invention are described in further detail with reference to embodiments.
Embodiment 1
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 8% fluorinated acrylate emulsion and 8 parts of first by 35 parts of mass concentrations in parts by weight
Base acrylic acid mixed preparing obtains waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, it embroiders
With the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, 60 parts of aqueous silicon elastic emulsions, 20 parts of polyamide and 8 parts of sealing ends are different
The mixing crosslinking of cyanate crosslinking agent, which is prepared, obtains finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Embodiment 2
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 8% fluorinated acrylate emulsion, 6 parts of methyl by 32 parts of mass concentrations in parts by weight
Acrylic acid, 12 parts of epoxychloropropane and 0.2 part of tricarboxylic ester mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 15 parts of amino-modified silicone oils, 8 parts of polyvinyl alcohol and 50 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, by 55 parts of aqueous silicon elastic emulsions, 25 parts of polyamide, 6 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent, 3 parts of silicone oil and 7 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Embodiment 3
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 10% fluorinated acrylate emulsion, 5 parts of first by 30 parts of mass concentrations in parts by weight
Base acrylic acid, 10 parts of epoxychloropropane and 0.1 part of tricarboxylic ester mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 50 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 10 parts of amino-modified silicone oils, 5 parts of polyvinyl alcohol and 40 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 1.5h at 110 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, by 50 parts of aqueous silicon elastic emulsions, 15 parts of polyamide, 5 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent, 2 parts of silicone oil and 5 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 1 time with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Embodiment 4
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 6% fluorinated acrylate emulsion, 10 parts of first by 40 parts of mass concentrations in parts by weight
Base acrylic acid, 20 parts of epoxychloropropane and 1 part of tricarboxylic ester mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 70 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 18 parts of amino-modified silicone oils, 10 parts of polyvinyl alcohol and 60 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 1h at 120 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, 70 parts of aqueous silicon elastic emulsions, 30 parts of polyamide, 10 parts of sealing ends are different
Cyanate crosslinking agent, 5 parts of silicone oil and 8 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 3 times with cleaning agent, then cleans 5 times with deionized water again to get needlework is arrived.
Embodiment 5
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 9% fluorinated acrylate emulsion, 7 parts of methyl by 38 parts of mass concentrations in parts by weight
Acrylic acid, 15 parts of epoxychloropropane and 0.5 part of neopelex mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 16 parts of amino-modified silicone oils, 7 parts of polyvinyl alcohol and 55 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 1.5h at 100 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, by 65 parts of aqueous silicon elastic emulsions, 20 parts of polyamide, 7 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent, 4 parts of silicone oil and 6 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 4 times with deionized water again to get needlework is arrived.
Comparative example 1
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
Comparative example 2
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, soften and embroider
It prepares softening agent: in parts by weight, 15 parts of amino-modified silicone oils, 8 parts of polyvinyl alcohol and 50 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
2, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
3, it arranges
Prepare finishing agent: in parts by weight, by 55 parts of aqueous silicon elastic emulsions, 25 parts of polyamide, 6 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent, 3 parts of silicone oil and 7 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
4, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Comparative example 3
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 8% fluorinated acrylate emulsion, 6 parts of methyl by 32 parts of mass concentrations in parts by weight
Acrylic acid, 12 parts of epoxychloropropane and 0.2 part of tricarboxylic ester mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 15 parts of amino-modified silicone oils, 8 parts of polyvinyl alcohol and 50 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it arranges
Prepare finishing agent: in parts by weight, by 55 parts of aqueous silicon elastic emulsions, 25 parts of polyamide, 6 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent, 3 parts of silicone oil and 7 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
4, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Comparative example 4
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 8% fluorinated acrylate emulsion, 6 parts of methyl by 32 parts of mass concentrations in parts by weight
Acrylic acid, 12 parts of epoxychloropropane and 0.2 part of tricarboxylic ester mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 15 parts of amino-modified silicone oils, 8 parts of polyvinyl alcohol and 50 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
4, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Comparative example 5
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 8% fluorinated acrylate emulsion, 6 parts of methyl by 32 parts of mass concentrations in parts by weight
Acrylic acid, 12 parts of epoxychloropropane and 0.2 part of tricarboxylic ester mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, it embroiders
With the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, by 55 parts of aqueous silicon elastic emulsions, 25 parts of polyamide, 6 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent, 3 parts of silicone oil and 7 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Comparative example 6
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
Prepare waterproofing agent: in parts by weight, by 6 parts of methacrylic acids, 12 parts of epoxychloropropane and 0.2 part of tricarboxylic acids
Ester mixed preparing obtains waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 15 parts of amino-modified silicone oils, 8 parts of polyvinyl alcohol and 50 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, by 55 parts of aqueous silicon elastic emulsions, 25 parts of polyamide, 6 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent, 3 parts of silicone oil and 7 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Comparative example 7
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 8% fluorinated acrylate emulsion and 0.2 part by 32 parts of mass concentrations in parts by weight
Tricarboxylic ester mixed preparing obtains waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 15 parts of amino-modified silicone oils, 8 parts of polyvinyl alcohol and 50 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, by 55 parts of aqueous silicon elastic emulsions, 25 parts of polyamide, 6 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent, 3 parts of silicone oil and 7 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Comparative example 8
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 8% fluorinated acrylate emulsion, 6 parts of methyl by 32 parts of mass concentrations in parts by weight
Acrylic acid, 12 parts of epoxychloropropane and 0.2 part of tricarboxylic ester mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 15 parts of amino-modified silicone oils, 8 parts of polyvinyl alcohol and 50 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, by 55 parts of aqueous silicon elastic emulsions, 6 parts of blocked isocyanate class crosslinkings
Agent, 3 parts of silicone oil and 7 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Comparative example 9
The embodiment of the present invention provides a kind of Miao ethnic group's needlework and preparation method thereof.
1, water-proofing treatment
It prepares waterproofing agent: being 8% fluorinated acrylate emulsion, 6 parts of methyl by 32 parts of mass concentrations in parts by weight
Acrylic acid, 12 parts of epoxychloropropane and 0.2 part of tricarboxylic ester mixed preparing obtain waterproofing agent；
Water-proofing treatment: using waterproofing agent treatment embroider line and figuratum base fabric is drawn；
Drying: embroider line and base fabric are dried at 60 DEG C.
2, soften and embroider
It prepares softening agent: in parts by weight, 15 parts of amino-modified silicone oils, 8 parts of polyvinyl alcohol and 50 parts of ethyl alcohol being mixed
It closes to prepare and obtains softening agent；
Softening: base fabric is handled using softening agent；
Embroidery: with the embroidered pattern of base fabric of the embroider line after water-proofing treatment after water-proofing treatment, embroidery first product is obtained.
3, it is formed
To embroider first product thermal finalization 2h at 100 DEG C.
4, it arranges
Prepare finishing agent: in parts by weight, by 55 parts of aqueous silicon elastic emulsions, 25 parts of polyamide, 6 parts of sealing end isocyanides
Esters of gallic acid crosslinking agent and 7 parts of ethyl acetate mixing crosslinkings prepare and obtain finishing agent；
It arranges: handling the embroidery first product after sizing using finishing agent.
5, it cleans
It is first cleaned 2 times with cleaning agent, then cleans 3 times with deionized water again to get needlework is arrived.
Waterproofness, wrinkle resistance and the flexibility of needlework made from Examples 1 to 5 and comparative example 1~9 are detected respectively, such as
Shown in table 1, table 2 and table 3:
Waterproofness, wrinkle resistance and the flexibility of needlework made from 1 Examples 1 to 5 of table
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Waterproofness | Very well | Very well | Very well | Very well | Very well |
| Wrinkle resistance | Very well | Very well | Very well | Very well | Very well |
| Flexibility | Very well | Very well | Very well | Very well | Very well |
Waterproofness, wrinkle resistance and the flexibility of needlework made from 2 comparative example 1~5 of table
| Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 | |
| Waterproofness | It is non-watertight | It is non-watertight | Very well | Very well | Very well |
| Wrinkle resistance | Many folds | Very well | Generally | Generally | Very well |
| Flexibility | It is very coarse | Very well | Very well | It is coarse | It is somewhat coarse |
Waterproofness, wrinkle resistance and the flexibility of needlework made from 3 comparative example 6~9 of table
It can be obtained by table 1, table 2 and table 3, by Examples 1 to 5 and the comparison of comparative example 1 it is found that directly sewing needlework obtained
Surface roughness and non-watertight, is easy to fade；By Examples 1 to 5 and the comparison of comparative example 2 it is found that the embroidery without water-proofing treatment
Product have no waterproof effect, are easy to fade；By Examples 1 to 5 and the comparison of comparative example 3,4 it is found that being only formed and arranging junction
The needlework crease resistance of reason is best；By Examples 1 to 5 and the comparison of comparative example 5 it is found that the needlework flexibility without sofening treatment
Poor, feel is bad；
By Examples 1 to 5 and the comparison of comparative example 6 it is found that fluorinated acrylate emulsion can form one on needlework surface
Layer film waterproof；By Examples 1 to 5 and the comparison of comparative example 7 it is found that methacrylic acid and epoxychloropropane have gumminess, energy
Enough make fluorinated acrylate emulsion in needlework surface filming；By Examples 1 to 5 and the comparison of comparative example 8 it is found that only aqueous silicon
Elastic emulsion and high-molecular polyamide by the way that silicon elasticity glue film could be formed after cross-linking agents, be attached to face liber surface and
Inside blister cavities, so that needlework be made to obtain excellent bending resistance and wrinkle recovery performance；By Examples 1 to 5 and comparative example 9
It is found that silicone oil is able to ascend the fluffy degree of fabric, raising wrinkle recovery adjusts out the feel of soft and smooth exquisiteness for comparison.
In conclusion a kind of preparation method of Miao ethnic group's needlework of the embodiment of the present invention, in Miao ethnic group's needlework preparation method
Waterproofing step is added and arranges step, enables Miao ethnic group's needlework waterproof prepared, prevents needlework from fading, embroider simultaneously
Locate very smooth, feel exquisiteness, it is bright and new beautiful.
A kind of Miao ethnic group's needlework provided in an embodiment of the present invention, bright and new beautiful at embroidery, waterproof performance is good, and needlework is resistance to
Mill property is good, and richness is high, and feel is fine and smooth.
Embodiments described above is a part of the embodiment of the present invention, instead of all the embodiments.Reality of the invention
The detailed description for applying example is not intended to limit the range of claimed invention, but is merely representative of selected implementation of the invention
Example.Based on the embodiments of the present invention, obtained by those of ordinary skill in the art without making creative efforts
Every other embodiment, shall fall within the protection scope of the present invention.
Claims (10)
1. a kind of Miao ethnic group's needlework preparation method, characterized in that it comprises: by embroider line and draw figuratum base fabric by waterproof
Processing obtains embroidery first product with the embroidered pattern of the base fabric of the embroider line after water-proofing treatment after water-proofing treatment, will
The embroidery first product obtains needlework after cleaning by sizing and arrangement processing；
In parts by weight, the waterproofing agent that water-proofing treatment uses includes 30~40 parts of mass concentrations for 6%~10% fluorine-containing third
Olefin(e) acid ester lotion and 5~10 parts of methacrylic acids；
In parts by weight, the finishing agent for arranging use includes 50~70 parts of aqueous silicon elastic emulsions, 15~30 parts of polyamide
With 5~10 parts of crosslinking agents.
2. Miao ethnic group's needlework preparation method according to claim 1, which is characterized in that the waterproofing agent further includes 10~20
Part epoxychloropropane and 0.1~1 part of surfactant.
3. Miao ethnic group's needlework preparation method according to claim 2, which is characterized in that according to parts by weight, the waterproof
Agent includes that 32~38 parts of mass concentrations are 6%~10% fluorinated acrylate emulsion, 5~8 parts of methacrylic acids, 12~18 parts of rings
Oxygen chloropropane and 0.1~0.5 part of surfactant.
4. Miao ethnic group's needlework preparation method according to claim 1, which is characterized in that according to parts by weight, the arrangement
Agent further includes 2~5 parts of silicone oil and 5~8 parts of ethyl acetate.
5. Miao ethnic group's needlework preparation method according to claim 1, which is characterized in that after water-proofing treatment, before embroidery, also
Including sofening treatment.
6. Miao ethnic group's needlework preparation method according to claim 5, which is characterized in that according to parts by weight, sofening treatment
The softening agent of use includes 10~18 parts of amino-modified silicone oils, 5~10 parts of polyvinyl alcohol and 40~60 parts of ethyl alcohol.
7. Miao ethnic group's needlework preparation method according to claim 1, which is characterized in that after water-proofing treatment, before embroidery, also
Including drying, the embroider line and the base fabric are dried at 50~70 DEG C.
8. Miao ethnic group's needlework preparation method according to claim 1, which is characterized in that the method for cleaning includes:
It is first cleaned 1~3 time with cleaning agent, is then cleaned 3~5 times with deionized water again.
9. Miao ethnic group's needlework preparation method according to claim 1, which is characterized in that the method that sizing uses thermal finalization,
The temperature of the thermal finalization is 100~120 DEG C, and the time of the thermal finalization is 1~2h.
10. a kind of Miao ethnic group's needlework, which is characterized in that by Miao ethnic group's needlework preparation method according to any one of claims 1 to 9
It is prepared.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109881491A (en) * | 2019-02-14 | 2019-06-14 | 宁波萌恒抽纱有限公司 | A kind of processing method that fish silk thread is embroidered |
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Application publication date: 20190111 |